NMR Restraints Grid
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NMR Restraints Grid |
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Result table
| image | mrblock_id | pdb_id | bmrb_id | cing | stage | position | program | type | subtype | subsubtype |
|
|
500811 |
2l28   |
17125 | cing | 1-original | 1 | XPLOR/CNS | distance | NOE | simple |
!Restraints used in calculations of Lactobacillus casei apoDHFR !NOEs !Long range NOEs !HN(i) - HN(j) assign (resid 58 and name hn ) (resid 36 and name hn ) 5.5 5.5 0.0 ! 498 15N assign (resid 58 and name hn ) (resid 37 and name hn ) 4.5 4.5 0.0 ! 1015 15N assign (resid 58 and name hn ) (resid 39 and name hn ) 4.5 4.5 0.0 ! 185 15N assign (resid 62 and name hn ) (resid 41 and name hn ) 4.5 4.5 0.0 ! 551 15N assign (resid 96 and name hn ) (resid 4 and name hn ) 4.6 4.6 0.0 ! 1319 15N assign (resid 97 and name hn ) (resid 40 and name hn ) 4.5 4.5 0.0 ! 1327 15N assign (resid 99 and name hn ) (resid 42 and name hn ) 4.5 4.5 0.0 ! 1119 15N assign (resid 114 and name hn ) (resid 3 and name hn ) 4.5 4.5 0.0 ! 356 15N assign (resid 114 and name hn ) (resid 5 and name hn ) 4.6 4.6 0.0 ! 360 15N assign (resid 116 and name hn ) (resid 5 and name hn ) 4.5 4.5 0.0 ! 1437 15N assign (resid 116 and name hn ) (resid 7 and name hn ) 4.5 4.5 0.0 ! 707 15N assign (resid 122 and name hn ) (resid 9 and name hn ) 5.5 5.5 0.0 ! 732 15N assign (resid 152 and name hn ) (resid 146 and name hn ) 4.5 4.5 0.0 ! 569 15N assign (resid 153 and name hn ) (resid 144 and name hn ) 4.5 4.5 0.0 ! 538 15N assign (resid 153 and name hn ) (resid 146 and name hn ) 4.6 4.6 0.0 ! 1609 15N assign (resid 154 and name hn ) (resid 117 and name hn ) 4.0 4.0 0.0 ! 1617 15N assign (resid 154 and name hn ) (resid 119 and name hn ) 5.1 5.1 0.0 ! 1618 15N assign (resid 154 and name hn ) (resid 144 and name hn ) 4.5 4.5 0.0 ! 1620 15N assign (resid 155 and name hn ) (resid 142 and name hn ) 3.5 3.5 0.0 ! 1555 15N assign (resid 156 and name hn ) (resid 115 and name hn ) 4.5 4.5 0.0 ! 1633 15N assign (resid 156 and name hn ) (resid 142 and name hn ) 5.3 5.3 0.0 ! 1632 15N assign (resid 157 and name hn ) (resid 139 and name hn ) 4.5 4.5 0.0 ! 1646 15N assign (resid 157 and name hn ) (resid 140 and name hn ) 3.5 3.5 0.0 ! 632 15N assign (resid 158 and name hn ) (resid 113 and name hn ) 4.5 4.5 0.0 ! 695 15N assign (resid 159 and name hn ) (resid 137 and name hn ) 3.5 3.5 0.0 ! 1656 15N assign (resid 159 and name hn ) (resid 138 and name hn ) 5.5 5.5 0.0 ! 1518 15N assign (resid 159 and name hn ) (resid 139 and name hn ) 4.5 4.5 0.0 ! 1655 15N assign (resid 160 and name hn ) (resid 112 and name hn ) 4.5 4.5 0.0 ! 181 15N assign (resid 160 and name hn ) (resid 137 and name hn ) 5.5 5.5 0.0 ! 1514 15N assign (resid 161 and name hn ) (resid 136 and name hn ) 4.8 4.8 0.0 ! 1242 15N assign (resid 161 and name hn ) (resid 137 and name hn ) 4.5 4.5 0.0 ! 1690 15N !HN(i) - Ha(j) assign (resid 2 and name hn ) (resid 95 and name ha ) 4.5 4.5 0.0 ! 1054 15N assign (resid 3 and name hn ) (resid 113 and name ha ) 4.5 4.5 0.0 ! 610 15N assign (resid 4 and name hn ) (resid 97 and name ha ) 3.5 3.5 0.0 ! 1056 15N assign (resid 5 and name hn ) (resid 115 and name ha ) 3.5 3.5 0.0 ! 387 D2O assign (resid 9 and name hn ) (resid 121 and name ha ) 4.5 4.5 0.0 ! 303 15N assign (resid 13 and name hn ) (resid 127 and name ha ) 4.5 4.5 0.0 ! 1076 15N assign (resid 36 and name hn ) (resid 57 and name ha ) 4.5 4.5 0.0 ! 819 15N assign (resid 40 and name hn ) (resid 96 and name ha ) 4.5 4.5 0.0 ! 1106 15N assign (resid 41 and name hn ) (resid 61 and name ha ) 4.5 4.5 0.0 ! 195 15N assign (resid 42 and name hn ) (resid 98 and name ha* ) 4.5 4.5 0.0 ! 1113 15N assign (resid 58 and name hn ) (resid 38 and name ha ) 5.0 5.0 0.0 ! 1098 15N assign (resid 61 and name hn ) (resid 75 and name ha ) 3.5 3.5 0.0 ! 1169 15N assign (resid 63 and name hn ) (resid 77 and name ha ) 3.5 3.5 0.0 ! 412 15N assign (resid 69 and name hn ) (resid 75 and name ha ) 6.8 6.8 0.0 ! 916 15N assign (resid 74 and name hn ) (resid 60 and name ha ) 3.5 3.5 0.0 ! 510 15N assign (resid 76 and name hn ) (resid 62 and name ha ) 4.5 4.5 0.0 ! 1227 15N assign (resid 96 and name hn ) (resid 3 and name ha ) 4.5 4.5 0.0 ! 344 15N assign (resid 98 and name hn ) (resid 41 and name ha ) 5.5 5.5 0.0 ! 1333 15N assign (resid 99 and name hn ) (resid 41 and name ha ) 5.5 5.5 0.0 ! 1343 15N assign (resid 112 and name hn ) (resid 2 and name ha ) 3.5 3.5 0.0 ! 136 13C assign (resid 114 and name hn ) (resid 4 and name ha ) 3.5 3.5 0.0 ! 359 15N assign (resid 116 and name hn ) (resid 5 and name ha ) 5.5 5.5 0.0 ! 1436 15N assign (resid 116 and name hn ) (resid 6 and name ha ) 3.5 3.5 0.0 ! 708 15N assign (resid 117 and name hn ) (resid 153 and name ha ) 4.5 4.5 0.0 ! 1438 15N assign (resid 118 and name hn ) (resid 8 and name ha ) 4.5 4.5 0.0 ! 364 15N assign (resid 120 and name hn ) (resid 150 and name ha ) 3.5 3.5 0.0 ! 499 13C assign (resid 125 and name hn ) (resid 15 and name ha ) 3.5 3.5 0.0 ! 576 15N assign (resid 137 and name hn ) (resid 158 and name ha ) 4.5 4.5 0.0 ! 804 15N assign (resid 137 and name hn ) (resid 159 and name ha ) 4.5 4.5 0.0 ! 807 15N assign (resid 137 and name hn ) (resid 160 and name ha ) 3.5 3.5 0.0 ! 2529 13C assign (resid 138 and name hn ) (resid 158 and name ha ) 5.5 5.5 0.0 ! 1523 15N assign (resid 139 and name hn ) (resid 158 and name ha ) 3.5 3.5 0.0 ! 846 13C assign (resid 140 and name hn ) (resid 158 and name ha ) 4.5 4.5 0.0 ! 628 15N assign (resid 143 and name hn ) (resid 154 and name ha ) 4.5 4.5 0.0 ! 1569 15N assign (resid 144 and name hn ) (resid 154 and name ha ) 3.5 3.5 0.0 ! 536 15N assign (resid 146 and name hn ) (resid 152 and name ha ) 3.5 3.5 0.0 ! 567 15N assign (resid 153 and name hn ) (resid 145 and name ha ) 4.5 4.5 0.0 ! 1615 15N assign (resid 154 and name hn ) (resid 118 and name ha ) 4.5 4.5 0.0 ! 1622 15N assign (resid 155 and name hn ) (resid 141 and name ha ) 4.5 4.5 0.0 ! 958 15N assign (resid 155 and name hn ) (resid 143 and name ha ) 3.5 3.5 0.0 ! 960 15N assign (resid 156 and name hn ) (resid 114 and name ha ) 4.6 4.6 0.0 ! 1634 15N assign (resid 156 and name hn ) (resid 116 and name ha ) 3.6 3.6 0.0 ! 1636 15N assign (resid 157 and name hn ) (resid 140 and name ha ) 4.8 4.8 0.0 ! 1647 15N assign (resid 157 and name hn ) (resid 141 and name ha ) 4.0 4.0 0.0 ! 619 15N assign (resid 158 and name hn ) (resid 112 and name ha ) 4.8 4.8 0.0 ! 692 15N assign (resid 159 and name hn ) (resid 136 and name ha ) 5.5 5.5 0.0 ! 1659 15N assign (resid 159 and name hn ) (resid 138 and name ha ) 4.0 4.0 0.0 ! 709 13C assign (resid 160 and name hn ) (resid 111 and name ha ) 4.5 4.5 0.0 ! 248 15N assign (resid 160 and name hn ) (resid 112 and name ha ) 3.5 3.5 0.0 ! 2169 13C assign (resid 160 and name hn ) (resid 136 and name ha ) 4.5 4.5 0.0 ! 249 15N assign (resid 161 and name hn ) (resid 136 and name ha ) 3.5 3.5 0.0 ! 1685 15N !Ha(i) - Ha(j) assign (resid 77 and name ha ) (resid 63 and name ha ) 4.5 4.5 0.0 ! 935 13C assign (resid 110 and name ha ) (resid 2 and name ha ) 4.6 4.6 0.0 ! 135 13C assign (resid 150 and name ha ) (resid 120 and name ha* ) 3.5 3.5 0.0 ! 261 D2O assign (resid 153 and name ha ) (resid 118 and name ha ) 3.5 3.5 0.0 ! 393 D2O assign (resid 158 and name ha ) (resid 138 and name ha ) 3.5 3.5 0.0 ! 136 D2O assign (resid 160 and name ha ) (resid 136 and name ha ) 3.5 3.5 0.0 ! 2534 13C ! Other long-range NOEs assign (resid 13 and name hg2*) (resid 5 and name hd1 ) 3.5 3.5 0.0 ! 1779 13C assign (resid 13 and name hg2*) (resid 5 and name he1 ) 4.5 4.5 0.0 ! 1778 13C assign (resid 13 and name hg2*) (resid 7 and name ha ) 4.5 4.5 0.0 ! 866 13C assign (resid 29 and name he* ) (resid 5 and name hn ) 4.5 4.5 0.0 ! 1058 15N assign (resid 46 and name hb* ) (resid 41 and name hg2*) 2.5 2.5 0.0 ! 1667 13C assign (resid 46 and name hd* ) (resid 41 and name hg1*) 3.8 3.8 0.0 ! 1918 13C assign (resid 46 and name hn ) (resid 41 and name hg2*) 3.5 3.5 0.0 ! 355 13C assign (resid 46 and name ha ) (resid 41 and name hg2*) 4.5 4.5 0.0 ! 1673 13C assign (resid 49 and name hz ) (resid 39 and name he* ) 3.5 3.5 0.0 ! 52 13C assign (resid 49 and name hd* ) (resid 41 and name hg2*) 3.5 3.5 0.0 ! 357 13C assign (resid 54 and name hd* ) (resid 39 and name he* ) 3.5 3.5 0.0 ! 838 13C assign (resid 54 and name hb* ) (resid 39 and name he* ) 4.0 4.0 0.0 ! 59 13C assign (resid 56 and name hb* ) (resid 36 and name hn ) 4.1 4.1 0.0 ! 821 15N assign (resid 57 and name hg* ) (resid 36 and name hn ) 5.5 5.5 0.0 ! 817 15N assign (resid 58 and name hg2*) (resid 38 and name hg12) 3.5 3.5 0.0 ! 2088 13C assign (resid 58 and name hg2*) (resid 38 and name hg11) 3.5 3.5 0.0 ! 2087 13C assign (resid 58 and name hb ) (resid 38 and name hg11) 3.6 3.6 0.0 ! 2086 13C assign (resid 58 and name hg2*) (resid 39 and name hn ) 3.9 3.9 0.0 ! 1419 13C assign (resid 59 and name hb* ) (resid 39 and name hn ) 5.5 5.5 0.0 ! 1101 15N assign (resid 59 and name hb* ) (resid 53 and name hb* ) 3.5 3.5 0.0 ! 1388 13C assign (resid 59 and name hd2*) (resid 54 and name hn ) 4.5 4.5 0.0 ! 1156 15N assign (resid 59 and name hd2*) (resid 54 and name hb* ) 4.5 4.5 0.0 ! 978 15N assign (resid 60 and name hg2*) (resid 38 and name hg2*) 2.5 2.5 0.0 ! 780 13C assign (resid 60 and name hg2*) (resid 39 and name hn ) 4.5 4.5 0.0 ! 1103 15N assign (resid 60 and name hb ) (resid 40 and name ha ) 3.5 3.5 0.0 ! 1959 13C assign (resid 60 and name hg2*) (resid 40 and name ha ) 3.5 3.5 0.0 ! 1453 13C assign (resid 60 and name hg2*) (resid 41 and name hn ) 4.5 4.5 0.0 ! 1108 15N assign (resid 61 and name hg2*) (resid 41 and name hg1*) 5.1 5.1 0.0 ! 797 13C assign (resid 61 and name hb ) (resid 41 and name hg2*) 5.1 5.1 0.0 ! 352 13C assign (resid 61 and name hg2*) (resid 41 and name hg2*) 3.0 3.0 0.0 ! 785 13C assign (resid 61 and name hg2*) (resid 41 and name hb ) 5.5 5.5 0.0 ! 788 13C assign (resid 61 and name ha ) (resid 41 and name hg2*) 3.5 3.5 0.0 ! 353 13C assign (resid 61 and name hg1*) (resid 43 and name he ) 4.5 4.5 0.0 ! 719 15N assign (resid 61 and name hg1*) (resid 43 and name hb2 ) 4.5 4.5 0.0 ! 536 13C assign (resid 61 and name hg2*) (resid 43 and name ha ) 3.5 3.5 0.0 ! 790 13C assign (resid 61 and name hg1*) (resid 43 and name hb1 ) 3.5 3.5 0.0 ! 537 13C assign (resid 61 and name hg1*) (resid 43 and name hg* ) 3.8 3.8 0.0 ! 1106 13C assign (resid 61 and name hg1*) (resid 43 and name ha ) 3.5 3.5 0.0 ! 805 13C assign (resid 61 and name hg2*) (resid 46 and name hb* ) 4.5 4.5 0.0 ! 1668 13C assign (resid 62 and name hn ) (resid 40 and name hg1*) 4.5 4.5 0.0 ! 1911 13C assign (resid 63 and name hg2*) (resid 43 and name hg* ) 3.6 3.6 0.0 ! 1107 13C assign (resid 63 and name hg2*) (resid 43 and name hb1 ) 3.5 3.5 0.0 ! 911 13C assign (resid 63 and name hg2*) (resid 43 and name hb2 ) 3.9 3.9 0.0 ! 910 13C assign (resid 63 and name hg2*) (resid 43 and name hd* ) 5.5 5.5 0.0 ! 662 13C assign (resid 63 and name hb ) (resid 43 and name hn ) 4.5 4.5 0.0 ! 721 15N assign (resid 68 and name he* ) (resid 43 and name he ) 4.5 4.5 0.0 ! 715 15N assign (resid 68 and name hd* ) (resid 43 and name hd* ) 5.6 5.6 0.0 ! 657 13C assign (resid 68 and name hb* ) (resid 61 and name hg* ) 5.5 5.5 0.0 ! 807 13C assign (resid 68 and name he* ) (resid 61 and name hg1*) 3.5 3.5 0.0 ! 801 13C assign (resid 68 and name hd* ) (resid 61 and name hg1*) 3.5 3.5 0.0 ! 802 13C assign (resid 68 and name he* ) (resid 61 and name hg2*) 3.5 3.5 0.0 ! 793 13C assign (resid 68 and name hd* ) (resid 61 and name hg2*) 4.5 4.5 0.0 ! 1966 13C assign (resid 68 and name hb1 ) (resid 63 and name hg2*) 3.5 3.5 0.0 ! 1820 13C assign (resid 68 and name he* ) (resid 63 and name hg2*) 4.5 4.5 0.0 ! 1824 13C assign (resid 68 and name hb2 ) (resid 63 and name hg2*) 3.5 3.5 0.0 ! 1821 13C assign (resid 68 and name hd* ) (resid 63 and name hg2*) 3.5 3.5 0.0 ! 1825 13C assign (resid 68 and name hn ) (resid 63 and name hg2*) 4.5 4.5 0.0 ! 489 13C assign (resid 70 and name hb* ) (resid 60 and name ha ) 5.0 5.0 0.0 ! 1508 13C assign (resid 70 and name hb* ) (resid 61 and name hg1*) 3.6 3.6 0.0 ! 810 13C assign (resid 70 and name hb* ) (resid 61 and name hg2*) 3.5 3.5 0.0 ! 345 13C assign (resid 70 and name hb* ) (resid 61 and name hn ) 4.5 4.5 0.0 ! 1166 15N assign (resid 70 and name hb* ) (resid 61 and name hb ) 3.5 3.5 0.0 ! 1963 13C assign (resid 72 and name ha* ) (resid 53 and name hb* ) 4.5 4.5 0.0 ! 1981 13C assign (resid 72 and name ha* ) (resid 53 and name hg* ) 3.5 3.5 0.0 ! 1984 13C assign (resid 73 and name hb* ) (resid 53 and name hb* ) 3.5 3.5 0.0 ! 571 13C assign (resid 73 and name hn ) (resid 53 and name hg* ) 5.5 5.5 0.0 ! 314 15N assign (resid 73 and name ha ) (resid 59 and name hb2 ) 4.5 4.5 0.0 ! 1957 13C assign (resid 73 and name hb* ) (resid 59 and name hb* ) 3.5 3.5 0.0 ! 653 13C assign (resid 73 and name ha ) (resid 59 and name hb* ) 4.5 4.5 0.0 ! 1956 13C assign (resid 73 and name ha ) (resid 61 and name hg2*) 5.5 5.5 0.0 ! 792 13C assign (resid 73 and name hb* ) (resid 61 and name hg2*) 3.0 3.0 0.0 ! 798 13C assign (resid 74 and name hn ) (resid 60 and name hg2*) 3.5 3.5 0.0 ! 1852 13C assign (resid 74 and name hb ) (resid 60 and name hg2*) 3.5 3.5 0.0 ! 2000 13C assign (resid 74 and name hb ) (resid 60 and name ha ) 3.5 3.5 0.0 ! 119 D2O assign (resid 74 and name hb ) (resid 61 and name hn ) 4.5 4.5 0.0 ! 1168 15N assign (resid 75 and name hg1*) (resid 61 and name hg2*) 5.5 5.5 0.0 ! 368 13C assign (resid 75 and name ha ) (resid 61 and name hb ) 3.5 3.5 0.0 ! 296 D2O assign (resid 75 and name hg1*) (resid 61 and name hb ) 3.5 3.5 0.0 ! 1866 13C assign (resid 75 and name hg2*) (resid 61 and name hg2*) 3.5 3.5 0.0 ! 2019 13C assign (resid 75 and name hg2*) (resid 61 and name hg1*) 3.8 3.8 0.0 ! 2020 13C assign (resid 75 and name hg2*) (resid 61 and name hb ) 3.5 3.5 0.0 ! 2018 13C assign (resid 75 and name hn ) (resid 61 and name hg* ) 5.1 5.1 0.0 ! 796 13C assign (resid 75 and name hg2*) (resid 61 and name hn ) 4.5 4.5 0.0 ! 1164 15N assign (resid 75 and name hg1*) (resid 61 and name hg1*) 3.5 3.5 0.0 ! 1864 13C assign (resid 75 and name hg2*) (resid 68 and name hb* ) 4.5 4.5 0.0 ! 2016 13C assign (resid 75 and name hg1*) (resid 68 and name hb2 ) 3.5 3.5 0.0 ! 1863 13C assign (resid 75 and name hg1*) (resid 68 and name hb1 ) 4.5 4.5 0.0 ! 1862 13C assign (resid 75 and name hg2*) (resid 68 and name hd* ) 3.5 3.5 0.0 ! 2013 13C assign (resid 75 and name hg2*) (resid 69 and name hg* ) 4.5 4.5 0.0 ! 1350 13C assign (resid 75 and name hg1*) (resid 69 and name hn ) 3.8 3.8 0.0 ! 924 15N assign (resid 75 and name hg2*) (resid 69 and name hn ) 4.5 4.5 0.0 ! 926 15N assign (resid 75 and name hn ) (resid 70 and name hb* ) 4.8 4.8 0.0 ! 1223 15N assign (resid 75 and name hg* ) (resid 70 and name ha ) 5.5 5.5 0.0 ! 1859 13C assign (resid 75 and name hg2*) (resid 70 and name hn ) 3.5 3.5 0.0 ! 253 15N assign (resid 75 and name hg* ) (resid 70 and name hb* ) 4.5 4.5 0.0 ! 1865 13C assign (resid 76 and name hn ) (resid 61 and name hb ) 4.5 4.5 0.0 ! 1230 15N assign (resid 76 and name hn ) (resid 62 and name hd* ) 4.6 4.6 0.0 ! 1710 13C assign (resid 76 and name hg2*) (resid 62 and name hb* ) 3.5 3.5 0.0 ! 1515 13C assign (resid 76 and name hg1*) (resid 62 and name hd* ) 4.5 4.5 0.0 ! 1718 13C assign (resid 76 and name hg2*) (resid 62 and name ha ) 2.5 2.5 0.0 ! 1519 13C assign (resid 76 and name hb ) (resid 62 and name hd* ) 3.5 3.5 0.0 ! 1722 13C assign (resid 77 and name ha ) (resid 62 and name hd* ) 3.5 3.5 0.0 ! 1709 13C assign (resid 77 and name hb* ) (resid 62 and name ha ) 5.1 5.1 0.0 ! 2026 13C assign (resid 77 and name hb1 ) (resid 62 and name hd* ) 4.6 4.6 0.0 ! 1717 13C assign (resid 77 and name ha ) (resid 63 and name hg2*) 4.5 4.5 0.0 ! 1968 13C assign (resid 77 and name hd2 ) (resid 63 and name hn ) 4.5 4.5 0.0 ! 1174 15N assign (resid 77 and name he1 ) (resid 66 and name ha ) 3.5 3.5 0.0 ! 83 13C assign (resid 78 and name hn ) (resid 62 and name hd* ) 3.5 3.5 0.0 ! 1698 13C assign (resid 78 and name ha ) (resid 62 and name hd* ) 3.5 3.5 0.0 ! 1697 13C assign (resid 79 and name hn ) (resid 62 and name hd* ) 3.5 3.5 0.0 ! 1712 13C assign (resid 79 and name ha ) (resid 62 and name hd* ) 3.5 3.5 0.0 ! 1716 13C assign (resid 81 and name hb* ) (resid 76 and name hg2*) 3.5 3.5 0.0 ! 1514 13C assign (resid 81 and name hb* ) (resid 76 and name hb ) 2.5 2.5 0.0 ! 1838 13C assign (resid 81 and name hb* ) (resid 76 and name hg1*) 2.5 2.5 0.0 ! 404 13C assign (resid 81 and name hn ) (resid 76 and name hb ) 4.5 4.5 0.0 ! 1261 15N assign (resid 82 and name hg2*) (resid 40 and name hg2*) 2.6 2.6 0.0 ! 1743 13C assign (resid 82 and name hg2*) (resid 62 and name hd* ) 2.5 2.5 0.0 ! 1741 13C assign (resid 82 and name hg2*) (resid 62 and name ha ) 4.6 4.6 0.0 ! 1732 13C assign (resid 82 and name hg2*) (resid 76 and name hg1*) 3.5 3.5 0.0 ! 1831 13C assign (resid 82 and name hg2*) (resid 76 and name hg2*) 2.5 2.5 0.0 ! 1516 13C assign (resid 82 and name hn ) (resid 76 and name hg2*) 3.9 3.9 0.0 ! 1522 13C assign (resid 82 and name hg2*) (resid 76 and name hb ) 3.5 3.5 0.0 ! 1737 13C assign (resid 82 and name ha ) (resid 76 and name hg2*) 3.5 3.5 0.0 ! 97 D2O assign (resid 82 and name ha ) (resid 76 and name hg1*) 3.5 3.5 0.0 ! 96 D2O assign (resid 82 and name hn ) (resid 76 and name hg1*) 3.5 3.5 0.0 ! 1833 13C assign (resid 82 and name hg2*) (resid 77 and name hn ) 4.5 4.5 0.0 ! 1730 13C assign (resid 85 and name he* ) (resid 38 and name hg2*) 3.5 3.5 0.0 ! 778 13C assign (resid 85 and name hd* ) (resid 38 and name hg2*) 2.5 2.5 0.0 ! 89 13C assign (resid 85 and name hd* ) (resid 38 and name hd1*) 2.5 2.5 0.0 ! 88 13C assign (resid 85 and name he* ) (resid 38 and name hd1*) 3.5 3.5 0.0 ! 209 13C assign (resid 85 and name he* ) (resid 58 and name hg2*) 3.5 3.5 0.0 ! 1412 13C assign (resid 85 and name he* ) (resid 74 and name hg2*) 3.5 3.5 0.0 ! 1489 13C assign (resid 85 and name he* ) (resid 74 and name hg1*) 3.5 3.5 0.0 ! 1990 13C assign (resid 85 and name hd* ) (resid 74 and name hg1*) 2.5 2.5 0.0 ! 90 13C assign (resid 86 and name ha ) (resid 38 and name hd1*) 2.6 2.6 0.0 ! 761 13C assign (resid 86 and name hb* ) (resid 38 and name hd1*) 3.5 3.5 0.0 ! 1827 13C assign (resid 89 and name hb1 ) (resid 38 and name hd1*) 3.5 3.5 0.0 ! 2073 13C assign (resid 89 and name ha ) (resid 38 and name hd1*) 4.6 4.6 0.0 ! 766 13C assign (resid 89 and name hb2 ) (resid 38 and name hd1*) 3.5 3.5 0.0 ! 2072 13C assign (resid 89 and name hn ) (resid 38 and name hd1*) 4.5 4.5 0.0 ! 1290 15N assign (resid 92 and name hb* ) (resid 38 and name hd1*) 3.5 3.5 0.0 ! 763 13C assign (resid 92 and name he21) (resid 38 and name hd1*) 4.5 4.5 0.0 ! 210 13C assign (resid 92 and name hn ) (resid 38 and name hd1*) 4.5 4.5 0.0 ! 774 15N assign (resid 92 and name hg* ) (resid 38 and name hd1*) 3.5 3.5 0.0 ! 1192 13C assign (resid 92 and name he21) (resid 58 and name hb ) 4.5 4.5 0.0 ! 778 15N assign (resid 92 and name he22) (resid 58 and name hb ) 4.5 4.5 0.0 ! 786 15N assign (resid 92 and name he21) (resid 58 and name hg2*) 4.5 4.5 0.0 ! 1420 13C assign (resid 94 and name ha ) (resid 38 and name hg2*) 3.5 3.5 0.0 ! 777 13C assign (resid 94 and name ha ) (resid 38 and name hb ) 3.5 3.5 0.0 ! 1196 13C assign (resid 94 and name hd* ) (resid 38 and name hb ) 3.5 3.5 0.0 ! 1199 13C assign (resid 94 and name hd* ) (resid 82 and name hg2*) 3.6 3.6 0.0 ! 1744 13C assign (resid 94 and name hd* ) (resid 83 and name hd* ) 2.6 2.6 0.0 ! 86 13C assign (resid 94 and name hd* ) (resid 86 and name ha ) 4.5 4.5 0.0 ! 2315 13C assign (resid 94 and name hd* ) (resid 86 and name hn ) 3.5 3.5 0.0 ! 2309 13C assign (resid 94 and name hd* ) (resid 86 and name hb* ) 2.5 2.5 0.0 ! 1761 13C assign (resid 94 and name hd* ) (resid 87 and name hn ) 5.5 5.5 0.0 ! 996 15N assign (resid 95 and name hg* ) (resid 2 and name hb* ) 2.5 2.5 0.0 ! 291 13C assign (resid 95 and name ha ) (resid 2 and name hb* ) 3.5 3.5 0.0 ! 293 13C assign (resid 95 and name hg* ) (resid 4 and name hn ) 4.5 4.5 0.0 ! 57 15N assign (resid 95 and name hn ) (resid 38 and name hb ) 4.5 4.5 0.0 ! 1202 13C assign (resid 95 and name hb ) (resid 39 and name ha ) 4.5 4.5 0.0 ! 2107 13C assign (resid 95 and name hg* ) (resid 40 and name hn ) 4.6 4.6 0.0 ! 1104 15N assign (resid 96 and name hn ) (resid 1 and name hg2*) 3.5 3.5 0.0 ! 1324 15N assign (resid 96 and name hn ) (resid 2 and name hb* ) 4.5 4.5 0.0 ! 1325 15N assign (resid 96 and name hn ) (resid 3 and name hd* ) 3.5 3.5 0.0 ! 343 15N assign (resid 96 and name hb ) (resid 3 and name ha ) 3.5 3.5 0.0 ! 2110 13C assign (resid 96 and name hb ) (resid 3 and name he* ) 4.5 4.5 0.0 ! 2113 13C assign (resid 96 and name hn ) (resid 3 and name he* ) 5.5 5.5 0.0 ! 1320 15N assign (resid 96 and name hg2*) (resid 3 and name he* ) 3.5 3.5 0.0 ! 440 13C assign (resid 96 and name hb ) (resid 3 and name hd* ) 4.5 4.5 0.0 ! 2111 13C assign (resid 96 and name hd1*) (resid 40 and name hg1*) 3.5 3.5 0.0 ! 1914 13C assign (resid 96 and name hd1*) (resid 40 and name hg2*) 2.5 2.5 0.0 ! 