NMR Restraints Grid |
Result table
image | mrblock_id | pdb_id | bmrb_id | cing | stage | program | type | subtype | subsubtype | item_count |
29599 | 1b4c | 4001 | cing | 2-parsed | STAR | distance | NOE | ambi | 1780 |
data_1b4c_MR_file_constraints save_Conversion_project _Study_list.Sf_category study_list _Study_list.Entry_ID parsed_1b4c _Study_list.ID 1 loop_ _Study.ID _Study.Name _Study.Type _Study.Details _Study.Entry_ID _Study.Study_list_ID 1 "Conversion project" NMR . parsed_1b4c 1 stop_ save_ save_entry_information _Entry.Sf_category entry_information _Entry.ID parsed_1b4c _Entry.Title "Original constraint list(s)" _Entry.Version_type original _Entry.Submission_date . _Entry.Accession_date . _Entry.Last_release_date . _Entry.Original_release_date . _Entry.Origination . _Entry.NMR_STAR_version 3.1 _Entry.Original_NMR_STAR_version . _Entry.Experimental_method NMR _Entry.Experimental_method_subtype . loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID PDB 1b4c "Master copy" parsed_1b4c stop_ save_ save_global_Org_file_characteristics _Constraint_stat_list.Sf_category constraint_statistics _Constraint_stat_list.Entry_ID parsed_1b4c _Constraint_stat_list.ID 1 loop_ _Constraint_file.ID _Constraint_file.Constraint_filename _Constraint_file.Software_ID _Constraint_file.Software_label _Constraint_file.Software_name _Constraint_file.Block_ID _Constraint_file.Constraint_type _Constraint_file.Constraint_subtype _Constraint_file.Constraint_subsubtype _Constraint_file.Constraint_number _Constraint_file.Entry_ID _Constraint_file.Constraint_stat_list_ID 1 1b4c.mr . . "MR format" 1 comment "Not applicable" "Not applicable" 0 parsed_1b4c 1 1 1b4c.mr . . XPLOR/CNS 2 distance NOE ambi 1780 parsed_1b4c 1 1 1b4c.mr . . XPLOR/CNS 3 "dihedral angle" "Not applicable" "Not applicable" 0 parsed_1b4c 1 1 1b4c.mr . . XPLOR/CNS 4 distance symmetry simple 0 parsed_1b4c 1 1 1b4c.mr . . XPLOR/CNS 5 distance "hydrogen bond" simple 0 parsed_1b4c 1 1 1b4c.mr . . XPLOR/CNS 6 "dipolar coupling" "Not applicable" "Not applicable" 0 parsed_1b4c 1 1 1b4c.mr . . "MR format" 7 "nomenclature mapping" "Not applicable" "Not applicable" 0 parsed_1b4c 1 stop_ save_ save_CNS/XPLOR_distance_constraints_2 _Distance_constraint_list.Sf_category distance_constraints _Distance_constraint_list.Entry_ID parsed_1b4c _Distance_constraint_list.ID 1 _Distance_constraint_list.Constraint_type NOE _Distance_constraint_list.Constraint_file_ID 1 _Distance_constraint_list.Block_ID 2 _Distance_constraint_list.Details "Generated by Wattos" loop_ _Dist_constraint_tree.Constraint_ID _Dist_constraint_tree.Node_ID _Dist_constraint_tree.Down_node_ID _Dist_constraint_tree.Right_node_ID _Dist_constraint_tree.Logic_operation _Dist_constraint_tree.Entry_ID _Dist_constraint_tree.Distance_constraint_list_ID 1 1 . . . parsed_1b4c 1 2 1 . . . parsed_1b4c 1 3 1 . . . parsed_1b4c 1 4 1 . . . parsed_1b4c 1 5 1 . . . parsed_1b4c 1 6 1 . . . parsed_1b4c 1 7 1 . . . parsed_1b4c 1 8 1 . . . parsed_1b4c 1 9 1 . . . parsed_1b4c 1 10 1 . . . parsed_1b4c 1 11 1 . . . parsed_1b4c 1 12 1 . . . parsed_1b4c 1 13 1 . . . parsed_1b4c 1 14 1 . . . parsed_1b4c 1 15 1 . . . parsed_1b4c 1 16 1 . . . parsed_1b4c 1 17 1 . . . parsed_1b4c 1 18 1 . . . parsed_1b4c 1 19 1 . . . parsed_1b4c 1 20 1 . . . parsed_1b4c 1 21 1 . . . parsed_1b4c 1 22 1 . . . parsed_1b4c 1 23 1 . . . parsed_1b4c 1 24 1 . . . parsed_1b4c 1 25 1 . . . parsed_1b4c 1 26 1 . . . parsed_1b4c 1 27 1 . . . parsed_1b4c 1 28 1 . . . parsed_1b4c 1 29 1 . . . parsed_1b4c 1 30 1 . . . parsed_1b4c 1 31 1 . . . parsed_1b4c 1 32 1 . . . parsed_1b4c 1 33 1 . . . parsed_1b4c 1 34 1 . . . parsed_1b4c 1 35 1 . . . parsed_1b4c 1 36 1 . . . parsed_1b4c 1 37 1 . . . parsed_1b4c 1 38 1 . . . parsed_1b4c 1 39 1 . . . parsed_1b4c 1 40 1 . . . parsed_1b4c 1 41 1 . . . parsed_1b4c 1 42 1 . . . parsed_1b4c 1 43 1 . . . parsed_1b4c 1 44 1 . . . parsed_1b4c 1 45 1 . . . parsed_1b4c 1 46 1 . . . parsed_1b4c 1 47 1 . . . parsed_1b4c 1 48 1 . . . parsed_1b4c 1 49 1 . . . parsed_1b4c 1 50 1 . . . parsed_1b4c 1 51 1 . . . parsed_1b4c 1 52 1 . . . parsed_1b4c 1 53 1 . . . parsed_1b4c 1 54 1 . . . parsed_1b4c 1 55 1 . . . parsed_1b4c 1 56 1 . . . parsed_1b4c 1 57 1 . . . parsed_1b4c 1 58 1 . . . parsed_1b4c 1 59 1 . . . parsed_1b4c 1 60 1 . . . parsed_1b4c 1 61 1 . . . parsed_1b4c 1 62 1 . . . parsed_1b4c 1 63 1 . . . parsed_1b4c 1 64 1 . . . parsed_1b4c 1 65 1 . . . parsed_1b4c 1 66 1 . . . parsed_1b4c 1 67 1 . . . parsed_1b4c 1 68 1 . . . parsed_1b4c 1 69 1 . . . parsed_1b4c 1 70 1 . . . parsed_1b4c 1 71 1 . . . parsed_1b4c 1 72 1 . . . parsed_1b4c 1 73 1 . . . parsed_1b4c 1 74 1 . . . parsed_1b4c 1 75 1 . . . parsed_1b4c 1 76 1 . . . parsed_1b4c 1 77 1 . . . parsed_1b4c 1 78 1 . . . parsed_1b4c 1 79 1 . . . parsed_1b4c 1 80 1 . . . parsed_1b4c 1 81 1 . . . parsed_1b4c 1 82 1 . . . parsed_1b4c 1 83 1 . . . parsed_1b4c 1 84 1 . . . parsed_1b4c 1 85 1 . . . parsed_1b4c 1 86 1 . . . parsed_1b4c 1 87 1 . . . parsed_1b4c 1 88 1 . . . parsed_1b4c 1 89 1 . . . parsed_1b4c 1 90 1 . . . parsed_1b4c 1 91 1 . . . parsed_1b4c 1 92 1 . . . parsed_1b4c 1 93 1 . . . parsed_1b4c 1 94 1 . . . parsed_1b4c 1 95 1 . . . parsed_1b4c 1 96 1 . . . parsed_1b4c 1 97 1 . . . parsed_1b4c 1 98 1 . . . parsed_1b4c 1 99 1 . . . parsed_1b4c 1 100 1 . . . parsed_1b4c 1 101 1 . . . parsed_1b4c 1 102 1 . . . parsed_1b4c 1 103 1 . . . parsed_1b4c 1 104 1 . . . parsed_1b4c 1 105 1 . . . parsed_1b4c 1 106 1 . . . parsed_1b4c 1 107 1 . . . parsed_1b4c 1 108 1 . . . parsed_1b4c 1 109 1 . . . parsed_1b4c 1 110 1 . . . parsed_1b4c 1 111 1 . . . parsed_1b4c 1 112 1 . . . parsed_1b4c 1 113 1 . . . parsed_1b4c 1 114 1 . . . parsed_1b4c 1 115 1 . . . parsed_1b4c 1 116 1 . . . parsed_1b4c 1 117 1 . . . parsed_1b4c 1 118 1 . . . parsed_1b4c 1 119 1 . . . parsed_1b4c 1 120 1 . . . parsed_1b4c 1 121 1 . . . parsed_1b4c 1 122 1 . . . parsed_1b4c 1 123 1 . . . parsed_1b4c 1 124 1 . . . parsed_1b4c 1 125 1 . . . parsed_1b4c 1 126 1 . . . parsed_1b4c 1 127 1 . . . parsed_1b4c 1 128 1 . . . parsed_1b4c 1 129 1 . . . parsed_1b4c 1 130 1 . . . parsed_1b4c 1 131 1 . . . parsed_1b4c 1 132 1 . . . parsed_1b4c 1 133 1 . . . parsed_1b4c 1 134 1 . . . parsed_1b4c 1 135 1 . . . parsed_1b4c 1 136 1 . . . parsed_1b4c 1 137 1 . . . parsed_1b4c 1 138 1 . . . parsed_1b4c 1 139 1 . . . parsed_1b4c 1 140 1 . . . parsed_1b4c 1 141 1 . . . parsed_1b4c 1 142 1 . . . parsed_1b4c 1 143 1 . . . parsed_1b4c 1 144 1 . . . parsed_1b4c 1 145 1 . . . parsed_1b4c 1 146 1 . . . parsed_1b4c 1 147 1 . . . parsed_1b4c 1 148 1 . . . parsed_1b4c 1 149 1 . . . parsed_1b4c 1 150 1 . . . parsed_1b4c 1 151 1 . . . parsed_1b4c 1 152 1 . . . parsed_1b4c 1 153 1 . . . parsed_1b4c 1 154 1 . . . parsed_1b4c 1 155 1 . . . parsed_1b4c 1 156 1 . . . parsed_1b4c 1 157 1 . . . parsed_1b4c 1 158 1 . . . parsed_1b4c 1 159 1 . . . parsed_1b4c 1 160 1 . . . parsed_1b4c 1 161 1 . . . parsed_1b4c 1 162 1 . . . parsed_1b4c 1 163 1 . . . parsed_1b4c 1 164 1 . . . parsed_1b4c 1 165 1 . . . parsed_1b4c 1 166 1 . . . parsed_1b4c 1 167 1 . . . parsed_1b4c 1 168 1 . . . parsed_1b4c 1 169 1 . . . parsed_1b4c 1 170 1 . . . parsed_1b4c 1 171 1 . . . parsed_1b4c 1 172 1 . . . parsed_1b4c 1 173 