2257 13C assign (resid 96 and name hd1*) (resid 40 and name hb ) 2.5 2.5 0.0 ! 388 13C assign (resid 96 and name hg2*) (resid 40 and name hg1*) 3.5 3.5 0.0 ! 2121 13C assign (resid 96 and name hg2*) (resid 40 and name hb ) 3.5 3.5 0.0 ! 448 13C assign (resid 96 and name hd1*) (resid 82 and name hg2*) 4.5 4.5 0.0 ! 1745 13C assign (resid 97 and name hb* ) (resid 4 and name hd2*) 3.5 3.5 0.0 ! 1846 13C assign (resid 97 and name hb* ) (resid 39 and name he* ) 3.5 3.5 0.0 ! 2124 13C assign (resid 97 and name hn ) (resid 40 and name hb ) 4.5 4.5 0.0 ! 988 15N assign (resid 97 and name hn ) (resid 40 and name hg2*) 4.6 4.6 0.0 ! 989 15N assign (resid 97 and name hb* ) (resid 41 and name hg1*) 2.5 2.5 0.0 ! 1925 13C assign (resid 97 and name hn ) (resid 41 and name hg1*) 4.5 4.5 0.0 ! 993 15N assign (resid 97 and name hb* ) (resid 45 and name hg2*) 4.0 4.0 0.0 ! 1845 13C assign (resid 98 and name hn ) (resid 40 and name hb ) 5.0 5.0 0.0 ! 1337 15N assign (resid 98 and name hn ) (resid 41 and name hg1*) 4.5 4.5 0.0 ! 1339 15N assign (resid 99 and name hn ) (resid 45 and name hg2*) 4.0 4.0 0.0 ! 1438 13C assign (resid 100 and name hb* ) (resid 13 and name hd1*) 3.5 3.5 0.0 ! 2129 13C assign (resid 100 and name hn ) (resid 13 and name hd1*) 4.5 4.5 0.0 ! 1571 13C assign (resid 102 and name hg2*) (resid 40 and name hb ) 3.6 3.6 0.0 ! 1550 13C assign (resid 102 and name hg2*) (resid 41 and name ha ) 4.5 4.5 0.0 ! 2133 13C assign (resid 102 and name hd1*) (resid 42 and name ha1 ) 3.5 3.5 0.0 ! 360 D2O assign (resid 102 and name hd1*) (resid 42 and name ha2 ) 3.5 3.5 0.0 ! 361 D2O assign (resid 102 and name hd1*) (resid 42 and name hn ) 4.0 4.0 0.0 ! 454 13C assign (resid 102 and name hd1*) (resid 43 and name hn ) 5.5 5.5 0.0 ! 453 13C assign (resid 102 and name hd1*) (resid 62 and name ha ) 4.5 4.5 0.0 ! 452 13C assign (resid 102 and name hd1*) (resid 62 and name hd* ) 3.5 3.5 0.0 ! 457 13C assign (resid 102 and name hg2*) (resid 96 and name hg2*) 2.5 2.5 0.0 ! 1826 13C assign (resid 103 and name he* ) (resid 4 and name hn ) 3.6 3.6 0.0 ! 17 15N assign (resid 103 and name ha ) (resid 96 and name hg2*) 3.5 3.5 0.0 ! 157 D2O assign (resid 103 and name hd* ) (resid 96 and name hg2*) 3.5 3.5 0.0 ! 439 13C assign (resid 103 and name he* ) (resid 98 and name hn ) 4.5 4.5 0.0 ! 1330 15N assign (resid 103 and name hz ) (resid 98 and name hn ) 5.1 5.1 0.0 ! 1331 15N assign (resid 105 and name hb* ) (resid 79 and name hg* ) 2.5 2.5 0.0 ! 1876 13C assign (resid 105 and name hn ) (resid 96 and name hg2*) 5.5 5.5 0.0 ! 1373 15N assign (resid 106 and name hb* ) (resid 3 and name he* ) 4.5 4.5 0.0 ! 2156 13C assign (resid 106 and name he* ) (resid 40 and name hg1*) 3.5 3.5 0.0 ! 1912 13C assign (resid 106 and name hz ) (resid 40 and name hg1*) 3.5 3.5 0.0 ! 1913 13C assign (resid 106 and name he* ) (resid 62 and name hd* ) 4.5 4.5 0.0 ! 1714 13C assign (resid 106 and name he* ) (resid 79 and name hb ) 5.0 5.0 0.0 ! 81 13C assign (resid 106 and name hz ) (resid 79 and name hg* ) 3.5 3.5 0.0 ! 2032 13C assign (resid 106 and name hb2 ) (resid 79 and name hg* ) 3.5 3.5 0.0 ! 1871 13C assign (resid 106 and name he* ) (resid 79 and name hg* ) 2.5 2.5 0.0 ! 84 13C assign (resid 106 and name he* ) (resid 80 and name hn ) 5.6 5.6 0.0 ! 1249 15N assign (resid 106 and name hz ) (resid 81 and name hn ) 6.0 6.0 0.0 ! 1262 15N assign (resid 106 and name hz ) (resid 81 and name hb* ) 5.6 5.6 0.0 ! 2035 13C assign (resid 106 and name he* ) (resid 82 and name hn ) 4.5 4.5 0.0 ! 336 15N assign (resid 106 and name hz ) (resid 82 and name hg2*) 3.5 3.5 0.0 ! 29 13C assign (resid 106 and name hz ) (resid 82 and name hg1*) 3.5 3.5 0.0 ! 55 13C assign (resid 106 and name he* ) (resid 82 and name hg1*) 2.5 2.5 0.0 ! 83 13C assign (resid 106 and name he* ) (resid 82 and name hb ) 4.5 4.5 0.0 ! 2049 13C assign (resid 106 and name he* ) (resid 82 and name hg2*) 3.5 3.5 0.0 ! 80 13C assign (resid 106 and name he* ) (resid 83 and name hn ) 4.5 4.5 0.0 ! 1265 15N assign (resid 106 and name he* ) (resid 96 and name hd1*) 4.5 4.5 0.0 ! 141 13C assign (resid 107 and name hn ) (resid 3 and name hd* ) 5.6 5.6 0.0 ! 1384 15N assign (resid 107 and name hn ) (resid 3 and name he* ) 4.5 4.5 0.0 ! 1381 15N assign (resid 109 and name hb2 ) (resid 83 and name he* ) 3.5 3.5 0.0 ! 594 13C assign (resid 109 and name hb1 ) (resid 83 and name he* ) 3.5 3.5 0.0 ! 593 13C assign (resid 110 and name ha ) (resid 1 and name ht* ) 4.5 4.5 0.0 ! 1050 15N assign (resid 110 and name hg1*) (resid 2 and name hn ) 4.5 4.5 0.0 ! 1689 13C assign (resid 110 and name hg1*) (resid 2 and name ha ) 3.5 3.5 0.0 ! 1682 13C assign (resid 110 and name hg1*) (resid 3 and name hn ) 3.5 3.5 0.0 ! 1688 13C assign (resid 110 and name hg1*) (resid 3 and name hd* ) 3.5 3.5 0.0 ! 1683 13C assign (resid 110 and name hg1*) (resid 3 and name hb* ) 4.5 4.5 0.0 ! 1678 13C assign (resid 111 and name hb* ) (resid 1 and name ht* ) 4.5 4.5 0.0 ! 490 15N assign (resid 111 and name ha ) (resid 1 and name ht* ) 3.7 3.7 0.0 ! 493 15N assign (resid 112 and name hg2*) (resid 1 and name ht* ) 4.7 4.7 0.0 ! 488 15N assign (resid 112 and name hb ) (resid 1 and name hb ) 5.8 5.8 0.0 ! 352 D2O assign (resid 112 and name hg2*) (resid 2 and name ha ) 4.5 4.5 0.0 ! 1406 13C assign (resid 112 and name hb ) (resid 2 and name ha ) 3.5 3.5 0.0 ! 48 13C assign (resid 112 and name hb ) (resid 2 and name hb* ) 3.5 3.5 0.0 ! 2163 13C assign (resid 112 and name hn ) (resid 2 and name hb* ) 4.5 4.5 0.0 ! 1877 13C assign (resid 113 and name ha ) (resid 2 and name hb* ) 3.9 3.9 0.0 ! 303 D2O assign (resid 113 and name hd2*) (resid 3 and name hd* ) 3.5 3.5 0.0 ! 2214 13C assign (resid 113 and name hd2*) (resid 3 and name hn ) 3.5 3.5 0.0 ! 2215 13C assign (resid 113 and name hd2*) (resid 3 and name hb* ) 4.5 4.5 0.0 ! 307 13C assign (resid 113 and name hb* ) (resid 4 and name ha ) 5.8 5.8 0.0 ! 2185 13C assign (resid 113 and name hd2*) (resid 5 and name he3 ) 5.0 5.0 0.0 ! 2219 13C assign (resid 113 and name hd1*) (resid 5 and name hz2 ) 5.5 5.5 0.0 ! 16 13C assign (resid 113 and name hd2*) (resid 5 and name hz3 ) 3.5 3.5 0.0 ! 2213 13C assign (resid 114 and name hd2*) (resid 2 and name ha ) 5.0 5.0 0.0 ! 2240 13C assign (resid 114 and name hd1*) (resid 2 and name hb* ) 3.5 3.5 0.0 ! 2232 13C assign (resid 114 and name hd1*) (resid 4 and name ha ) 3.5 3.5 0.0 ! 2229 13C assign (resid 114 and name hb* ) (resid 4 and name ha ) 4.5 4.5 0.0 ! 2224 13C assign (resid 114 and name hb1 ) (resid 5 and name hn ) 5.0 5.0 0.0 ! 70 15N assign (resid 114 and name hd1*) (resid 33 and name he22) 4.5 4.5 0.0 ! 379 15N assign (resid 115 and name ha ) (resid 5 and name he3 ) 4.5 4.5 0.0 ! 385 D2O assign (resid 115 and name hg2*) (resid 5 and name hz2 ) 4.5 4.5 0.0 ! 1534 13C assign (resid 115 and name hg1*) (resid 5 and name he1 ) 4.5 4.5 0.0 ! 1460 13C assign (resid 115 and name hg1*) (resid 5 and name hz2 ) 3.5 3.5 0.0 ! 1463 13C assign (resid 115 and name hg1*) (resid 7 and name hn ) 5.5 5.5 0.0 ! 71 15N assign (resid 115 and name hg2*) (resid 7 and name hn ) 4.5 4.5 0.0 ! 73 15N assign (resid 116 and name hb ) (resid 6 and name hb* ) 4.5 4.5 0.0 ! 180 13C assign (resid 116 and name hg2*) (resid 6 and name hb* ) 3.8 3.8 0.0 ! 1446 13C assign (resid 116 and name hb ) (resid 6 and name ha ) 3.8 3.8 0.0 ! 187 D2O assign (resid 116 and name hg2*) (resid 6 and name ha ) 4.5 4.5 0.0 ! 189 D2O assign (resid 116 and name hb ) (resid 7 and name hn ) 4.5 4.5 0.0 ! 77 15N assign (resid 118 and name hb* ) (resid 8 and name ha ) 4.5 4.5 0.0 ! 1143 13C assign (resid 121 and name hb* ) (resid 9 and name he ) 4.5 4.5 0.0 ! 727 15N assign (resid 121 and name hb* ) (resid 9 and name hn ) 4.5 4.5 0.0 ! 733 15N assign (resid 121 and name hb* ) (resid 9 and name hg* ) 4.5 4.5 0.0 ! 1138 13C assign (resid 121 and name ha ) (resid 9 and name hg* ) 4.5 4.5 0.0 ! 1139 13C assign (resid 122 and name hd* ) (resid 8 and name hn ) 4.8 4.8 0.0 ! 371 15N assign (resid 122 and name hd* ) (resid 9 and name hn ) 4.5 4.5 0.0 ! 123 15N assign (resid 122 and name he* ) (resid 9 and name hn ) 4.6 4.6 0.0 ! 731 15N assign (resid 124 and name ha* ) (resid 12 and name hd1*) 4.5 4.5 0.0 ! 1076 13C assign (resid 124 and name hn ) (resid 12 and name hd2*) 4.5 4.5 0.0 ! 671 15N assign (resid 124 and name hn ) (resid 12 and name hd1*) 3.5 3.5 0.0 ! 667 15N assign (resid 124 and name ha* ) (resid 15 and name hb* ) 5.5 5.5 0.0 ! 1078 13C assign (resid 125 and name hn ) (resid 12 and name hd2*) 5.5 5.5 0.0 ! 1454 15N assign (resid 125 and name hn ) (resid 12 and name hd1*) 4.5 4.5 0.0 ! 580 15N assign (resid 125 and name hn ) (resid 15 and name hg1 ) 4.5 4.5 0.0 ! 579 15N assign (resid 125 and name hn ) (resid 15 and name hb1 ) 4.5 4.5 0.0 ! 578 15N assign (resid 125 and name hn ) (resid 15 and name he* ) 4.5 4.5 0.0 ! 577 15N assign (resid 126 and name hg2*) (resid 13 and name hd1*) 2.5 2.5 0.0 ! 2381 13C assign (resid 126 and name hg2*) (resid 100 and name hb* ) 2.6 2.6 0.0 ! 2379 13C assign (resid 126 and name hg2*) (resid 100 and name hn ) 4.5 4.5 0.0 ! 2382 13C assign (resid 127 and name hb* ) (resid 12 and name ha ) 5.5 5.5 0.0 ! 2386 13C assign (resid 128 and name he* ) (resid 3 and name he* ) 3.5 3.5 0.0 ! 20 13C assign (resid 128 and name he* ) (resid 3 and name hd* ) 3.5 3.5 0.0 ! 17 13C assign (resid 128 and name he* ) (resid 5 and name hz2 ) 3.5 3.5 0.0 ! 14 13C assign (resid 128 and name hn ) (resid 13 and name hg2*) 4.5 4.5 0.0 ! 1777 13C assign (resid 128 and name ha ) (resid 13 and name hd1*) 3.5 3.5 0.0 ! 751 13C assign (resid 128 and name he* ) (resid 103 and name hd* ) 3.5 3.5 0.0 ! 197 13C assign (resid 128 and name he* ) (resid 103 and name hb2 ) 3.5 3.5 0.0 ! 192 13C assign (resid 129 and name hg2*) (resid 100 and name ha ) 3.5 3.5 0.0 ! 1496 13C assign (resid 129 and name hg2*) (resid 100 and name hb* ) 2.6 2.6 0.0 ! 2130 13C assign (resid 129 and name hg2*) (resid 103 and name hb2 ) 3.5 3.5 0.0 ! 2147 13C assign (resid 129 and name hg2*) (resid 103 and name hb1 ) 3.5 3.5 0.0 ! 2148 13C assign (resid 129 and name hd1*) (resid 103 and name hb2 ) 3.5 3.5 0.0 ! 2142 13C assign (resid 129 and name hd1*) (resid 103 and name hb1 ) 4.5 4.5 0.0 ! 2143 13C assign (resid 129 and name hb ) (resid 104 and name hb ) 3.5 3.5 0.0 ! 173 13C assign (resid 129 and name hd1*) (resid 104 and name hb ) 2.5 2.5 0.0 ! 193 13C assign (resid 129 and name hd1*) (resid 104 and name hg2*) 3.8 3.8 0.0 ! 1885 13C assign (resid 129 and name hd1*) (resid 104 and name hn ) 3.5 3.5 0.0 ! 203 13C assign (resid 129 and name hg12) (resid 104 and name hn ) 4.5 4.5 0.0 ! 1369 15N assign (resid 129 and name hg2*) (resid 104 and name hn ) 3.5 3.5 0.0 ! 1504 13C assign (resid 129 and name hg2*) (resid 104 and name hb ) 3.5 3.5 0.0 ! 2343 13C assign (resid 129 and name hd1*) (resid 107 and name hn ) 4.5 4.5 0.0 ! 192 13C assign (resid 129 and name hd1*) (resid 107 and name hd* ) 3.5 3.5 0.0 ! 198 13C assign (resid 131 and name hd1*) (resid 5 and name hz2 ) 3.5 3.5 0.0 ! 1789 13C assign (resid 131 and name hd2*) (resid 113 and name hd1*) 4.5 4.5 0.0 ! 2208 13C assign (resid 131 and name hd1*) (resid 113 and name hd2*) 3.5 3.5 0.0 ! 2203 13C assign (resid 131 and name hd1*) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 3 13C assign (resid 133 and name hz3 ) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 73 13C assign (resid 133 and name hh2 ) (resid 113 and name hb2 ) 4.5 4.5 0.0 ! 2184 13C assign (resid 133 and name he3 ) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 11 13C assign (resid 133 and name hh2 ) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 2198 13C assign (resid 133 and name hz2 ) (resid 113 and name hd1*) 4.6 4.6 0.0 ! 71 13C assign (resid 133 and name hh2 ) (resid 114 and name hn ) 5.5 5.5 0.0 ! 1425 15N assign (resid 133 and name hh2 ) (resid 115 and name hg1*) 2.5 2.5 0.0 ! 1458 13C assign (resid 133 and name hh2 ) (resid 115 and name hg2*) 3.5 3.5 0.0 ! 1530 13C assign (resid 133 and name hz3 ) (resid 115 and name hg1*) 3.5 3.5 0.0 ! 2246 13C assign (resid 133 and name hz2 ) (resid 115 and name hg2*) 4.5 4.5 0.0 ! 2249 13C assign (resid 133 and name hz2 ) (resid 115 and name hg1*) 4.5 4.5 0.0 ! 1465 13C assign (resid 136 and name he* ) (resid 110 and name hg1*) 3.5 3.5 0.0 ! 1684 13C assign (resid 136 and name hd* ) (resid 113 and name hg ) 4.5 4.5 0.0 ! 1794 13C assign (resid 136 and name hd* ) (resid 113 and name hn ) 4.5 4.5 0.0 ! 145 15N assign (resid 136 and name hb2 ) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 2194 13C assign (resid 136 and name hd* ) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 6 13C assign (resid 136 and name he* ) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 2200 13C assign (resid 136 and name he* ) (resid 113 and name hd2*) 3.5 3.5 0.0 ! 2220 13C assign (resid 136 and name he* ) (resid 113 and name hn ) 4.8 4.8 0.0 ! 1420 15N assign (resid 136 and name hd* ) (resid 131 and name hd2*) 3.6 3.6 0.0 ! 2450 13C assign (resid 137 and name hn ) (resid 113 and name hg ) 6.0 6.0 0.0 ! 813 15N assign (resid 137 and name hn ) (resid 113 and name hd1*) 4.6 4.6 0.0 ! 816 15N assign (resid 150 and name hb* ) (resid 120 and name ha2 ) 3.5 3.5 0.0 ! 500 13C assign (resid 150 and name hb* ) (resid 120 and name ha1 ) 3.5 3.5 0.0 ! 1098 13C assign (resid 150 and name hb* ) (resid 120 and name hn ) 3.6 3.6 0.0 ! 421 15N assign (resid 151 and name hb2 ) (resid 146 and name hb1 ) 4.5 4.5 0.0 ! 2327 13C assign (resid 152 and name hg2*) (resid 144 and name hn ) 4.5 4.5 0.0 ! 2507 13C assign (resid 152 and name hg2*) (resid 145 and name hg2 ) 3.5 3.5 0.0 ! 1279 13C assign (resid 152 and name hg2*) (resid 145 and name hg1 ) 3.5 3.5 0.0 ! 1280 13C assign (resid 152 and name hg2*) (resid 145 and name ha ) 2.5 2.5 0.0 ! 561 13C assign (resid 152 and name hg2*) (resid 145 and name hb* ) 3.5 3.5 0.0 ! 1215 13C assign (resid 152 and name hg2*) (resid 146 and name hn ) 3.5 3.5 0.0 ! 563 13C assign (resid 152 and name hb ) (resid 146 and name hn ) 4.6 4.6 0.0 ! 568 15N assign (resid 152 and name hn ) (resid 146 and name hb* ) 4.5 4.5 0.0 ! 1604 15N assign (resid 153 and name ha ) (resid 117 and name hb* ) 4.5 4.5 0.0 ! 2281 13C assign (resid 153 and name ha ) (resid 118 and name hg ) 4.5 4.5 0.0 ! 2282 13C assign (resid 153 and name hn ) (resid 144 and name hg* ) 4.5 4.5 0.0 ! 1613 15N assign (resid 154 and name hn ) (resid 116 and name hg2*) 4.5 4.5 0.0 ! 1629 15N assign (resid 154 and name hb ) (resid 117 and name hb* ) 3.5 3.5 0.0 ! 1116 13C assign (resid 154 and name hn ) (resid 117 and name hb* ) 4.5 4.5 0.0 ! 1627 15N assign (resid 154 and name hg2*) (resid 141 and name ha ) 3.5 3.5 0.0 ! 19 D2O assign (resid 154 and name hg2*) (resid 141 and name hb2 ) 3.5 3.5 0.0 ! 2515 13C assign (resid 154 and name hn ) (resid 143 and name hg2*) 3.6 3.6 0.0 ! 1837 13C assign (resid 154 and name hg2*) (resid 143 and name hn ) 4.5 4.5 0.0 ! 1566 15N assign (resid 154 and name hg2*) (resid 143 and name ha ) 3.5 3.5 0.0 ! 2511 13C assign (resid 154 and name hb ) (resid 143 and name hn ) 5.5 5.5 0.0 ! 2369 13C assign (resid 154 and name hb ) (resid 144 and name hn ) 5.6 5.6 0.0 ! 537 15N assign (resid 154 and name hg2*) (resid 144 and name hn ) 4.6 4.6 0.0 ! 541 15N assign (resid 154 and name hn ) (resid 144 and name hg* ) 4.9 4.9 0.0 ! 1630 15N assign (resid 155 and name hb* ) (resid 142 and name hb* ) 4.5 3.5 0.0 ! 2480 13C assign (resid 155 and name hn ) (resid 142 and name hb1 ) 4.5 4.5 0.0 ! 954 15N assign (resid 155 and name he* ) (resid 144 and name hg* ) 3.5 3.5 0.0 ! 1849 13C assign (resid 155 and name hd* ) (resid 144 and name hg* ) 2.5 2.5 0.0 ! 104 13C assign (resid 156 and name hb1 ) (resid 115 and name hg1*) 4.5 4.5 0.0 ! 1467 13C assign (resid 156 and name hb1 ) (resid 115 and name hg2*) 3.5 3.5 0.0 ! 1535 13C assign (resid 156 and name hn ) (resid 115 and name hg2*) 4.5 4.5 0.0 ! 1641 15N assign (resid 156 and name hn ) (resid 115 and name hg1*) 5.5 5.5 0.0 ! 1642 15N assign (resid 156 and name ha ) (resid 138 and name hd2 ) 4.5 4.5 0.0 ! 958 13C assign (resid 157 and name hg* ) (resid 112 and name hg2*) 2.8 2.8 0.0 ! 1410 13C assign (resid 157 and name hg* ) (resid 112 and name ha ) 5.5 5.5 0.0 ! 23 D2O assign (resid 157 and name ha ) (resid 112 and name hg2*) 4.5 4.5 0.0 ! 328 13C assign (resid 157 and name hb ) (resid 114 and name hd2*) 4.5 4.5 0.0 ! 2237 13C assign (resid 157 and name hn ) (resid 139 and name hg* ) 4.0 4.0 0.0 ! 1474 13C assign (resid 157 and name hb ) (resid 139 and name hg* ) 2.5 2.5 0.0 ! 1484 13C assign (resid 157 and name hg* ) (resid 140 and name hb2 ) 2.5 2.5 0.0 ! 1038 13C assign (resid 157 and name hg* ) (resid 140 and name hb1 ) 3.5 3.5 0.0 ! 1039 13C assign (resid 157 and name hb ) (resid 140 and name hb* ) 3.5 3.5 0.0 ! 1040 13C assign (resid 157 and name hn ) (resid 140 and name hb2 ) 3.5 3.5 0.0 ! 1648 15N assign (resid 158 and name hn ) (resid 112 and name hg2*) 3.5 3.5 0.0 ! 1398 13C assign (resid 158 and name hb* ) (resid 113 and name hg ) 4.5 4.5 0.0 ! 2353 13C assign (resid 158 and name hb* ) (resid 113 and name hn ) 4.5 4.5 0.0 ! 1423 15N assign (resid 158 and name hb* ) (resid 113 and name hb* ) 5.5 5.5 0.0 ! 2354 13C assign (resid 158 and name hd1 ) (resid 113 and name hd1*) 3.9 3.9 0.0 ! 2201 13C assign (resid 158 and name hb* ) (resid 113 and name hd2*) 4.5 4.5 0.0 ! 2355 13C assign (resid 158 and name hb2 ) (resid 113 and name hg ) 4.5 4.5 0.0 ! 2356 13C assign (resid 158 and name hb* ) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 2192 13C assign (resid 158 and name hd1 ) (resid 114 and name hn ) 4.6 4.6 0.0 ! 1163 15N assign (resid 158 and name hn ) (resid 114 and name hd2*) 4.5 4.5 0.0 ! 2243 13C assign (resid 158 and name hd1 ) (resid 114 and name ha ) 3.8 3.8 0.0 ! 201 13C assign (resid 158 and name he1 ) (resid 115 and name hg1*) 5.5 5.5 0.0 ! 1459 13C assign (resid 158 and name hd1 ) (resid 115 and name hg1*) 3.5 3.5 0.0 ! 173 13C assign (resid 158 and name he1 ) (resid 115 and name hg2*) 3.5 3.5 0.0 ! 1533 13C assign (resid 158 and name hd1 ) (resid 115 and name hg2*) 5.5 5.5 0.0 ! 174 13C assign (resid 158 and name hn ) (resid 115 and name hg* ) 5.5 5.5 0.0 ! 2250 13C assign (resid 158 and name hd1 ) (resid 133 and name hz3 ) 4.5 4.5 0.0 ! 172 13C assign (resid 158 and name he3 ) (resid 136 and name hb2 ) 4.5 4.5 0.0 ! 578 13C assign (resid 158 and name he3 ) (resid 136 and name hb1 ) 3.5 3.5 0.0 ! 579 13C assign (resid 158 and name he3 ) (resid 137 and name hg2*) 4.5 4.5 0.0 ! 1426 13C assign (resid 158 and name he3 ) (resid 137 and name hn ) 3.5 3.5 0.0 ! 799 15N assign (resid 158 and name he3 ) (resid 137 and name hb ) 5.5 5.5 0.0 ! 2454 13C assign (resid 158 and name he3 ) (resid 137 and name ha ) 3.5 3.5 0.0 ! 102 D2O assign (resid 158 and name he3 ) (resid 138 and name hg* ) 6.0 6.0 0.0 ! 1700 13C assign (resid 158 and name he3 ) (resid 138 and name ha ) 3.5 3.5 0.0 ! 706 13C assign (resid 158 and name he3 ) (resid 138 and name hn ) 3.5 3.5 0.0 ! 1521 15N assign (resid 158 and name hz2 ) (resid 138 and name he* ) 4.5 4.5 0.0 ! 969 13C assign (resid 158 and name he3 ) (resid 138 and name hb1 ) 4.6 4.6 0.0 ! 2465 13C assign (resid 158 and name he3 ) (resid 138 and name hb2 ) 3.5 3.5 0.0 ! 2466 13C assign (resid 158 and name he3 ) (resid 138 and name hg* ) 5.0 5.0 0.0 ! 1701 13C assign (resid 158 and name hz2 ) (resid 138 and name hd* ) 3.5 3.5 0.0 ! 956 13C assign (resid 158 and name hn ) (resid 139 and name hg* ) 4.5 4.5 0.0 ! 2251 13C assign (resid 158 and name ha ) (resid 139 and name hg* ) 2.8 2.8 0.0 ! 1476 13C assign (resid 159 and name ha ) (resid 110 and name hg1*) 5.5 5.5 0.0 ! 1691 13C assign (resid 159 and name hg1 ) (resid 112 and name hg2*) 3.6 3.6 0.0 ! 1408 13C assign (resid 159 and name hg2 ) (resid 112 and name hg2*) 3.5 3.5 0.0 ! 2164 13C assign (resid 159 and name ha ) (resid 112 and name hg2*) 3.5 3.5 0.0 ! 2526 13C assign (resid 159 and name hn ) (resid 113 and name hd1*) 5.5 5.5 0.0 ! 1672 15N assign (resid 159 and name hn ) (resid 113 and name hb2 ) 5.8 5.8 0.0 ! 1669 15N assign (resid 159 and name hn ) (resid 136 and name hd* ) 4.5 4.5 0.0 ! 1652 15N assign (resid 159 and name hn ) (resid 136 and name hb* ) 4.5 4.5 0.0 ! 1663 15N assign (resid 159 and name ha ) (resid 136 and name hd* ) 3.6 3.6 0.0 ! 312 D2O assign (resid 159 and name hn ) (resid 137 and name hg2*) 3.6 3.6 0.0 ! 1429 13C assign (resid 159 and name hb* ) (resid 137 and name hg2*) 3.5 3.5 0.0 ! 1430 13C assign (resid 159 and name hb1 ) (resid 137 and name hb ) 4.6 4.6 0.0 ! 156 13C assign (resid 159 and name hn ) (resid 137 and name hb ) 4.5 4.5 0.0 ! 149 13C assign (resid 159 and name hn ) (resid 138 and name hb* ) 5.5 5.5 0.0 ! 1670 15N assign (resid 159 and name ha ) (resid 139 and name hg* ) 5.5 5.5 0.0 ! 1477 13C assign (resid 159 and name hg* ) (resid 139 and name hg* ) 4.5 4.5 0.0 ! 1480 13C assign (resid 159 and name hn ) (resid 139 and name hb ) 5.6 5.6 0.0 ! 2473 13C assign (resid 159 and name hg1 ) (resid 139 and name hg* ) 2.5 2.5 0.0 ! 