1 . . . parsed_1b4c 1 174 1 . . . parsed_1b4c 1 175 1 . . . parsed_1b4c 1 176 1 . . . parsed_1b4c 1 177 1 . . . parsed_1b4c 1 178 1 . . . parsed_1b4c 1 179 1 . . . parsed_1b4c 1 180 1 . . . parsed_1b4c 1 181 1 . . . parsed_1b4c 1 182 1 . . . parsed_1b4c 1 183 1 . . . parsed_1b4c 1 184 1 . . . parsed_1b4c 1 185 1 . . . parsed_1b4c 1 186 1 . . . parsed_1b4c 1 187 1 . . . parsed_1b4c 1 188 1 . . . parsed_1b4c 1 189 1 . . . parsed_1b4c 1 190 1 . . . parsed_1b4c 1 191 1 . . . parsed_1b4c 1 192 1 . . . parsed_1b4c 1 193 1 . . . parsed_1b4c 1 194 1 . . . parsed_1b4c 1 195 1 . . . parsed_1b4c 1 196 1 . . . parsed_1b4c 1 197 1 . . . parsed_1b4c 1 198 1 . . . parsed_1b4c 1 199 1 . . . parsed_1b4c 1 200 1 . . . parsed_1b4c 1 201 1 . . . parsed_1b4c 1 202 1 . . . parsed_1b4c 1 203 1 . . . parsed_1b4c 1 204 1 . . . parsed_1b4c 1 205 1 . . . parsed_1b4c 1 206 1 . . . parsed_1b4c 1 207 1 . . . parsed_1b4c 1 208 1 . . . parsed_1b4c 1 209 1 . . . parsed_1b4c 1 210 1 . . . parsed_1b4c 1 211 1 . . . parsed_1b4c 1 212 1 . . . parsed_1b4c 1 213 1 . . . parsed_1b4c 1 214 1 . . . parsed_1b4c 1 215 1 . . . parsed_1b4c 1 216 1 . . . parsed_1b4c 1 217 1 . . . parsed_1b4c 1 218 1 . . . parsed_1b4c 1 219 1 . . . parsed_1b4c 1 220 1 . . . parsed_1b4c 1 221 1 . . . parsed_1b4c 1 222 1 . . . parsed_1b4c 1 223 1 . . . parsed_1b4c 1 224 1 . . . parsed_1b4c 1 225 1 . . . parsed_1b4c 1 226 1 . . . parsed_1b4c 1 227 1 . . . parsed_1b4c 1 228 1 . . . parsed_1b4c 1 229 1 . . . parsed_1b4c 1 230 1 . . . parsed_1b4c 1 231 1 . . . parsed_1b4c 1 232 1 . . . parsed_1b4c 1 233 1 . . . parsed_1b4c 1 234 1 . . . parsed_1b4c 1 235 1 . . . parsed_1b4c 1 236 1 . . . parsed_1b4c 1 237 1 . . . parsed_1b4c 1 238 1 . . . parsed_1b4c 1 239 1 . . . parsed_1b4c 1 240 1 . . . parsed_1b4c 1 241 1 . . . parsed_1b4c 1 242 1 . . . parsed_1b4c 1 243 1 . . . parsed_1b4c 1 244 1 . . . parsed_1b4c 1 245 1 . . . parsed_1b4c 1 246 1 . . . parsed_1b4c 1 247 1 . . . parsed_1b4c 1 248 1 . . . parsed_1b4c 1 249 1 . . . parsed_1b4c 1 250 1 . . . parsed_1b4c 1 251 1 . . . parsed_1b4c 1 252 1 . . . parsed_1b4c 1 253 1 . . . parsed_1b4c 1 254 1 . . . parsed_1b4c 1 255 1 . . . parsed_1b4c 1 256 1 . . . parsed_1b4c 1 257 1 . . . parsed_1b4c 1 258 1 . . . parsed_1b4c 1 259 1 . . . parsed_1b4c 1 260 1 . . . parsed_1b4c 1 261 1 . . . parsed_1b4c 1 262 1 . . . parsed_1b4c 1 263 1 . . . parsed_1b4c 1 264 1 . . . parsed_1b4c 1 265 1 . . . parsed_1b4c 1 266 1 . . . parsed_1b4c 1 267 1 . . . parsed_1b4c 1 268 1 . . . parsed_1b4c 1 269 1 . . . parsed_1b4c 1 270 1 . . . parsed_1b4c 1 271 1 . . . parsed_1b4c 1 272 1 . . . parsed_1b4c 1 273 1 . . . parsed_1b4c 1 274 1 . . . parsed_1b4c 1 275 1 . . . parsed_1b4c 1 276 1 . . . parsed_1b4c 1 277 1 . . . parsed_1b4c 1 278 1 . . . parsed_1b4c 1 279 1 . . . parsed_1b4c 1 280 1 . . . parsed_1b4c 1 281 1 . . . parsed_1b4c 1 282 1 . . . parsed_1b4c 1 283 1 . . . parsed_1b4c 1 284 1 . . . parsed_1b4c 1 285 1 . . . parsed_1b4c 1 286 1 . . . parsed_1b4c 1 287 1 . . . parsed_1b4c 1 288 1 . . . parsed_1b4c 1 289 1 . . . parsed_1b4c 1 290 1 . . . parsed_1b4c 1 291 1 . . . parsed_1b4c 1 292 1 . . . parsed_1b4c 1 293 1 . . . parsed_1b4c 1 294 1 . . . parsed_1b4c 1 295 1 . . . parsed_1b4c 1 296 1 . . . parsed_1b4c 1 297 1 . . . parsed_1b4c 1 298 1 . . . parsed_1b4c 1 299 1 . . . parsed_1b4c 1 300 1 . . . parsed_1b4c 1 301 1 . . . parsed_1b4c 1 302 1 . . . parsed_1b4c 1 303 1 . . . parsed_1b4c 1 304 1 . . . parsed_1b4c 1 305 1 . . . parsed_1b4c 1 306 1 . . . parsed_1b4c 1 307 1 . . . parsed_1b4c 1 308 1 . . . parsed_1b4c 1 309 1 . . . parsed_1b4c 1 310 1 . . . parsed_1b4c 1 311 1 . . . parsed_1b4c 1 312 1 . . . parsed_1b4c 1 313 1 . . . parsed_1b4c 1 314 1 . . . parsed_1b4c 1 315 1 . . . parsed_1b4c 1 316 1 . . . parsed_1b4c 1 317 1 . . . parsed_1b4c 1 318 1 . . . parsed_1b4c 1 319 1 . . . parsed_1b4c 1 320 1 . . . parsed_1b4c 1 321 1 . . . parsed_1b4c 1 322 1 . . . parsed_1b4c 1 323 1 . . . parsed_1b4c 1 324 1 . . . parsed_1b4c 1 325 1 . . . parsed_1b4c 1 326 1 . . . parsed_1b4c 1 327 1 . . . parsed_1b4c 1 328 1 . . . parsed_1b4c 1 329 1 . . . parsed_1b4c 1 330 1 . . . parsed_1b4c 1 331 1 . . . parsed_1b4c 1 332 1 . . . parsed_1b4c 1 333 1 . . . parsed_1b4c 1 334 1 . . . parsed_1b4c 1 335 1 . . . parsed_1b4c 1 336 1 . . . parsed_1b4c 1 337 1 . . . parsed_1b4c 1 338 1 . . . parsed_1b4c 1 339 1 . . . parsed_1b4c 1 340 1 . . . parsed_1b4c 1 341 1 . . . parsed_1b4c 1 342 1 . . . parsed_1b4c 1 343 1 . . . parsed_1b4c 1 344 1 . . . parsed_1b4c 1 345 1 . . . parsed_1b4c 1 346 1 . . . parsed_1b4c 1 347 1 . . . parsed_1b4c 1 348 1 . . . parsed_1b4c 1 349 1 . . . parsed_1b4c 1 350 1 . . . parsed_1b4c 1 351 1 . . . parsed_1b4c 1 352 1 . . . parsed_1b4c 1 353 1 . . . parsed_1b4c 1 354 1 . . . parsed_1b4c 1 355 1 . . . parsed_1b4c 1 356 1 . . . parsed_1b4c 1 357 1 . . . parsed_1b4c 1 358 1 . . . parsed_1b4c 1 359 1 . . . parsed_1b4c 1 360 1 . . . parsed_1b4c 1 361 1 . . . parsed_1b4c 1 362 1 . . . parsed_1b4c 1 363 1 . . . parsed_1b4c 1 364 1 . . . parsed_1b4c 1 365 1 . . . parsed_1b4c 1 366 1 . . . parsed_1b4c 1 367 1 . . . parsed_1b4c 1 368 1 . . . parsed_1b4c 1 369 1 . . . parsed_1b4c 1 370 1 . . . parsed_1b4c 1 371 1 . . . parsed_1b4c 1 372 1 . . . parsed_1b4c 1 373 1 . . . parsed_1b4c 1 374 1 . . . parsed_1b4c 1 375 1 . . . parsed_1b4c 1 376 1 . . . parsed_1b4c 1 377 1 . . . parsed_1b4c 1 378 1 . . . parsed_1b4c 1 379 1 . . . parsed_1b4c 1 380 1 . . . parsed_1b4c 1 381 1 . . . parsed_1b4c 1 382 1 . . . parsed_1b4c 1 383 1 . . . parsed_1b4c 1 384 1 . . . parsed_1b4c 1 385 1 . . . parsed_1b4c 1 386 1 . . . parsed_1b4c 1 387 1 . . . parsed_1b4c 1 388 1 . . . parsed_1b4c 1 389 1 . . . parsed_1b4c 1 390 1 . . . parsed_1b4c 1 391 1 . . . parsed_1b4c 1 392 1 . . . parsed_1b4c 1 393 1 . . . parsed_1b4c 1 394 1 . . . parsed_1b4c 1 395 1 . . . parsed_1b4c 1 396 1 . . . parsed_1b4c 1 397 1 . . . parsed_1b4c 1 398 1 . . . parsed_1b4c 1 399 1 . . . parsed_1b4c 1 400 1 . . . parsed_1b4c 1 401 1 . . . parsed_1b4c 1 402 1 . . . parsed_1b4c 1 403 1 . . . parsed_1b4c 1 404 1 . . . parsed_1b4c 1 405 1 . . . parsed_1b4c 1 406 1 . . . parsed_1b4c 1 407 1 . . . parsed_1b4c 1 408 1 . . . parsed_1b4c 1 409 1 . . . parsed_1b4c 1 410 1 . . . parsed_1b4c 1 411 1 . . . parsed_1b4c 1 412 1 . . . parsed_1b4c 1 413 1 . . . parsed_1b4c 1 414 1 . . . parsed_1b4c 1 415 1 . . . parsed_1b4c 1 416 1 . . . parsed_1b4c 1 417 1 . . . parsed_1b4c 1 418 1 . . . parsed_1b4c 1 419 1 . . . parsed_1b4c 1 420 1 . . . parsed_1b4c 1 421 1 . . . parsed_1b4c 1 422 1 . . . parsed_1b4c 1 423 1 . . . parsed_1b4c 1 424 1 . . . parsed_1b4c 1 425 1 . . . parsed_1b4c 1 426 1 . . . parsed_1b4c 1 427 1 . . . parsed_1b4c 1 428 1 . . . parsed_1b4c 1 429 1 . . . parsed_1b4c 1 430 1 . . . parsed_1b4c 1 431 1 . . . parsed_1b4c 1 432 1 . . . parsed_1b4c 1 433 1 . . . parsed_1b4c 1 434 1 . . . parsed_1b4c 1 435 1 . . . parsed_1b4c 1 436 1 . . . parsed_1b4c 1 437 1 . . . parsed_1b4c 1 438 1 . . . parsed_1b4c 1 439 1 . . . parsed_1b4c 1 440 1 . . . parsed_1b4c 1 441 1 . . . parsed_1b4c 1 442 1 . . . parsed_1b4c 1 443 1 . . . parsed_1b4c 1 444 1 . . . parsed_1b4c 1 445 1 . . . parsed_1b4c 1 446 1 . . . parsed_1b4c 1 447 1 . . . parsed_1b4c 1 448 1 . . . parsed_1b4c 1 449 1 . . . parsed_1b4c 1 450 1 . . . parsed_1b4c 1 451 1 . . . parsed_1b4c 1 452 1 . . . parsed_1b4c 1 453 1 . . . parsed_1b4c 1 454 1 . . . parsed_1b4c 1 455 1 . . . parsed_1b4c 1 456 1 . . . parsed_1b4c 1 457 1 . . . parsed_1b4c 1 458 1 . . . parsed_1b4c 1 459 1 . . . parsed_1b4c 1 460 1 . . . parsed_1b4c 1 461 1 . . . parsed_1b4c 1 462 1 . . . parsed_1b4c 1 463 1 . . . parsed_1b4c 1 464 1 . . . parsed_1b4c 1 465 1 . . . parsed_1b4c 1 466 1 . . . parsed_1b4c 1 467 1 . . . parsed_1b4c 1 468 1 . . . parsed_1b4c 1 469 1 . . . parsed_1b4c 1 470 1 . . . parsed_1b4c 1 471 1 . . . parsed_1b4c 1 472 1 . . . parsed_1b4c 1 473 1 . . . parsed_1b4c 1 474 1 . . . parsed_1b4c 1 475 1 . . . parsed_1b4c 1 476 1 . . . parsed_1b4c 1 477 1 . . . parsed_1b4c 1 478 1 . . . parsed_1b4c 1 479 1 . . . parsed_1b4c 1 480 1 . . . parsed_1b4c 1 481 1 . . . parsed_1b4c 1 482 1 . . . parsed_1b4c 1 483 1 . . . parsed_1b4c 1 484 1 . . . parsed_1b4c 1 485 1 . . . parsed_1b4c 1 486 1 . . . parsed_1b4c 1 487 1 . . . parsed_1b4c 1 488 1 . . . parsed_1b4c 1 489 1 . . . parsed_1b4c 1 490 1 . . . parsed_1b4c 1 491 1 . . . parsed_1b4c 1 492 1 . . . parsed_1b4c 1 493 1 . . . parsed_1b4c 1 494 1 . . . parsed_1b4c 1 495 1 . . . parsed_1b4c 1 496 1 . . . parsed_1b4c 1 497 1 . . . parsed_1b4c 1 498 1 . . . parsed_1b4c 1 499 1 . . . parsed_1b4c 1 500 1 . . . parsed_1b4c 1 501 1 . . . parsed_1b4c 1 502 1 . . . parsed_1b4c 1 503 1 . . . parsed_1b4c 1 504 1 . . . parsed_1b4c 1 505 1 . . . parsed_1b4c 1 506 1 . . . parsed_1b4c 1 507 1 . . . parsed_1b4c 1 508 1 . . . parsed_1b4c 1 509 1 . . . parsed_1b4c 1 510 1 . . . parsed_1b4c 1 511 1 . . . parsed_1b4c 1 512 1 . . . parsed_1b4c 1 513 1 . . . parsed_1b4c 1 514 1 . . . parsed_1b4c 1 515 1 . . . parsed_1b4c 1 516 1 . . . parsed_1b4c 1 517 1 . . . parsed_1b4c 1 518 1 . . . parsed_1b4c 1 519 1 . . . parsed_1b4c 1 520 1 . . . parsed_1b4c 1 521 1 . . . parsed_1b4c 1 522 1 . . . parsed_1b4c 1 523 1 . . . parsed_1b4c 1 524 1 . . . parsed_1b4c 1 525 1 . . . parsed_1b4c 1 526 1 . . . parsed_1b4c 1 527 1 . . . parsed_1b4c 1 528 1 . . . parsed_1b4c 1 529 1 . . . parsed_1b4c 1 530 1 . . . parsed_1b4c 1 531 1 . . . parsed_1b4c 1 532 1 . . . parsed_1b4c 1 533 1 . . . parsed_1b4c 1 534 1 . . . parsed_1b4c 1 535 1 . . . parsed_1b4c 1 536 1 . . . parsed_1b4c 1 537 1 . . . parsed_1b4c 1 538 1 . . . parsed_1b4c 1 539 1 . . . parsed_1b4c 1 540 1 . . . parsed_1b4c 1 541 1 . . . parsed_1b4c 1 542 1 . . . parsed_1b4c 1 543 1 . . . parsed_1b4c 1 544 1 . . . parsed_1b4c 1 545 1 . . . parsed_1b4c 1 546 1 . . . parsed_1b4c 1 547 1 . . . parsed_1b4c 1 548 1 . . . parsed_1b4c 1 549 1 . . . parsed_1b4c 1 550 1 . . . parsed_1b4c 1 551 1 . . . parsed_1b4c 1 552 1 . . . parsed_1b4c 1 553 1 . . . parsed_1b4c 1 554 1 . . . parsed_1b4c 1 555 1 . . . parsed_1b4c 1 556 1 . . . parsed_1b4c 1 557 1 . . . parsed_1b4c 1 558 1 . . . parsed_1b4c 1 559 1 . . . parsed_1b4c 1 560 1 . . . parsed_1b4c 1 561 1 . . . parsed_1b4c 1 562 1 . . . parsed_1b4c 1 563 1 . . . parsed_1b4c 1 564 1 . . . parsed_1b4c 1 565 1 . . . parsed_1b4c 1 566 1 . . . parsed_1b4c 1 567 1 . . . parsed_1b4c 1 568 1 . . . parsed_1b4c 1 569 1 . . . parsed_1b4c 1 570 1 . . . parsed_1b4c 1 571 1 . . . parsed_1b4c 1 572 1 . . . parsed_1b4c 1 573 1 . . . parsed_1b4c 1 574 1 . . . parsed_1b4c 1 575 1 . . . parsed_1b4c 1 576 1 . . . parsed_1b4c 1 577 1 . . . parsed_1b4c 1 578 1 . . . parsed_1b4c 1 579 1 . . . parsed_1b4c 1 580 1 . . . parsed_1b4c 1 581 1 . . . parsed_1b4c 1 582 1 . . . parsed_1b4c 1 583 1 . . . parsed_1b4c 1 584 1 . . . parsed_1b4c 1 585 1 . . . parsed_1b4c 1 586 1 . . . parsed_1b4c 1 587 1 . . . parsed_1b4c 1 588 1 . . . parsed_1b4c 1 589 1 . . . parsed_1b4c 1 590 1 . . . parsed_1b4c 1 591 1 . . . parsed_1b4c 1 592 1 . . . parsed_1b4c 1 593 1 . . . parsed_1b4c 1 594 1 . . . parsed_1b4c 1 595 1 . . . parsed_1b4c 1 596 1 . . . parsed_1b4c 1 597 1 . . . parsed_1b4c 1 598 1 . . . parsed_1b4c 1 599 1 . . . parsed_1b4c 1 600 1 . . . parsed_1b4c 1 601 1 . . . parsed_1b4c 1 602 1 . . . parsed_1b4c 1 603 1 . . . parsed_1b4c 1 604 1 . . . parsed_1b4c 1 605 1 . . . parsed_1b4c 1 606 1 . . . parsed_1b4c 1 607 1 . . . parsed_1b4c 1 608 1 . . . parsed_1b4c 1 609 1 . . . parsed_1b4c 1 610 1 . . . parsed_1b4c 1 611 1 . . . parsed_1b4c 1 612 1 . . . parsed_1b4c 1 613 1 . . . parsed_1b4c 1 614 1 . . . parsed_1b4c 1 615 1 . . . parsed_1b4c 1 616 1 . . . parsed_1b4c 1 617 1 . . . parsed_1b4c 1 618 1 . . . parsed_1b4c 1 619 1 . . . parsed_1b4c 1 620 1 . . . parsed_1b4c 1 621 1 . . . parsed_1b4c 1 622 1 . . . parsed_1b4c 1 623 1 . . . parsed_1b4c 1 624 1 . . . parsed_1b4c 1 625 1 . . . parsed_1b4c 1 626 1 . . . parsed_1b4c 1 627 1 . . . parsed_1b4c 1 628 1 . . . parsed_1b4c 1 629 1 . . . parsed_1b4c 1 630 1 . . . parsed_1b4c 1 631 1 . . . parsed_1b4c 1 632 1 . . . parsed_1b4c 1 633 1 . . . parsed_1b4c 1 634 1 . . . parsed_1b4c 1 635 1 . . . parsed_1b4c 1 636 1 . . . parsed_1b4c 1 637 1 . . . parsed_1b4c 1 638 1 . . . parsed_1b4c 1 639 1 . . . parsed_1b4c 1 640 1 . . . parsed_1b4c 1 641 1 . . . parsed_1b4c 1 642 1 . . . parsed_1b4c 1 643 1 . . . parsed_1b4c 1 644 1 . . . parsed_1b4c 1 645 1 . . . parsed_1b4c 1 646 1 . . . parsed_1b4c 1 647 1 . . . parsed_1b4c 1 648 1 . . . parsed_1b4c 1 649 1 . . . parsed_1b4c 1 650 1 . . . parsed_1b4c 1 651 1 . . . parsed_1b4c 1 652 1 . . . parsed_1b4c 1 653 1 . . . parsed_1b4c 1 654 1 . . . parsed_1b4c 1 655 1 . . . parsed_1b4c 1 656 1 . . . parsed_1b4c 1 657 1 . . . parsed_1b4c 1 658 1 . . . parsed_1b4c 1 659 1 . . . parsed_1b4c 1 660 1 . . . parsed_1b4c 1 661 1 . . . parsed_1b4c 1 662 1 . . . parsed_1b4c 1 663 1 . . . parsed_1b4c 1 664 1 . . . parsed_1b4c 1 665 1 . . . parsed_1b4c 1 666 1 . . . parsed_1b4c 1 667 1 . . . parsed_1b4c 1 668 1 . . . parsed_1b4c 1 669 1 . . . parsed_1b4c 1 670 1 . . . parsed_1b4c 1 671 1 . . . parsed_1b4c 1 672 1 . . . parsed_1b4c 1 673 1 . . . parsed_1b4c 1 674 1 . . . parsed_1b4c 1 675 1 . . . parsed_1b4c 1 676 1 . . . parsed_1b4c 1 677 1 . . . parsed_1b4c 1 678 1 . . . parsed_1b4c 1 679 1 . . . parsed_1b4c 1 680 1 . . . parsed_1b4c 1 681 1 . . . parsed_1b4c 1 682 1 . . . parsed_1b4c 1 683 1 . . . parsed_1b4c 1 684 1 . . . parsed_1b4c 1 685 1 . . . parsed_1b4c 1 686 1 . . . parsed_1b4c 1 687 1 . . . parsed_1b4c 1 688 1 . . . parsed_1b4c 1 689 1 . . . parsed_1b4c 1 690 1 . . . parsed_1b4c 1 691 1 . . . parsed_1b4c 1 692 1 . . . parsed_1b4c 1 693 1 . . . parsed_1b4c 1 694 1 . . . parsed_1b4c 1 695 1 . . . parsed_1b4c 1 696 1 . . . parsed_1b4c 1 697 1 . . . parsed_1b4c 1 698 1 . . . parsed_1b4c 1 699 1 . . . parsed_1b4c 1 700 1 . . . parsed_1b4c 1 701 1 . . . parsed_1b4c 1 702 1 . . . parsed_1b4c 1 703 1 . . . parsed_1b4c 1 704 1 . . . parsed_1b4c 1 705 1 . . . parsed_1b4c 1 706 1 . . . parsed_1b4c 1 707 1 . . . parsed_1b4c 1 708 1 . . . parsed_1b4c 1 709 1 . . . parsed_1b4c 1 710 1 . . . parsed_1b4c 1 711 1 . . . parsed_1b4c 1 712 1 . . . parsed_1b4c 1 713 1 . . . parsed_1b4c 1 714 1 . . . parsed_1b4c 1 715 1 . . . parsed_1b4c 1 716 1 . . . parsed_1b4c 1 717 1 . . . parsed_1b4c 1 718 1 . . . parsed_1b4c 1 719 1 . . . parsed_1b4c 1 720 1 . . . parsed_1b4c 1 721 1 . . . parsed_1b4c 1 722 1 . . . parsed_1b4c 1 723 1 . . . parsed_1b4c 