1479 13C assign (resid 159 and name he22) (resid 139 and name hg* ) 3.5 3.5 0.0 ! 1475 13C assign (resid 159 and name he21) (resid 139 and name hg* ) 3.5 3.5 0.0 ! 880 15N assign (resid 159 and name hb2 ) (resid 139 and name hg* ) 3.5 3.5 0.0 ! 2527 13C assign (resid 159 and name hn ) (resid 139 and name hg* ) 3.5 3.5 0.0 ! 1472 13C assign (resid 160 and name hn ) (resid 111 and name hb* ) 4.6 4.6 0.0 ! 1152 13C assign (resid 160 and name hd* ) (resid 111 and name hb* ) 4.5 4.5 0.0 ! 1155 13C assign (resid 160 and name hb* ) (resid 111 and name hb* ) 5.5 5.5 0.0 ! 1156 13C assign (resid 160 and name hg* ) (resid 111 and name ha ) 3.5 3.5 0.0 ! 1589 13C assign (resid 160 and name hn ) (resid 136 and name hd* ) 3.5 3.5 0.0 ! 241 15N assign (resid 160 and name ha ) (resid 136 and name hd* ) 3.5 3.5 0.0 ! 2532 13C assign (resid 160 and name ha ) (resid 136 and name he* ) 4.0 4.0 0.0 ! 2533 13C assign (resid 160 and name hn ) (resid 136 and name he* ) 3.5 3.5 0.0 ! 1673 15N assign (resid 160 and name ha ) (resid 137 and name hg2*) 6.0 6.0 0.0 ! 2538 13C assign (resid 161 and name hg2 ) (resid 136 and name ha ) 4.5 4.5 0.0 ! 986 13C assign (resid 161 and name hg1 ) (resid 136 and name ha ) 4.5 4.5 0.0 ! 987 13C assign (resid 161 and name hn ) (resid 136 and name hd* ) 4.5 4.5 0.0 ! 1686 15N assign (resid 161 and name hn ) (resid 136 and name hb* ) 4.5 4.5 0.0 ! 1682 15N assign (resid 161 and name he* ) (resid 137 and name hg2*) 3.5 3.5 0.0 ! 1422 13C assign (resid 161 and name he* ) (resid 137 and name hb ) 3.5 3.5 0.0 ! 16 D2O assign (resid 161 and name hg1 ) (resid 137 and name hb ) 4.5 4.5 0.0 ! 160 13C assign (resid 161 and name he* ) (resid 137 and name hn ) 4.5 4.5 0.0 ! 812 15N assign (resid 161 and name hg1 ) (resid 137 and name hn ) 4.5 4.5 0.0 ! 815 15N assign (resid 161 and name hn ) (resid 137 and name hg2*) 6.0 6.0 0.0 ! 1677 15N !Medium-range NOEs !HN(i) - HN(i+4) assign (resid 12 and name hn ) (resid 8 and name hn ) 4.5 4.5 0.0 ! 372 15N assign (resid 82 and name hn ) (resid 78 and name hn ) 4.5 4.5 0.0 ! 1263 15N !HN(i) - HN(i+3) assign (resid 11 and name hn ) (resid 8 and name hn ) 4.5 4.5 0.0 ! 373 15N assign (resid 81 and name hn ) (resid 78 and name hn ) 3.5 3.5 0.0 ! 117 15N assign (resid 87 and name hn ) (resid 84 and name hn ) 4.6 4.6 0.0 ! 1271 15N assign (resid 102 and name hn ) (resid 99 and name hn ) 4.5 4.5 0.0 ! 1353 15N assign (resid 107 and name hn ) (resid 104 and name hn ) 5.0 5.0 0.0 ! 1356 15N assign (resid 110 and name hn ) (resid 107 and name hn ) 5.0 5.0 0.0 ! 1401 15N assign (resid 151 and name hn ) (resid 148 and name hn ) 4.5 4.5 0.0 ! 1579 15N !HN(i) - HN(i+2) assign (resid 12 and name hn ) (resid 10 and name hn ) 4.5 4.5 0.0 ! 406 15N assign (resid 68 and name hn ) (resid 66 and name hn ) 4.5 4.5 0.0 ! 1187 15N assign (resid 73 and name hn ) (resid 71 and name hn ) 4.5 4.5 0.0 ! 468 15N assign (resid 80 and name hn ) (resid 78 and name hn ) 4.5 4.5 0.0 ! 1248 15N assign (resid 82 and name hn ) (resid 80 and name hn ) 4.5 4.5 0.0 ! 1251 15N assign (resid 83 and name hn ) (resid 81 and name hn ) 4.5 4.5 0.0 ! 1264 15N assign (resid 87 and name hn ) (resid 85 and name hn ) 4.5 4.5 0.0 ! 1037 15N assign (resid 89 and name hn ) (resid 87 and name hn ) 4.5 4.5 0.0 ! 220 15N assign (resid 91 and name hn ) (resid 89 and name hn ) 5.5 5.5 0.0 ! 1305 15N assign (resid 104 and name hn ) (resid 102 and name hn ) 5.5 5.5 0.0 ! 1349 15N assign (resid 108 and name hn ) (resid 106 and name hn ) 4.6 4.6 0.0 ! 1379 15N assign (resid 109 and name hn ) (resid 107 and name hn ) 4.5 4.5 0.0 ! 1400 15N assign (resid 110 and name hn ) (resid 108 and name hn ) 4.5 4.5 0.0 ! 522 15N assign (resid 134 and name hn ) (resid 132 and name hn ) 5.5 5.5 0.0 ! 1474 15N assign (resid 135 and name hn ) (resid 133 and name hn ) 4.5 4.5 0.0 ! 1495 15N assign (resid 152 and name hn ) (resid 150 and name hn ) 4.5 4.5 0.0 ! 1595 15N !Ha(i) - HN(i+3) assign (resid 31 and name ha ) (resid 34 and name hn ) 4.5 4.5 0.0 ! 1084 15N assign (resid 43 and name ha ) (resid 46 and name hn ) 3.5 3.5 0.0 ! 1029 15N assign (resid 44 and name ha ) (resid 47 and name hn ) 4.5 4.5 0.0 ! 837 15N assign (resid 45 and name ha ) (resid 48 and name hn ) 4.5 4.5 0.0 ! 1137 15N assign (resid 46 and name ha ) (resid 49 and name hn ) 4.5 4.5 0.0 ! 1143 15N assign (resid 78 and name ha ) (resid 81 and name hn ) 4.8 4.8 0.0 ! 119 15N assign (resid 79 and name ha ) (resid 82 and name hn ) 3.5 3.5 0.0 ! 1091 15N assign (resid 80 and name ha ) (resid 83 and name hn ) 3.8 3.8 0.0 ! 1266 15N assign (resid 82 and name ha ) (resid 85 and name hn ) 3.5 3.5 0.0 ! 1047 15N assign (resid 83 and name ha ) (resid 86 and name hn ) 3.5 3.5 0.0 ! 1273 15N assign (resid 84 and name ha ) (resid 87 and name hn ) 3.5 3.5 0.0 ! 218 15N assign (resid 86 and name ha ) (resid 89 and name hn ) 3.5 3.5 0.0 ! 1287 15N assign (resid 102 and name ha ) (resid 105 and name hn ) 3.6 3.6 0.0 ! 153 15N assign (resid 103 and name ha ) (resid 106 and name hn ) 4.5 4.5 0.0 ! 1377 15N assign (resid 107 and name ha ) (resid 110 and name hn ) 4.5 4.5 0.0 ! 1403 15N assign (resid 132 and name ha ) (resid 135 and name hn ) 4.5 4.5 0.0 ! 1511 15N assign (resid 133 and name ha ) (resid 136 and name hn ) 3.5 3.5 0.0 ! 858 13C !Ha(i) - HN(i+2) assign (resid 23 and name ha ) (resid 25 and name hn ) 4.5 4.5 0.0 ! 86 15N assign (resid 55 and name ha ) (resid 57 and name hn ) 5.5 5.5 0.0 ! 824 15N assign (resid 65 and name ha ) (resid 67 and name hn ) 4.5 4.5 0.0 ! 1181 15N assign (resid 66 and name ha ) (resid 68 and name hn ) 4.5 4.5 0.0 ! 1195 15N assign (resid 76 and name ha ) (resid 78 and name hn ) 4.5 4.5 0.0 ! 1005 15N assign (resid 78 and name ha ) (resid 80 and name hn ) 4.5 4.5 0.0 ! 1252 15N assign (resid 79 and name ha ) (resid 81 and name hn ) 4.5 4.5 0.0 ! 163 15N assign (resid 89 and name ha ) (resid 91 and name hn ) 3.5 3.5 0.0 ! 1304 15N assign (resid 96 and name ha ) (resid 98 and name hn ) 5.5 5.5 0.0 ! 1334 15N assign (resid 106 and name ha ) (resid 108 and name hn ) 4.5 4.5 0.0 ! 1398 15N assign (resid 118 and name ha ) (resid 120 and name hn ) 5.5 5.5 0.0 ! 1446 15N assign (resid 132 and name ha ) (resid 134 and name hn ) 3.5 3.5 0.0 ! 1496 15N assign (resid 133 and name ha ) (resid 135 and name hn ) 4.5 4.5 0.0 ! 857 13C assign (resid 148 and name ha ) (resid 150 and name hn ) 4.5 4.5 0.0 ! 429 15N !HN(i) - Hb(i+2,3,4) assign (resid 11 and name hn ) (resid 7 and name hb* ) 4.5 4.5 0.0 ! 743 15N assign (resid 11 and name hn ) (resid 8 and name hb2 ) 4.5 4.5 0.0 ! 740 15N assign (resid 42 and name hn ) (resid 45 and name hb ) 4.5 4.5 0.0 ! 1115 15N assign (resid 51 and name hn ) (resid 49 and name hb* ) 3.5 3.5 0.0 ! 388 15N assign (resid 54 and name hn ) (resid 57 and name hb* ) 4.5 4.5 0.0 ! 1948 13C assign (resid 57 and name hn ) (resid 54 and name hb1 ) 4.5 4.5 0.0 ! 828 15N assign (resid 57 and name hn ) (resid 54 and name hb2 ) 3.5 3.5 0.0 ! 826 15N assign (resid 68 and name hn ) (resid 65 and name hb* ) 3.5 3.5 0.0 ! 1970 13C assign (resid 73 and name hn ) (resid 70 and name hb* ) 3.5 3.5 0.0 ! 1512 13C assign (resid 77 and name hn ) (resid 81 and name hb* ) 3.5 3.5 0.0 ! 1548 13C assign (resid 78 and name hn ) (resid 76 and name hb ) 3.5 3.5 0.0 ! 1255 13C assign (resid 78 and name hn ) (resid 81 and name hb* ) 2.5 2.5 0.0 ! 1547 13C assign (resid 80 and name hn ) (resid 78 and name hb* ) 3.5 3.5 0.0 ! 1254 15N assign (resid 81 and name hn ) (resid 78 and name hb* ) 4.5 4.5 0.0 ! 162 15N assign (resid 81 and name hn ) (resid 79 and name hb ) 5.5 5.5 0.0 ! 1259 15N assign (resid 82 and name hn ) (resid 80 and name hb* ) 4.6 4.6 0.0 ! 1567 13C assign (resid 84 and name hn ) (resid 80 and name hb* ) 5.0 5.0 0.0 ! 2034 13C assign (resid 88 and name hn ) (resid 84 and name hb* ) 5.5 5.5 0.0 ! 909 15N assign (resid 99 and name hn ) (resid 102 and name hb ) 4.5 4.5 0.0 ! 34 15N assign (resid 107 and name hn ) (resid 104 and name hb ) 5.8 5.8 0.0 ! 2342 13C assign (resid 120 and name hn ) (resid 118 and name hb* ) 4.5 4.5 0.0 ! 444 15N assign (resid 135 and name hn ) (resid 132 and name hb* ) 4.5 4.5 0.0 ! 1285 13C assign (resid 136 and name hn ) (resid 132 and name hb2 ) 5.9 5.9 0.0 ! 1289 13C assign (resid 140 and name hn ) (resid 138 and name hb2 ) 5.5 5.5 0.0 ! 634 15N assign (resid 148 and name hn ) (resid 146 and name hb1 ) 4.5 4.5 0.0 ! 2495 13C assign (resid 148 and name hn ) (resid 146 and name hb2 ) 3.5 3.5 0.0 ! 2494 13C assign (resid 148 and name hn ) (resid 151 and name hb1 ) 4.6 4.6 0.0 ! 1589 15N assign (resid 148 and name hn ) (resid 151 and name hb2 ) 4.5 4.5 0.0 ! 1590 15N assign (resid 158 and name hn ) (resid 156 and name hb* ) 4.8 4.8 0.0 ! 923 13C !Ha(i) - Hb(i+2,3,4) assign (resid 43 and name ha ) (resid 46 and name hb* ) 3.5 3.5 0.0 ! 1933 13C assign (resid 44 and name ha ) (resid 47 and name hb2 ) 3.5 3.5 0.0 ! 1241 13C assign (resid 44 and name ha ) (resid 47 and name hb1 ) 4.3 4.3 0.0 ! 1240 13C assign (resid 45 and name ha ) (resid 48 and name hb* ) 4.5 4.5 0.0 ! 1934 13C assign (resid 70 and name ha ) (resid 73 and name hb* ) 5.5 5.5 0.0 ! 13C assign (resid 75 and name ha ) (resid 73 and name hb* ) 5.5 5.5 0.0 ! 13C assign (resid 78 and name ha ) (resid 80 and name hb* ) 5.5 5.5 0.0 ! 1568 13C assign (resid 78 and name ha ) (resid 81 and name hb* ) 4.5 4.5 0.0 ! 2037 13C assign (resid 79 and name ha ) (resid 82 and name hb ) 3.5 3.5 0.0 ! 2045 13C assign (resid 80 and name ha ) (resid 83 and name hb* ) 3.5 3.5 0.0 ! 522 13C assign (resid 81 and name ha ) (resid 84 and name hb* ) 2.5 2.5 0.0 ! 165 D2O assign (resid 83 and name ha ) (resid 86 and name hb* ) 2.5 2.5 0.0 ! 216 D2O assign (resid 84 and name ha ) (resid 87 and name hb* ) 3.5 3.5 0.0 ! 368 D2O assign (resid 85 and name ha ) (resid 88 and name hb* ) 3.5 3.5 0.0 ! 372 D2O assign (resid 86 and name ha ) (resid 89 and name hb* ) 4.5 4.5 0.0 ! 2069 13C assign (resid 89 and name ha ) (resid 91 and name hb* ) 4.1 4.1 0.0 ! 2080 13C assign (resid 100 and name ha ) (resid 103 and name hb1 ) 4.5 4.5 0.0 ! 2141 13C assign (resid 100 and name ha ) (resid 103 and name hb2 ) 3.5 3.5 0.0 ! 2140 13C assign (resid 102 and name ha ) (resid 105 and name hb* ) 3.5 3.5 0.0 ! 1805 13C assign (resid 104 and name ha ) (resid 107 and name hb* ) 3.5 3.5 0.0 ! 374 D2O assign (resid 133 and name ha ) (resid 136 and name hb* ) 4.5 4.5 0.0 ! 851 13C assign (resid 144 and name ha ) (resid 142 and name hb* ) 5.6 5.6 0.0 ! 2492 13C ! Other medium-range NOEs assign (resid 7 and name ha ) (resid 5 and name hd1 ) 5.5 5.5 0.0 ! 868 13C assign (resid 11 and name hn ) (resid 7 and name he22) 4.6 4.6 0.0 ! 1064 15N assign (resid 11 and name hn ) (resid 7 and name he21) 4.5 4.5 0.0 ! 737 15N assign (resid 11 and name hn ) (resid 7 and name hg1 ) 4.6 4.6 0.0 ! 1067 15N assign (resid 35 and name hg* ) (resid 32 and name ha ) 2.5 2.5 0.0 ! 356 D2O assign (resid 41 and name hg1*) (resid 39 and name he* ) 3.5 3.5 0.0 ! 1924 13C assign (resid 41 and name hg2*) (resid 39 and name he* ) 3.5 3.5 0.0 ! 57 13C assign (resid 43 and name ha ) (resid 41 and name hg2*) 4.5 4.5 0.0 ! 359 13C assign (resid 44 and name hn ) (resid 42 and name ha1 ) 4.5 4.5 0.0 ! 1123 15N assign (resid 44 and name hn ) (resid 42 and name ha2 ) 4.6 4.6 0.0 ! 240 15N assign (resid 44 and name hb1 ) (resid 42 and name ha1 ) 4.6 4.6 0.0 ! 1931 13C assign (resid 45 and name hb ) (resid 41 and name hg2*) 3.5 3.5 0.0 ! 360 13C assign (resid 45 and name hb ) (resid 41 and name hb ) 3.5 3.5 0.0 ! 169 13C assign (resid 45 and name hg2*) (resid 42 and name hn ) 3.5 3.5 0.0 ! 1111 15N assign (resid 45 and name hn ) (resid 43 and name hd1 ) 4.6 4.6 0.0 ! 1130 15N assign (resid 48 and name hn ) (resid 45 and name hg2*) 5.5 5.5 0.0 ! 1141 15N assign (resid 57 and name hb2 ) (resid 54 and name hb2 ) 5.5 5.5 0.0 ! 1936 13C assign (resid 59 and name hd2*) (resid 57 and name hb* ) 4.5 4.5 0.0 ! 1946 13C assign (resid 60 and name ha ) (resid 58 and name hg2*) 5.5 5.5 0.0 ! 1414 13C assign (resid 63 and name hg2*) (resid 61 and name hb ) 4.0 4.0 0.0 ! 1967 13C assign (resid 63 and name hg2*) (resid 61 and name hg1*) 2.5 2.5 0.0 ! 481 13C assign (resid 63 and name hb ) (resid 61 and name hg1*) 4.5 4.5 0.0 ! 278 13C assign (resid 65 and name hn ) (resid 63 and name hg2*) 3.5 3.5 0.0 ! 796 15N assign (resid 65 and name hb* ) (resid 63 and name hg2*) 3.5 3.5 0.0 ! 1822 13C assign (resid 67 and name hn ) (resid 63 and name hg2*) 5.5 5.5 0.0 ! 1185 15N assign (resid 67 and name hn ) (resid 65 and name he2*) 5.5 5.5 0.0 ! 1179 15N assign (resid 67 and name hn ) (resid 65 and name hg* ) 3.5 3.5 0.0 ! 1182 15N assign (resid 67 and name hn ) (resid 65 and name he21) 4.5 4.5 0.0 ! 1178 15N assign (resid 68 and name hn ) (resid 65 and name hg* ) 3.5 3.5 0.0 ! 1198 15N assign (resid 68 and name hn ) (resid 65 and name he21) 4.5 4.5 0.0 ! 1188 15N assign (resid 68 and name hb1 ) (resid 65 and name hb* ) 3.5 3.5 0.0 ! 1971 13C assign (resid 68 and name hb2 ) (resid 65 and name hb* ) 3.5 3.5 0.0 ! 555 13C assign (resid 70 and name hb* ) (resid 68 and name he* ) 3.5 3.5 0.0 ! 1509 13C assign (resid 70 and name hn ) (resid 68 and name hd* ) 4.6 4.6 0.0 ! 1207 15N assign (resid 70 and name hb* ) (resid 68 and name hd* ) 3.7 3.7 0.0 ! 93 13C assign (resid 78 and name hn ) (resid 76 and name hg1*) 4.5 4.5 0.0 ! 402 13C assign (resid 78 and name hn ) (resid 76 and name hg2*) 3.5 3.5 0.0 ! 1521 13C assign (resid 80 and name hb* ) (resid 78 and name hb* ) 3.5 3.5 0.0 ! 1634 13C assign (resid 81 and name hb* ) (resid 78 and name hb* ) 3.6 3.6 0.0 ! 1841 13C assign (resid 81 and name hn ) (resid 79 and name hg* ) 5.0 5.0 0.0 ! 1256 15N assign (resid 82 and name hg2*) (resid 78 and name hn ) 4.5 4.5 0.0 ! 1724 13C assign (resid 82 and name hg2*) (resid 78 and name ha ) 4.5 4.5 0.0 ! 1733 13C assign (resid 82 and name hn ) (resid 79 and name hg* ) 4.5 4.5 0.0 ! 1093 15N assign (resid 82 and name hb ) (resid 79 and name hg* ) 3.5 3.5 0.0 ! 2044 13C assign (resid 82 and name hg2*) (resid 79 and name hn ) 4.5 4.5 0.0 ! 1728 13C assign (resid 82 and name hg2*) (resid 79 and name ha ) 3.5 3.5 0.0 ! 1735 13C assign (resid 83 and name he* ) (resid 79 and name hg* ) 3.5 3.5 0.0 ! 2260 13C assign (resid 83 and name hd* ) (resid 79 and name hg* ) 3.0 3.0 0.0 ! 85 13C assign (resid 83 and name hn ) (resid 79 and name hg* ) 4.5 4.5 0.0 ! 1269 15N assign (resid 83 and name hb* ) (resid 80 and name hb* ) 4.5 4.5 0.0 ! 1569 13C assign (resid 83 and name hd* ) (resid 80 and name ha ) 3.1 3.1 0.0 ! 62 13C assign (resid 84 and name hn ) (resid 82 and name hg2*) 5.5 5.5 0.0 ! 1729 13C assign (resid 86 and name hb* ) (resid 82 and name hg1*) 3.5 3.5 0.0 ! 2041 13C assign (resid 86 and name hn ) (resid 82 and name hg1*) 4.5 4.5 0.0 ! 1280 15N assign (resid 86 and name hb* ) (resid 83 and name hd* ) 3.5 3.5 0.0 ! 65 13C assign (resid 87 and name hb* ) (resid 84 and name hb* ) 4.0 4.0 0.0 ! 1819 13C assign (resid 87 and name hg1 ) (resid 84 and name ha ) 3.5 3.5 0.0 ! 1605 13C assign (resid 87 and name hg2 ) (resid 84 and name ha ) 3.5 3.5 0.0 ! 1606 13C assign (resid 88 and name he2*) (resid 85 and name hn ) 4.5 4.5 0.0 ! 1034 15N assign (resid 88 and name he2*) (resid 86 and name hn ) 4.8 4.8 0.0 ! 1282 15N assign (resid 89 and name he1 ) (resid 85 and name he* ) 4.0 4.0 0.0 ! 56 13C assign (resid 89 and name hd2 ) (resid 86 and name hn ) 5.0 5.0 0.0 ! 1272 15N assign (resid 90 and name ha ) (resid 87 and name ha ) 4.8 4.8 0.0 ! 338 D2O assign (resid 90 and name hd1 ) (resid 87 and name ha ) 5.5 5.5 0.0 ! 218 13C assign (resid 90 and name hd* ) (resid 88 and name hn ) 4.5 4.5 0.0 ! 911 15N assign (resid 92 and name hn ) (resid 90 and name hd2 ) 5.5 5.5 0.0 ! 1309 15N assign (resid 96 and name hd1*) (resid 94 and name hd* ) 2.5 2.5 0.0 ! 1759 13C assign (resid 98 and name hn ) (resid 96 and name hg2*) 3.5 3.5 0.0 ! 1341 15N assign (resid 102 and name hg2*) (resid 98 and name ha* ) 3.6 3.6 0.0 ! 2139 13C assign (resid 102 and name hd1*) (resid 98 and name hn ) 6.0 6.0 0.0 ! 1340 15N assign (resid 102 and name hg2*) (resid 98 and name hn ) 4.5 4.5 0.0 ! 2134 13C assign (resid 102 and name hg11) (resid 99 and name hn ) 3.5 3.5 0.0 ! 35 15N assign (resid 102 and name hg12) (resid 99 and name hn ) 3.5 3.5 0.0 ! 36 15N assign (resid 102 and name hd1*) (resid 99 and name hn ) 4.5 4.5 0.0 ! 37 15N assign (resid 102 and name hn ) (resid 99 and name ha* ) 4.5 4.5 0.0 ! 46 15N assign (resid 103 and name hd* ) (resid 100 and name ha ) 3.5 3.5 0.0 ! 260 D2O assign (resid 105 and name hb* ) (resid 102 and name hd1*) 3.5 3.5 0.0 ! 1747 13C assign (resid 106 and name hn ) (resid 102 and name hg2*) 4.0 4.0 0.0 ! 2137 13C assign (resid 106 and name he* ) (resid 102 and name hg2*) 4.5 4.5 0.0 ! 2138 13C assign (resid 106 and name he* ) (resid 102 and name hd1*) 3.1 3.1 0.0 ! 82 13C assign (resid 107 and name he* ) (resid 104 and name hg2*) 3.6 3.6 0.0 ! 1882 13C assign (resid 107 and name hb* ) (resid 104 and name hg2*) 4.6 4.6 0.0 ! 1884 13C assign (resid 107 and name hd* ) (resid 104 and name hg2*) 3.6 3.6 0.0 ! 1886 13C assign (resid 107 and name hd* ) (resid 104 and name hb ) 3.5 3.5 0.0 ! 174 13C assign (resid 109 and name hb2 ) (resid 106 and name hd* ) 4.5 4.5 0.0 ! 1162 13C assign (resid 110 and name hg2*) (resid 107 and name hn ) 4.5 4.5 0.0 ! 1394 15N assign (resid 110 and name hg2*) (resid 108 and name hn ) 4.5 4.5 0.0 ! 599 15N assign (resid 112 and name hn ) (resid 110 and name hg1*) 2.5 2.5 0.0 ! 1686 13C assign (resid 113 and name hg ) (resid 110 and name hg1*) 3.5 3.5 0.0 ! 1694 13C assign (resid 113 and name ha ) (resid 110 and name hg1*) 3.5 3.5 0.0 ! 1681 13C assign (resid 113 and name hn ) (resid 110 and name hg1*) 4.5 4.5 0.0 ! 1690 13C assign (resid 113 and name hd1*) (resid 110 and name hg1*) 4.5 4.5 0.0 ! 1692 13C assign (resid 114 and name ha ) (resid 112 and name hg2*) 4.8 4.8 0.0 ! 1407 13C assign (resid 114 and name hg ) (resid 112 and name hg2*) 3.5 3.5 0.0 ! 1409 13C assign (resid 114 and name hd2*) (resid 112 and name hg2*) 2.5 2.5 0.0 ! 1411 13C assign (resid 115 and name hg2*) (resid 113 and name hd1*) 5.5 5.5 0.0 ! 2409 13C assign (resid 115 and name hg1*) (resid 113 and name hd1*) 4.5 4.5 0.0 ! 1470 13C assign (resid 122 and name he* ) (resid 120 and name hn ) 5.5 5.5 0.0 ! 450 15N assign (resid 131 and name hd2*) (resid 128 and name he* ) 3.6 3.6 0.0 ! 194 13C assign (resid 131 and name hg ) (resid 128 and name he* ) 4.5 4.5 0.0 ! 2400 13C assign (resid 131 and name hd1*) (resid 128 and name he* ) 3.5 3.5 0.0 ! 193 13C assign (resid 131 and name hd2*) (resid 129 and name hd1*) 3.5 3.5 0.0 ! 205 13C assign (resid 131 and name hd1*) (resid 129 and name hd1*) 5.5 5.5 0.0 ! 1765 13C assign (resid 131 and name hn ) (resid 129 and name hd1*) 5.5 5.5 0.0 ! 1466 15N assign (resid 133 and name he1 ) (resid 131 and name hd1*) 4.5 4.5 0.0 ! 1792 13C assign (resid 133 and name hh2 ) (resid 131 and name hd2*) 4.8 4.8 0.0 ! 2451 13C assign (resid 133 and name he1 ) (resid 131 and name hb1 ) 3.8 3.8 0.0 ! 916 13C assign (resid 133 and name he1 ) (resid 131 and name hb2 ) 4.5 4.5 0.0 ! 917 13C assign (resid 133 and name he1 ) (resid 131 and name hn ) 4.5 4.5 0.0 ! 644 15N assign (resid 133 and name hh2 ) (resid 131 and name hd1*) 3.5 3.5 0.0 ! 1788 13C assign (resid 133 and name hz2 ) (resid 131 and name hd1*) 3.5 3.5 0.0 ! 1790 13C assign (resid 133 and name hn ) (resid 131 and name hd2*) 5.5 5.5 0.0 ! 1483 15N assign (resid 134 and name hn ) (resid 132 and name hd22) 3.8 3.8 0.0 ! 1497 15N assign (resid 134 and name hn ) (resid 132 and name hd21) 4.5 4.5 0.0 ! 1499 15N assign (resid 134 and name hb1 ) (resid 132 and name hd22) 4.5 4.5 0.0 ! 2452 13C assign (resid 134 and name hb2 ) (resid 132 and name hd22) 3.5 3.5 0.0 ! 1380 13C assign (resid 135 and name hn ) (resid 132 and name hd22) 3.6 3.6 0.0 ! 554 15N assign (resid 135 and name hn ) (resid 132 and name hd21) 4.5 4.5 0.0 ! 638 15N assign (resid 136 and name he* ) (resid 132 and name hn ) 4.5 4.5 0.0 ! 1471 15N assign (resid 136 and name hd* ) (resid 133 and name ha ) 4.5 4.5 0.0 ! 853 13C assign (resid 136 and name he* ) (resid 133 and name ha ) 5.8 5.8 0.0 ! 854 13C assign (resid 136 and name hn ) (resid 133 and name he3 ) 5.5 5.5 0.0 ! 1237 15N assign (resid 139 and name hg* ) (resid 137 and name hg2*) 2.5 2.5 0.0 ! 1431 13C assign (resid 139 and name ha ) (resid 137 and name hg2*) 4.5 4.5 0.0 ! 2478 13C assign (resid 140 and name hn ) (resid 138 and name hg2 ) 3.8 3.8 0.0 ! 633 15N assign (resid 141 and name ha ) (resid 138 and name hd2 ) 4.1 4.1 0.0 ! 402 D2O assign (resid 141 and name hb2 ) (resid 138 and name hd2 ) 4.5 4.5 0.0 ! 954 13C assign (resid 141 and name hb2 ) (resid 138 and name hd1 ) 4.5 4.5 0.0 ! 955 13C assign (resid 141 and name hn ) (resid 139 and name hg* ) 5.5 5.5 0.0 ! 1543 15N assign (resid 145 and name hb* ) (resid 143 and name hg2*) 4.6 4.6 0.0 ! 1834 13C assign (resid 145 and name hg* ) (resid 143 and name hg2*) 3.5 3.5 0.0 ! 1277 13C assign (resid 146 and name hn ) (resid 144 and name hg* ) 4.1 4.1 0.0 ! 