1 724 1 . . . parsed_1b4c 1 725 1 . . . parsed_1b4c 1 726 1 . . . parsed_1b4c 1 727 1 . . . parsed_1b4c 1 728 1 . . . parsed_1b4c 1 729 1 . . . parsed_1b4c 1 730 1 . . . parsed_1b4c 1 731 1 . . . parsed_1b4c 1 732 1 . . . parsed_1b4c 1 733 1 . . . parsed_1b4c 1 734 1 . . . parsed_1b4c 1 735 1 . . . parsed_1b4c 1 736 1 . . . parsed_1b4c 1 737 1 . . . parsed_1b4c 1 738 1 . . . parsed_1b4c 1 739 1 . . . parsed_1b4c 1 740 1 . . . parsed_1b4c 1 741 1 . . . parsed_1b4c 1 742 1 . . . parsed_1b4c 1 743 1 . . . parsed_1b4c 1 744 1 . . . parsed_1b4c 1 745 1 . . . parsed_1b4c 1 746 1 . . . parsed_1b4c 1 747 1 . . . parsed_1b4c 1 748 1 . . . parsed_1b4c 1 749 1 . . . parsed_1b4c 1 750 1 . . . parsed_1b4c 1 751 1 . . . parsed_1b4c 1 752 1 . . . parsed_1b4c 1 753 1 . . . parsed_1b4c 1 754 1 . . . parsed_1b4c 1 755 1 . . . parsed_1b4c 1 756 1 . . . parsed_1b4c 1 757 1 . . . parsed_1b4c 1 758 1 . . . parsed_1b4c 1 759 1 . . . parsed_1b4c 1 760 1 . . . parsed_1b4c 1 761 1 . . . parsed_1b4c 1 762 1 . . . parsed_1b4c 1 763 1 . . . parsed_1b4c 1 764 1 . . . parsed_1b4c 1 765 1 . . . parsed_1b4c 1 766 1 . . . parsed_1b4c 1 767 1 . . . parsed_1b4c 1 768 1 . . . parsed_1b4c 1 769 1 . . . parsed_1b4c 1 770 1 . . . parsed_1b4c 1 771 1 . . . parsed_1b4c 1 772 1 . . . parsed_1b4c 1 773 1 . . . parsed_1b4c 1 774 1 . . . parsed_1b4c 1 775 1 . . . parsed_1b4c 1 776 1 . . . parsed_1b4c 1 777 1 . . . parsed_1b4c 1 778 1 . . . parsed_1b4c 1 779 1 . . . parsed_1b4c 1 780 1 . . . parsed_1b4c 1 781 1 . . . parsed_1b4c 1 782 1 . . . parsed_1b4c 1 783 1 . . . parsed_1b4c 1 784 1 . . . parsed_1b4c 1 785 1 . . . parsed_1b4c 1 786 1 . . . parsed_1b4c 1 787 1 . . . parsed_1b4c 1 788 1 . . . parsed_1b4c 1 789 1 . . . parsed_1b4c 1 790 1 . . . parsed_1b4c 1 791 1 . . . parsed_1b4c 1 792 1 . . . parsed_1b4c 1 793 1 . . . parsed_1b4c 1 794 1 . . . parsed_1b4c 1 795 1 . . . parsed_1b4c 1 796 1 . . . parsed_1b4c 1 797 1 . . . parsed_1b4c 1 798 1 . . . parsed_1b4c 1 799 1 . . . parsed_1b4c 1 800 1 . . . parsed_1b4c 1 801 1 . . . parsed_1b4c 1 802 1 . . . parsed_1b4c 1 803 1 . . . parsed_1b4c 1 804 1 . . . parsed_1b4c 1 805 1 . . . parsed_1b4c 1 806 1 . . . parsed_1b4c 1 807 1 . . . parsed_1b4c 1 808 1 . . . parsed_1b4c 1 809 1 . . . parsed_1b4c 1 810 1 . . . parsed_1b4c 1 811 1 . . . parsed_1b4c 1 812 1 . . . parsed_1b4c 1 813 1 . . . parsed_1b4c 1 814 1 . . . parsed_1b4c 1 815 1 . . . parsed_1b4c 1 816 1 . . . parsed_1b4c 1 817 1 . . . parsed_1b4c 1 818 1 . . . parsed_1b4c 1 819 1 . . . parsed_1b4c 1 820 1 . . . parsed_1b4c 1 821 1 . . . parsed_1b4c 1 822 1 . . . parsed_1b4c 1 823 1 . . . parsed_1b4c 1 824 1 . . . parsed_1b4c 1 825 1 . . . parsed_1b4c 1 826 1 . . . parsed_1b4c 1 827 1 . . . parsed_1b4c 1 828 1 . . . parsed_1b4c 1 829 1 . . . parsed_1b4c 1 830 1 . . . parsed_1b4c 1 831 1 . . . parsed_1b4c 1 832 1 . . . parsed_1b4c 1 833 1 . . . parsed_1b4c 1 834 1 . . . parsed_1b4c 1 835 1 . . . parsed_1b4c 1 836 1 . . . parsed_1b4c 1 837 1 . . . parsed_1b4c 1 838 1 . . . parsed_1b4c 1 839 1 . . . parsed_1b4c 1 840 1 . . . parsed_1b4c 1 841 1 . . . parsed_1b4c 1 842 1 . . . parsed_1b4c 1 843 1 . . . parsed_1b4c 1 844 1 . . . parsed_1b4c 1 845 1 . . . parsed_1b4c 1 846 1 . . . parsed_1b4c 1 847 1 . . . parsed_1b4c 1 848 1 . . . parsed_1b4c 1 849 1 . . . parsed_1b4c 1 850 1 . . . parsed_1b4c 1 851 1 . . . parsed_1b4c 1 852 1 . . . parsed_1b4c 1 853 1 . . . parsed_1b4c 1 854 1 . . . parsed_1b4c 1 855 1 . . . parsed_1b4c 1 856 1 . . . parsed_1b4c 1 857 1 . . . parsed_1b4c 1 858 1 . . . parsed_1b4c 1 859 1 . . . parsed_1b4c 1 860 1 . . . parsed_1b4c 1 861 1 . . . parsed_1b4c 1 862 1 . . . parsed_1b4c 1 863 1 . . . parsed_1b4c 1 864 1 . . . parsed_1b4c 1 865 1 . . . parsed_1b4c 1 866 1 . . . parsed_1b4c 1 867 1 . . . parsed_1b4c 1 868 1 . . . parsed_1b4c 1 869 1 . . . parsed_1b4c 1 870 1 . . . parsed_1b4c 1 871 1 . . . parsed_1b4c 1 872 1 . . . parsed_1b4c 1 873 1 . . . parsed_1b4c 1 874 1 . . . parsed_1b4c 1 875 1 . . . parsed_1b4c 1 876 1 . . . parsed_1b4c 1 877 1 . . . parsed_1b4c 1 878 1 . . . parsed_1b4c 1 879 1 . . . parsed_1b4c 1 880 1 . . . parsed_1b4c 1 881 1 . . . parsed_1b4c 1 882 1 . . . parsed_1b4c 1 883 1 . . . parsed_1b4c 1 884 1 . . . parsed_1b4c 1 885 1 . . . parsed_1b4c 1 886 1 . . . parsed_1b4c 1 887 1 . . . parsed_1b4c 1 888 1 . . . parsed_1b4c 1 889 1 . . . parsed_1b4c 1 890 1 . . . parsed_1b4c 1 891 1 . . . parsed_1b4c 1 892 1 . . . parsed_1b4c 1 893 1 . . . parsed_1b4c 1 894 1 . . . parsed_1b4c 1 895 1 . . . parsed_1b4c 1 896 1 . . . parsed_1b4c 1 897 1 . . . parsed_1b4c 1 898 1 . . . parsed_1b4c 1 899 1 . . . parsed_1b4c 1 900 1 . . . parsed_1b4c 1 901 1 . . . parsed_1b4c 1 902 1 . . . parsed_1b4c 1 903 1 . . . parsed_1b4c 1 904 1 . . . parsed_1b4c 1 905 1 . . . parsed_1b4c 1 906 1 . . . parsed_1b4c 1 907 1 . . . parsed_1b4c 1 908 1 . . . parsed_1b4c 1 909 1 . . . parsed_1b4c 1 910 1 . . . parsed_1b4c 1 911 1 . . . parsed_1b4c 1 912 1 . . . parsed_1b4c 1 913 1 . . . parsed_1b4c 1 914 1 . . . parsed_1b4c 1 915 1 . . . parsed_1b4c 1 916 1 . . . parsed_1b4c 1 917 1 . . . parsed_1b4c 1 918 1 . . . parsed_1b4c 1 919 1 . . . parsed_1b4c 1 920 1 . . . parsed_1b4c 1 921 1 . . . parsed_1b4c 1 922 1 . . . parsed_1b4c 1 923 1 . . . parsed_1b4c 1 924 1 . . . parsed_1b4c 1 925 1 . . . parsed_1b4c 1 926 1 . . . parsed_1b4c 1 927 1 . . . parsed_1b4c 1 928 1 . . . parsed_1b4c 1 929 1 . . . parsed_1b4c 1 930 1 . . . parsed_1b4c 1 931 1 . . . parsed_1b4c 1 932 1 . . . parsed_1b4c 1 933 1 . . . parsed_1b4c 1 934 1 . . . parsed_1b4c 1 935 1 . . . parsed_1b4c 1 936 1 . . . parsed_1b4c 1 937 1 . . . parsed_1b4c 1 938 1 . . . parsed_1b4c 1 939 1 . . . parsed_1b4c 1 940 1 . . . parsed_1b4c 1 941 1 . . . parsed_1b4c 1 942 1 . . . parsed_1b4c 1 943 1 . . . parsed_1b4c 1 944 1 . . . parsed_1b4c 1 945 1 . . . parsed_1b4c 1 946 1 . . . parsed_1b4c 1 947 1 . . . parsed_1b4c 1 948 1 . . . parsed_1b4c 1 949 1 . . . parsed_1b4c 1 950 1 . . . parsed_1b4c 1 951 1 . . . parsed_1b4c 1 952 1 . . . parsed_1b4c 1 953 1 . . . parsed_1b4c 1 954 1 . . . parsed_1b4c 1 955 1 . . . parsed_1b4c 1 956 1 . . . parsed_1b4c 1 957 1 . . . parsed_1b4c 1 958 1 . . . parsed_1b4c 1 959 1 . . . parsed_1b4c 1 960 1 . . . parsed_1b4c 1 961 1 . . . parsed_1b4c 1 962 1 . . . parsed_1b4c 1 963 1 . . . parsed_1b4c 1 964 1 . . . parsed_1b4c 1 965 1 . . . parsed_1b4c 1 966 1 . . . parsed_1b4c 1 967 1 . . . parsed_1b4c 1 968 1 . . . parsed_1b4c 1 969 1 . . . parsed_1b4c 1 970 1 . . . parsed_1b4c 1 971 1 . . . parsed_1b4c 1 972 1 . . . parsed_1b4c 1 973 1 . . . parsed_1b4c 1 974 1 . . . parsed_1b4c 1 975 1 . . . parsed_1b4c 1 976 1 . . . parsed_1b4c 1 977 1 . . . parsed_1b4c 1 978 1 . . . parsed_1b4c 1 979 1 . . . parsed_1b4c 1 980 1 . . . parsed_1b4c 1 981 1 . . . parsed_1b4c 1 982 1 . . . parsed_1b4c 1 983 1 . . . parsed_1b4c 1 984 1 . . . parsed_1b4c 1 985 1 . . . parsed_1b4c 1 986 1 . . . parsed_1b4c 1 987 1 . . . parsed_1b4c 1 988 1 . . . parsed_1b4c 1 989 1 . . . parsed_1b4c 1 990 1 . . . parsed_1b4c 1 991 1 . . . parsed_1b4c 1 992 1 . . . parsed_1b4c 1 993 1 . . . parsed_1b4c 1 994 1 . . . parsed_1b4c 1 995 1 . . . parsed_1b4c 1 996 1 . . . parsed_1b4c 1 997 1 . . . parsed_1b4c 1 998 1 . . . parsed_1b4c 1 999 