562 15N assign (resid 150 and name hb* ) (resid 148 and name hd22) 4.5 4.5 0.0 ! 970 15N assign (resid 150 and name hb* ) (resid 148 and name hd21) 4.5 4.5 0.0 ! 973 15N assign (resid 150 and name hn ) (resid 148 and name hd22) 4.5 4.5 0.0 ! 1095 15N assign (resid 151 and name hb2 ) (resid 148 and name hb2 ) 4.5 4.5 0.0 ! 2498 13C assign (resid 151 and name hd1*) (resid 148 and name hb2 ) 3.5 3.5 0.0 ! 517 13C assign (resid 151 and name hg ) (resid 148 and name hn ) 4.5 4.5 0.0 ! 1591 15N assign (resid 151 and name hd1*) (resid 148 and name hb1 ) 3.5 3.5 0.0 ! 518 13C assign (resid 151 and name hd2*) (resid 148 and name hb1 ) 4.5 4.5 0.0 ! 525 13C assign (resid 151 and name hg ) (resid 148 and name hd22) 4.5 4.5 0.0 ! 971 15N assign (resid 151 and name hg ) (resid 148 and name hd21) 4.5 4.5 0.0 ! 972 15N assign (resid 151 and name hd1*) (resid 148 and name hd21) 3.5 3.5 0.0 ! 974 15N assign (resid 151 and name hd2*) (resid 148 and name hd22) 5.5 5.5 0.0 ! 975 15N assign (resid 151 and name hd1*) (resid 148 and name hd22) 4.5 4.5 0.0 ! 969 15N assign (resid 151 and name hd* ) (resid 148 and name hn ) 4.5 4.5 0.0 ! 1594 15N assign (resid 156 and name ha ) (resid 154 and name hg2*) 4.1 4.1 0.0 ! 308 D2O assign (resid 156 and name hn ) (resid 154 and name hg2*) 4.5 4.5 0.0 ! 1644 15N assign (resid 158 and name he1 ) (resid 156 and name hb2 ) 3.5 3.5 0.0 ! 182 13C assign (resid 158 and name he1 ) (resid 156 and name hb1 ) 3.5 3.5 0.0 ! 183 13C assign (resid 158 and name hd1 ) (resid 156 and name hb2 ) 3.6 3.6 0.0 ! 925 13C assign (resid 158 and name hd1 ) (resid 156 and name hb1 ) 3.6 3.6 0.0 ! 926 13C assign (resid 158 and name hd1 ) (resid 156 and name hn ) 5.6 5.6 0.0 ! 679 15N assign (resid 159 and name ha ) (resid 157 and name hg* ) 5.0 5.0 0.0 ! 313 D2O !Sequential NOEs !HN(i) - HN(i+1) assign (resid 8 and name hn ) (resid 7 and name hn ) 4.8 4.8 0.0 ! 80 15N assign (resid 9 and name hn ) (resid 8 and name hn ) 4.5 4.5 0.0 ! 122 15N assign (resid 10 and name hn ) (resid 9 and name hn ) 4.5 4.5 0.0 ! 275 15N assign (resid 11 and name hn ) (resid 10 and name hn ) 3.5 3.5 0.0 ! 736 15N assign (resid 12 and name hn ) (resid 11 and name hn ) 3.5 3.5 0.0 ! 735 15N assign (resid 14 and name hn ) (resid 13 and name hn ) 5.5 5.5 0.0 ! 1077 15N assign (resid 33 and name hn ) (resid 32 and name hn ) 4.5 4.5 0.0 ! 456 15N assign (resid 34 and name hn ) (resid 33 and name hn ) 4.5 4.5 0.0 ! 102 15N assign (resid 35 and name hn ) (resid 34 and name hn ) 4.5 4.5 0.0 ! 92 15N assign (resid 37 and name hn ) (resid 36 and name hn ) 4.5 4.5 0.0 ! 325 15N assign (resid 38 and name hn ) (resid 37 and name hn ) 4.5 4.5 0.0 ! 1038 15N assign (resid 44 and name hn ) (resid 43 and name hn ) 4.5 4.5 0.0 ! 614 15N assign (resid 45 and name hn ) (resid 44 and name hn ) 3.5 3.5 0.0 ! 1128 15N assign (resid 46 and name hn ) (resid 45 and name hn ) 3.5 3.5 0.0 ! 1026 15N assign (resid 47 and name hn ) (resid 46 and name hn ) 4.5 4.5 0.0 ! 1027 15N assign (resid 48 and name hn ) (resid 47 and name hn ) 4.5 4.5 0.0 ! 1135 15N assign (resid 52 and name hn ) (resid 51 and name hn ) 4.5 4.5 0.0 ! 383 15N assign (resid 57 and name hn ) (resid 56 and name hn ) 3.5 3.5 0.0 ! 1148 15N assign (resid 59 and name hn ) (resid 58 and name hn ) 4.5 4.5 0.0 ! 1016 15N assign (resid 63 and name hn ) (resid 62 and name hn ) 4.5 4.5 0.0 ! 1175 15N assign (resid 66 and name hn ) (resid 65 and name hn ) 4.8 4.8 0.0 ! 790 15N assign (resid 67 and name hn ) (resid 66 and name hn ) 3.5 3.5 0.0 ! 230 15N assign (resid 68 and name hn ) (resid 67 and name hn ) 2.5 2.5 0.0 ! 1186 15N assign (resid 69 and name hn ) (resid 68 and name hn ) 5.0 5.0 0.0 ! 1189 15N assign (resid 70 and name hn ) (resid 69 and name hn ) 4.5 4.5 0.0 ! 912 15N assign (resid 71 and name hn ) (resid 70 and name hn ) 4.5 4.5 0.0 ! 764 15N assign (resid 72 and name hn ) (resid 71 and name hn ) 4.5 4.5 0.0 ! 572 15N assign (resid 73 and name hn ) (resid 72 and name hn ) 3.5 3.5 0.0 ! 312 15N assign (resid 74 and name hn ) (resid 73 and name hn ) 5.0 5.0 0.0 ! 1211 15N assign (resid 75 and name hn ) (resid 74 and name hn ) 5.5 5.5 0.0 ! 1210 15N assign (resid 76 and name hn ) (resid 75 and name hn ) 4.3 4.3 0.0 ! 1221 15N assign (resid 78 and name hn ) (resid 77 and name hn ) 2.5 2.5 0.0 ! 1075 15N assign (resid 79 and name hn ) (resid 78 and name hn ) 4.5 4.5 0.0 ! 1235 15N assign (resid 82 and name hn ) (resid 81 and name hn ) 3.5 3.5 0.0 ! 337 15N assign (resid 83 and name hn ) (resid 82 and name hn ) 3.5 3.5 0.0 ! 295 15N assign (resid 84 and name hn ) (resid 83 and name hn ) 3.0 3.0 0.0 ! 294 15N assign (resid 85 and name hn ) (resid 84 and name hn ) 3.5 3.5 0.0 ! 1036 15N assign (resid 86 and name hn ) (resid 85 and name hn ) 3.5 3.5 0.0 ! 1035 15N assign (resid 87 and name hn ) (resid 86 and name hn ) 3.5 3.5 0.0 ! 290 15N assign (resid 88 and name hn ) (resid 87 and name hn ) 3.5 3.5 0.0 ! 899 15N assign (resid 89 and name hn ) (resid 88 and name hn ) 3.5 3.5 0.0 ! 900 15N assign (resid 92 and name hn ) (resid 91 and name hn ) 3.5 3.5 0.0 ! 1306 15N assign (resid 93 and name hn ) (resid 92 and name hn ) 5.0 5.0 0.0 ! 771 15N assign (resid 98 and name hn ) (resid 97 and name hn ) 3.5 3.5 0.0 ! 1332 15N assign (resid 100 and name hn ) (resid 99 and name hn ) 4.5 4.5 0.0 ! 754 15N assign (resid 102 and name hn ) (resid 101 and name hn ) 4.5 4.5 0.0 ! 1348 15N assign (resid 103 and name hn ) (resid 102 and name hn ) 3.5 3.5 0.0 ! 39 15N assign (resid 104 and name hn ) (resid 103 and name hn ) 3.5 3.5 0.0 ! 1355 15N assign (resid 105 and name hn ) (resid 104 and name hn ) 3.5 3.5 0.0 ! 1357 15N assign (resid 106 and name hn ) (resid 105 and name hn ) 3.5 3.5 0.0 ! 150 15N assign (resid 108 and name hn ) (resid 107 and name hn ) 3.5 3.5 0.0 ! 1382 15N assign (resid 109 and name hn ) (resid 108 and name hn ) 2.6 2.6 0.0 ! 604 15N assign (resid 110 and name hn ) (resid 109 and name hn ) 3.5 3.5 0.0 ! 521 15N assign (resid 111 and name hn ) (resid 110 and name hn ) 5.5 5.5 0.0 ! 1405 15N assign (resid 112 and name hn ) (resid 111 and name hn ) 3.5 3.5 0.0 ! 191 15N assign (resid 114 and name hn ) (resid 113 and name hn ) 4.6 4.6 0.0 ! 1419 15N assign (resid 117 and name hn ) (resid 116 and name hn ) 5.5 5.5 0.0 ! 1439 15N assign (resid 121 and name hn ) (resid 120 and name hn ) 4.6 4.6 0.0 ! 422 15N assign (resid 123 and name hn ) (resid 122 and name hn ) 4.5 4.5 0.0 ! 676 15N assign (resid 125 and name hn ) (resid 124 and name hn ) 4.5 4.5 0.0 ! 662 15N assign (resid 126 and name hn ) (resid 125 and name hn ) 3.5 3.5 0.0 ! 573 15N assign (resid 132 and name hn ) (resid 131 and name hn ) 4.8 4.8 0.0 ! 1469 15N assign (resid 133 and name hn ) (resid 132 and name hn ) 4.5 4.5 0.0 ! 1493 15N assign (resid 134 and name hn ) (resid 133 and name hn ) 3.5 3.5 0.0 ! 1500 15N assign (resid 135 and name hn ) (resid 134 and name hn ) 3.5 3.5 0.0 ! 1501 15N assign (resid 136 and name hn ) (resid 135 and name hn ) 3.5 3.5 0.0 ! 553 15N assign (resid 137 and name hn ) (resid 136 and name hn ) 5.0 5.0 0.0 ! 803 15N assign (resid 138 and name hn ) (resid 137 and name hn ) 4.5 4.5 0.0 ! 1519 15N assign (resid 139 and name hn ) (resid 138 and name hn ) 5.5 5.5 0.0 ! 1520 15N assign (resid 140 and name hn ) (resid 139 and name hn ) 3.5 3.5 0.0 ! 631 15N assign (resid 141 and name hn ) (resid 140 and name hn ) 4.5 4.5 0.0 ! 1537 15N assign (resid 142 and name hn ) (resid 141 and name hn ) 4.5 4.5 0.0 ! 1536 15N assign (resid 145 and name hn ) (resid 144 and name hn ) 4.5 4.5 0.0 ! 1574 15N assign (resid 146 and name hn ) (resid 145 and name hn ) 5.5 5.5 0.0 ! 1573 15N assign (resid 147 and name hn ) (resid 146 and name hn ) 4.6 4.6 0.0 ! 570 15N assign (resid 148 and name hn ) (resid 147 and name hn ) 3.5 3.5 0.0 ! 1578 15N assign (resid 151 and name hn ) (resid 150 and name hn ) 3.5 3.5 0.0 ! 431 15N assign (resid 152 and name hn ) (resid 151 and name hn ) 3.5 3.5 0.0 ! 432 15N assign (resid 153 and name hn ) (resid 152 and name hn ) 4.5 4.5 0.0 ! 624 15N assign (resid 156 and name hn ) (resid 155 and name hn ) 4.5 4.5 0.0 ! 950 15N assign (resid 158 and name hn ) (resid 157 and name hn ) 4.5 4.5 0.0 ! 690 15N assign (resid 159 and name hn ) (resid 158 and name hn ) 5.0 5.0 0.0 ! 1657 15N assign (resid 160 and name hn ) (resid 159 and name hn ) 4.5 4.5 0.0 ! 1675 15N assign (resid 161 and name hn ) (resid 160 and name hn ) 5.0 5.0 0.0 ! 1689 15N assign (resid 162 and name hn ) (resid 161 and name hn ) 4.5 4.5 0.0 ! 1688 15N !Ha(i) - HN(i+1) assign (resid 2 and name ha ) (resid 3 and name hn ) 2.5 2.5 0.0 ! 137 13C assign (resid 3 and name ha ) (resid 4 and name hn ) 3.5 3.5 0.0 ! 54 15N assign (resid 4 and name ha ) (resid 5 and name hn ) 3.5 3.5 0.0 ! 312 13C assign (resid 5 and name ha ) (resid 6 and name hn ) 4.5 4.5 0.0 ! 366 15N assign (resid 6 and name ha ) (resid 7 and name hn ) 3.5 3.5 0.0 ! 78 15N assign (resid 7 and name ha ) (resid 8 and name hn ) 3.5 3.5 0.0 ! 867 13C assign (resid 8 and name ha ) (resid 9 and name hn ) 3.5 3.5 0.0 ! 299 15N assign (resid 10 and name ha ) (resid 11 and name hn ) 4.5 4.5 0.0 ! 738 15N assign (resid 11 and name ha2 ) (resid 12 and name hn ) 4.5 4.5 0.0 ! 544 15N assign (resid 32 and name ha ) (resid 33 and name hn ) 4.5 4.5 0.0 ! 943 15N assign (resid 33 and name ha ) (resid 34 and name hn ) 4.5 4.5 0.0 ! 96 15N assign (resid 35 and name ha ) (resid 36 and name hn ) 3.5 3.5 0.0 ! 326 15N assign (resid 36 and name ha* ) (resid 37 and name hn ) 3.5 3.5 0.0 ! 1042 15N assign (resid 38 and name ha ) (resid 39 and name hn ) 2.5 2.5 0.0 ! 287 15N assign (resid 39 and name ha ) (resid 40 and name hn ) 3.5 3.5 0.0 ! 758 13C assign (resid 40 and name ha ) (resid 41 and name hn ) 3.5 3.5 0.0 ! 193 15N assign (resid 41 and name ha ) (resid 42 and name hn ) 3.5 3.5 0.0 ! 1118 15N assign (resid 42 and name ha1 ) (resid 43 and name hn ) 3.5 3.5 0.0 ! 618 15N assign (resid 42 and name ha2 ) (resid 43 and name hn ) 4.5 4.5 0.0 ! 613 15N assign (resid 43 and name ha ) (resid 44 and name hn ) 4.5 4.5 0.0 ! 239 15N assign (resid 44 and name ha ) (resid 45 and name hn ) 3.8 3.8 0.0 ! 497 15N assign (resid 45 and name ha ) (resid 46 and name hn ) 4.5 4.5 0.0 ! 1030 15N assign (resid 47 and name ha ) (resid 48 and name hn ) 4.0 4.0 0.0 ! 1138 15N assign (resid 48 and name ha ) (resid 49 and name hn ) 4.5 4.5 0.0 ! 318 15N assign (resid 50 and name ha ) (resid 51 and name hn ) 4.5 4.5 0.0 ! 386 15N assign (resid 53 and name ha ) (resid 54 and name hn ) 3.5 3.5 0.0 ! 397 15N assign (resid 55 and name ha ) (resid 56 and name hn ) 3.5 3.5 0.0 ! 1021 15N assign (resid 56 and name ha ) (resid 57 and name hn ) 3.5 3.5 0.0 ! 822 15N assign (resid 57 and name ha ) (resid 58 and name hn ) 3.5 3.5 0.0 ! 1019 15N assign (resid 58 and name ha ) (resid 59 and name hn ) 3.5 3.5 0.0 ! 682 15N assign (resid 59 and name ha ) (resid 60 and name hn ) 2.5 2.5 0.0 ! 507 15N assign (resid 60 and name ha ) (resid 61 and name hn ) 3.5 3.5 0.0 ! 710 15N assign (resid 61 and name ha ) (resid 62 and name hn ) 3.5 3.5 0.0 ! 545 15N assign (resid 64 and name ha ) (resid 65 and name hn ) 4.5 4.5 0.0 ! 934 15N assign (resid 65 and name ha ) (resid 66 and name hn ) 2.5 2.5 0.0 ! 231 15N assign (resid 66 and name ha ) (resid 67 and name hn ) 3.5 3.5 0.0 ! 223 15N assign (resid 67 and name ha ) (resid 68 and name hn ) 3.5 3.5 0.0 ! 873 13C assign (resid 68 and name ha ) (resid 69 and name hn ) 2.5 2.5 0.0 ! 918 15N assign (resid 70 and name ha ) (resid 71 and name hn ) 2.5 2.5 0.0 ! 766 15N assign (resid 72 and name ha1 ) (resid 73 and name hn ) 3.5 3.5 0.0 ! 308 15N assign (resid 72 and name ha2 ) (resid 73 and name hn ) 3.8 3.8 0.0 ! 23 13C assign (resid 74 and name ha ) (resid 75 and name hn ) 2.5 2.5 0.0 ! 1213 15N assign (resid 75 and name ha ) (resid 76 and name hn ) 3.5 3.5 0.0 ! 262 15N assign (resid 76 and name ha ) (resid 77 and name hn ) 3.5 3.5 0.0 ! 1080 15N assign (resid 77 and name ha ) (resid 78 and name hn ) 3.6 3.6 0.0 ! 1002 15N assign (resid 78 and name ha ) (resid 79 and name hn ) 3.5 3.5 0.0 ! 1241 15N assign (resid 79 and name ha ) (resid 80 and name hn ) 3.5 3.5 0.0 ! 273 13C assign (resid 81 and name ha ) (resid 82 and name hn ) 3.8 3.8 0.0 ! 423 15N assign (resid 82 and name ha ) (resid 83 and name hn ) 4.0 4.0 0.0 ! 2350 13C assign (resid 83 and name ha ) (resid 84 and name hn ) 3.8 3.8 0.0 ! 762 15N assign (resid 84 and name ha ) (resid 85 and name hn ) 4.0 4.0 0.0 ! 1049 15N assign (resid 85 and name ha ) (resid 86 and name hn ) 4.0 4.0 0.0 ! 1274 15N assign (resid 88 and name ha ) (resid 89 and name hn ) 3.5 3.5 0.0 ! 1286 15N assign (resid 90 and name ha ) (resid 89 and name hn ) 4.5 4.5 0.0 ! 21 15N assign (resid 90 and name ha ) (resid 91 and name hn ) 3.5 3.5 0.0 ! 2429 13C assign (resid 91 and name ha ) (resid 92 and name hn ) 3.8 3.8 0.0 ! 773 15N assign (resid 94 and name ha ) (resid 95 and name hn ) 3.5 3.5 0.0 ! 243 D2O assign (resid 95 and name ha ) (resid 96 and name hn ) 3.5 3.5 0.0 ! 341 15N assign (resid 96 and name ha ) (resid 97 and name hn ) 3.5 3.5 0.0 ! 250 15N assign (resid 97 and name ha ) (resid 98 and name hn ) 4.5 4.5 0.0 ! 1342 15N assign (resid 98 and name ha* ) (resid 99 and name hn ) 3.5 3.5 0.0 ! 33 15N assign (resid 100 and name ha ) (resid 101 and name hn ) 4.0 4.0 0.0 ! 1345 15N assign (resid 101 and name ha ) (resid 102 and name hn ) 4.5 4.5 0.0 ! 1350 15N assign (resid 102 and name ha ) (resid 103 and name hn ) 4.0 4.0 0.0 ! 23 15N assign (resid 103 and name ha ) (resid 104 and name hn ) 4.5 4.5 0.0 ! 1362 15N assign (resid 104 and name ha ) (resid 105 and name hn ) 3.5 3.5 0.0 ! 152 15N assign (resid 106 and name ha ) (resid 107 and name hn ) 4.5 4.5 0.0 ! 1385 15N assign (resid 107 and name ha ) (resid 108 and name hn ) 4.5 4.5 0.0 ! 601 15N assign (resid 109 and name ha ) (resid 110 and name hn ) 3.6 3.6 0.0 ! 520 15N assign (resid 110 and name ha ) (resid 111 and name hn ) 4.5 4.5 0.0 ! 745 15N assign (resid 111 and name ha ) (resid 112 and name hn ) 4.5 4.5 0.0 ! 1408 15N assign (resid 112 and name ha ) (resid 113 and name hn ) 2.5 2.5 0.0 ! 47 13C assign (resid 113 and name ha ) (resid 114 and name hn ) 3.5 3.5 0.0 ! 376 D2O assign (resid 114 and name ha ) (resid 113 and name hn ) 5.5 5.5 0.0 ! 1421 15N assign (resid 114 and name ha ) (resid 115 and name hn ) 3.5 3.5 0.0 ! 380 D2O assign (resid 115 and name ha ) (resid 116 and name hn ) 3.5 3.5 0.0 ! 704 15N assign (resid 117 and name ha ) (resid 118 and name hn ) 3.5 3.5 0.0 ! 363 15N assign (resid 120 and name ha2 ) (resid 121 and name hn ) 3.5 3.5 0.0 ! 15 13C assign (resid 120 and name ha1 ) (resid 121 and name hn ) 3.5 3.5 0.0 ! 20 13C assign (resid 122 and name ha ) (resid 123 and name hn ) 3.5 3.5 0.0 ! 673 15N assign (resid 123 and name ha ) (resid 124 and name hn ) 3.5 3.5 0.0 ! 664 15N assign (resid 124 and name ha2 ) (resid 125 and name hn ) 3.5 3.5 0.0 ! 36 13C assign (resid 124 and name ha1 ) (resid 125 and name hn ) 3.5 3.5 0.0 ! 35 13C assign (resid 126 and name ha ) (resid 127 and name hn ) 3.5 3.5 0.0 ! 640 15N assign (resid 128 and name ha ) (resid 129 and name hn ) 3.5 3.5 0.0 ! 283 15N assign (resid 130 and name ha ) (resid 131 and name hn ) 2.5 2.5 0.0 ! 2437 13C assign (resid 131 and name ha ) (resid 132 and name hn ) 3.5 3.5 0.0 ! 1467 15N assign (resid 132 and name ha ) (resid 133 and name hn ) 3.5 3.5 0.0 ! 1482 15N assign (resid 133 and name ha ) (resid 134 and name hn ) 3.6 3.6 0.0 ! 1504 15N assign (resid 135 and name ha ) (resid 136 and name hn ) 3.6 3.6 0.0 ! 484 15N assign (resid 136 and name ha ) (resid 137 and name hn ) 3.5 3.5 0.0 ! 50 13C assign (resid 137 and name ha ) (resid 138 and name hn ) 2.5 2.5 0.0 ! 1524 15N assign (resid 138 and name ha ) (resid 139 and name hn ) 2.5 2.5 0.0 ! 708 13C assign (resid 139 and name ha ) (resid 140 and name hn ) 3.5 3.5 0.0 ! 2476 13C assign (resid 140 and name ha ) (resid 141 and name hn ) 2.5 2.5 0.0 ! 1534 15N assign (resid 141 and name ha ) (resid 140 and name hn ) 5.5 5.5 0.0 ! 629 15N assign (resid 141 and name ha ) (resid 142 and name hn ) 3.5 3.5 0.0 ! 1552 15N assign (resid 142 and name ha ) (resid 143 and name hn ) 2.5 2.5 0.0 ! 1570 15N assign (resid 143 and name ha ) (resid 144 and name hn ) 3.5 3.5 0.0 ! 535 15N assign (resid 144 and name ha ) (resid 145 and name hn ) 2.5 2.5 0.0 ! 2484 13C assign (resid 145 and name ha ) (resid 146 and name hn ) 3.5 3.5 0.0 ! 565 15N assign (resid 146 and name ha ) (resid 147 and name hn ) 3.0 3.0 0.0 ! 1577 15N assign (resid 147 and name ha ) (resid 148 and name hn ) 4.5 4.5 0.0 ! 1584 15N assign (resid 149 and name ha ) (resid 148 and name hn ) 5.5 5.5 0.0 ! 1582 15N assign (resid 149 and name ha ) (resid 150 and name hn ) 3.6 3.6 0.0 ! 1597 15N assign (resid 150 and name ha ) (resid 151 and name hn ) 4.5 4.5 0.0 ! 440 15N assign (resid 151 and name ha ) (resid 152 and name hn ) 3.5 3.5 0.0 ! 463 15N assign (resid 153 and name ha ) (resid 154 and name hn ) 3.5 3.5 0.0 ! 941 13C assign (resid 154 and name ha ) (resid 155 and name hn ) 2.5 2.5 0.0 ! 957 15N assign (resid 155 and name ha ) (resid 156 and name hn ) 3.5 3.5 0.0 ! 1635 15N assign (resid 156 and name ha ) (resid 157 and name hn ) 3.5 3.5 0.0 ! 307 D2O assign (resid 157 and name ha ) (resid 158 and name hn ) 2.5 2.5 0.0 ! 49 13C assign (resid 158 and name ha ) (resid 159 and name hn ) 2.5 2.5 0.0 ! 48 13C assign (resid 159 and name ha ) (resid 160 and name hn ) 2.5 2.5 0.0 ! 315 13C assign (resid 160 and name ha ) (resid 161 and name hn ) 2.5 2.5 0.0 ! 2531 13C !Hb(i) - HN(i+1) assign (resid 1 and name hb ) (resid 2 and name hn ) 4.5 4.5 0.0 ! 1053 15N assign (resid 2 and name hb* ) (resid 3 and name hn ) 3.5 3.5 0.0 ! 295 13C assign (resid 3 and name hb* ) (resid 4 and name hn ) 4.5 4.5 0.0 ! 1905 13C assign (resid 5 and name hb* ) (resid 6 and name hn ) 2.5 2.5 0.0 ! 915 13C assign (resid 6 and name hb* ) (resid 7 and name hn ) 3.5 3.5 0.0 ! 75 15N assign (resid 7 and name hb* ) (resid 8 and name hn ) 3.5 3.5 0.0 ! 1191 13C assign (resid 9 and name hb2 ) (resid 10 and name hn ) 4.5 4.5 0.0 ! 1063 15N assign (resid 10 and name hb1 ) (resid 11 and name hn ) 3.5 3.5 0.0 ! 1147 13C assign (resid 10 and name hb2 ) (resid 11 and name hn ) 4.5 4.5 0.0 ! 1146 13C assign (resid 24 and name hb2 ) (resid 25 and name hn ) 4.5 4.5 0.0 ! 1083 15N assign (resid 32 and name hb* ) (resid 33 and name hn ) 3.5 3.5 0.0 ! 1808 13C assign (resid 35 and name hb ) (resid 36 and name hn ) 3.5 3.5 0.0 ! 330 15N assign (resid 38 and name hb ) (resid 39 and name hn ) 4.6 4.6 0.0 ! 594 15N assign (resid 40 and name hb ) (resid 41 and name hn ) 4.0 4.0 0.0 ! 418 13C assign (resid 43 and name hb* ) (resid 44 and name hn ) 3.5 3.5 0.0 ! 530 13C assign (resid 45 and name hb ) (resid 46 and name hn ) 4.5 4.5 0.0 ! 1028 15N assign (resid 47 and name hb2 ) (resid 48 and name hn ) 3.5 3.5 0.0 ! 1139 15N assign (resid 47 and name hb1 ) (resid 48 and name hn ) 4.5 4.5 0.0 ! 1140 15N assign (resid 48 and name hb* ) (resid 49 and name hn ) 4.5 4.5 0.0 ! 320 15N assign (resid 50 and name hb2 ) (resid 51 and name hn ) 3.5 3.5 0.0 ! 1637 13C assign (resid 50 and name hb1 ) (resid 51 and name hn ) 4.5 4.5 0.0 ! 1663 13C assign (resid 51 and name hb* ) (resid 52 and name hn ) 4.0 4.0 0.0 ! 1363 13C assign (resid 53 and name hb* ) (resid 54 and name hn ) 3.5 3.5 0.0 ! 399 15N assign (resid 55 and name hb* ) (resid 56 and name hn ) 4.5 4.5 0.0 ! 1229 13C assign (resid 57 and name hb1 ) (resid 58 and name hn ) 4.5 4.5 0.0 ! 1150 15N assign (resid 58 and name hb ) (resid 59 and name hn ) 4.5 4.5 0.0 ! 1152 15N assign (resid 59 and name hb* ) (resid 60 and name hn ) 4.5 4.5 0.0 ! 505 15N assign (resid 64 and name hb* ) (resid 65 and name hn ) 4.5 4.5 0.0 ! 933 15N assign (resid 65 and name hb* ) (resid 66 and name hn ) 4.5 4.5 0.0 ! 1355 13C assign (resid 66 and name hb* ) (resid 67 and name hn ) 3.5 3.5 0.0 ! 1183 15N assign (resid 67 and name hb* ) (resid 68 and name hn ) 4.5 4.5 0.0 ! 882 13C assign (resid 68 and name hb* ) (resid 69 and name hn ) 3.6 3.6 0.0 ! 1977 13C assign (resid 69 and name hb2 ) (resid 70 and name hn ) 3.2 3.2 0.0 ! 1295 13C assign (resid 69 and name hb1 ) (resid 70 and name hn ) 4.5 4.5 0.0 ! 1205 13C assign (resid 70 and name hb* ) (resid 71 and name hn ) 3.5 3.5 0.0 ! 343 13C assign (resid 71 and name hb* ) (resid 72 and name hn ) 4.5 4.5 0.0 ! 1169 13C assign (resid 73 and name hb* ) (resid 74 and name hn ) 2.5 2.5 0.0 ! 568 13C assign (resid 75 and name hb ) (resid 76 and name hn ) 4.5 4.5 0.0 ! 1228 15N assign (resid 76 and name hb ) (resid 77 and name hn ) 2.5 2.5 0.0 ! 1254 13C assign (resid 77 and name hb* ) (resid 78 and name hn ) 4.5 4.5 0.0 ! 1013 15N assign (resid 78 and name hb* ) (resid 79 and name hn ) 3.5 3.5 0.0 ! 1631 13C assign (resid 79 and name hb ) (resid 80 and name hn ) 3.5 3.5 0.0 ! 1255 15N assign (resid 80 and name hb* ) (resid 81 and name hn ) 3.5 3.5 0.0 ! 1257 15N assign (resid 81 and name hb* ) (resid 82 and name hn ) 3.5 3.5 0.0 ! 74 13C assign (resid 82 and name hb ) (resid 81 and name hn ) 5.5 5.5 0.0 ! 164 15N assign (resid 82 and name hb ) (resid 83 and name hn ) 3.5 3.5 0.0 ! 2048 13C assign (resid 83 and name hb* ) (resid 84 and name hn ) 3.5 3.5 0.0 ! 524 13C assign (resid 84 and name hb* ) (resid 85 and name hn ) 3.0 3.0 0.0 ! 1813 13C assign (resid 85 and name hb2 ) (resid 86 and name hn ) 3.8 3.8 0.0 ! 1277 15N assign (resid 85 and name hb1 ) (resid 86 and name hn ) 4.5 4.5 0.0 ! 1278 15N assign (resid 86 and name hb* ) (resid 87 and name hn ) 3.5 3.5 0.0 ! 407 13C assign (resid 87 and name hb* ) (resid 88 and name hn ) 3.5 3.5 0.0 ! 1596 13C assign (resid 88 and name hb* ) (resid 89 and name hn ) 3.5 3.5 0.0 ! 1329 13C assign (resid 89 and name hb2 ) (resid 88 and name hn ) 4.5 4.5 0.0 ! 910 15N assign (resid 90 and name hb1 ) (resid 91 and name hn ) 4.8 4.8 0.0 ! 1617 13C assign (resid 90 and name hb2 ) (resid 91 and name hn ) 4.5 4.5 0.0 ! 1618 13C assign (resid 91 and name hb* ) (resid 92 and name hn ) 3.5 3.5 0.0 ! 1385 13C assign (resid 92 and name hb* ) (resid 93 and name hn ) 3.5 3.5 0.0 ! 1194 13C assign (resid 94 and name hb1 ) (resid 95 and name hn ) 4.5 4.5 0.0 ! 1317 15N assign (resid 95 and name hb ) (resid 96 and name hn ) 4.5 4.5 0.0 ! 340 15N assign (resid 97 and name hb* ) (resid 98 and name hn ) 4.0 4.0 0.0 ! 1546 13C assign (resid 100 and name hb* ) (resid 101 and name hn ) 3.5 3.5 0.0 ! 488 13C assign (resid 102 and name hb ) (resid 103 and name hn ) 3.5 3.5 0.0 ! 26 15N assign (resid 103 and name hb* ) (resid 104 and name hn ) 4.5 4.5 0.0 ! 1363 15N assign (resid 105 and name hb* ) (resid 106 and name hn ) 3.5 3.5 0.0 ! 1807 13C assign (resid 106 and name hb* ) (resid 107 and name hn ) 4.5 4.5 0.0 ! 1389 15N assign (resid 107 and name hb* ) (resid 108 and name hn ) 3.6 3.6 0.0 ! 1164 13C assign (resid 108 and name hb* ) (resid 109 and name hn ) 4.5 4.5 0.0 ! 750 15N assign (resid 109 and name hb1 ) (resid 110 and name hn ) 4.0 4.0 0.0 ! 591 13C assign (resid 109 and name hb2 ) (resid 110 and name hn ) 3.5 3.5 0.0 ! 590 13C assign (resid 110 and name hb ) (resid 111 and name hn ) 4.5 4.5 0.0 ! 2005 13C assign (resid 111 and name hb* ) (resid 112 and name hn ) 4.5 4.5 0.0 ! 1158 13C assign (resid 112 and name hb ) (resid 113 and name hn ) 5.5 5.5 0.0 ! 1424 15N assign (resid 113 and name hb* ) (resid 114 and name hn ) 5.5 5.5 0.0 ! 2183 13C assign (resid 115 and name hb ) (resid 116 and name hn ) 4.5 4.5 0.0 ! 703 15N assign (resid 117 and name hb* ) (resid 118 and name hn ) 4.5 4.5 0.0 ! 1111 13C assign (resid 122 and name hb* ) (resid 123 and name hn ) 3.5 3.5 0.0 ! 1089 13C assign (resid 123 and name hb* ) (resid 124 and name hn ) 3.5 3.5 0.0 ! 1082 13C assign (resid 126 and name hb ) (resid 127 and name hn ) 5.5 5.5 0.0 ! 1457 15N assign (resid 127 and name hb* ) (resid 128 and name hn ) 4.5 4.5 0.0 ! 1065 13C assign (resid 130 and name hb* ) (resid 131 and name hn ) 3.8 3.8 0.0 ! 1051 13C assign (resid 131 and name hb* ) (resid 132 and name hn ) 3.5 3.5 0.0 ! 85 13C assign (resid 132 and name hb* ) (resid 133 and name hn ) 4.5 4.5 0.0 ! 1287 13C assign (resid 133 and name hb* ) (resid 134 and name hn ) 3.5 3.5 0.0 ! 259 13C assign (resid 135 and name hb* ) (resid 136 and name hn ) 3.5 3.5 0.0 ! 1042 13C assign (resid 136 and name hb* ) (resid 137 and name hn ) 3.5 3.5 0.0 ! 583 13C assign (resid 137 and name hb ) (resid 138 and name hn ) 4.5 4.5 0.0 ! 151 13C assign (resid 138 and name hb1 ) (resid 139 and name hn ) 5.5 5.5 0.0 ! 2470 13C assign (resid 138 and name hb2 ) (resid 139 and name hn ) 4.5 4.5 0.0 ! 2469 13C assign (resid 139 and name hb ) (resid 140 and name hn ) 4.5 4.5 0.0 ! 1219 13C assign (resid 140 and name hb* ) (resid 141 and name hn ) 4.5 4.5 0.0 ! 1033 13C assign (resid 141 and name hb* ) (resid 142 and name hn ) 4.5 4.5 0.0 ! 1553 15N assign (resid 142 and name hb* ) (resid 143 and name hn ) 4.5 4.5 0.0 ! 1009 13C assign (resid 145 and name hb* ) (resid 146 and name hn ) 4.5 4.5 0.0 ! 1211 13C assign (resid 147 and name hb ) (resid 148 and name hn ) 4.5 4.5 0.0 ! 146 13C assign (resid 149 and name hb* ) (resid 150 and name hn ) 3.5 3.5 0.0 ! 1003 13C assign (resid 150 and name hb* ) (resid 151 and name hn ) 3.5 3.5 0.0 ! 434 15N assign (resid 151 and name hb* ) (resid 152 and name hn ) 4.5 4.5 0.0 ! 1605 15N assign (resid 153 and name hb* ) (resid 154 and name hn ) 4.5 4.5 0.0 ! 1625 15N assign (resid 154 and name hb ) (resid 155 and name hn ) 4.5 4.5 0.0 ! 959 15N assign (resid 155 and name hb2 ) (resid 156 and name hn ) 4.6 4.6 0.0 ! 1637 15N assign (resid 155 and name hb1 ) (resid 156 and name hn ) 5.5 5.5 0.0 ! 1645 15N assign (resid 156 and name hb* ) (resid 157 and name hn ) 4.5 4.5 0.0 ! 927 13C assign (resid 158 and name hb2 ) (resid 159 and name hn ) 4.5 4.5 0.0 ! 2362 13C assign (resid 158 and name hb1 ) (resid 159 and name hn ) 5.5 5.5 0.0 ! 1664 15N assign (resid 159 and name hb* ) (resid 160 and name hn ) 4.5 4.5 0.0 ! 1223 13C assign (resid 161 and name hb* ) (resid 162 and name hn ) 2.5 2.5 0.0 ! 975 13C !Other sequential NOEs assign (resid 2 and name hn ) (resid 1 and name ht* ) 3.5 3.5 0.0 ! 485 15N assign (resid 4 and name hn ) (resid 3 and name hd* ) 4.5 4.5 0.0 ! 16 15N assign (resid 5 and name hn ) (resid 4 and name hd1*) 4.5 4.5 0.0 ! 598 13C assign (resid 5 and name hn ) (resid 4 and name hd2*) 4.5 4.5 0.0 ! 1059 15N assign (resid 5 and name he3 ) (resid 4 and name hd1*) 4.5 4.5 0.0 ! 600 13C assign (resid 6 and name hn ) (resid 5 and name he3 ) 6.0 6.0 0.0 ! 369 15N assign (resid 10 and name hn ) (resid 9 and name hd* ) 3.5 3.5 0.0 ! 692 13C assign (resid 10 and name hn ) (resid 9 and name hg* ) 3.5 3.5 0.0 ! 1131 13C assign (resid 25 and name hn ) (resid 24 and name hg2 ) 4.5 4.5 0.0 ! 85 15N assign (resid 35 and name hg* ) (resid 34 and name hn ) 3.5 3.5 0.0 ! 324 15N assign (resid 36 and name hn ) (resid 35 and name hg* ) 3.5 3.5 0.0 ! 328 15N assign (resid 39 and name hn ) (resid 38 and name hd1*) 6.0 6.0 0.0 ! 208 13C assign (resid 39 and name hn ) (resid 38 and name hg2*) 3.5 3.5 0.0 ! 775 13C assign (resid 40 and name hn ) (resid 39 and name he* ) 4.5 4.5 0.0 ! 837 13C assign (resid 40 and name ha ) (resid 39 and name he* ) 4.5 4.5 0.0 ! 836 13C assign (resid 41 and name hn ) (resid 40 and name hg1*) 3.5 3.5 0.0 ! 335 15N assign (resid 41 and name hg2*) (resid 40 and name ha ) 4.0 4.0 0.0 ! 358 13C assign (resid 41 and name hn ) (resid 40 and name hg2*) 4.5 4.5 0.0 ! 196 15N assign (resid 42 and name hn ) (resid 41 and name hg1*) 4.5 4.5 0.0 ! 1917 13C assign (resid 42 and name hn ) (resid 41 and name hg2*) 4.0 4.0 0.0 ! 356 13C assign (resid 46 and name hn ) (resid 45 and name hg2*) 3.8 3.8 0.0 ! 1132 15N assign (resid 50 and name hd1 ) (resid 49 and name hb* ) 4.5 4.5 0.0 ! 896 13C assign (resid 51 and name hn ) (resid 50 and name hd* ) 4.5 4.5 0.0 ! 461 13C assign (resid 51 and name hn ) (resid 50 and name hg2 ) 4.5 4.5 0.0 ! 389 15N assign (resid 51 and name hb2 ) (resid 50 and name hb1 ) 4.5 4.5 0.0 ! 1660 13C assign (resid 51 and name hb1 ) (resid 50 and name hb1 ) 5.4 5.4 0.0 ! 1661 13C assign (resid 52 and name hn ) (resid 51 and name hg* ) 3.5 3.5 0.0 ! 1370 13C assign (resid 55 and name hd2 ) (resid 54 and name hd2*) 3.5 3.5 0.0 ! 606 13C assign (resid 55 and name hd1 ) (resid 54 and name hb1 ) 4.5 4.5 0.0 ! 1652 13C assign (resid 55 and name hd2 ) (resid 54 and name hb1 ) 4.5 4.5 0.0 ! 1651 13C assign (resid 55 and name hd1 ) (resid 54 and name hb2 ) 5.0 5.0 0.0 ! 1941 13C assign (resid 55 and name hd2 ) (resid 54 and name ha ) 3.5 3.5 0.0 ! 79 D2O assign (resid 55 and name hd1 ) (resid 54 and name ha ) 3.5 3.5 0.0 ! 80 D2O assign (resid 55 and name hd1 ) (resid 54 and name hd2*) 3.5 3.5 0.0 ! 607 13C assign (resid 56 and name hg* ) (resid 55 and name ha ) 4.5 4.5 0.0 ! 1643 13C assign (resid 57 and name hg* ) (resid 56 and name ha ) 5.5 5.5 0.0 ! 344 D2O assign (resid 57 and name hn ) (resid 56 and name hg* ) 4.5 4.5 0.0 ! 831 15N assign (resid 59 and name hn ) (resid 58 and name hg2*) 3.5 3.5 0.0 ! 1413 13C assign (resid 59 and name hd21) (resid 58 and name hn ) 4.5 4.5 0.0 ! 1017 15N assign (resid 61 and name hn ) (resid 60 and name hg1*) 3.5 3.5 0.0 ! 1442 13C assign (resid 61 and name hn ) (resid 60 and name hg2*) 4.5 4.5 0.0 ! 1851 13C assign (resid 62 and name hn ) (resid 61 and name hg1*) 3.5 3.5 0.0 ! 803 13C assign (resid 62 and name hn ) (resid 61 and name hg2*) 4.5 4.5 0.0 ! 795 13C assign (resid 63 and name hn ) (resid 62 and name hg ) 4.5 4.5 0.0 ! 1752 13C assign (resid 63 and name hn ) (resid 62 and name hd* ) 4.5 4.5 0.0 ! 1711 13C assign (resid 66 and name hn ) (resid 65 and name hg* ) 3.5 3.5 0.0 ! 1336 13C assign (resid 69 and name hn ) (resid 68 and name he* ) 4.0 4.0 0.0 ! 915 15N assign (resid 69 and name hn ) (resid 68 and name hd* ) 2.6 2.6 0.0 ! 914 15N assign (resid 70 and name hn ) (resid 69 and name he22) 4.5 4.5 0.0 ! 865 15N assign (resid 70 and name hn ) (resid 69 and name he21) 4.5 4.5 0.0 ! 864 15N assign (resid 70 and name hn ) (resid 69 and name hg* ) 3.7 3.7 0.0 ! 1345 13C assign (resid 72 and name hn ) (resid 71 and name hg* ) 4.5 4.5 0.0 ! 1175 13C assign (resid 74 and name hg1*) (resid 73 and name hb* ) 5.5 5.5 0.0 ! 1995 13C assign (resid 74 and name hb ) (resid 73 and name ha ) 5.5 5.5 0.0 ! 1997 13C assign (resid 74 and name hg2*) (resid 73 and name hb* ) 4.5 4.5 0.0 ! 1491 13C assign (resid 74 and name hb ) (resid 73 and name hb* ) 5.5 5.5 0.0 ! 2001 13C assign (resid 74 and name hg2*) (resid 73 and name ha ) 5.5 5.5 0.0 ! 1485 13C assign (resid 74 and name hg1*) (resid 73 and name ha ) 5.6 5.6 0.0 ! 1991 13C assign (resid 75 and name ha ) (resid 74 and name hg1*) 4.0 4.0 0.0 ! 1993 13C assign (resid 75 and name hn ) (resid 74 and name hg* ) 3.5 3.5 0.0 ! 1488 13C assign (resid 75 and name hg1*) (resid 74 and name ha ) 5.6 5.6 0.0 ! 1861 13C assign (resid 76 and name hn ) (resid 75 and name hg2*) 4.5 4.5 0.0 ! 2011 13C assign (resid 76 and name hg* ) (resid 75 and name hn ) 3.9 3.9 0.0 ! 1523 13C assign (resid 76 and name hg1*) (resid 75 and name ha ) 4.5 4.5 0.0 ! 1832 13C assign (resid 77 and name ha ) (resid 76 and name hg2*) 5.5 5.5 0.0 ! 1520 13C assign (resid 77 and name hn ) (resid 76 and name hg* ) 3.5 3.5 0.0 ! 771 13C assign (resid 80 and name hb* ) (resid 79 and name hg* ) 4.5 4.5 0.0 ! 62 13C assign (resid 80 and name hn ) (resid 79 and name hg* ) 4.5 4.5 0.0 ! 146 15N assign (resid 82 and name ha ) (resid 81 and name hb* ) 4.5 4.5 0.0 ! 1840 13C assign (resid 82 and name hg2*) (resid 81 and name hb* ) 3.5 3.5 0.0 ! 1839 13C assign (resid 82 and name hg2*) (resid 81 and name hn ) 4.5 4.5 0.0 ! 1258 15N assign (resid 83 and name hn ) (resid 82 and name hg2*) 4.5 4.5 0.0 ! 1727 13C assign (resid 83 and name hn ) (resid 82 and name hg1*) 3.5 3.5 0.0 ! 1268 15N assign (resid 84 and name hb* ) (resid 83 and name hb* ) 4.5 4.5 0.0 ! 1816 13C assign (resid 84 and name hn ) (resid 83 and name hd* ) 5.5 5.5 0.0 ! 158 15N assign (resid 85 and name hb* ) (resid 84 and name hb* ) 4.5 4.5 0.0 ! 1818 13C assign (resid 86 and name ha ) (resid 85 and name hd* ) 3.5 3.5 0.0 ! 211 D2O assign (resid 86 and name hn ) (resid 85 and name hd* ) 3.5 3.5 0.0 ! 291 15N assign (resid 89 and name hd2 ) (resid 88 and name hn ) 4.5 4.5 0.0 ! 901 15N assign (resid 89 and name hn ) (resid 88 and name hg* ) 5.5 5.5 0.0 ! 25 15N assign (resid 90 and name hd1 ) (resid 89 and name hn ) 3.5 3.5 0.0 ! 222 13C assign (resid 90 and name hd2 ) (resid 89 and name hn ) 3.8 3.8 0.0 ! 221 13C assign (resid 90 and name hd2 ) (resid 89 and name ha ) 2.5 2.5 0.0 ! 315 D2O assign (resid 90 and name hd1 ) (resid 89 and name ha ) 3.5 3.5 0.0 ! 333 D2O assign (resid 91 and name hn ) (resid 90 and name hd* ) 4.5 4.5 0.0 ! 224 13C assign (resid 91 and name hn ) (resid 90 and name hg1 ) 5.0 5.0 0.0 ! 1625 13C assign (resid 91 and name hn ) (resid 90 and name hg2 ) 3.5 3.5 0.0 ! 1626 13C assign (resid 93 and name hn ) (resid 92 and name he21) 4.5 4.5 0.0 ! 788 15N assign (resid 95 and name hn ) (resid 94 and name hd* ) 3.5 3.5 0.0 ! 2307 13C assign (resid 96 and name hn ) (resid 95 and name hg* ) 3.5 3.5 0.0 ! 2101 13C assign (resid 97 and name hn ) (resid 96 and name hd1*) 4.5 4.5 0.0 ! 138 13C assign (resid 97 and name hn ) (resid 96 and name hg2*) 3.5 3.5 0.0 ! 441 13C assign (resid 98 and name ha* ) (resid 97 and name hb* ) 4.5 4.5 0.0 ! 1542 13C assign (resid 102 and name hg1*) (resid 101 and name hg* ) 3.5 3.5 0.0 ! 1307 13C assign (resid 102 and name hg1*) (resid 101 and name hn ) 5.5 5.5 0.0 ! 74 15N assign (resid 102 and name hd1*) (resid 101 and name hn ) 5.5 5.5 0.0 ! 72 15N assign (resid 102 and name hd1*) (resid 101 and name he2*) 4.5 4.5 0.0 ! 874 15N assign (resid 102 and name hd1*) (resid 101 and name hb* ) 4.5 4.5 0.0 ! 5 13C assign (resid 102 and name hd1*) (resid 101 and name hg* ) 3.5 3.5 0.0 ! 1306 13C assign (resid 103 and name hd* ) (resid 102 and name hn ) 5.5 5.5 0.0 ! 40 15N assign (resid 103 and name hn ) (resid 102 and name hg2*) 3.8 3.8 0.0 ! 2136 13C assign (resid 103 and name hn ) (resid 102 and name hg1*) 4.5 4.5 0.0 ! 1293 15N assign (resid 103 and name hn ) (resid 102 and name hd1*) 5.5 5.5 0.0 ! 455 13C assign (resid 104 and name hn ) (resid 103 and name hd* ) 4.8 4.8 0.0 ! 1359 15N assign (resid 105 and name hn ) (resid 104 and name hg2*) 3.5 3.5 0.0 ! 1888 13C assign (resid 108 and name hn ) (resid 107 and name hg* ) 4.5 4.5 0.0 ! 620 13C assign (resid 108 and name hn ) (resid 107 and name he* ) 4.5 4.5 0.0 ! 600 15N assign (resid 108 and name hn ) (resid 107 and name hg2 ) 3.5 3.5 0.0 ! 619 13C assign (resid 108 and name hn ) (resid 107 and name hd* ) 4.5 4.5 0.0 ! 605 15N assign (resid 110 and name ha ) (resid 109 and name hb2 ) 5.5 5.5 0.0 ! 1159 13C assign (resid 111 and name hn ) (resid 110 and name hg2*) 4.5 4.5 0.0 ! 746 15N assign (resid 111 and name hn ) (resid 110 and name hg1*) 3.5 3.5 0.0 ! 1687 13C assign (resid 113 and name hn ) (resid 112 and name hg2*) 3.5 3.5 0.0 ! 1399 13C assign (resid 114 and name hn ) (resid 113 and name hd2*) 4.5 4.5 0.0 ! 2216 13C assign (resid 114 and name hn ) (resid 113 and name hd1*) 5.5 5.5 0.0 ! 1427 15N assign (resid 115 and name hn ) (resid 114 and name hd2*) 4.5 4.5 0.0 ! 2241 13C assign (resid 115 and name hg1*) (resid 114 and name ha ) 5.5 5.5 0.0 ! 1529 13C assign (resid 116 and name hn ) (resid 115 and name hg1*) 4.5 4.5 0.0 ! 1461 13C assign (resid 116 and name hn ) (resid 115 and name hg2*) 3.5 3.5 0.0 ! 1532 13C assign (resid 116 and name hg2*) (resid 115 and name ha ) 4.8 4.8 0.0 ! 2255 13C assign (resid 117 and name hn ) (resid 116 and name hg2*) 3.6 3.6 0.0 ! 1443 15N assign (resid 123 and name hn ) (resid 122 and name hd* ) 4.5 4.5 0.0 ! 675 15N assign (resid 124 and name hn ) (resid 123 and name hg2 ) 3.5 3.5 0.0 ! 669 15N assign (resid 124 and name hn ) (resid 123 and name hg1 ) 4.5 4.5 0.0 ! 670 15N assign (resid 127 and name hn ) (resid 126 and name hg2*) 3.5 3.5 0.0 ! 2376 13C assign (resid 129 and name hg11) (resid 128 and name he* ) 3.5 3.5 0.0 ! 170 13C assign (resid 129 and name hg12) (resid 128 and name he* ) 3.5 3.5 0.0 ! 195 13C assign (resid 129 and name hn ) (resid 128 and name he* ) 4.5 4.5 0.0 ! 2392 13C assign (resid 129 and name hg2*) (resid 128 and name he* ) 4.5 4.5 0.0 ! 2408 13C assign (resid 129 and name hg2*) (resid 128 and name ha ) 3.6 3.6 0.0 ! 1495 13C assign (resid 129 and name hn ) (resid 128 and name hg1 ) 3.5 3.5 0.0 ! 826 13C assign (resid 129 and name hn ) (resid 128 and name hg2 ) 4.5 4.5 0.0 ! 1057 13C assign (resid 129 and name hd1*) (resid 128 and name he* ) 3.5 3.5 0.0 ! 196 13C assign (resid 130 and name hd1 ) (resid 129 and name hb ) 3.5 3.5 0.0 ! 2423 13C assign (resid 130 and name hd2 ) (resid 129 and name hb ) 3.5 3.5 0.0 ! 2422 13C assign (resid 130 and name hd1 ) (resid 129 and name hg2*) 3.5 3.5 0.0 ! 1497 13C assign (resid 130 and name hd2 ) (resid 129 and name hg2*) 3.5 3.5 0.0 ! 1498 13C assign (resid 130 and name hd1 ) (resid 129 and name ha ) 3.5 3.5 0.0 ! 289 D2O assign (resid 130 and name hd2 ) (resid 129 and name ha ) 3.5 3.5 0.0 ! 288 D2O assign (resid 131 and name hn ) (resid 130 and name hg* ) 5.5 5.5 0.0 ! 648 15N assign (resid 131 and name hn ) (resid 130 and name hd* ) 5.5 5.5 0.0 ! 1464 15N assign (resid 132 and name hb* ) (resid 131 and name ha ) 5.5 5.5 0.0 ! 1293 13C assign (resid 132 and name hn ) (resid 131 and name hg ) 4.5 4.5 0.0 ! 1475 15N assign (resid 132 and name hn ) (resid 131 and name hd1*) 4.8 4.8 0.0 ! 1791 13C assign (resid 132 and name hn ) (resid 131 and name hd2*) 3.5 3.5 0.0 ! 2446 13C assign (resid 133 and name hd1 ) (resid 132 and name hn ) 6.0 6.0 0.0 ! 1473 15N assign (resid 133 and name hn ) (resid 132 and name hd2*) 4.5 4.5 0.0 ! 1490 15N assign (resid 134 and name hn ) (resid 133 and name hd1 ) 5.0 5.0 0.0 ! 1498 15N assign (resid 134 and name hn ) (resid 133 and name he3 ) 6.0 6.0 0.0 ! 1502 15N assign (resid 136 and name hd* ) (resid 135 and name hb1 ) 3.5 3.5 0.0 ! 1045 13C assign (resid 137 and name hn ) (resid 136 and name hd* ) 3.5 3.5 0.0 ! 111 13C assign (resid 137 and name hb ) (resid 136 and name ha ) 4.5 4.5 0.0 ! 152 13C assign (resid 138 and name hn ) (resid 137 and name hg2*) 3.5 3.5 0.0 ! 1427 13C assign (resid 138 and name hb* ) (resid 137 and name ha ) 5.5 5.5 0.0 ! 2463 13C assign (resid 139 and name hn ) (resid 138 and name hg2 ) 4.5 4.5 0.0 ! 532 15N assign (resid 139 and name hg* ) (resid 138 and name ha ) 3.5 3.5 0.0 ! 1481 13C assign (resid 139 and name hn ) (resid 138 and name hg1 ) 4.5 4.5 0.0 ! 951 15N assign (resid 140 and name hn ) (resid 139 and name hg* ) 3.5 3.5 0.0 ! 1473 13C assign (resid 143 and name hn ) (resid 142 and name hg2 ) 3.6 3.6 0.0 ! 1023 13C assign (resid 143 and name hn ) (resid 142 and name hg1 ) 3.6 3.6 0.0 ! 1024 13C assign (resid 144 and name hn ) (resid 143 and name hg2*) 3.5 3.5 0.0 ! 597 13C assign (resid 145 and name hb* ) (resid 144 and name ha ) 4.8 4.8 0.0 ! 1214 13C assign (resid 145 and name hg* ) (resid 144 and name ha ) 4.5 4.5 0.0 ! 1275 13C assign (resid 145 and name hn ) (resid 144 and name hg* ) 2.9 2.9 0.0 ! 430 13C assign (resid 145 and name hb* ) (resid 144 and name hg* ) 4.5 4.5 0.0 ! 2493 13C assign (resid 146 and name hn ) (resid 145 and name hg* ) 5.5 5.5 0.0 ! 1269 13C assign (resid 147 and name hg2*) (resid 146 and name ha ) 4.5 4.5 0.0 ! 1892 13C assign (resid 148 and name hn ) (resid 147 and name hg2*) 4.0 4.0 0.0 ! 1890 13C assign (resid 149 and name hd* ) (resid 148 and name hb* ) 3.5 3.5 0.0 ! 2497 13C assign (resid 149 and name hg* ) (resid 148 and name ha ) 4.5 4.5 0.0 ! 995 13C assign (resid 149 and name hd* ) (resid 148 and name ha ) 2.5 2.5 0.0 ! 250 D2O assign (resid 150 and name hn ) (resid 149 and name hd2 ) 3.5 3.5 0.0 ! 45 13C assign (resid 150 and name hn ) (resid 149 and name hg* ) 3.0 3.0 0.0 ! 999 13C assign (resid 150 and name hn ) (resid 149 and name hd1 ) 4.5 4.5 0.0 ! 46 13C assign (resid 151 and name hd2*) (resid 150 and name hn ) 4.6 4.6 0.0 ! 1600 15N assign (resid 151 and name hd1*) (resid 150 and name hn ) 5.5 5.5 0.0 ! 1601 15N assign (resid 152 and name hn ) (resid 151 and name hd2*) 4.5 4.5 0.0 ! 460 15N assign (resid 153 and name ha ) (resid 152 and name hg2*) 4.5 4.5 0.0 ! 2506 13C assign (resid 153 and name hn ) (resid 152 and name hg2*) 4.5 4.5 0.0 ! 564 13C assign (resid 155 and name hn ) (resid 154 and name hg2*) 2.5 2.5 0.0 ! 2513 13C assign (resid 156 and name hn ) (resid 155 and name hd* ) 4.5 4.5 0.0 ! 678 15N assign (resid 158 and name hd1 ) (resid 157 and name hn ) 5.0 5.0 0.0 ! 622 15N assign (resid 158 and name hn ) (resid 157 and name hg* ) 3.5 3.5 0.0 ! 331 13C assign (resid 159 and name hn ) (resid 158 and name he3 ) 4.1 4.1 0.0 ! 1653 15N assign (resid 160 and name hn ) (resid 159 and name hg* ) 4.5 4.5 0.0 ! 1316 13C assign (resid 161 and name hn ) (resid 160 and name hg1 ) 4.5 4.5 0.0 ! 1590 13C assign (resid 161 and name hn ) (resid 160 and name hg2 ) 3.5 3.5 0.0 ! 1591 13C assign (resid 162 and name hn ) (resid 161 and name hg1 ) 5.5 5.5 0.0 ! 990 13C assign (resid 162 and name hn ) (resid 161 and name he* ) 4.5 4.5 0.0 ! 478 15N !Intra-residue NOEs !Ha(i) - HN(i) assign (resid 2 and name ha ) (resid 2 and name hn ) 3.5 3.5 0.0 ! 51 13C assign (resid 4 and name ha ) (resid 4 and name hn ) 3.5 3.5 0.0 ! 311 13C assign (resid 5 and name ha ) (resid 5 and name hn ) 4.5 4.5 0.0 ! 66 15N assign (resid 6 and name ha ) (resid 6 and name hn ) 4.5 4.5 0.0 ! 367 15N assign (resid 7 and name ha ) (resid 7 and name hn ) 4.5 4.5 0.0 ! 79 15N assign (resid 8 and name ha ) (resid 8 and name hn ) 4.5 4.5 0.0 ! 374 15N assign (resid 9 and name ha ) (resid 9 and name hn ) 3.5 3.5 0.0 ! 304 15N assign (resid 10 and name ha ) (resid 10 and name hn ) 3.5 3.5 0.0 ! 272 15N assign (resid 11 and name ha1 ) (resid 11 and name hn ) 3.5 3.5 0.0 ! 741 15N assign (resid 11 and name ha2 ) (resid 11 and name hn ) 3.5 3.5 0.0 ! 739 15N assign (resid 12 and name ha ) (resid 12 and name hn ) 4.5 4.5 0.0 ! 1450 15N assign (resid 25 and name ha ) (resid 25 and name hn ) 4.5 4.5 0.0 ! 1052 15N assign (resid 32 and name ha ) (resid 32 and name hn ) 3.5 3.5 0.0 ! 410 15N assign (resid 33 and name ha ) (resid 33 and name hn ) 3.5 3.5 0.0 ! 106 15N assign (resid 36 and name ha1 ) (resid 36 and name hn ) 3.5 3.5 0.0 ! 327 15N assign (resid 36 and name ha2 ) (resid 36 and name hn ) 3.5 3.5 0.0 ! 329 15N assign (resid 37 and name ha ) (resid 37 and name hn ) 4.5 4.5 0.0 ! 1040 15N assign (resid 39 and name ha ) (resid 39 and name hn ) 4.5 4.5 0.0 ! 288 15N assign (resid 40 and name ha ) (resid 40 and name hn ) 4.5 4.5 0.0 ! 334 15N assign (resid 41 and name ha ) (resid 41 and name hn ) 3.5 3.5 0.0 ! 194 15N assign (resid 42 and name ha1 ) (resid 42 and name hn ) 4.5 4.5 0.0 ! 1116 15N assign (resid 42 and name ha2 ) (resid 42 and name hn ) 3.5 3.5 0.0 ! 1114 15N assign (resid 43 and name ha ) (resid 43 and name hn ) 3.5 3.5 0.0 ! 615 15N assign (resid 44 and name ha ) (resid 44 and name hn ) 3.5 3.5 0.0 ! 236 15N assign (resid 45 and name ha ) (resid 45 and name hn ) 3.5 3.5 0.0 ! 496 15N assign (resid 46 and name ha ) (resid 46 and name hn ) 4.5 4.5 0.0 ! 1672 13C assign (resid 47 and name ha ) (resid 47 and name hn ) 3.5 3.5 0.0 ! 838 15N assign (resid 48 and name ha ) (resid 48 and name hn ) 3.5 3.5 0.0 ! 1136 15N assign (resid 49 and name ha ) (resid 49 and name hn ) 3.5 3.5 0.0 ! 321 15N assign (resid 51 and name ha ) (resid 51 and name hn ) 3.5 3.5 0.0 ! 384 15N assign (resid 52 and name ha ) (resid 52 and name hn ) 3.5 3.5 0.0 ! 166 15N assign (resid 54 and name ha ) (resid 54 and name hn ) 3.5 3.5 0.0 ! 398 15N assign (resid 56 and name ha ) (resid 56 and name hn ) 3.5 3.5 0.0 ! 1022 15N assign (resid 57 and name ha ) (resid 57 and name hn ) 3.5 3.5 0.0 ! 823 15N assign (resid 58 and name ha ) (resid 58 and name hn ) 4.5 4.5 0.0 ! 1018 15N assign (resid 59 and name ha ) (resid 59 and name hn ) 3.5 3.5 0.0 ! 684 15N assign (resid 60 and name ha ) (resid 60 and name hn ) 3.5 3.5 0.0 ! 506 15N assign (resid 63 and name ha ) (resid 63 and name hn ) 3.5 3.5 0.0 ! 415 15N assign (resid 65 and name ha ) (resid 65 and name hn ) 3.5 3.5 0.0 ! 793 15N assign (resid 66 and name ha ) (resid 66 and name hn ) 3.5 3.5 0.0 ! 232 15N assign (resid 67 and name ha ) (resid 67 and name hn ) 3.5 3.5 0.0 ! 874 13C assign (resid 68 and name ha ) (resid 68 and name hn ) 3.5 3.5 0.0 ! 1194 15N assign (resid 69 and name ha ) (resid 69 and name hn ) 3.5 3.5 0.0 ! 917 15N assign (resid 70 and name ha ) (resid 70 and name hn ) 3.5 3.5 0.0 ! 251 15N assign (resid 71 and name ha ) (resid 71 and name hn ) 3.5 3.5 0.0 ! 763 15N assign (resid 72 and name ha2 ) (resid 72 and name hn ) 2.5 2.5 0.0 ! 24 13C assign (resid 73 and name ha ) (resid 73 and name hn ) 3.5 3.5 0.0 ! 310 15N assign (resid 74 and name ha ) (resid 74 and name hn ) 3.5 3.5 0.0 ! 2485 13C assign (resid 75 and name ha ) (resid 75 and name hn ) 3.5 3.5 0.0 ! 1220 15N assign (resid 76 and name ha ) (resid 76 and name hn ) 3.5 3.5 0.0 ! 261 15N assign (resid 77 and name ha ) (resid 77 and name hn ) 3.5 3.5 0.0 ! 1081 15N assign (resid 78 and name ha ) (resid 78 and name hn ) 3.5 3.5 0.0 ! 1004 15N assign (resid 80 and name ha ) (resid 80 and name hn ) 3.5 3.5 0.0 ! 148 15N assign (resid 81 and name ha ) (resid 81 and name hn ) 3.5 3.5 0.0 ! 120 15N assign (resid 82 and name ha ) (resid 82 and name hn ) 3.5 3.5 0.0 ! 98 D2O assign (resid 83 and name ha ) (resid 83 and name hn ) 3.5 3.5 0.0 ! 298 15N assign (resid 84 and name ha ) (resid 84 and name hn ) 3.5 3.5 0.0 ! 157 15N assign (resid 85 and name ha ) (resid 85 and name hn ) 3.5 3.5 0.0 ! 255 D2O assign (resid 86 and name ha ) (resid 86 and name hn ) 3.5 3.5 0.0 ! 1276 15N assign (resid 87 and name ha ) (resid 87 and name hn ) 3.5 3.5 0.0 ! 217 15N assign (resid 88 and name ha ) (resid 88 and name hn ) 3.5 3.5 0.0 ! 902 15N assign (resid 89 and name ha ) (resid 89 and name hn ) 3.5 3.5 0.0 ! 20 15N assign (resid 91 and name ha ) (resid 91 and name hn ) 3.5 3.5 0.0 ! 1303 15N assign (resid 92 and name ha ) (resid 92 and name hn ) 3.5 3.5 0.0 ! 777 15N assign (resid 96 and name ha ) (resid 96 and name hn ) 4.5 4.5 0.0 ! 342 15N assign (resid 97 and name ha ) (resid 97 and name hn ) 4.5 4.5 0.0 ! 2171 13C assign (resid 98 and name ha2 ) (resid 98 and name hn ) 3.5 3.5 0.0 ! 1168 13C assign (resid 98 and name ha1 ) (resid 98 and name hn ) 3.5 3.5 0.0 ! 10 13C assign (resid 99 and name ha2 ) (resid 99 and name hn ) 3.5 3.5 0.0 ! 31 15N assign (resid 99 and name ha1 ) (resid 99 and name hn ) 4.5 4.5 0.0 ! 32 15N assign (resid 100 and name ha ) (resid 100 and name hn ) 3.5 3.5 0.0 ! 731 13C assign (resid 101 and name ha ) (resid 101 and name hn ) 4.5 4.5 0.0 ! 353 15N assign (resid 102 and name ha ) (resid 102 and name hn ) 3.5 3.5 0.0 ! 45 15N assign (resid 103 and name ha ) (resid 103 and name hn ) 3.5 3.5 0.0 ! 22 15N assign (resid 104 and name ha ) (resid 104 and name hn ) 3.5 3.5 0.0 ! 1361 15N assign (resid 105 and name ha ) (resid 105 and name hn ) 3.5 3.5 0.0 ! 155 15N assign (resid 106 and name ha ) (resid 106 and name hn ) 3.5 3.5 0.0 ! 1378 15N assign (resid 107 and name ha ) (resid 107 and name hn ) 3.5 3.5 0.0 ! 1386 15N assign (resid 108 and name ha ) (resid 108 and name hn ) 3.5 3.5 0.0 ! 602 15N assign (resid 110 and name ha ) (resid 110 and name hn ) 3.5 3.5 0.0 ! 517 15N assign (resid 112 and name ha ) (resid 112 and name hn ) 4.5 4.5 0.0 ! 2170 13C assign (resid 113 and name ha ) (resid 113 and name hn ) 5.5 5.5 0.0 ! 1422 15N assign (resid 114 and name ha ) (resid 114 and name hn ) 3.5 3.5 0.0 ! 358 15N assign (resid 115 and name ha ) (resid 115 and name hn ) 3.5 3.5 0.0 ! 386 D2O assign (resid 119 and name ha ) (resid 119 and name hn ) 3.5 3.5 0.0 ! 1445 15N assign (resid 120 and name ha2 ) (resid 120 and name hn ) 4.5 4.5 0.0 ! 418 15N assign (resid 120 and name ha1 ) (resid 120 and name hn ) 3.5 3.5 0.0 ! 2286 13C assign (resid 123 and name ha ) (resid 123 and name hn ) 3.5 3.5 0.0 ! 674 15N assign (resid 124 and name ha2 ) (resid 124 and name hn ) 3.5 3.5 0.0 ! 34 13C assign (resid 124 and name ha1 ) (resid 124 and name hn ) 3.5 3.5 0.0 ! 33 13C assign (resid 125 and name ha ) (resid 125 and name hn ) 3.5 3.5 0.0 ! 575 15N assign (resid 127 and name ha ) (resid 127 and name hn ) 4.5 4.5 0.0 ! 639 15N assign (resid 129 and name ha ) (resid 129 and name hn ) 4.5 4.5 0.0 ! 284 15N assign (resid 131 and name ha ) (resid 131 and name hn ) 3.5 3.5 0.0 ! 650 15N assign (resid 132 and name ha ) (resid 132 and name hn ) 3.5 3.5 0.0 ! 471 15N assign (resid 133 and name ha ) (resid 133 and name hn ) 3.5 3.5 0.0 ! 856 13C assign (resid 134 and name ha ) (resid 134 and name hn ) 3.5 3.5 0.0 ! 1503 15N assign (resid 135 and name ha ) (resid 135 and name hn ) 3.5 3.5 0.0 ! 555 15N assign (resid 136 and name ha ) (resid 136 and name hn ) 3.5 3.5 0.0 ! 481 15N assign (resid 137 and name ha ) (resid 137 and name hn ) 3.5 3.5 0.0 ! 806 15N assign (resid 138 and name ha ) (resid 138 and name hn ) 3.5 3.5 0.0 ! 707 13C assign (resid 139 and name ha ) (resid 139 and name hn ) 3.5 3.5 0.0 ! 2475 13C assign (resid 140 and name ha ) (resid 140 and name hn ) 3.5 3.5 0.0 ! 627 15N assign (resid 141 and name ha ) (resid 141 and name hn ) 3.5 3.5 0.0 ! 1532 15N assign (resid 144 and name ha ) (resid 144 and name hn ) 3.5 3.5 0.0 ! 2486 13C assign (resid 145 and name ha ) (resid 145 and name hn ) 3.5 3.5 0.0 ! 1549 15N assign (resid 146 and name ha ) (resid 146 and name hn ) 3.5 3.5 0.0 ! 566 15N assign (resid 147 and name ha ) (resid 147 and name hn ) 3.5 3.5 0.0 ! 751 15N assign (resid 148 and name ha ) (resid 148 and name hn ) 3.5 3.5 0.0 ! 2 15N assign (resid 150 and name ha ) (resid 150 and name hn ) 3.5 3.5 0.0 ! 498 13C assign (resid 151 and name ha ) (resid 151 and name hn ) 3.5 3.5 0.0 ! 433 15N assign (resid 152 and name ha ) (resid 152 and name hn ) 3.5 3.5 0.0 ! 465 15N assign (resid 153 and name ha ) (resid 153 and name hn ) 4.5 4.5 0.0 ! 625 15N assign (resid 154 and name ha ) (resid 154 and name hn ) 4.5 4.5 0.0 ! 1621 15N assign (resid 158 and name ha ) (resid 158 and name hn ) 4.5 4.5 0.0 ! 848 13C assign (resid 159 and name ha ) (resid 159 and name hn ) 3.5 3.5 0.0 ! 316 13C assign (resid 160 and name ha ) (resid 160 and name hn ) 3.5 3.5 0.0 ! 2530 13C assign (resid 161 and name ha ) (resid 161 and name hn ) 3.5 3.5 0.0 ! 1683 15N assign (resid 162 and name ha ) (resid 162 and name hn ) 3.5 3.5 0.0 ! 472 15N !Hb(i) - HN(i) assign (resid 2 and name hb* ) (resid 2 and name hn ) 3.5 3.5 0.0 ! 296 13C assign (resid 4 and name hb* ) (resid 4 and name hn ) 4.5 4.5 0.0 ! 55 15N assign (resid 5 and name hb* ) (resid 5 and name hn ) 4.5 4.5 0.0 ! 69 15N assign (resid 7 and name hb* ) (resid 7 and name hn ) 4.5 4.5 0.0 ! 76 15N assign (resid 9 and name hb* ) (resid 9 and name hn ) 3.5 3.5 0.0 ! 1929 13C assign (resid 10 and name hb* ) (resid 10 and name hn ) 3.5 3.5 0.0 ! 387 13C assign (resid 12 and name hb* ) (resid 12 and name hn ) 3.5 3.5 0.0 ! 644 13C assign (resid 25 and name hb* ) (resid 25 and name hn ) 4.5 4.5 0.0 ! 84 15N assign (resid 32 and name hb* ) (resid 32 and name hn ) 2.5 2.5 0.0 ! 410 13C assign (resid 33 and name hb* ) (resid 33 and name hn ) 4.5 4.5 0.0 ! 108 15N assign (resid 34 and name hb ) (resid 34 and name hn ) 4.5 4.5 0.0 ! 97 15N assign (resid 37 and name hb* ) (resid 37 and name hn ) 4.5 4.5 0.0 ! 1043 15N assign (resid 38 and name hb ) (resid 38 and name hn ) 3.5 3.5 0.0 ! 1195 13C assign (resid 40 and name hb ) (resid 40 and name hn ) 3.5 3.5 0.0 ! 419 13C assign (resid 43 and name hb* ) (resid 43 and name hn ) 3.5 3.5 0.0 ! 528 13C assign (resid 44 and name hb* ) (resid 44 and name hn ) 3.5 3.5 0.0 ! 1127 15N assign (resid 45 and name hb ) (resid 45 and name hn ) 4.5 4.5 0.0 ! 171 13C assign (resid 46 and name hb* ) (resid 46 and name hn ) 3.5 3.5 0.0 ! 1666 13C assign (resid 47 and name hb* ) (resid 47 and name hn ) 3.5 3.5 0.0 ! 1242 13C assign (resid 48 and name hb* ) (resid 48 and name hn ) 3.5 3.5 0.0 ! 1091 13C assign (resid 49 and name hb* ) (resid 49 and name hn ) 3.5 3.5 0.0 ! 893 13C assign (resid 51 and name hb* ) (resid 51 and name hn ) 3.5 3.5 0.0 ! 1362 13C assign (resid 52 and name hb* ) (resid 52 and name hn ) 3.5 3.5 0.0 ! 589 15N assign (resid 54 and name hb* ) (resid 54 and name hn ) 4.5 4.5 0.0 ! 1940 13C assign (resid 56 and name hb* ) (resid 56 and name hn ) 4.5 4.5 0.0 ! 1639 13C assign (resid 57 and name hb* ) (resid 57 and name hn ) 4.5 4.5 0.0 ! 832 15N assign (resid 58 and name hb ) (resid 58 and name hn ) 3.5 3.5 0.0 ! 1908 13C assign (resid 59 and name hb* ) (resid 59 and name hn ) 3.5 3.5 0.0 ! 650 13C assign (resid 60 and name hb ) (resid 60 and name hn ) 3.5 3.5 0.0 ! 1961 13C assign (resid 61 and name hb ) (resid 61 and name hn ) 3.5 3.5 0.0 ! 1962 13C assign (resid 62 and name hb* ) (resid 62 and name hn ) 3.5 3.5 0.0 ! 97 13C assign (resid 63 and name hb ) (resid 63 and name hn ) 4.5 4.5 0.0 ! 280 13C assign (resid 65 and name hb* ) (resid 65 and name hn ) 3.5 3.5 0.0 ! 1354 13C assign (resid 66 and name hb2 ) (resid 66 and name hn ) 2.5 2.5 0.0 ! 336 13C assign (resid 66 and name hb1 ) (resid 66 and name hn ) 3.6 3.6 0.0 ! 337 13C assign (resid 67 and name hb* ) (resid 67 and name hn ) 3.0 3.0 0.0 ! 883 13C assign (resid 68 and name hb* ) (resid 68 and name hn ) 3.5 3.5 0.0 ! 549 13C assign (resid 69 and name hb1 ) (resid 69 and name hn ) 4.5 4.5 0.0 ! 1204 13C assign (resid 69 and name hb2 ) (resid 69 and name hn ) 3.5 3.5 0.0 ! 1203 13C assign (resid 70 and name hb* ) (resid 70 and name hn ) 3.5 3.5 0.0 ! 254 15N assign (resid 71 and name hb* ) (resid 71 and name hn ) 2.5 2.5 0.0 ! 449 13C assign (resid 73 and name hb* ) (resid 73 and name hn ) 2.5 2.5 0.0 ! 567 13C assign (resid 74 and name hb ) (resid 74 and name hn ) 3.5 3.5 0.0 ! 2002 13C assign (resid 75 and name hb ) (resid 75 and name hn ) 3.5 3.5 0.0 ! 363 13C assign (resid 76 and name hb ) (resid 76 and name hn ) 4.5 4.5 0.0 ! 1229 15N assign (resid 77 and name hb2 ) (resid 77 and name hn ) 3.5 3.5 0.0 ! 2029 13C assign (resid 77 and name hb1 ) (resid 77 and name hn ) 4.5 4.5 0.0 ! 2030 13C assign (resid 78 and name hb* ) (resid 78 and name hn ) 3.5 3.5 0.0 ! 1630 13C assign (resid 79 and name hb ) (resid 79 and name hn ) 3.5 3.5 0.0 ! 1238 15N assign (resid 80 and name hb* ) (resid 80 and name hn ) 2.5 2.5 0.0 ! 1566 13C assign (resid 81 and name hb* ) (resid 81 and name hn ) 2.5 2.5 0.0 ! 75 13C assign (resid 82 and name hb ) (resid 82 and name hn ) 2.6 2.6 0.0 ! 2047 13C assign (resid 83 and name hb2 ) (resid 83 and name hn ) 3.5 3.5 0.0 ! 2051 13C assign (resid 83 and name hb1 ) (resid 83 and name hn ) 3.8 3.8 0.0 ! 297 15N assign (resid 84 and name hb* ) (resid 84 and name hn ) 2.5 2.5 0.0 ! 1810 13C assign (resid 85 and name hb2 ) (resid 85 and name hn ) 3.5 3.5 0.0 ! 2062 13C assign (resid 85 and name hb1 ) (resid 85 and name hn ) 3.5 3.5 0.0 ! 2063 13C assign (resid 86 and name hb* ) (resid 86 and name hn ) 2.5 2.5 0.0 ! 408 13C assign (resid 87 and name hb* ) (resid 87 and name hn ) 2.5 2.5 0.0 ! 1595 13C assign (resid 88 and name hb* ) (resid 88 and name hn ) 2.5 2.5 0.0 ! 905 15N assign (resid 89 and name hb1 ) (resid 89 and name hn ) 4.5 4.5 0.0 ! 2071 13C assign (resid 89 and name hb2 ) (resid 89 and name hn ) 3.5 3.5 0.0 ! 2070 13C assign (resid 91 and name hb* ) (resid 91 and name hn ) 2.5 2.5 0.0 ! 1384 13C assign (resid 92 and name hb* ) (resid 92 and name hn ) 3.5 3.5 0.0 ! 1179 13C assign (resid 94 and name hb2 ) (resid 94 and name hn ) 4.5 4.5 0.0 ! 112 13C assign (resid 94 and name hb1 ) (resid 94 and name hn ) 3.5 3.5 0.0 ! 111 13C assign (resid 95 and name hb ) (resid 95 and name hn ) 4.5 4.5 0.0 ! 2104 13C assign (resid 96 and name hb ) (resid 96 and name hn ) 3.5 3.5 0.0 ! 2109 13C assign (resid 97 and name hb* ) (resid 97 and name hn ) 3.5 3.5 0.0 ! 1842 13C assign (resid 100 and name hb* ) (resid 100 and name hn ) 2.5 2.5 0.0 ! 487 13C assign (resid 101 and name hb* ) (resid 101 and name hn ) 3.5 3.5 0.0 ! 351 15N assign (resid 102 and name hb ) (resid 102 and name hn ) 3.5 3.5 0.0 ! 41 15N assign (resid 103 and name hb1 ) (resid 103 and name hn ) 4.5 4.5 0.0 ! 2144 13C assign (resid 103 and name hb2 ) (resid 103 and name hn ) 4.5 4.5 0.0 ! 2145 13C assign (resid 104 and name hb ) (resid 104 and name hn ) 3.5 3.5 0.0 ! 178 13C assign (resid 105 and name hb* ) (resid 105 and name hn ) 2.5 2.5 0.0 ! 65 13C assign (resid 106 and name hb* ) (resid 106 and name hn ) 3.5 3.5 0.0 ! 2154 13C assign (resid 107 and name hb* ) (resid 107 and name hn ) 2.5 2.5 0.0 ! 1163 13C assign (resid 108 and name hb2 ) (resid 108 and name hn ) 3.0 3.0 0.0 ! 2161 13C assign (resid 108 and name hb1 ) (resid 108 and name hn ) 3.0 3.0 0.0 ! 2160 13C assign (resid 109 and name hb2 ) (resid 109 and name hn ) 2.6 2.6 0.0 ! 588 13C assign (resid 109 and name hb1 ) (resid 109 and name hn ) 4.5 4.5 0.0 ! 589 13C assign (resid 110 and name hb ) (resid 110 and name hn ) 2.6 2.6 0.0 ! 2004 13C assign (resid 111 and name hb2 ) (resid 111 and name hn ) 4.5 4.5 0.0 ! 1150 13C assign (resid 111 and name hb1 ) (resid 111 and name hn ) 4.5 4.5 0.0 ! 1151 13C assign (resid 112 and name hb ) (resid 112 and name hn ) 3.5 3.5 0.0 ! 2162 13C assign (resid 113 and name hb2 ) (resid 113 and name hn ) 3.5 3.5 0.0 ! 139 15N assign (resid 113 and name hb1 ) (resid 113 and name hn ) 4.5 4.5 0.0 ! 140 15N assign (resid 114 and name hb1 ) (resid 114 and name hn ) 4.5 4.5 0.0 ! 2225 13C assign (resid 116 and name hb ) (resid 116 and name hn ) 3.5 3.5 0.0 ! 179 13C assign (resid 117 and name hb* ) (resid 117 and name hn ) 3.5 3.5 0.0 ! 1109 13C assign (resid 118 and name hb* ) (resid 118 and name hn ) 4.5 4.5 0.0 ! 2275 13C assign (resid 119 and name hb* ) (resid 119 and name hn ) 2.5 2.5 0.0 ! 501 13C assign (resid 121 and name hb* ) (resid 121 and name hn ) 3.5 3.5 0.0 ! 1095 13C assign (resid 123 and name hb* ) (resid 123 and name hn ) 2.5 2.5 0.0 ! 1081 13C assign (resid 125 and name hb2 ) (resid 125 and name hn ) 4.5 4.5 0.0 ! 1071 13C assign (resid 125 and name hb1 ) (resid 125 and name hn ) 3.5 3.5 0.0 ! 1074 13C assign (resid 127 and name hb1 ) (resid 127 and name hn ) 3.5 3.5 0.0 ! 1063 13C assign (resid 127 and name hb2 ) (resid 127 and name hn ) 3.5 3.5 0.0 ! 1062 13C assign (resid 129 and name hb ) (resid 129 and name hn ) 4.0 4.0 0.0 ! 2425 13C assign (resid 131 and name hb2 ) (resid 131 and name hn ) 3.5 3.5 0.0 ! 83 13C assign (resid 131 and name hb1 ) (resid 131 and name hn ) 3.5 3.5 0.0 ! 82 13C assign (resid 132 and name hb2 ) (resid 132 and name hn ) 2.5 2.5 0.0 ! 1281 13C assign (resid 132 and name hb1 ) (resid 132 and name hn ) 3.5 3.5 0.0 ! 1282 13C assign (resid 133 and name hb2 ) (resid 133 and name hn ) 3.5 3.5 0.0 ! 261 13C assign (resid 133 and name hb1 ) (resid 133 and name hn ) 4.0 4.0 0.0 ! 262 13C assign (resid 134 and name hb2 ) (resid 134 and name hn ) 3.5 3.5 0.0 ! 1506 15N assign (resid 134 and name hb1 ) (resid 134 and name hn ) 4.5 4.5 0.0 ! 1508 15N assign (resid 135 and name hb1 ) (resid 135 and name hn ) 3.0 3.0 0.0 ! 1041 13C assign (resid 135 and name hb2 ) (resid 135 and name hn ) 3.0 3.0 0.0 ! 1044 13C assign (resid 136 and name hb* ) (resid 136 and name hn ) 3.5 3.5 0.0 ! 580 13C assign (resid 137 and name hb ) (resid 137 and name hn ) 3.5 3.5 0.0 ! 399 D2O assign (resid 138 and name hb1 ) (resid 138 and name hn ) 3.0 3.0 0.0 ! 2467 13C assign (resid 138 and name hb2 ) (resid 138 and name hn ) 3.5 3.5 0.0 ! 2468 13C assign (resid 139 and name hb ) (resid 139 and name hn ) 4.5 4.5 0.0 ! 1218 13C assign (resid 140 and name hb* ) (resid 140 and name hn ) 3.5 3.5 0.0 ! 1035 13C assign (resid 141 and name hb* ) (resid 141 and name hn ) 3.5 3.5 0.0 ! 275 13C assign (resid 142 and name hb* ) (resid 142 and name hn ) 3.5 3.5 0.0 ! 1011 13C assign (resid 143 and name hb ) (resid 143 and name hn ) 2.9 2.9 0.0 ! 2372 13C assign (resid 144 and name hb ) (resid 144 and name hn ) 3.5 3.5 0.0 ! 540 15N assign (resid 145 and name hb* ) (resid 145 and name hn ) 3.0 3.0 0.0 ! 1212 13C assign (resid 146 and name hb* ) (resid 146 and name hn ) 3.5 3.5 0.0 ! 635 13C assign (resid 147 and name hb ) (resid 147 and name hn ) 4.0 4.0 0.0 ! 144 13C assign (resid 148 and name hb* ) (resid 148 and name hn ) 3.5 3.5 0.0 ! 516 13C assign (resid 150 and name hb* ) (resid 150 and name hn ) 2.5 2.5 0.0 ! 546 13C assign (resid 151 and name hb* ) (resid 151 and name hn ) 3.5 3.5 0.0 ! 639 13C assign (resid 152 and name hb ) (resid 152 and name hn ) 3.5 3.5 0.0 ! 464 15N assign (resid 154 and name hb ) (resid 154 and name hn ) 3.5 3.5 0.0 ! 161 13C assign (resid 155 and name hb1 ) (resid 155 and name hn ) 4.5 4.5 0.0 ! 955 15N assign (resid 155 and name hb2 ) (resid 155 and name hn ) 3.5 3.5 0.0 ! 524 15N assign (resid 156 and name hb* ) (resid 156 and name hn ) 4.5 4.5 0.0 ! 1639 15N assign (resid 157 and name hb ) (resid 157 and name hn ) 3.5 3.5 0.0 ! 543 15N assign (resid 158 and name hb2 ) (resid 158 and name hn ) 3.5 3.5 0.0 ! 1649 15N assign (resid 158 and name hb1 ) (resid 158 and name hn ) 4.5 4.5 0.0 ! 2363 13C assign (resid 159 and name hb1 ) (resid 159 and name hn ) 4.0 4.0 0.0 ! 1222 13C assign (resid 159 and name hb2 ) (resid 159 and name hn ) 3.0 3.0 0.0 ! 1221 13C assign (resid 160 and name hb* ) (resid 160 and name hn ) 3.5 3.5 0.0 ! 243 15N assign (resid 161 and name hb* ) (resid 161 and name hn ) 3.5 3.5 0.0 ! 972 13C assign (resid 162 and name hb* ) (resid 162 and name hn ) 2.5 2.5 0.0 ! 1395 13C !Ha(i) - Hb(i) assign (resid 5 and name ha ) (resid 5 and name hb* ) 3.5 3.5 0.0 ! 234 D2O assign (resid 7 and name ha ) (resid 7 and name hb* ) 4.5 4.5 0.0 ! 1390 13C assign (resid 9 and name ha ) (resid 9 and name hb2 ) 3.5 3.5 0.0 ! 1125 13C assign (resid 9 and name ha ) (resid 9 and name hb1 ) 2.5 2.5 0.0 ! 224 D2O assign (resid 10 and name ha ) (resid 10 and name hb* ) 3.5 3.5 0.0 ! 304 D2O assign (resid 12 and name ha ) (resid 12 and name hb* ) 4.5 4.5 0.0 ! 2330 13C assign (resid 13 and name ha ) (resid 13 and name hb ) 3.5 3.5 0.0 ! 1770 13C assign (resid 34 and name ha ) (resid 34 and name hb ) 3.5 3.5 0.0 ! 185 13C assign (resid 35 and name ha ) (resid 35 and name hb ) 3.5 3.5 0.0 ! 238 D2O assign (resid 38 and name ha ) (resid 38 and name hb ) 5.5 5.5 0.0 ! 1197 13C assign (resid 40 and name ha ) (resid 40 and name hb ) 3.5 3.5 0.0 ! 417 13C assign (resid 43 and name ha ) (resid 43 and name hb1 ) 3.5 3.5 0.0 ! 533 13C assign (resid 43 and name ha ) (resid 43 and name hb2 ) 3.5 3.5 0.0 ! 532 13C assign (resid 44 and name ha ) (resid 44 and name hb* ) 3.5 3.5 0.0 ! 149 D2O assign (resid 46 and name ha ) (resid 46 and name hb* ) 3.5 3.5 0.0 ! 346 D2O assign (resid 47 and name ha ) (resid 47 and name hb2 ) 3.5 3.5 0.0 ! 1236 13C assign (resid 47 and name ha ) (resid 47 and name hb1 ) 3.5 3.5 0.0 ! 1237 13C assign (resid 48 and name ha ) (resid 48 and name hb* ) 2.5 2.5 0.0 ! 236 D2O assign (resid 49 and name ha ) (resid 49 and name hb* ) 4.5 4.5 0.0 ! 894 13C assign (resid 50 and name ha ) (resid 50 and name hb1 ) 3.5 3.5 0.0 ! 1662 13C assign (resid 50 and name ha ) (resid 50 and name hb2 ) 3.5 3.5 0.0 ! 1664 13C assign (resid 51 and name ha ) (resid 51 and name hb1 ) 3.5 3.5 0.0 ! 1358 13C assign (resid 51 and name ha ) (resid 51 and name hb2 ) 3.5 3.5 0.0 ! 1357 13C assign (resid 52 and name ha ) (resid 52 and name hb* ) 4.5 4.5 0.0 ! 1935 13C assign (resid 54 and name ha ) (resid 54 and name hb1 ) 4.5 4.5 0.0 ! 1938 13C assign (resid 54 and name ha ) (resid 54 and name hb2 ) 4.5 4.5 0.0 ! 118 13C assign (resid 55 and name ha ) (resid 55 and name hb2 ) 3.5 3.5 0.0 ! 1231 13C assign (resid 55 and name ha ) (resid 55 and name hb1 ) 2.5 2.5 0.0 ! 1232 13C assign (resid 56 and name ha ) (resid 56 and name hb1 ) 2.5 2.5 0.0 ! 341 D2O assign (resid 56 and name ha ) (resid 56 and name hb2 ) 3.5 3.5 0.0 ! 345 D2O assign (resid 57 and name ha ) (resid 57 and name hb1 ) 3.5 3.5 0.0 ! 1945 13C assign (resid 57 and name ha ) (resid 57 and name hb2 ) 3.5 3.5 0.0 ! 1944 13C assign (resid 58 and name ha ) (resid 58 and name hb ) 3.5 3.5 0.0 ! 1909 13C assign (resid 59 and name ha ) (resid 59 and name hb2 ) 4.5 4.5 0.0 ! 649 13C assign (resid 59 and name ha ) (resid 59 and name hb1 ) 3.5 3.5 0.0 ! 648 13C assign (resid 60 and name ha ) (resid 60 and name hb ) 4.5 4.5 0.0 ! 1960 13C assign (resid 61 and name ha ) (resid 61 and name hb ) 3.5 3.5 0.0 ! 172 D2O assign (resid 62 and name ha ) (resid 62 and name hb1 ) 3.5 3.5 0.0 ! 96 13C assign (resid 62 and name ha ) (resid 62 and name hb2 ) 3.5 3.5 0.0 ! 95 13C assign (resid 63 and name ha ) (resid 63 and name hb ) 4.5 4.5 0.0 ! 279 13C assign (resid 64 and name ha ) (resid 64 and name hb1 ) 3.5 3.5 0.0 ! 254 13C assign (resid 64 and name ha ) (resid 64 and name hb2 ) 2.6 2.6 0.0 ! 2351 13C assign (resid 66 and name ha ) (resid 66 and name hb1 ) 3.5 3.5 0.0 ! 144 D2O assign (resid 66 and name ha ) (resid 66 and name hb2 ) 3.5 3.5 0.0 ! 143 D2O assign (resid 67 and name ha ) (resid 67 and name hb* ) 2.5 2.5 0.0 ! 879 13C assign (resid 68 and name ha ) (resid 68 and name hb* ) 3.5 3.5 0.0 ! 548 13C assign (resid 69 and name ha ) (resid 69 and name hb* ) 3.5 3.5 0.0 ! 1206 13C assign (resid 71 and name ha ) (resid 71 and name hb* ) 2.5 2.5 0.0 ! 1171 13C assign (resid 74 and name ha ) (resid 74 and name hb ) 3.5 3.5 0.0 ! 2491 13C assign (resid 75 and name ha ) (resid 75 and name hb ) 3.5 3.5 0.0 ! 179 D2O assign (resid 76 and name ha ) (resid 76 and name hb ) 2.6 2.6 0.0 ! 177 D2O assign (resid 77 and name ha ) (resid 77 and name hb1 ) 2.5 2.5 0.0 ! 63 13C assign (resid 77 and name ha ) (resid 77 and name hb2 ) 3.5 3.5 0.0 ! 64 13C assign (resid 78 and name ha ) (resid 78 and name hb* ) 2.8 2.8 0.0 ! 1629 13C assign (resid 79 and name ha ) (resid 79 and name hb ) 3.5 3.5 0.0 ! 91 D2O assign (resid 82 and name ha ) (resid 82 and name hb ) 3.5 3.5 0.0 ! 2347 13C assign (resid 83 and name ha ) (resid 83 and name hb2 ) 3.5 3.5 0.0 ! 215 D2O assign (resid 83 and name ha ) (resid 83 and name hb1 ) 3.5 3.5 0.0 ! 214 D2O assign (resid 85 and name ha ) (resid 85 and name hb2 ) 3.5 3.5 0.0 ! 371 D2O assign (resid 85 and name ha ) (resid 85 and name hb1 ) 3.5 3.5 0.0 ! 370 D2O assign (resid 87 and name ha ) (resid 87 and name hb* ) 2.5 2.5 0.0 ! 1594 13C assign (resid 88 and name ha ) (resid 88 and name hb* ) 2.5 2.5 0.0 ! 1326 13C assign (resid 89 and name ha ) (resid 89 and name hb2 ) 3.5 3.5 0.0 ! 332 D2O assign (resid 89 and name ha ) (resid 89 and name hb1 ) 3.5 3.5 0.0 ! 2068 13C assign (resid 90 and name ha ) (resid 90 and name hb1 ) 2.5 2.5 0.0 ! 336 D2O assign (resid 90 and name ha ) (resid 90 and name hb2 ) 3.5 3.5 0.0 ! 335 D2O assign (resid 91 and name ha ) (resid 91 and name hb* ) 2.6 2.6 0.0 ! 1386 13C assign (resid 92 and name ha ) (resid 92 and name hb* ) 4.5 4.5 0.0 ! 1180 13C assign (resid 94 and name ha ) (resid 94 and name hb2 ) 2.8 2.8 0.0 ! 193 D2O assign (resid 94 and name ha ) (resid 94 and name hb1 ) 3.5 3.5 0.0 ! 281 D2O assign (resid 95 and name ha ) (resid 95 and name hb ) 3.5 3.5 0.0 ! 2105 13C assign (resid 103 and name ha ) (resid 103 and name hb2 ) 3.5 3.5 0.0 ! 158 D2O assign (resid 104 and name ha ) (resid 104 and name hb ) 3.5 3.5 0.0 ! 177 13C assign (resid 106 and name ha ) (resid 106 and name hb1 ) 4.5 4.5 0.0 ! 2153 13C assign (resid 107 and name ha ) (resid 107 and name hb* ) 3.5 3.5 0.0 ! 1165 13C assign (resid 108 and name ha ) (resid 108 and name hb1 ) 3.5 3.5 0.0 ! 878 13C assign (resid 109 and name ha ) (resid 109 and name hb2 ) 3.5 3.5 0.0 ! 586 13C assign (resid 109 and name ha ) (resid 109 and name hb1 ) 3.5 3.5 0.0 ! 587 13C assign (resid 110 and name ha ) (resid 110 and name hb ) 3.5 3.5 0.0 ! 2003 13C assign (resid 111 and name ha ) (resid 111 and name hb1 ) 3.5 3.5 0.0 ! 1067 13C assign (resid 111 and name ha ) (resid 111 and name hb2 ) 2.6 2.6 0.0 ! 1068 13C assign (resid 112 and name ha ) (resid 112 and name hb ) 3.5 3.5 0.0 ! 24 D2O assign (resid 115 and name ha ) (resid 115 and name hb ) 4.5 4.5 0.0 ! 2245 13C assign (resid 117 and name ha ) (resid 117 and name hb* ) 3.5 3.5 0.0 ! 1113 13C assign (resid 118 and name ha ) (resid 118 and name hb* ) 4.5 4.5 0.0 ! 1101 13C assign (resid 121 and name ha ) (resid 121 and name hb* ) 2.5 2.5 0.0 ! 325 D2O assign (resid 122 and name ha ) (resid 122 and name hb2 ) 3.5 3.5 0.0 ! 2289 13C assign (resid 122 and name ha ) (resid 122 and name hb1 ) 4.5 4.5 0.0 ! 2290 13C assign (resid 123 and name ha ) (resid 123 and name hb* ) 3.5 3.5 0.0 ! 1080 13C assign (resid 125 and name ha ) (resid 125 and name hb* ) 3.5 3.5 0.0 ! 1073 13C assign (resid 127 and name ha ) (resid 127 and name hb1 ) 4.5 4.5 0.0 ! 1059 13C assign (resid 127 and name ha ) (resid 127 and name hb2 ) 5.5 5.5 0.0 ! 1060 13C assign (resid 129 and name ha ) (resid 129 and name hb ) 3.5 3.5 0.0 ! 203 D2O assign (resid 130 and name ha ) (resid 130 and name hb1 ) 2.5 2.5 0.0 ! 2434 13C assign (resid 130 and name ha ) (resid 130 and name hb2 ) 3.5 3.5 0.0 ! 2435 13C assign (resid 131 and name ha ) (resid 131 and name hb* ) 3.5 3.5 0.0 ! 81 13C assign (resid 132 and name ha ) (resid 132 and name hb* ) 3.5 3.5 0.0 ! 252 13C assign (resid 133 and name ha ) (resid 133 and name hb* ) 3.5 3.5 0.0 ! 850 13C assign (resid 134 and name ha ) (resid 134 and name hb* ) 2.5 2.5 0.0 ! 1382 13C assign (resid 135 and name ha ) (resid 135 and name hb* ) 3.5 3.5 0.0 ! 877 13C assign (resid 136 and name ha ) (resid 136 and name hb* ) 3.5 3.5 0.0 ! 577 13C assign (resid 137 and name ha ) (resid 137 and name hb ) 3.5 3.5 0.0 ! 2 D2O assign (resid 138 and name ha ) (resid 138 and name hb* ) 3.5 3.5 0.0 ! 141 D2O assign (resid 139 and name ha ) (resid 139 and name hb ) 2.5 2.5 0.0 ! 2477 13C assign (resid 140 and name ha ) (resid 140 and name hb* ) 2.5 2.5 0.0 ! 1036 13C assign (resid 141 and name ha ) (resid 141 and name hb* ) 3.5 3.5 0.0 ! 17 D2O assign (resid 142 and name ha ) (resid 142 and name hb* ) 3.5 3.5 0.0 ! 1008 13C assign (resid 143 and name ha ) (resid 143 and name hb ) 3.5 3.5 0.0 ! 2373 13C assign (resid 144 and name ha ) (resid 144 and name hb ) 3.5 3.5 0.0 ! 2490 13C assign (resid 145 and name ha ) (resid 145 and name hb* ) 3.5 3.5 0.0 ! 1213 13C assign (resid 146 and name ha ) (resid 146 and name hb* ) 4.5 4.5 0.0 ! 633 13C assign (resid 147 and name ha ) (resid 147 and name hb ) 3.0 3.0 0.0 ! 274 D2O assign (resid 148 and name ha ) (resid 148 and name hb* ) 3.5 3.5 0.0 ! 253 D2O assign (resid 149 and name ha ) (resid 149 and name hb* ) 2.5 2.5 0.0 ! 1001 13C assign (resid 151 and name ha ) (resid 151 and name hb* ) 4.5 4.5 0.0 ! 637 13C assign (resid 153 and name ha ) (resid 153 and name hb2 ) 4.5 4.5 0.0 ! 939 13C assign (resid 153 and name ha ) (resid 153 and name hb1 ) 3.5 3.5 0.0 ! 317 D2O assign (resid 154 and name ha ) (resid 154 and name hb ) 4.5 4.5 0.0 ! 162 13C assign (resid 155 and name ha ) (resid 155 and name hb* ) 4.5 4.5 0.0 ! 2521 13C assign (resid 156 and name ha ) (resid 156 and name hb* ) 3.5 3.5 0.0 ! 305 D2O assign (resid 157 and name ha ) (resid 157 and name hb ) 3.5 3.5 0.0 ! 326 13C assign (resid 158 and name ha ) (resid 158 and name hb* ) 3.5 3.5 0.0 ! 841 13C assign (resid 159 and name ha ) (resid 159 and name hb* ) 3.0 3.0 0.0 ! 311 D2O assign (resid 160 and name ha ) (resid 160 and name hb* ) 3.5 3.5 0.0 ! 151 D2O assign (resid 161 and name ha ) (resid 161 and name hb* ) 3.5 3.5 0.0 ! 977 13C !Other intra-residue NOEs assign (resid 1 and name ha ) (resid 1 and name ht* ) 3.5 3.5 0.0 ! 491 15N assign (resid 1 and name hb ) (resid 1 and name ht* ) 3.5 3.5 0.0 ! 1051 15N assign (resid 1 and name hg2*) (resid 1 and name hb ) 3.5 3.5 0.0 ! 352 D2O assign (resid 1 and name hg2*) (resid 1 and name ht* ) 4.5 4.5 0.0 ! 490 15N assign (resid 3 and name ha ) (resid 3 and name hd* ) 3.5 3.5 0.0 ! 104 13C assign (resid 3 and name hd* ) (resid 3 and name hn ) 4.5 4.5 0.0 ! 4 15N assign (resid 3 and name hd* ) (resid 3 and name hb* ) 3.5 3.5 0.0 ! 304 13C assign (resid 3 and name he* ) (resid 3 and name ha ) 4.5 4.5 0.0 ! 54 13C assign (resid 4 and name hd2*) (resid 4 and name hb* ) 3.5 3.5 0.0 ! 104 13C assign (resid 4 and name hd2*) (resid 4 and name hn ) 4.5 4.5 0.0 ! 58 15N assign (resid 4 and name hd1*) (resid 4 and name ha ) 3.5 3.5 0.0 ! 308 13C assign (resid 5 and name ha ) (resid 5 and name he3 ) 4.5 4.5 0.0 ! 234 D2O assign (resid 5 and name ha ) (resid 5 and name hd1 ) 4.5 4.5 0.0 ! 120 13C assign (resid 5 and name he3 ) (resid 5 and name hb* ) 3.5 3.5 0.0 ! 915 13C assign (resid 5 and name he3 ) (resid 5 and name hn ) 4.5 4.5 0.0 ! 64 15N assign (resid 5 and name hb* ) (resid 5 and name hd1 ) 3.5 3.5 0.0 ! 121 13C assign (resid 7 and name hg1 ) (resid 7 and name ha ) 4.5 4.5 0.0 ! 866 13C assign (resid 7 and name hg2 ) (resid 7 and name hn ) 4.5 4.5 0.0 ! 747 15N assign (resid 9 and name hb1 ) (resid 9 and name he ) 4.5 4.5 0.0 ! 731 15N assign (resid 9 and name ha ) (resid 9 and name he ) 5.5 5.5 0.0 ! 595 15N assign (resid 9 and name hb2 ) (resid 9 and name hd* ) 3.5 3.5 0.0 ! 1128 13C assign (resid 9 and name hn ) (resid 9 and name he ) 4.5 4.5 0.0 ! 596 15N assign (resid 9 and name hb1 ) (resid 9 and name hd* ) 3.0 3.0 0.0 ! 683 13C assign (resid 9 and name hg* ) (resid 9 and name hd* ) 2.5 2.5 0.0 ! 684 13C assign (resid 9 and name hn ) (resid 9 and name hg* ) 3.5 3.5 0.0 ! 301 15N assign (resid 9 and name he ) (resid 9 and name hd* ) 3.5 3.5 0.0 ! 688 13C assign (resid 9 and name hd* ) (resid 9 and name ha ) 4.5 4.5 0.0 ! 685 13C assign (resid 9 and name ha ) (resid 9 and name hg* ) 3.5 3.5 0.0 ! 1135 13C assign (resid 9 and name hg* ) (resid 9 and name he ) 3.5 3.5 0.0 ! 1134 13C assign (resid 9 and name hd* ) (resid 9 and name hn ) 3.5 3.5 0.0 ! 691 13C assign (resid 9 and name hb2 ) (resid 9 and name he ) 4.5 4.5 0.0 ! 732 15N assign (resid 12 and name hd2*) (resid 12 and name hb* ) 4.5 4.5 0.0 ! 643 13C assign (resid 12 and name ha ) (resid 12 and name hg ) 4.5 4.5 0.0 ! 2341 13C assign (resid 12 and name hd1*) (resid 12 and name hn ) 5.5 5.5 0.0 ! 410 15N assign (resid 12 and name hn ) (resid 12 and name hg ) 4.5 4.5 0.0 ! 409 15N assign (resid 12 and name hd1*) (resid 12 and name hb* ) 3.5 3.5 0.0 ! 642 13C assign (resid 13 and name ha ) (resid 13 and name hg2*) 3.5 3.5 0.0 ! 1775 13C assign (resid 13 and name hd1*) (resid 13 and name hn ) 3.6 3.6 0.0 ! 754 13C assign (resid 13 and name ha ) (resid 13 and name hd1*) 4.5 4.5 0.0 ! 1770 13C assign (resid 13 and name hb ) (resid 13 and name hd1*) 3.5 3.5 0.0 ! 747 13C assign (resid 29 and name hd* ) (resid 29 and name hb1 ) 3.5 3.5 0.0 ! 554 13C assign (resid 29 and name ha ) (resid 29 and name he* ) 4.5 4.5 0.0 ! 30 13C assign (resid 29 and name hd* ) (resid 29 and name hb2 ) 3.5 3.5 0.0 ! 553 13C assign (resid 29 and name ha ) (resid 29 and name hd* ) 3.5 3.5 0.0 ! 116 D2O assign (resid 31 and name hd* ) (resid 31 and name he ) 4.5 4.5 0.0 ! 728 15N assign (resid 33 and name ha ) (resid 33 and name he22) 5.5 5.5 0.0 ! 948 15N assign (resid 33 and name hg1 ) (resid 33 and name hn ) 3.5 3.5 0.0 ! 109 15N assign (resid 34 and name hg2*) (resid 34 and name hn ) 3.5 3.5 0.0 ! 187 13C assign (resid 34 and name ha ) (resid 34 and name hg2*) 3.5 3.5 0.0 ! 186 13C assign (resid 35 and name hg* ) (resid 35 and name ha ) 2.5 2.5 0.0 ! 238 D2O assign (resid 37 and name ha ) (resid 37 and name hg* ) 3.5 3.5 0.0 ! 1677 13C assign (resid 37 and name hn ) (resid 37 and name hg* ) 3.5 3.5 0.0 ! 1676 13C assign (resid 37 and name he* ) (resid 37 and name hg* ) 3.5 3.5 0.0 ! 1678 13C assign (resid 38 and name hd1*) (resid 38 and name hb ) 3.5 3.5 0.0 ! 1199 13C assign (resid 38 and name ha ) (resid 38 and name hd1*) 4.5 4.5 0.0 ! 756 13C assign (resid 38 and name hn ) (resid 38 and name hg2*) 4.5 4.5 0.0 ! 776 13C assign (resid 38 and name hg2*) (resid 38 and name hb ) 3.5 3.5 0.0 ! 1201 13C assign (resid 38 and name ha ) (resid 38 and name hg2*) 3.5 3.5 0.0 ! 774 13C assign (resid 39 and name he* ) (resid 39 and name hn ) 4.5 4.5 0.0 ! 51 13C assign (resid 40 and name ha ) (resid 40 and name hg1*) 3.5 3.5 0.0 ! 421 13C assign (resid 40 and name hn ) (resid 40 and name hg1*) 4.5 4.5 0.0 ! 432 13C assign (resid 40 and name ha ) (resid 40 and name hg2*) 3.5 3.5 0.0 ! 423 13C assign (resid 40 and name hg2*) (resid 40 and name hn ) 3.5 3.5 0.0 ! 426 13C assign (resid 41 and name hg2*) (resid 41 and name hn ) 3.5 3.5 0.0 ! 354 13C assign (resid 41 and name ha ) (resid 41 and name hg1*) 3.5 3.5 0.0 ! 1923 13C assign (resid 41 and name hg1*) (resid 41 and name hn ) 3.5 3.5 0.0 ! 1919 13C assign (resid 41 and name ha ) (resid 41 and name hg2*) 3.5 3.5 0.0 ! 347 13C assign (resid 43 and name he ) (resid 43 and name hd1 ) 4.5 4.5 0.0 ! 719 15N assign (resid 43 and name hb* ) (resid 43 and name he ) 4.5 4.5 0.0 ! 720 15N assign (resid 43 and name hd2 ) (resid 43 and name hb2 ) 4.5 4.5 0.0 ! 1931 13C assign (resid 43 and name he ) (resid 43 and name hd2 ) 3.5 3.5 0.0 ! 659 13C assign (resid 43 and name hd* ) (resid 43 and name hn ) 4.5 4.5 0.0 ! 619 15N assign (resid 44 and name hd* ) (resid 44 and name ha ) 3.5 3.5 0.0 ! 146 D2O assign (resid 44 and name hg* ) (resid 44 and name ha ) 3.5 3.5 0.0 ! 147 D2O assign (resid 45 and name hg2*) (resid 45 and name hn ) 4.5 4.5 0.0 ! 497 15N assign (resid 45 and name ha ) (resid 45 and name hg2*) 3.5 3.5 0.0 ! 283 13C assign (resid 46 and name hd* ) (resid 46 and name ha ) 3.5 3.5 0.0 ! 1673 13C assign (resid 46 and name hd* ) (resid 46 and name hb* ) 4.5 4.5 0.0 ! 1667 13C assign (resid 46 and name hd* ) (resid 46 and name hn ) 4.5 4.5 0.0 ! 1031 15N assign (resid 47 and name ha ) (resid 47 and name hg* ) 3.5 3.5 0.0 ! 1250 13C assign (resid 47 and name hg* ) (resid 47 and name hn ) 3.5 3.5 0.0 ! 1253 13C assign (resid 51 and name he* ) (resid 51 and name hg* ) 3.5 3.5 0.0 ! 1368 13C assign (resid 51 and name he* ) (resid 51 and name hb2 ) 3.5 3.5 0.0 ! 1360 13C assign (resid 51 and name he* ) (resid 51 and name hn ) 4.6 4.6 0.0 ! 389 15N assign (resid 51 and name hn ) (resid 51 and name hg* ) 4.5 4.5 0.0 ! 395 15N assign (resid 51 and name hg* ) (resid 51 and name hb* ) 2.5 2.5 0.0 ! 1366 13C assign (resid 51 and name ha ) (resid 51 and name hg* ) 3.5 3.5 0.0 ! 1369 13C assign (resid 52 and name hb* ) (resid 52 and name he ) 4.5 4.5 0.0 ! 591 15N assign (resid 52 and name ha ) (resid 52 and name he ) 4.5 4.5 0.0 ! 586 15N assign (resid 52 and name hg* ) (resid 52 and name hn ) 3.5 3.5 0.0 ! 594 15N assign (resid 54 and name hd2*) (resid 54 and name hn ) 4.5 4.5 0.0 ! 404 15N assign (resid 54 and name hn ) (resid 54 and name hg ) 3.5 3.5 0.0 ! 403 15N assign (resid 54 and name hd2*) (resid 54 and name hb* ) 3.5 3.5 0.0 ! 117 13C assign (resid 54 and name ha ) (resid 54 and name hd2*) 3.5 3.5 0.0 ! 469 13C assign (resid 54 and name hb* ) (resid 54 and name hd1*) 3.5 3.5 0.0 ! 115 13C assign (resid 54 and name ha ) (resid 54 and name hg ) 3.5 3.5 0.0 ! 473 13C assign (resid 54 and name hd1*) (resid 54 and name hn ) 4.5 4.5 0.0 ! 405 15N assign (resid 55 and name hd* ) (resid 55 and name hb* ) 4.5 4.5 0.0 ! 1658 13C assign (resid 55 and name hg* ) (resid 55 and name hd1 ) 2.5 2.5 0.0 ! 1650 13C assign (resid 55 and name hb1 ) (resid 55 and name hd1 ) 3.5 3.5 0.0 ! 1652 13C assign (resid 56 and name hg* ) (resid 56 and name hn ) 3.5 3.5 0.0 ! 375 13C assign (resid 56 and name hb* ) (resid 56 and name hg* ) 3.5 3.5 0.0 ! 1648 13C assign (resid 56 and name ha ) (resid 56 and name hg2 ) 3.5 3.5 0.0 ! 376 13C assign (resid 56 and name hg* ) (resid 56 and name ha ) 3.5 3.5 0.0 ! 377 13C assign (resid 57 and name hg* ) (resid 57 and name hn ) 4.5 4.5 0.0 ! 831 15N assign (resid 58 and name ha ) (resid 58 and name hg2*) 2.5 2.5 0.0 ! 272 D2O assign (resid 58 and name hg2*) (resid 58 and name hb ) 3.5 3.5 0.0 ! 1417 13C assign (resid 58 and name hn ) (resid 58 and name hg2*) 4.5 4.5 0.0 ! 1419 13C assign (resid 59 and name hn ) (resid 59 and name hd21) 4.5 4.5 0.0 ! 684 15N assign (resid 59 and name hd21) (resid 59 and name hb* ) 3.5 3.5 0.0 ! 1374 13C assign (resid 59 and name hb2 ) (resid 59 and name hd21) 5.5 5.5 0.0 ! 991 15N assign (resid 59 and name hb1 ) (resid 59 and name hd21) 4.5 4.5 0.0 ! 992 15N assign (resid 59 and name hd22) (resid 59 and name hn ) 4.5 4.5 0.0 ! 691 15N assign (resid 59 and name ha ) (resid 59 and name hd21) 4.5 4.5 0.0 ! 986 15N assign (resid 60 and name hg1*) (resid 60 and name ha ) 2.5 2.5 0.0 ! 120 D2O assign (resid 60 and name hg2*) (resid 60 and name ha ) 3.5 3.5 0.0 ! 1453 13C assign (resid 60 and name hn ) (resid 60 and name hg1*) 4.5 4.5 0.0 ! 506 15N assign (resid 60 and name hn ) (resid 60 and name hg2*) 3.5 3.5 0.0 ! 359 15N assign (resid 61 and name hg2*) (resid 61 and name hn ) 3.5 3.5 0.0 ! 714 15N assign (resid 61 and name ha ) (resid 61 and name hg2*) 3.5 3.5 0.0 ! 170 D2O assign (resid 61 and name hg1*) (resid 61 and name hn ) 4.5 4.5 0.0 ! 805 13C assign (resid 61 and name hg1*) (resid 61 and name ha ) 3.5 3.5 0.0 ! 171 D2O assign (resid 62 and name hd* ) (resid 62 and name hb1 ) 3.5 3.5 0.0 ! 92 13C assign (resid 62 and name ha ) (resid 62 and name hd* ) 3.5 3.5 0.0 ! 1701 13C assign (resid 62 and name hg ) (resid 62 and name hn ) 4.5 4.5 0.0 ! 1759 13C assign (resid 62 and name hd* ) (resid 62 and name hb2 ) 3.5 3.5 0.0 ! 93 13C assign (resid 62 and name ha ) (resid 62 and name hg ) 3.5 3.5 0.0 ! 1755 13C assign (resid 62 and name hn ) (resid 62 and name hd* ) 4.5 4.5 0.0 ! 549 15N assign (resid 62 and name hb1 ) (resid 62 and name hg ) 3.5 3.5 0.0 ! 91 13C assign (resid 62 and name hb* ) (resid 62 and name hd* ) 3.5 3.5 0.0 ! 1723 13C assign (resid 63 and name ha ) (resid 63 and name hg2*) 3.5 3.5 0.0 ! 490 13C assign (resid 63 and name hn ) (resid 63 and name hg2*) 3.5 3.5 0.0 ! 1179 15N assign (resid 64 and name hb2 ) (resid 64 and name hd2 ) 3.5 3.5 0.0 ! 74 13C assign (resid 64 and name hb* ) (resid 64 and name hd2 ) 3.5 3.5 0.0 ! 75 13C assign (resid 64 and name ha ) (resid 64 and name hd2 ) 3.5 3.5 0.0 ! 36 13C assign (resid 65 and name hb* ) (resid 65 and name he21) 4.5 4.5 0.0 ! 932 15N assign (resid 65 and name hg* ) (resid 65 and name hn ) 4.5 4.5 0.0 ! 1357 13C assign (resid 65 and name hg* ) (resid 65 and name he21) 3.5 3.5 0.0 ! 1335 13C assign (resid 65 and name ha ) (resid 65 and name he21) 4.5 4.5 0.0 ! 934 15N assign (resid 65 and name hg* ) (resid 65 and name he22) 3.5 3.5 0.0 ! 933 15N assign (resid 65 and name hn ) (resid 65 and name he2*) 4.5 4.5 0.0 ! 935 15N assign (resid 66 and name hg* ) (resid 66 and name hn ) 3.5 3.5 0.0 ! 236 15N assign (resid 66 and name hg* ) (resid 66 and name hb* ) 3.5 3.5 0.0 ! 339 13C assign (resid 66 and name hg* ) (resid 66 and name ha ) 3.5 3.5 0.0 ! 142 D2O assign (resid 68 and name hd* ) (resid 68 and name hn ) 4.5 4.5 0.0 ! 1196 15N assign (resid 68 and name ha ) (resid 68 and name hd* ) 3.5 3.5 0.0 ! 38 13C assign (resid 69 and name ha ) (resid 69 and name hg* ) 3.5 3.5 0.0 ! 1343 13C assign (resid 69 and name hg* ) (resid 69 and name he22) 3.5 3.5 0.0 ! 864 15N assign (resid 69 and name hg* ) (resid 69 and name hn ) 4.5 4.5 0.0 ! 1345 13C assign (resid 69 and name ha ) (resid 69 and name he21) 4.5 4.5 0.0 ! 867 15N assign (resid 69 and name ha ) (resid 69 and name he22) 4.5 4.5 0.0 ! 866 15N assign (resid 69 and name hb* ) (resid 69 and name hg* ) 3.5 3.5 0.0 ! 1348 13C assign (resid 69 and name hg* ) (resid 69 and name hb2 ) 2.5 2.5 0.0 ! 1211 13C assign (resid 69 and name hg* ) (resid 69 and name he21) 3.5 3.5 0.0 ! 1344 13C assign (resid 69 and name hb* ) (resid 69 and name he22) 4.5 4.5 0.0 ! 1211 15N assign (resid 69 and name hb* ) (resid 69 and name he21) 4.5 4.5 0.0 ! 1212 15N assign (resid 71 and name hg* ) (resid 71 and name hb* ) 2.5 2.5 0.0 ! 1174 13C assign (resid 71 and name hn ) (resid 71 and name hg* ) 3.5 3.5 0.0 ! 773 15N assign (resid 71 and name ha ) (resid 71 and name hg* ) 2.5 2.5 0.0 ! 1173 13C assign (resid 74 and name ha ) (resid 74 and name hg1*) 3.5 3.5 0.0 ! 2492 13C assign (resid 74 and name ha ) (resid 74 and name hg2*) 3.5 3.5 0.0 ! 2491 13C assign (resid 74 and name hn ) (resid 74 and name hg* ) 3.5 3.5 0.0 ! 515 15N assign (resid 75 and name hg1*) (resid 75 and name ha ) 2.5 2.5 0.0 ! 366 13C assign (resid 75 and name hn ) (resid 75 and name hg* ) 3.5 3.5 0.0 ! 1870 13C assign (resid 75 and name hg2*) (resid 75 and name ha ) 2.6 2.6 0.0 ! 365 13C assign (resid 76 and name hg1*) (resid 76 and name hn ) 3.5 3.5 0.0 ! 1231 15N assign (resid 76 and name hg2*) (resid 76 and name hn ) 3.5 3.5 0.0 ! 1230 15N assign (resid 76 and name hg1*) (resid 76 and name ha ) 2.5 2.5 0.0 ! 403 13C assign (resid 76 and name ha ) (resid 76 and name hg2*) 3.5 3.5 0.0 ! 175 D2O assign (resid 77 and name hd2 ) (resid 77 and name hb* ) 3.5 3.5 0.0 ! 2031 13C assign (resid 79 and name hg* ) (resid 79 and name ha ) 2.5 2.5 0.0 ! 268 13C assign (resid 79 and name hg* ) (resid 79 and name hn ) 3.5 3.5 0.0 ! 1245 15N assign (resid 82 and name hg2*) (resid 82 and name ha ) 2.5 2.5 0.0 ! 2347 13C assign (resid 82 and name hg1*) (resid 82 and name ha ) 2.5 2.5 0.0 ! 2348 13C assign (resid 82 and name hn ) (resid 82 and name hg1*) 4.5 4.5 0.0 ! 1855 13C assign (resid 82 and name hn ) (resid 82 and name hg2*) 2.5 2.5 0.0 ! 1725 13C assign (resid 83 and name hd* ) (resid 83 and name hn ) 3.5 3.5 0.0 ! 294 15N assign (resid 83 and name hd* ) (resid 83 and name ha ) 2.5 2.5 0.0 ! 165 13C assign (resid 85 and name ha ) (resid 85 and name hd* ) 3.5 3.5 0.0 ! 370 D2O assign (resid 85 and name hd* ) (resid 85 and name hn ) 4.5 4.5 0.0 ! 1038 15N assign (resid 87 and name he* ) (resid 87 and name hn ) 4.5 4.5 0.0 ! 1005 15N assign (resid 87 and name hn ) (resid 87 and name hg* ) 3.5 3.5 0.0 ! 1605 13C assign (resid 87 and name ha ) (resid 87 and name hg* ) 3.5 3.5 0.0 ! 1603 13C assign (resid 87 and name he* ) (resid 87 and name hg1 ) 3.5 3.5 0.0 ! 1609 13C assign (resid 87 and name he* ) (resid 87 and name hb* ) 3.5 3.5 0.0 ! 1602 13C assign (resid 88 and name hb* ) (resid 88 and name he22) 3.5 3.5 0.0 ! 1326 13C assign (resid 88 and name ha ) (resid 88 and name he21) 4.5 4.5 0.0 ! 895 15N assign (resid 88 and name hn ) (resid 88 and name hg* ) 3.5 3.5 0.0 ! 907 15N assign (resid 88 and name hg* ) (resid 88 and name he22) 4.5 4.5 0.0 ! 898 15N assign (resid 88 and name ha ) (resid 88 and name hg* ) 3.5 3.5 0.0 ! 1339 13C assign (resid 88 and name ha ) (resid 88 and name he2*) 5.5 5.5 0.0 ! 894 15N assign (resid 89 and name hb* ) (resid 89 and name hd2 ) 4.5 4.5 0.0 ! 62 13C assign (resid 89 and name hd2 ) (resid 89 and name hn ) 4.5 4.5 0.0 ! 1297 15N assign (resid 89 and name hd2 ) (resid 89 and name ha ) 4.5 4.5 0.0 ! 335 D2O assign (resid 90 and name ha ) (resid 90 and name hd* ) 3.5 3.5 0.0 ! 214 13C assign (resid 90 and name hd* ) (resid 90 and name hb* ) 3.5 3.5 0.0 ! 1616 13C assign (resid 92 and name ha ) (resid 92 and name hg* ) 3.5 3.5 0.0 ! 1186 13C assign (resid 92 and name hn ) (resid 92 and name he21) 5.5 5.5 0.0 ! 793 15N assign (resid 92 and name hn ) (resid 92 and name hg* ) 3.5 3.5 0.0 ! 1316 15N assign (resid 92 and name hg2 ) (resid 92 and name hn ) 3.5 3.5 0.0 ! 780 15N assign (resid 94 and name hg ) (resid 94 and name hb1 ) 4.5 4.5 0.0 ! 2094 13C assign (resid 94 and name hg ) (resid 94 and name hb2 ) 4.5 4.5 0.0 ! 2095 13C assign (resid 94 and name hn ) (resid 94 and name hd* ) 4.5 4.5 0.0 ! 2311 13C assign (resid 94 and name hd* ) (resid 94 and name ha ) 3.5 3.5 0.0 ! 1760 13C assign (resid 94 and name hd* ) (resid 94 and name hb2 ) 2.5 2.5 0.0 ! 1762 13C assign (resid 94 and name hd* ) (resid 94 and name hb1 ) 3.5 3.5 0.0 ! 107 13C assign (resid 95 and name hn ) (resid 95 and name hg* ) 4.5 4.5 0.0 ! 62 15N assign (resid 96 and name hg11) (resid 96 and name hb ) 3.5 3.5 0.0 ! 2267 13C assign (resid 96 and name hb ) (resid 96 and name hd1*) 3.5 3.5 0.0 ! 2120 13C assign (resid 96 and name hg2*) (resid 96 and name hd1*) 3.5 3.5 0.0 ! 447 13C assign (resid 96 and name hb ) (resid 96 and name hg12) 3.5 3.5 0.0 ! 2118 13C assign (resid 96 and name hn ) (resid 96 and name hg11) 4.5 4.5 0.0 ! 2265 13C assign (resid 96 and name hd1*) (resid 96 and name hg11) 3.5 3.5 0.0 ! 390 13C assign (resid 96 and name hd1*) (resid 96 and name hn ) 3.5 3.5 0.0 ! 139 13C assign (resid 96 and name hg2*) (resid 96 and name hb ) 3.5 3.5 0.0 ! 446 13C assign (resid 96 and name hg2*) (resid 96 and name hn ) 4.5 4.5 0.0 ! 443 13C assign (resid 96 and name hg12) (resid 96 and name hd1*) 3.5 3.5 0.0 ! 2270 13C assign (resid 96 and name hn ) (resid 96 and name hg12) 3.5 3.5 0.0 ! 2264 13C assign (resid 96 and name ha ) (resid 96 and name hd1*) 3.5 3.5 0.0 ! 198 D2O assign (resid 96 and name ha ) (resid 96 and name hg2*) 3.5 3.5 0.0 ! 199 D2O assign (resid 101 and name ha ) (resid 101 and name hg* ) 3.5 3.5 0.0 ! 1301 13C assign (resid 101 and name hn ) (resid 101 and name hg* ) 4.5 4.5 0.0 ! 1352 15N assign (resid 102 and name ha ) (resid 102 and name hg2*) 3.5 3.5 0.0 ! 126 13C assign (resid 102 and name hd1*) (resid 102 and name hn ) 4.5 4.5 0.0 ! 456 13C assign (resid 102 and name hg1*) (resid 102 and name hn ) 3.5 3.5 0.0 ! 1358 15N assign (resid 102 and name ha ) (resid 102 and name hd1*) 2.5 2.5 0.0 ! 450 13C assign (resid 102 and name hb ) (resid 102 and name hd1*) 3.5 3.5 0.0 ! 4 13C assign (resid 102 and name hn ) (resid 102 and name hg2*) 4.5 4.5 0.0 ! 2138 13C assign (resid 103 and name hd* ) (resid 103 and name hb* ) 4.5 4.5 0.0 ! 2149 13C assign (resid 103 and name ha ) (resid 103 and name hd* ) 2.5 2.5 0.0 ! 159 D2O assign (resid 103 and name hz ) (resid 103 and name hd* ) 4.5 4.5 0.0 ! 112 13C assign (resid 103 and name hd* ) (resid 103 and name hn ) 3.5 3.5 0.0 ! 171 15N assign (resid 104 and name hg2*) (resid 104 and name hb ) 2.5 2.5 0.0 ! 1883 13C assign (resid 104 and name ha ) (resid 104 and name hg2*) 3.5 3.5 0.0 ! 376 D2O assign (resid 104 and name hn ) (resid 104 and name hg2*) 3.5 3.5 0.0 ! 1373 15N assign (resid 106 and name ha ) (resid 106 and name hd* ) 3.5 3.5 0.0 ! 34 13C assign (resid 107 and name hn ) (resid 107 and name hg* ) 3.5 3.5 0.0 ! 1397 15N assign (resid 107 and name ha ) (resid 107 and name hg* ) 3.5 3.5 0.0 ! 624 13C assign (resid 107 and name hg2 ) (resid 107 and name hn ) 3.5 3.5 0.0 ! 1399 15N assign (resid 110 and name hg2*) (resid 110 and name hn ) 3.5 3.5 0.0 ! 519 15N assign (resid 110 and name hg1*) (resid 110 and name hn ) 4.5 4.5 0.0 ! 1687 13C assign (resid 110 and name ha ) (resid 110 and name hg1*) 3.5 3.5 0.0 ! 1679 13C assign (resid 112 and name hg2*) (resid 112 and name ha ) 3.5 3.5 0.0 ! 1398 13C assign (resid 112 and name hg2*) (resid 112 and name hb ) 2.5 2.5 0.0 ! 1397 13C assign (resid 112 and name hn ) (resid 112 and name hg2*) 4.5 4.5 0.0 ! 180 15N assign (resid 113 and name hb1 ) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 2179 13C assign (resid 113 and name hb2 ) (resid 113 and name hd1*) 3.5 3.5 0.0 ! 2178 13C assign (resid 113 and name hg ) (resid 113 and name hb1 ) 3.5 3.5 0.0 ! 2182 13C assign (resid 113 and name ha ) (resid 113 and name hg ) 4.5 4.5 0.0 ! 1795 13C assign (resid 113 and name hn ) (resid 113 and name hg ) 3.5 3.5 0.0 ! 137 15N assign (resid 113 and name hn ) (resid 113 and name hd1*) 4.5 4.5 0.0 ! 138 15N assign (resid 113 and name hd2*) (resid 113 and name hb1 ) 3.5 3.5 0.0 ! 2209 13C assign (resid 113 and name hg ) (resid 113 and name hb2 ) 3.5 3.5 0.0 ! 2183 13C assign (resid 113 and name ha ) (resid 113 and name hd1*) 4.5 4.5 0.0 ! 356 D2O assign (resid 113 and name ha ) (resid 113 and name hd2*) 3.5 3.5 0.0 ! 207 D2O assign (resid 113 and name hn ) (resid 113 and name hd2*) 4.5 4.5 0.0 ! 143 15N assign (resid 113 and name hb2 ) (resid 113 and name hd2*) 3.5 3.5 0.0 ! 2180 13C assign (resid 114 and name hg ) (resid 114 and name hb2 ) 4.5 4.5 0.0 ! 2229 13C assign (resid 114 and name hd1*) (resid 114 and name hb1 ) 3.5 3.5 0.0 ! 2230 13C assign (resid 114 and name hd1*) (resid 114 and name hn ) 4.5 4.5 0.0 ! 2233 13C assign (resid 114 and name hd2*) (resid 114 and name ha ) 2.5 2.5 0.0 ! 2242 13C assign (resid 114 and name hb1 ) (resid 114 and name hd2*) 3.5 3.5 0.0 ! 2237 13C assign (resid 114 and name hb2 ) (resid 114 and name hd2*) 3.5 3.5 0.0 ! 2238 13C assign (resid 114 and name hn ) (resid 114 and name hd2*) 4.5 4.5 0.0 ! 1432 15N assign (resid 114 and name hb2 ) (resid 114 and name hd1*) 3.5 3.5 0.0 ! 459 13C assign (resid 114 and name hd1*) (resid 114 and name ha ) 4.5 4.5 0.0 ! 2231 13C assign (resid 115 and name hg2*) (resid 115 and name ha ) 3.5 3.5 0.0 ! 1467 13C assign (resid 115 and name hg1*) (resid 115 and name ha ) 3.5 3.5 0.0 ! 1539 13C assign (resid 115 and name hg1*) (resid 115 and name hn ) 3.5 3.5 0.0 ! 1532 13C assign (resid 115 and name hn ) (resid 115 and name hg2*) 5.5 5.5 0.0 ! 1463 13C assign (resid 116 and name hg2*) (resid 116 and name hb ) 3.5 3.5 0.0 ! 2257 13C assign (resid 116 and name hg2*) (resid 116 and name ha ) 3.5 3.5 0.0 ! 1449 13C assign (resid 116 and name hn ) (resid 116 and name hg2*) 3.6 3.6 0.0 ! 1442 13C assign (resid 117 and name hd* ) (resid 117 and name hb* ) 3.5 3.5 0.0 ! 1121 13C assign (resid 117 and name hg* ) (resid 117 and name hb* ) 3.5 3.5 0.0 ! 1123 13C assign (resid 118 and name hd2*) (resid 118 and name hb* ) 4.5 4.5 0.0 ! 2280 13C assign (resid 118 and name hd1*) (resid 118 and name hb* ) 4.5 4.5 0.0 ! 2281 13C assign (resid 118 and name hg ) (resid 118 and name hb* ) 3.5 3.5 0.0 ! 1146 13C assign (resid 118 and name hd2*) (resid 118 and name hn ) 5.5 5.5 0.0 ! 447 15N assign (resid 118 and name hd1*) (resid 118 and name hn ) 4.5 4.5 0.0 ! 1450 15N assign (resid 123 and name ha ) (resid 123 and name hg* ) 3.5 3.5 0.0 ! 2295 13C assign (resid 123 and name hg* ) (resid 123 and name hn ) 3.5 3.5 0.0 ! 1318 15N assign (resid 126 and name ha ) (resid 126 and name hg2*) 2.5 2.5 0.0 ! 178 D2O assign (resid 126 and name hn ) (resid 126 and name hg2*) 4.5 4.5 0.0 ! 2378 13C assign (resid 127 and name he* ) (resid 127 and name hb* ) 4.5 4.5 0.0 ! 2388 13C assign (resid 127 and name hd* ) (resid 127 and name hb* ) 3.5 3.5 0.0 ! 2393 13C assign (resid 128 and name ha ) (resid 128 and name he* ) 4.5 4.5 0.0 ! 2397 13C assign (resid 129 and name hn ) (resid 129 and name hg2*) 3.5 3.5 0.0 ! 280 15N assign (resid 129 and name hd1*) (resid 129 and name hb ) 3.5 3.5 0.0 ! 202 13C assign (resid 129 and name hg1*) (resid 129 and name hn ) 3.5 3.5 0.0 ! 282 15N assign (resid 129 and name hb ) (resid 129 and name hg2*) 2.5 2.5 0.0 ! 1494 13C assign (resid 129 and name hd1*) (resid 129 and name hg2*) 3.0 3.0 0.0 ! 1501 13C assign (resid 129 and name hg2*) (resid 129 and name ha ) 3.5 3.5 0.0 ! 109 D2O assign (resid 129 and name ha ) (resid 129 and name hd1*) 4.5 4.5 0.0 ! 195 13C assign (resid 130 and name hg* ) (resid 130 and name ha ) 3.5 3.5 0.0 ! 2440 13C assign (resid 131 and name hb2 ) (resid 131 and name hd1*) 3.5 3.5 0.0 ! 86 13C assign (resid 131 and name ha ) (resid 131 and name hd1*) 4.5 4.5 0.0 ! 1789 13C assign (resid 131 and name hg ) (resid 131 and name hb2 ) 3.5 3.5 0.0 ! 2445 13C assign (resid 131 and name hn ) (resid 131 and name hg ) 4.5 4.5 0.0 ! 649 15N assign (resid 131 and name ha ) (resid 131 and name hd2*) 2.5 2.5 0.0 ! 2448 13C assign (resid 131 and name hn ) (resid 131 and name hd2*) 4.5 4.5 0.0 ! 655 15N assign (resid 131 and name hd1*) (resid 131 and name hn ) 4.5 4.5 0.0 ! 132 15N assign (resid 131 and name hg ) (resid 131 and name hb1 ) 3.5 3.5 0.0 ! 87 13C assign (resid 131 and name hb1 ) (resid 131 and name hd1*) 3.5 3.5 0.0 ! 1786 13C assign (resid 131 and name hd1*) (resid 131 and name hb* ) 3.5 3.5 0.0 ! 121 13C assign (resid 132 and name ha ) (resid 132 and name hd2*) 4.5 4.5 0.0 ! 852 15N assign (resid 132 and name hn ) (resid 132 and name hd2*) 5.5 5.5 0.0 ! 1476 15N assign (resid 132 and name hd22) (resid 132 and name hb2 ) 4.5 4.5 0.0 ! 1292 13C assign (resid 132 and name hd22) (resid 132 and name hb1 ) 4.5 4.5 0.0 ! 1293 13C assign (resid 133 and name hd1 ) (resid 133 and name hn ) 3.5 3.5 0.0 ! 1497 15N assign (resid 133 and name he3 ) (resid 133 and name hn ) 5.0 5.0 0.0 ! 1495 15N assign (resid 133 and name hd1 ) (resid 133 and name ha ) 4.8 4.8 0.0 ! 65 13C assign (resid 133 and name hb2 ) (resid 133 and name hd1 ) 3.5 3.5 0.0 ! 263 13C assign (resid 133 and name he1 ) (resid 133 and name hn ) 4.6 4.6 0.0 ! 1500 15N assign (resid 133 and name he3 ) (resid 133 and name hb2 ) 4.5 4.5 0.0 ! 257 13C assign (resid 133 and name he3 ) (resid 133 and name hb1 ) 4.5 4.5 0.0 ! 258 13C assign (resid 133 and name hd1 ) (resid 133 and name hb1 ) 4.5 4.5 0.0 ! 264 13C assign (resid 133 and name he3 ) (resid 133 and name ha ) 3.5 3.5 0.0 ! 853 13C assign (resid 136 and name hd* ) (resid 136 and name hb2 ) 3.5 3.5 0.0 ! 2457 13C assign (resid 136 and name hd* ) (resid 136 and name hn ) 3.5 3.5 0.0 ! 1242 15N assign (resid 136 and name hd* ) (resid 136 and name hb1 ) 3.5 3.5 0.0 ! 584 13C assign (resid 137 and name hg2*) (resid 137 and name hn ) 4.5 4.5 0.0 ! 1429 13C assign (resid 137 and name hg2*) (resid 137 and name ha ) 3.5 3.5 0.0 ! 1425 13C assign (resid 137 and name hg2*) (resid 137 and name hb ) 2.5 2.5 0.0 ! 1424 13C assign (resid 138 and name he2 ) (resid 138 and name hd2 ) 3.5 3.5 0.0 ! 968 13C assign (resid 138 and name hg1 ) (resid 138 and name ha ) 3.5 3.5 0.0 ! 1697 13C assign (resid 138 and name he* ) (resid 138 and name hd* ) 3.5 3.5 0.0 ! 946 13C assign (resid 138 and name hg* ) (resid 138 and name hn ) 4.5 4.5 0.0 ! 1536 15N assign (resid 138 and name hb2 ) (resid 138 and name hd2 ) 3.5 3.5 0.0 ! 947 13C assign (resid 138 and name hg2 ) (resid 138 and name hd1 ) 3.5 3.5 0.0 ! 1706 13C assign (resid 138 and name hg1 ) (resid 138 and name hb2 ) 3.5 3.5 0.0 ! 1710 13C assign (resid 138 and name hg1 ) (resid 138 and name hd1 ) 3.5 3.5 0.0 ! 1708 13C assign (resid 138 and name hg1 ) (resid 138 and name hd2 ) 3.5 3.5 0.0 ! 952 13C assign (resid 138 and name ha ) (resid 138 and name hd1 ) 3.5 3.5 0.0 ! 953 13C assign (resid 138 and name ha ) (resid 138 and name hd2 ) 4.5 4.5 0.0 ! 954 13C assign (resid 138 and name hb* ) (resid 138 and name he* ) 4.5 4.5 0.0 ! 2466 13C assign (resid 138 and name hg* ) (resid 138 and name he* ) 4.5 4.5 0.0 ! 964 13C assign (resid 138 and name hg* ) (resid 138 and name hb* ) 3.5 3.5 0.0 ! 2459 13C assign (resid 138 and name ha ) (resid 138 and name hg2 ) 4.0 4.0 0.0 ! 701 13C assign (resid 138 and name he1 ) (resid 138 and name hd2 ) 3.5 3.5 0.0 ! 969 13C assign (resid 138 and name hb* ) (resid 138 and name hd1 ) 3.5 3.5 0.0 ! 948 13C assign (resid 139 and name ha ) (resid 139 and name hg* ) 2.5 2.5 0.0 ! 2478 13C assign (resid 139 and name hn ) (resid 139 and name hg* ) 3.5 3.5 0.0 ! 958 15N assign (resid 142 and name hd* ) (resid 142 and name he ) 4.5 4.5 0.0 ! 1566 15N assign (resid 142 and name hd* ) (resid 142 and name hb* ) 3.5 3.5 0.0 ! 1017 13C assign (resid 142 and name hg* ) (resid 142 and name hb* ) 3.5 3.5 0.0 ! 1018 13C assign (resid 142 and name hd* ) (resid 142 and name hg* ) 3.5 3.5 0.0 ! 1032 13C assign (resid 142 and name ha ) (resid 142 and name hg1 ) 3.5 3.5 0.0 ! 1022 13C assign (resid 142 and name ha ) (resid 142 and name hg2 ) 3.5 3.5 0.0 ! 1023 13C assign (resid 142 and name hn ) (resid 142 and name hg* ) 4.5 4.5 0.0 ! 1026 13C assign (resid 143 and name hg2*) (resid 143 and name hb ) 2.5 2.5 0.0 ! 2486 13C assign (resid 143 and name hg2*) (resid 143 and name hn ) 4.5 4.5 0.0 ! 1569 15N assign (resid 143 and name ha ) (resid 143 and name hg2*) 3.5 3.5 0.0 ! 596 13C assign (resid 144 and name ha ) (resid 144 and name hg* ) 2.5 2.5 0.0 ! 434 13C assign (resid 144 and name hn ) (resid 144 and name hg* ) 3.5 3.5 0.0 ! 542 15N assign (resid 145 and name hn ) (resid 145 and name hg2 ) 3.5 3.5 0.0 ! 1268 13C assign (resid 145 and name hn ) (resid 145 and name hg1 ) 3.5 3.5 0.0 ! 1271 13C assign (resid 145 and name ha ) (resid 145 and name hg2 ) 4.5 4.5 0.0 ! 1272 13C assign (resid 145 and name ha ) (resid 145 and name hg1 ) 3.5 3.5 0.0 ! 1273 13C assign (resid 145 and name hb* ) (resid 145 and name hg2 ) 2.5 2.5 0.0 ! 1274 13C assign (resid 145 and name hb* ) (resid 145 and name hg1 ) 2.5 2.5 0.0 ! 1275 13C assign (resid 147 and name hn ) (resid 147 and name hg2*) 3.5 3.5 0.0 ! 451 15N assign (resid 147 and name hb ) (resid 147 and name hg2*) 2.5 2.5 0.0 ! 148 13C assign (resid 147 and name ha ) (resid 147 and name hg2*) 2.5 2.5 0.0 ! 1897 13C assign (resid 148 and name hb2 ) (resid 148 and name hd22) 4.5 4.5 0.0 ! 511 13C assign (resid 148 and name hb1 ) (resid 148 and name hd22) 4.5 4.5 0.0 ! 512 13C assign (resid 148 and name ha ) (resid 148 and name hd21) 4.5 4.5 0.0 ! 969 15N assign (resid 148 and name ha ) (resid 148 and name hd22) 4.5 4.5 0.0 ! 970 15N assign (resid 148 and name hn ) (resid 148 and name hd2*) 5.5 5.5 0.0 ! 1586 15N assign (resid 148 and name hb2 ) (resid 148 and name hd21) 3.5 3.5 0.0 ! 513 13C assign (resid 148 and name hb1 ) (resid 148 and name hd21) 3.5 3.5 0.0 ! 514 13C assign (resid 149 and name hd1 ) (resid 149 and name hg* ) 2.5 2.5 0.0 ! 997 13C assign (resid 149 and name hd2 ) (resid 149 and name hg* ) 2.5 2.5 0.0 ! 998 13C assign (resid 149 and name ha ) (resid 149 and name hg* ) 3.8 3.8 0.0 ! 999 13C assign (resid 149 and name hd2 ) (resid 149 and name hb1 ) 4.5 4.5 0.0 ! 1006 13C assign (resid 149 and name hd1 ) (resid 149 and name hb1 ) 4.5 4.5 0.0 ! 2505 13C assign (resid 149 and name ha ) (resid 149 and name hd1 ) 4.5 4.5 0.0 ! 2503 13C assign (resid 151 and name ha ) (resid 151 and name hd1*) 4.5 4.5 0.0 ! 2241 13C assign (resid 151 and name hd1*) (resid 151 and name hb2 ) 3.5 3.5 0.0 ! 2327 13C assign (resid 151 and name hd2*) (resid 151 and name hb2 ) 3.5 3.5 0.0 ! 2328 13C assign (resid 151 and name hd1*) (resid 151 and name hb1 ) 4.5 4.5 0.0 ! 2329 13C assign (resid 151 and name ha ) (resid 151 and name hg ) 3.5 3.5 0.0 ! 2506 13C assign (resid 151 and name hd2*) (resid 151 and name hn ) 4.5 4.5 0.0 ! 437 15N assign (resid 151 and name hd1*) (resid 151 and name hn ) 4.5 4.5 0.0 ! 445 15N assign (resid 152 and name hg2*) (resid 152 and name ha ) 3.5 3.5 0.0 ! 562 13C assign (resid 152 and name hg2*) (resid 152 and name hn ) 4.5 4.5 0.0 ! 565 13C assign (resid 152 and name hb ) (resid 152 and name hg2*) 2.5 2.5 0.0 ! 560 13C assign (resid 153 and name he1 ) (resid 153 and name hd2 ) 4.5 4.5 0.0 ! 80 13C assign (resid 154 and name ha ) (resid 154 and name hg2*) 3.5 3.5 0.0 ! 2513 13C assign (resid 154 and name hn ) (resid 154 and name hg2*) 4.5 4.5 0.0 ! 1634 15N assign (resid 154 and name hb ) (resid 154 and name hg2*) 2.5 2.5 0.0 ! 2518 13C assign (resid 155 and name hd* ) (resid 155 and name hn ) 4.5 4.5 0.0 ! 953 15N assign (resid 155 and name ha ) (resid 155 and name hd* ) 3.5 3.5 0.0 ! 100 13C assign (resid 157 and name hg* ) (resid 157 and name ha ) 2.5 2.5 0.0 ! 1392 13C assign (resid 157 and name hg* ) (resid 157 and name hn ) 3.5 3.5 0.0 ! 1393 13C assign (resid 158 and name hd1 ) (resid 158 and name hb1 ) 4.5 4.5 0.0 ! 2361 13C assign (resid 158 and name hd1 ) (resid 158 and name hb2 ) 4.5 4.5 0.0 ! 2362 13C assign (resid 158 and name he3 ) (resid 158 and name hb1 ) 4.5 4.5 0.0 ! 2363 13C assign (resid 158 and name he3 ) (resid 158 and name hb2 ) 4.5 4.5 0.0 ! 2364 13C assign (resid 158 and name hd1 ) (resid 158 and name ha ) 4.5 4.5 0.0 ! 200 13C assign (resid 158 and name hn ) (resid 158 and name hd1 ) 4.5 4.5 0.0 ! 1656 15N assign (resid 158 and name he3 ) (resid 158 and name ha ) 3.8 3.8 0.0 ! 846 13C assign (resid 159 and name hg2 ) (resid 159 and name ha ) 3.5 3.5 0.0 ! 1321 13C assign (resid 159 and name hg1 ) (resid 159 and name ha ) 3.5 3.5 0.0 ! 1320 13C assign (resid 159 and name hb1 ) (resid 159 and name he22) 4.5 4.5 0.0 ! 889 15N assign (resid 159 and name hb2 ) (resid 159 and name he22) 4.5 4.5 0.0 ! 892 15N assign (resid 159 and name hn ) (resid 159 and name hg1 ) 4.5 4.5 0.0 ! 1671 15N assign (resid 159 and name hn ) (resid 159 and name hg2 ) 4.5 4.5 0.0 ! 1672 15N assign (resid 160 and name hg1 ) (resid 160 and name ha ) 3.5 3.5 0.0 ! 1590 13C assign (resid 160 and name hd* ) (resid 160 and name ha ) 4.5 4.5 0.0 ! 153 D2O assign (resid 160 and name he* ) (resid 160 and name ha ) 4.5 4.5 0.0 ! 2539 13C assign (resid 160 and name hd* ) (resid 160 and name hn ) 4.5 4.5 0.0 ! 246 15N assign (resid 160 and name ha ) (resid 160 and name hg* ) 3.5 3.5 0.0 ! 1587 13C assign (resid 160 and name he* ) (resid 160 and name hg* ) 3.5 3.5 0.0 ! 1589 13C assign (resid 160 and name hn ) (resid 160 and name hg* ) 4.5 4.5 0.0 ! 1595 13C assign (resid 161 and name ha ) (resid 161 and name hg* ) 3.5 3.5 0.0 ! 983 13C assign (resid 161 and name he* ) (resid 161 and name hg1 ) 3.5 3.5 0.0 ! 985 13C assign (resid 161 and name he* ) (resid 161 and name hg2 ) 3.5 3.5 0.0 ! 986 13C assign (resid 161 and name hn ) (resid 161 and name hg2 ) 3.5 3.5 0.0 ! 989 13C assign (resid 161 and name hn ) (resid 161 and name hg1 ) 3.5 3.5 0.0 ! 1685 15N assign (resid 161 and name he* ) (resid 161 and name hn ) 4.5 4.5 0.0 ! 1687 15N
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