1 . . . parsed_1b4c 1 1000 1 . . . parsed_1b4c 1 1001 1 . . . parsed_1b4c 1 1002 1 . . . parsed_1b4c 1 1003 1 . . . parsed_1b4c 1 1004 1 . . . parsed_1b4c 1 1005 1 . . . parsed_1b4c 1 1006 1 . . . parsed_1b4c 1 1007 1 . . . parsed_1b4c 1 1008 1 . . . parsed_1b4c 1 1009 1 . . . parsed_1b4c 1 1010 1 . . . parsed_1b4c 1 1011 1 . . . parsed_1b4c 1 1012 1 . . . parsed_1b4c 1 1013 1 . . . parsed_1b4c 1 1014 1 . . . parsed_1b4c 1 1015 1 . . . parsed_1b4c 1 1016 1 . . . parsed_1b4c 1 1017 1 . . . parsed_1b4c 1 1018 1 . . . parsed_1b4c 1 1019 1 . . . parsed_1b4c 1 1020 1 . . . parsed_1b4c 1 1021 1 . . . parsed_1b4c 1 1022 1 . . . parsed_1b4c 1 1023 1 . . . parsed_1b4c 1 1024 1 . . . parsed_1b4c 1 1025 1 . . . parsed_1b4c 1 1026 1 . . . parsed_1b4c 1 1027 1 . . . parsed_1b4c 1 1028 1 . . . parsed_1b4c 1 1029 1 . . . parsed_1b4c 1 1030 1 . . . parsed_1b4c 1 1031 1 . . . parsed_1b4c 1 1032 1 . . . parsed_1b4c 1 1033 1 . . . parsed_1b4c 1 1034 1 . . . parsed_1b4c 1 1035 1 . . . parsed_1b4c 1 1036 1 . . . parsed_1b4c 1 1037 1 . . . parsed_1b4c 1 1038 1 . . . parsed_1b4c 1 1039 1 . . . parsed_1b4c 1 1040 1 . . . parsed_1b4c 1 1041 1 . . . parsed_1b4c 1 1042 1 . . . parsed_1b4c 1 1043 1 . . . parsed_1b4c 1 1044 1 . . . parsed_1b4c 1 1045 1 . . . parsed_1b4c 1 1046 1 . . . parsed_1b4c 1 1047 1 . . . parsed_1b4c 1 1048 1 . . . parsed_1b4c 1 1049 1 . . . parsed_1b4c 1 1050 1 . . . parsed_1b4c 1 1051 1 . . . parsed_1b4c 1 1052 1 . . . parsed_1b4c 1 1053 1 . . . parsed_1b4c 1 1054 1 . . . parsed_1b4c 1 1055 1 . . . parsed_1b4c 1 1056 1 . . . parsed_1b4c 1 1057 1 . . . parsed_1b4c 1 1058 1 . . . parsed_1b4c 1 1059 1 . . . parsed_1b4c 1 1060 1 . . . parsed_1b4c 1 1061 1 . . . parsed_1b4c 1 1062 1 . . . parsed_1b4c 1 1063 1 . . . parsed_1b4c 1 1064 1 . . . parsed_1b4c 1 1065 1 . . . parsed_1b4c 1 1066 1 . . . parsed_1b4c 1 1067 1 . . . parsed_1b4c 1 1068 1 . . . parsed_1b4c 1 1069 1 . . . parsed_1b4c 1 1070 1 . . . parsed_1b4c 1 1071 1 . . . parsed_1b4c 1 1072 1 . . . parsed_1b4c 1 1073 1 . . . parsed_1b4c 1 1074 1 . . . parsed_1b4c 1 1075 1 . . . parsed_1b4c 1 1076 1 . . . parsed_1b4c 1 1077 1 . . . parsed_1b4c 1 1078 1 . . . parsed_1b4c 1 1079 1 . . . parsed_1b4c 1 1080 1 . . . parsed_1b4c 1 1081 1 . . . parsed_1b4c 1 1082 1 . . . parsed_1b4c 1 1083 1 . . . parsed_1b4c 1 1084 1 . . . parsed_1b4c 1 1085 1 . . . parsed_1b4c 1 1086 1 . . . parsed_1b4c 1 1087 1 . . . parsed_1b4c 1 1088 1 . . . parsed_1b4c 1 1089 1 . . . parsed_1b4c 1 1090 1 . . . parsed_1b4c 1 1091 1 . . . parsed_1b4c 1 1092 1 . . . parsed_1b4c 1 1093 1 . . . parsed_1b4c 1 1094 1 . . . parsed_1b4c 1 1095 1 . . . parsed_1b4c 1 1096 1 . . . parsed_1b4c 1 1097 1 . . . parsed_1b4c 1 1098 1 . . . parsed_1b4c 1 1099 1 . . . parsed_1b4c 1 1100 1 . . . parsed_1b4c 1 1101 1 . . . parsed_1b4c 1 1102 1 . . . parsed_1b4c 1 1103 1 . . . parsed_1b4c 1 1104 1 . . . parsed_1b4c 1 1105 1 . . . parsed_1b4c 1 1106 1 . . . parsed_1b4c 1 1107 1 . . . parsed_1b4c 1 1108 1 . . . parsed_1b4c 1 1109 1 . . . parsed_1b4c 1 1110 1 . . . parsed_1b4c 1 1111 1 . . . parsed_1b4c 1 1112 1 . . . parsed_1b4c 1 1113 1 . . . parsed_1b4c 1 1114 1 . . . parsed_1b4c 1 1115 1 . . . parsed_1b4c 1 1116 1 . . . parsed_1b4c 1 1117 1 . . . parsed_1b4c 1 1118 1 . . . parsed_1b4c 1 1119 1 . . . parsed_1b4c 1 1120 1 . . . parsed_1b4c 1 1121 1 . . . parsed_1b4c 1 1122 1 . . . parsed_1b4c 1 1123 1 . . . parsed_1b4c 1 1124 1 . . . parsed_1b4c 1 1125 1 . . . parsed_1b4c 1 1126 1 . . . parsed_1b4c 1 1127 1 . . . parsed_1b4c 1 1128 1 . . . parsed_1b4c 1 1129 1 . . . parsed_1b4c 1 1130 1 . . . parsed_1b4c 1 1131 1 . . . parsed_1b4c 1 1132 1 . . . parsed_1b4c 1 1133 1 . . . parsed_1b4c 1 1134 1 . . . parsed_1b4c 1 1135 1 . . . parsed_1b4c 1 1136 1 . . . parsed_1b4c 1 1137 1 . . . parsed_1b4c 1 1138 1 . . . parsed_1b4c 1 1139 1 . . . parsed_1b4c 1 1140 1 . . . parsed_1b4c 1 1141 1 . . . parsed_1b4c 1 1142 1 . . . parsed_1b4c 1 1143 1 . . . parsed_1b4c 1 1144 1 . . . parsed_1b4c 1 1145 1 . . . parsed_1b4c 1 1146 1 . . . parsed_1b4c 1 1147 1 . . . parsed_1b4c 1 1148 1 . . . parsed_1b4c 1 1149 1 . . . parsed_1b4c 1 1150 1 . . . parsed_1b4c 1 1151 1 . . . parsed_1b4c 1 1152 1 . . . parsed_1b4c 1 1153 1 . . . parsed_1b4c 1 1154 1 . . . parsed_1b4c 1 1155 1 . . . parsed_1b4c 1 1156 1 . . . parsed_1b4c 1 1157 1 . . . parsed_1b4c 1 1158 1 . . . parsed_1b4c 1 1159 1 . . . parsed_1b4c 1 1160 1 . . . parsed_1b4c 1 1161 1 . . . parsed_1b4c 1 1162 1 . . . parsed_1b4c 1 1163 1 . . . parsed_1b4c 1 1164 1 . . . parsed_1b4c 1 1165 1 . . . parsed_1b4c 1 1166 1 . . . parsed_1b4c 1 1167 1 . . . parsed_1b4c 1 1168 1 . . . parsed_1b4c 1 1169 1 . . . parsed_1b4c 1 1170 1 . . . parsed_1b4c 1 1171 1 . . . parsed_1b4c 1 1172 1 . . . parsed_1b4c 1 1173 1 . . . parsed_1b4c 1 1174 1 . . . parsed_1b4c 1 1175 1 . . . parsed_1b4c 1 1176 1 . . . parsed_1b4c 1 1177 1 . . . parsed_1b4c 1 1178 1 . . . parsed_1b4c 1 1179 1 . . . parsed_1b4c 1 1180 1 . . . parsed_1b4c 1 1181 1 . . . parsed_1b4c 1 1182 1 . . . parsed_1b4c 1 1183 1 . . . parsed_1b4c 1 1184 1 . . . parsed_1b4c 1 1185 1 . . . parsed_1b4c 1 1186 1 . . . parsed_1b4c 1 1187 1 . . . parsed_1b4c 1 1188 1 . . . parsed_1b4c 1 1189 1 . . . parsed_1b4c 1 1190 1 . . . parsed_1b4c 1 1191 1 . . . parsed_1b4c 1 1192 1 . . . parsed_1b4c 1 1193 1 . . . parsed_1b4c 1 1194 1 . . . parsed_1b4c 1 1195 1 . . . parsed_1b4c 1 1196 1 . . . parsed_1b4c 1 1197 1 . . . parsed_1b4c 1 1198 1 . . . parsed_1b4c 1 1199 1 . . . parsed_1b4c 1 1200 1 . . . parsed_1b4c 1 1201 1 . . . parsed_1b4c 1 1202 1 . . . parsed_1b4c 1 1203 1 . . . parsed_1b4c 1 1204 1 . . . parsed_1b4c 1 1205 1 . . . parsed_1b4c 1 1206 1 . . . parsed_1b4c 1 1207 1 . . . parsed_1b4c 1 1208 1 . . . parsed_1b4c 1 1209 1 . . . parsed_1b4c 1 1210 1 . . . parsed_1b4c 1 1211 1 . . . parsed_1b4c 1 1212 1 . . . parsed_1b4c 1 1213 1 . . . parsed_1b4c 1 1214 1 . . . parsed_1b4c 1 1215 1 . . . parsed_1b4c 1 1216 1 . . . parsed_1b4c 1 1217 1 . . . parsed_1b4c 1 1218 1 . . . parsed_1b4c 1 1219 1 . . . parsed_1b4c 1 1220 1 . . . parsed_1b4c 1 1221 1 . . . parsed_1b4c 1 1222 1 . . . parsed_1b4c 1 1223 1 . . . parsed_1b4c 1 1224 1 . . . parsed_1b4c 1 1225 1 . . . parsed_1b4c 1 1226 1 . . . parsed_1b4c 1 1227 1 . . . parsed_1b4c 1 1228 1 . . . parsed_1b4c 1 1229 1 . . . parsed_1b4c 1 1230 1 . . . parsed_1b4c 1 1231 1 . . . parsed_1b4c 1 1232 1 . . . parsed_1b4c 1 1233 1 . . . parsed_1b4c 1 1234 1 . . . parsed_1b4c 1 1235 1 . . . parsed_1b4c 1 1236 1 . . . parsed_1b4c 1 1237 1 . . . parsed_1b4c 1 1238 1 . . . parsed_1b4c 1 1239 1 . . . parsed_1b4c 1 1240 1 . . . parsed_1b4c 1 1241 1 . . . parsed_1b4c 1 1242 1 . . . parsed_1b4c 1 1243 1 . . . parsed_1b4c 1 1244 1 . . . parsed_1b4c 1 1245 1 . . . parsed_1b4c 1 1246 1 . . . parsed_1b4c 1 1247 1 . . . parsed_1b4c 1 1248 1 . . . parsed_1b4c 1 1249 1 . . . parsed_1b4c 1 1250 1 . . . parsed_1b4c 1 1251 1 . . . parsed_1b4c 1 1252 1 . . . parsed_1b4c 1 1253 1 . . . parsed_1b4c 1 1254 1 . . . parsed_1b4c 1 1255 1 . . . parsed_1b4c 1 1256 1 . . . parsed_1b4c 1 1257 1 . . . parsed_1b4c 1 1258 1 . . . parsed_1b4c 1 1259 1 . . . parsed_1b4c 1 1260 1 . . . parsed_1b4c 1 1261 1 . . . parsed_1b4c 1 1262 1 . . . parsed_1b4c 1 1263 1 . . . parsed_1b4c 1 1264 1 . . . parsed_1b4c 1 1265 1 . . . parsed_1b4c 1 1266 1 . . . parsed_1b4c 1 1267 1 . . . parsed_1b4c 1 1268 1 . . . parsed_1b4c 1 1269 1 . . . parsed_1b4c 1 1270 1 . . . parsed_1b4c 1 1271 1 . . . parsed_1b4c 1 1272 1 . . . parsed_1b4c 1 1273 1 . . . parsed_1b4c 1 1274 1 . . . parsed_1b4c 1 1275 1 . . . parsed_1b4c 1 1276 1 . . . parsed_1b4c 1 1277 1 . . . parsed_1b4c 1 1278 1 . . . parsed_1b4c 1 1279 1 . . . parsed_1b4c 1 1280 1 . . . parsed_1b4c 1 1281 1 . . . parsed_1b4c 1 1282 1 . . . parsed_1b4c 1 1283 1 . . . parsed_1b4c 1 1284 1 . . . parsed_1b4c 1 1285 1 . . . parsed_1b4c 1 1286 1 . . . parsed_1b4c 1 1287 1 . . . parsed_1b4c 1 1288 1 . . . parsed_1b4c 1 1289 1 . . . parsed_1b4c 1 1290 1 . . . parsed_1b4c 1 1291 1 . . . parsed_1b4c 1 1292 1 . . . parsed_1b4c 1 1293 1 . . . parsed_1b4c 1 1294 1 . . . parsed_1b4c 1 1295 1 . . . parsed_1b4c 1 1296 1 . . . parsed_1b4c 1 1297 1 . . . parsed_1b4c 1 1298 1 . . . parsed_1b4c 1 1299 1 . . . parsed_1b4c 1 1300 1 . . . parsed_1b4c 1 1301 1 . . . parsed_1b4c 1 1302 1 . . . parsed_1b4c 1 1303 1 . . . parsed_1b4c 1 1304 1 . . . parsed_1b4c 1 1305 1 . . . parsed_1b4c 1 1306 1 . . . parsed_1b4c 1 1307 1 . . . parsed_1b4c 1 1308 1 . . . parsed_1b4c 1 1309 1 . . . parsed_1b4c 1 1310 1 . . . parsed_1b4c 1 1311 1 . . . parsed_1b4c 1 1312 1 . . . parsed_1b4c 1 1313 1 . . . parsed_1b4c 1 1314 1 . . . parsed_1b4c 1 1315 1 . . . parsed_1b4c 1 1316 1 . . . parsed_1b4c 1 1317 1 . . . parsed_1b4c 1 1318 1 . . . parsed_1b4c 1 1319 1 . . . parsed_1b4c 1 1320 1 . . . parsed_1b4c 1 1321 1 . . . parsed_1b4c 1 1322 1 . . . parsed_1b4c 1 1323 1 . . . parsed_1b4c 1 1324 1 . . . parsed_1b4c 1 1325 1 . . . parsed_1b4c 1 1326 1 . . . parsed_1b4c 1 1327 1 . . . parsed_1b4c 1 1328 1 . . . parsed_1b4c 1 1329 1 . . . parsed_1b4c 1 1330 1 . . . parsed_1b4c 1 1331 1 . . . parsed_1b4c 1 1332 1 . . . parsed_1b4c 1 1333 1 . . . parsed_1b4c 1 1334 1 . . . parsed_1b4c 1 1335 1 . . . parsed_1b4c 1 1336 1 . . . parsed_1b4c 1 1337 1 . . . parsed_1b4c 1 1338 1 . . . parsed_1b4c 1 1339 1 . . . parsed_1b4c 1 1340 1 . . . parsed_1b4c 1 1341 1 . . . parsed_1b4c 1 1342 1 . . . parsed_1b4c 1 1343 1 . . . parsed_1b4c 1 1344 1 . . . parsed_1b4c 1 1345 1 . . . parsed_1b4c 1 1346 1 . . . parsed_1b4c 1 1347 1 . . . parsed_1b4c 1 1348 1 . . . parsed_1b4c 1 1349 1 . . . parsed_1b4c 1 1350 1 . . . parsed_1b4c 1 1351 1 . . . parsed_1b4c 1 1352 1 . . . parsed_1b4c 1 1353 1 . . . parsed_1b4c 1 1354 1 . . . parsed_1b4c 1 1355 1 . . . parsed_1b4c 1 1356 1 . . . parsed_1b4c 1 1357 1 . . . parsed_1b4c 1 1358 1 . . . parsed_1b4c 1 1359 1 . . . parsed_1b4c 1 1360 1 . . . parsed_1b4c 1 1361 1 . . . parsed_1b4c 1 1362 1 . . . parsed_1b4c 1 1363 1 . . . parsed_1b4c 1 1364 1 . . . parsed_1b4c 1 1365 1 . . . parsed_1b4c 1 1366 1 . . . parsed_1b4c 1 1367 1 . . . parsed_1b4c 1 1368 1 . . . parsed_1b4c 1 1369 1 . . . parsed_1b4c 1 1370 1 . . . parsed_1b4c 1 1371 1 . . . parsed_1b4c 1 1372 1 . . . parsed_1b4c 1 1373 1 . . . parsed_1b4c 1 1374 1 . . . parsed_1b4c 1 1375 1 . . . parsed_1b4c 1 1376 1 . . . parsed_1b4c 1 1377 1 . . . parsed_1b4c 1 1378 1 . . . parsed_1b4c 1 1379 1 . . . parsed_1b4c 1 1380 1 . . . parsed_1b4c 1 1381 1 . . . parsed_1b4c 1 1382 1 . . . parsed_1b4c 1 1383 1 . . . parsed_1b4c 1 1384 1 . . . parsed_1b4c 1 1385 1 . . . parsed_1b4c 1 1386 1 . . . parsed_1b4c 1 1387 1 . . . parsed_1b4c 1 1388 1 . . . parsed_1b4c 1 1389 1 . . . parsed_1b4c 1 1390 1 . . . parsed_1b4c 1 1391 1 . . . parsed_1b4c 1 1392 1 . . . parsed_1b4c 1 1393 1 . . . parsed_1b4c 1 1394 1 . . . parsed_1b4c 1 1395 1 . . . parsed_1b4c 1 1396 1 . . . parsed_1b4c 1 1397 1 . . . parsed_1b4c 1 1398 1 . . . parsed_1b4c 1 1399 1 . . . parsed_1b4c 1 1400 1 . . . parsed_1b4c 1 1401 1 . . . parsed_1b4c 1 1402 1 . . . parsed_1b4c 1 1403 1 . . . parsed_1b4c 1 1404 1 . . . parsed_1b4c 1 1405 1 . . . parsed_1b4c 1 1406 1 . . . parsed_1b4c 1 1407 1 . . . parsed_1b4c 1 1408 1 . . . parsed_1b4c 1 1409 1 . . . parsed_1b4c 1 1410 1 . . . parsed_1b4c 1 1411 1 . . . parsed_1b4c 1 1412 1 . . . parsed_1b4c 1 1413 1 . . . parsed_1b4c 1 1414 1 . . . parsed_1b4c 1 1415 1 . . . parsed_1b4c 1 1416 1 . . . parsed_1b4c 1 1417 1 . . . parsed_1b4c 1 1418 1 . . . parsed_1b4c 1 1419 1 . . . parsed_1b4c 1 1420 1 . . . parsed_1b4c 1 1421 1 . . . parsed_1b4c 1 1422 1 . . . parsed_1b4c 1 1423 1 . . . parsed_1b4c 1 1424 1 . . . parsed_1b4c 1 1425 1 . . . parsed_1b4c 1 1426 1 . . . parsed_1b4c 1 1427 1 . . . parsed_1b4c 1 1428 1 . . . parsed_1b4c 1 1429 1 . . . parsed_1b4c 1 1430 1 . . . parsed_1b4c 1 1431 1 . . . parsed_1b4c 1 1432 1 . . . parsed_1b4c 1 1433 1 . . . parsed_1b4c 1 1434 1 . . . parsed_1b4c 1 1435 1 . . . parsed_1b4c 1 1436 1 . . . parsed_1b4c 1 1437 1 . . . parsed_1b4c 1 1438 1 . . . parsed_1b4c 1 1439 1 . . . parsed_1b4c 1 1440 1 . . . parsed_1b4c 1 1441 1 . . . parsed_1b4c 1 1442 1 . . . parsed_1b4c 1 1443 1 . . . parsed_1b4c 1 1444 1 . . . parsed_1b4c 1 1445 1 . . . parsed_1b4c 1 1446 1 . . . parsed_1b4c 1 1447 1 . . . parsed_1b4c 1 1448 1 . . . parsed_1b4c 1 1449 1 . . . parsed_1b4c 1 1450 1 . . . parsed_1b4c 1 1451 1 . . . parsed_1b4c 1 1452 1 . . . parsed_1b4c 1 1453 1 . . . parsed_1b4c 1 1454 1 . . . parsed_1b4c 1 1455 1 . . . parsed_1b4c 1 1456 1 . . . parsed_1b4c 1 1457 1 . . . parsed_1b4c 1 1458 1 . . . parsed_1b4c 1 1459 1 . . . parsed_1b4c 1 1460 1 . . . parsed_1b4c 1 1461 1 . . . parsed_1b4c 1 1462 1 . . . parsed_1b4c 1 1463 1 . . . parsed_1b4c 1 1464 1 . . . parsed_1b4c 1 1465 1 . . . parsed_1b4c 1 1466 1 . . . parsed_1b4c 1 1467 1 . . . parsed_1b4c 1 1468 1 . . . parsed_1b4c 1 1469 1 . . . parsed_1b4c 1 1470 1 . . . parsed_1b4c 1 1471 1 . . . parsed_1b4c 1 1472 1 . . . parsed_1b4c 1 1473 1 . . . parsed_1b4c 1 1474 1 . . . parsed_1b4c 1 1475 1 . . . parsed_1b4c 1 1476 1 . . . parsed_1b4c 1 1477 1 . . . parsed_1b4c 1 1478 1 . . . parsed_1b4c 1 1479 1 . . . parsed_1b4c 1 1480 1 . . . parsed_1b4c 1 1481 1 . . . parsed_1b4c 1 1482 1 . . . parsed_1b4c 1 1483 1 . . . parsed_1b4c 1 1484 1 . . . parsed_1b4c 1 1485 1 . . . parsed_1b4c 1 1486 1 . . . parsed_1b4c 1 1487 1 . . . parsed_1b4c 1 1488 1 . . . parsed_1b4c 1 1489 1 . . . parsed_1b4c 1 1490 1 . . . parsed_1b4c 1 1491 1 . . . parsed_1b4c 1 1492 1 . . . parsed_1b4c 1 1493 1 . . . parsed_1b4c 1 1494 1 . . . parsed_1b4c 1 1495 1 . . . parsed_1b4c 1 1496 1 . . . parsed_1b4c 1 1497 1 . . . parsed_1b4c 1 1498 1 . . . parsed_1b4c 1 1499 1 . . . parsed_1b4c 1 1500 1 . . . parsed_1b4c 1 1501 1 . . . parsed_1b4c 1 1502 1 . . . parsed_1b4c 1 1503 1 . . . parsed_1b4c 1 1504 1 . . . parsed_1b4c 1 1505 1 . . . parsed_1b4c 1 1506 1 . . . parsed_1b4c 1 1507 1 . . . parsed_1b4c 1 1508 1 . . . parsed_1b4c 1 1509 1 . . . parsed_1b4c 1 1510 1 . . . parsed_1b4c 1 1511 1 . . . parsed_1b4c 1 1512 1 . . . parsed_1b4c 1 1513 1 . . . parsed_1b4c 1 1514 1 . . . parsed_1b4c 1 1515 1 . . . parsed_1b4c 1 1516 1 . . . parsed_1b4c 1 1517 1 . . . parsed_1b4c 1 1518 1 . . . parsed_1b4c 1 1519 1 . . . parsed_1b4c 1 1520 1 . . . parsed_1b4c 1 1521 1 . . . parsed_1b4c 1 1522 1 . . . parsed_1b4c 1 1523 1 . . . parsed_1b4c 1 1524 1 . . . parsed_1b4c 1 1525 1 . . . parsed_1b4c 1 1526 1 . . . parsed_1b4c 1 1527 1 . . . parsed_1b4c 1 1528 1 . . . parsed_1b4c 1 1529 1 . . . parsed_1b4c 1 1530 1 . . . parsed_1b4c 1 1531 1 . . . parsed_1b4c 1 1532 1 . . . parsed_1b4c 1 1533 1 . . . parsed_1b4c 1 1534 1 . . . parsed_1b4c 1 1535 1 . . . parsed_1b4c 1 1536 1 . . . parsed_1b4c 1 1537 1 . . . parsed_1b4c 1 1538 1 . . . parsed_1b4c 1 1539 1 . . . parsed_1b4c 1 1540 1 . . . parsed_1b4c 1 1541 1 . . . parsed_1b4c 1 1542 1 . . . parsed_1b4c 1 1543 1 . . . parsed_1b4c 1 1544 1 . . . parsed_1b4c 1 1545 1 . . . parsed_1b4c 1 1546 1 . . . parsed_1b4c 1 1547 1 . . . parsed_1b4c 1 1548 1 . . . parsed_1b4c 1 1549 1 . . . parsed_1b4c 1 1550 1 . . . parsed_1b4c 1 1551 1 . . . parsed_1b4c 1 1552 1 . . . parsed_1b4c 1 1553 1 . . . parsed_1b4c 1 1554 1 . . . parsed_1b4c 1 1555 1 . . . parsed_1b4c 1 1556 1 . . . parsed_1b4c 1 1557 1 . . . parsed_1b4c 1 1558 1 . . . parsed_1b4c 1 1559 1 . . . parsed_1b4c 1 1560 1 . . . parsed_1b4c 1 1561 1 . . . parsed_1b4c 1 1562 1 . . . parsed_1b4c 1 1563 1 . . . parsed_1b4c 1 1564 1 . . . parsed_1b4c 1 1565 1 . . . parsed_1b4c 1 1566 1 . . . parsed_1b4c 1 1567 1 . . . parsed_1b4c 1 1568 1 . . . parsed_1b4c 1 1569 1 . . . parsed_1b4c 1 1570 1 . . . parsed_1b4c 1 1571 1 . . . parsed_1b4c 1 1572 1 . . . parsed_1b4c 1 1573 1 . . . parsed_1b4c 1 1574 1 . . . parsed_1b4c 1 1575 1 . . . parsed_1b4c 1 1576 1 . . . parsed_1b4c 1 1577 1 . . . parsed_1b4c 1 1578 1 . . . parsed_1b4c 1 1579 1 . . . parsed_1b4c 1 1580 1 . . . parsed_1b4c 1 1581 1 . . . parsed_1b4c 1 1582 1 . . . parsed_1b4c 1 1583 1 . . . parsed_1b4c 1 1584 1 . . . parsed_1b4c 1 1585 1 . . . parsed_1b4c 1 1586 1 . . . parsed_1b4c 1 1587 1 . . . parsed_1b4c 1 1588 1 . . . parsed_1b4c 1 1589 1 . . . parsed_1b4c 1 1590 1 . . . parsed_1b4c 1 1591 1 . . . parsed_1b4c 1 1592 1 . . . parsed_1b4c 1 1593 1 . . . parsed_1b4c 1 1594 1 . . . parsed_1b4c 1 1595 1 . . . parsed_1b4c 1 1596 1 . . . parsed_1b4c 1 1597 1 . . . parsed_1b4c 1 1598 1 . . . parsed_1b4c 1 1599 1 . . . parsed_1b4c 1 1600 1 . . . parsed_1b4c 1 1601 1 . . . parsed_1b4c 1 1602 1 . . . parsed_1b4c 1 1603 1 . . . parsed_1b4c 1 1604 1 . . . parsed_1b4c 1 1605 1 . . . parsed_1b4c 1 1606 1 . . . parsed_1b4c 1 1607 1 . . . parsed_1b4c 1 1608 1 . . . parsed_1b4c 1 1609 1 . . . parsed_1b4c 1 1610 1 . . . parsed_1b4c 1 1611 1 . . . parsed_1b4c 1 1612 1 . . . parsed_1b4c 1 1613 1 . . . parsed_1b4c 1 1614 1 . . . parsed_1b4c 1 1615 1 . . . parsed_1b4c 1 1616 1 . . . parsed_1b4c 1 1617 1 . . . parsed_1b4c 1 1618 1 . . . parsed_1b4c 1 1619 1 . . . parsed_1b4c 1 1620 1 . . . parsed_1b4c 1 1621 1 . . . parsed_1b4c 1 1622 1 . . . parsed_1b4c 1 1623 1 . . . parsed_1b4c 1 1624 1 . . . parsed_1b4c 1 1625 1 . . . parsed_1b4c 1 1626 1 . . . parsed_1b4c 1 1627 1 . . . parsed_1b4c 1 1628 1 . . . parsed_1b4c 1 1629 1 . . . parsed_1b4c 1 1630 1 . . . parsed_1b4c 1 1631 1 . . . parsed_1b4c 1 1632 1 . . . parsed_1b4c 1 1633 1 . . . parsed_1b4c 1 1634 1 . . . parsed_1b4c 1 1635 1 . . . parsed_1b4c 1 1636 1 . . . parsed_1b4c 1 1637 1 . . . parsed_1b4c 1 1638 1 . . . parsed_1b4c 1 1639 1 . . . parsed_1b4c 1 1640 1 . . . parsed_1b4c 1 1641 1 . . . parsed_1b4c 1 1642 1 . . . parsed_1b4c 1 1643 1 . . . parsed_1b4c 1 1644 1 . . . parsed_1b4c 1 1645 1 . . . parsed_1b4c 1 1646 1 . . . parsed_1b4c 1 1647 1 . . . parsed_1b4c 1 1648 1 . . . parsed_1b4c 1 1649 1 . . . parsed_1b4c 1 1650 1 . . . parsed_1b4c 1 1651 1 . . . parsed_1b4c 1 1652 1 . . . parsed_1b4c 1 1653 1 . . . parsed_1b4c 1 1654 1 . . . parsed_1b4c 1 1655 1 . . . parsed_1b4c 1 1656 1 . . . parsed_1b4c 1 1657 1 . . . parsed_1b4c 1 1658 1 . . . parsed_1b4c 1 1659 1 . . . parsed_1b4c 1 1660 1 . . . parsed_1b4c 1 1661 1 . . . parsed_1b4c 1 1662 1 . . . parsed_1b4c 1 1663 1 . . . parsed_1b4c 1 1664 1 . . . parsed_1b4c 1 1665 1 . . . parsed_1b4c 1 1666 1 . . . parsed_1b4c 1 1667 1 . . . parsed_1b4c 1 1668 1 . . . parsed_1b4c 1 1669 1 . . . parsed_1b4c 1 1670 1 . . . parsed_1b4c 1 1671 1 . . . parsed_1b4c 1 1672 1 . . . parsed_1b4c 1 1673 1 . . . parsed_1b4c 1 1674 1 . . . parsed_1b4c 1 1675 1 . . . parsed_1b4c 1 1676 1 . . . parsed_1b4c 1 1677 1 . . . parsed_1b4c 1 1678 1 . . . parsed_1b4c 1 1679 1 . . . parsed_1b4c 1 1680 1 . . . parsed_1b4c 1 1681 1 . . . parsed_1b4c 1 1682 1 . . . parsed_1b4c 1 1683 1 . . . parsed_1b4c 1 1684 1 . . . parsed_1b4c 1 1685 1 . . . parsed_1b4c 1 1686 1 . . . parsed_1b4c 1 1687 1 . . . parsed_1b4c 1 1688 1 . . . parsed_1b4c 1 1689 1 . . . parsed_1b4c 1 1690 1 . . . parsed_1b4c 1 1691 1 . . . parsed_1b4c 1 1692 1 . . . parsed_1b4c 1 1693 1 . . . parsed_1b4c 1 1694 1 . . . parsed_1b4c 1 1695 1 . . . parsed_1b4c 1 1696 1 . . . parsed_1b4c 1 1697 1 . . . parsed_1b4c 1 1698 1 . . . parsed_1b4c 1 1699 1 . . . parsed_1b4c 1 1700 1 . . . parsed_1b4c 1 1701 1 . . . parsed_1b4c 1 1702 1 . . . parsed_1b4c 1 1703 1 . . . parsed_1b4c 1 1704 1 . . . parsed_1b4c 1 1705 1 . . . parsed_1b4c 1 1706 1 . . . parsed_1b4c 1 1707 1 . . . parsed_1b4c 1 1708 1 . . . parsed_1b4c 1 1709 1 . . . parsed_1b4c 1 1710 1 . . . parsed_1b4c 1 1711 1 . . . parsed_1b4c 1 1712 1 . . . parsed_1b4c 1 1713 1 . . . parsed_1b4c 1 1714 1 . . . parsed_1b4c 1 1715 1 . . . parsed_1b4c 1 1716 1 . . . parsed_1b4c 1 1717 1 . . . parsed_1b4c 1 1718 1 . . . parsed_1b4c 1 1719 1 . . . parsed_1b4c 1 1720 1 . . . parsed_1b4c 1 1721 1 . . . parsed_1b4c 1 1722 1 . . . parsed_1b4c 1 1723 1 . . . parsed_1b4c 1 1724 1 . . . parsed_1b4c 1 1725 1 . . . parsed_1b4c 1 1726 1 . . . parsed_1b4c 1 1727 1 . . . parsed_1b4c 1 1728 1 . . . parsed_1b4c 1 1729 1 . . . parsed_1b4c 1 1730 1 . . . parsed_1b4c 1 1731 1 . . . parsed_1b4c 1 1732 1 . . . parsed_1b4c 1 1733 1 . . . parsed_1b4c 1 1734 1 . . . parsed_1b4c 1 1735 1 . . . parsed_1b4c 1 1736 1 . . . parsed_1b4c 1 1737 1 . . . parsed_1b4c 1 1738 1 . . . parsed_1b4c 1 1739 1 . . . parsed_1b4c 1 1740 1 . . . parsed_1b4c 1 1741 1 . . . parsed_1b4c 1 1742 1 . . . parsed_1b4c 1 1743 1 . . . parsed_1b4c 1 1744 1 . . . parsed_1b4c 1 1745 1 . . . parsed_1b4c 1 1746 1 . . . parsed_1b4c 1 1747 1 . . . parsed_1b4c 1 1748 1 . . . parsed_1b4c 1 1749 1 . . . parsed_1b4c 1 1750 1 . . . parsed_1b4c 1 1751 1 . . . parsed_1b4c 1 1752 1 . . . parsed_1b4c 1 1753 1 . . . parsed_1b4c 1 1754 1 . . . parsed_1b4c 1 1755 1 . . . parsed_1b4c 1 1756 1 . . . parsed_1b4c 1 1757 1 . . . parsed_1b4c 1 1758 1 . . . parsed_1b4c 1 1759 1 . . . parsed_1b4c 1 1760 1 . . . parsed_1b4c 1 1761 1 . . . parsed_1b4c 1 1762 1 . . . parsed_1b4c 1 1763 1 . . . parsed_1b4c 1 1764 1 . . . parsed_1b4c 1 1765 1 . . . parsed_1b4c 1 1766 1 . . . parsed_1b4c 1 1767 1 . . . parsed_1b4c 1 1768 1 . . . parsed_1b4c 1 1769 1 . . . parsed_1b4c 1 1770 1 . . . parsed_1b4c 1 1771 1 . . . parsed_1b4c 1 1772 1 . . . parsed_1b4c 1 1773 1 . . . parsed_1b4c 1 1774 1 . . . parsed_1b4c 1 1775 1 . . . parsed_1b4c 1 1776 1 . . . parsed_1b4c 1 1777 1 . . . parsed_1b4c 1 1778 1 . . . parsed_1b4c 1 1779 1 . . . parsed_1b4c 1 1780 1 . . . parsed_1b4c 1 stop_ loop_ _Dist_constraint.Tree_node_member_constraint_ID _Dist_constraint.Tree_node_member_node_ID _Dist_constraint.Constraint_tree_node_member_ID _Dist_constraint.Assembly_atom_ID _Dist_constraint.Entity_assembly_ID _Dist_constraint.Entity_ID _Dist_constraint.Comp_index_ID _Dist_constraint.Seq_ID _Dist_constraint.Comp_ID _Dist_constraint.Atom_ID _Dist_constraint.Resonance_ID _Dist_constraint.Auth_asym_ID _Dist_constraint.Auth_seq_ID _Dist_constraint.Auth_comp_ID _Dist_constraint.Auth_atom_ID _Dist_constraint.Entry_ID _Dist_constraint.Distance_constraint_list_ID 1 1 1 . . . . . . . . sbm1 2 . ha parsed_1b4c 1 1 1 2 . . . . . . . . sbm1 2 . hn parsed_1b4c 1 2 1 1 . . . . . . . . sbm2 2 . ha parsed_1b4c 1 2 1 2 . . . . . . . . sbm2 2 . hn parsed_1b4c 1 3 1 1 . . . . . . . . sbm1 2 . hb* parsed_1b4c 1 3 1 2 . . . . . . . . sbm1 2 . hn parsed_1b4c 1 4 1 1 . . . . . . . . sbm2 2 . hb* parsed_1b4c 1 4 1 2 . . . . . . . . sbm2 2 . hn parsed_1b4c 1 5 1 1 . . . . . . . . sbm1 3 . ha parsed_1b4c 1 5 1 2 . . . . . . . . sbm1 3 . hn parsed_1b4c 1 6 1 1 . . . . . . . . sbm2 3 . ha parsed_1b4c 1 6 1 2 . . . . . . . . sbm2 3 . hn parsed_1b4c 1 7 1 1 . . . . . . . . sbm1 3 . hb* parsed_1b4c 1 7 1 2 . . . . . . . . sbm1 3 . hn parsed_1b4c 1 8 1 1 . . . . . . . . sbm2 3 . hb* parsed_1b4c 1 8 1 2 . . . . . . . . sbm2 3 . hn parsed_1b4c 1 9 1 1 . . . . . . . . sbm1 4 . hb* parsed_1b4c 1 9 1 2 . . . . . . . . sbm1 4 . hn parsed_1b4c 1 10 1 1 . . . . . . . . sbm2 4 . hb* parsed_1b4c 1 10 1 2 . . . . . . . . sbm2 4 . hn parsed_1b4c 1 11 1 1 . . . . . . . . sbm1 5 . ha parsed_1b4c 1 11 1 2 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 12 1 1 . . . . . . . . sbm2 5 . ha parsed_1b4c 1 12 1 2 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 13 1 1 . . . . . . . . sbm1 5 . hb* parsed_1b4c 1 13 1 2 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 14 1 1 . . . . . . . . sbm2 5 . hb* parsed_1b4c 1 14 1 2 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 15 1 1 . . . . . . . . sbm1 5 . hd* parsed_1b4c 1 15 1 2 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 16 1 1 . . . . . . . . sbm2 5 . hd* parsed_1b4c 1 16 1 2 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 17 1 1 . . . . . . . . sbm1 6 . hb* parsed_1b4c 1 17 1 2 . . . . . . . . sbm1 6 . hn parsed_1b4c 1 18 1 1 . . . . . . . . sbm2 6 . hb* parsed_1b4c 1 18 1 2 . . . . . . . . sbm2 6 . hn parsed_1b4c 1 19 1 1 . . . . . . . . sbm1 7 . ha parsed_1b4c 1 19 1 2 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 20 1 1 . . . . . . . . sbm2 7 . ha parsed_1b4c 1 20 1 2 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 21 1 1 . . . . . . . . sbm1 7 . hb* parsed_1b4c 1 21 1 2 . . . . . . . . sbm1 7 . hn parsed_1b4c 1 22 1 1 . . . . . . . . sbm2 7 . hb* parsed_1b4c 1 22 1 2 . . . . . . . . sbm2 7 . hn parsed_1b4c 1 23 1 1 . . . . . . . . sbm1 8 . hb parsed_1b4c 1 23 1 2 . . . . . . . . sbm1 8 . hn parsed_1b4c 1 24 1 1 . . . . . . . . sbm2 8 . hb parsed_1b4c 1 24 1 2 . . . . . . . . sbm2 8 . hn parsed_1b4c 1 25 1 1 . . . . . . . . sbm1 9 . hb* parsed_1b4c 1 25 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 26 1 1 . . . . . . . . sbm2 9 . hb* parsed_1b4c 1 26 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 27 1 1 . . . . . . . . sbm1 10 . hb* parsed_1b4c 1 27 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 28 1 1 . . . . . . . . sbm2 10 . hb* parsed_1b4c 1 28 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 29 1 1 . . . . . . . . sbm1 11 . hb parsed_1b4c 1 29 1 2 . . . . . . . . sbm1 11 . hn parsed_1b4c 1 30 1 1 . . . . . . . . sbm2 11 . hb parsed_1b4c 1 30 1 2 . . . . . . . . sbm2 11 . hn parsed_1b4c 1 31 1 1 . . . . . . . . sbm1 12 . hb* parsed_1b4c 1 31 1 2 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 32 1 1 . . . . . . . . sbm2 12 . hb* parsed_1b4c 1 32 1 2 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 33 1 1 . . . . . . . . sbm1 13 . ha parsed_1b4c 1 33 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 34 1 1 . . . . . . . . sbm2 13 . ha parsed_1b4c 1 34 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 35 1 1 . . . . . . . . sbm1 13 . hb parsed_1b4c 1 35 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 36 1 1 . . . . . . . . sbm2 13 . hb parsed_1b4c 1 36 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 37 1 1 . . . . . . . . sbm1 14 . ha parsed_1b4c 1 37 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 38 1 1 . . . . . . . . sbm2 14 . ha parsed_1b4c 1 38 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 39 1 1 . . . . . . . . sbm1 14 . hb* parsed_1b4c 1 39 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 40 1 1 . . . . . . . . sbm2 14 . hb* parsed_1b4c 1 40 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 41 1 1 . . . . . . . . sbm1 14 . hd* parsed_1b4c 1 41 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 42 1 1 . . . . . . . . sbm2 14 . hd* parsed_1b4c 1 42 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 43 1 1 . . . . . . . . sbm1 15 . hb* parsed_1b4c 1 43 1 2 . . . . . . . . sbm1 15 . hn parsed_1b4c 1 44 1 1 . . . . . . . . sbm2 15 . hb* parsed_1b4c 1 44 1 2 . . . . . . . . sbm2 15 . hn parsed_1b4c 1 45 1 1 . . . . . . . . sbm1 16 . ha parsed_1b4c 1 45 1 2 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 46 1 1 . . . . . . . . sbm2 16 . ha parsed_1b4c 1 46 1 2 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 47 1 1 . . . . . . . . sbm1 16 . hb* parsed_1b4c 1 47 1 2 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 48 1 1 . . . . . . . . sbm2 16 . hb* parsed_1b4c 1 48 1 2 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 49 1 1 . . . . . . . . sbm1 17 . ha parsed_1b4c 1 49 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 50 1 1 . . . . . . . . sbm2 17 . ha parsed_1b4c 1 50 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 51 1 1 . . . . . . . . sbm1 17 . hb* parsed_1b4c 1 51 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 52 1 1 . . . . . . . . sbm2 17 . hb* parsed_1b4c 1 52 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 53 1 1 . . . . . . . . sbm1 19 . ha* parsed_1b4c 1 53 1 2 . . . . . . . . sbm1 19 . hn parsed_1b4c 1 54 1 1 . . . . . . . . sbm2 19 . ha* parsed_1b4c 1 54 1 2 . . . . . . . . sbm2 19 . hn parsed_1b4c 1 55 1 1 . . . . . . . . sbm1 20 . ha parsed_1b4c 1 55 1 2 . . . . . . . . sbm1 20 . hn parsed_1b4c 1 56 1 1 . . . . . . . . sbm2 20 . ha parsed_1b4c 1 56 1 2 . . . . . . . . sbm2 20 . hn parsed_1b4c 1 57 1 1 . . . . . . . . sbm1 20 . hb* parsed_1b4c 1 57 1 2 . . . . . . . . sbm1 20 . hn parsed_1b4c 1 58 1 1 . . . . . . . . sbm2 20 . hb* parsed_1b4c 1 58 1 2 . . . . . . . . sbm2 20 . hn parsed_1b4c 1 59 1 1 . . . . . . . . sbm1 21 . hb* parsed_1b4c 1 59 1 2 . . . . . . . . sbm1 21 . hn parsed_1b4c 1 60 1 1 . . . . . . . . sbm2 21 . hb* parsed_1b4c 1 60 1 2 . . . . . . . . sbm2 21 . hn parsed_1b4c 1 61 1 1 . . . . . . . . sbm1 22 . ha* parsed_1b4c 1 61 1 2 . . . . . . . . sbm1 22 . hn parsed_1b4c 1 62 1 1 . . . . . . . . sbm2 22 . ha* parsed_1b4c 1 62 1 2 . . . . . . . . sbm2 22 . hn parsed_1b4c 1 63 1 1 . . . . . . . . sbm1 23 . ha parsed_1b4c 1 63 1 2 . . . . . . . . sbm1 23 . hn parsed_1b4c 1 64 1 1 . . . . . . . . sbm2 23 . ha parsed_1b4c 1 64 1 2 . . . . . . . . sbm2 23 . hn parsed_1b4c 1 65 1 1 . . . . . . . . sbm1 23 . hb* parsed_1b4c 1 65 1 2 . . . . . . . . sbm1 23 . hn parsed_1b4c 1 66 1 1 . . . . . . . . sbm2 23 . hb* parsed_1b4c 1 66 1 2 . . . . . . . . sbm2 23 . hn parsed_1b4c 1 67 1 1 . . . . . . . . sbm1 24 . hb* parsed_1b4c 1 67 1 2 . . . . . . . . sbm1 24 . hn parsed_1b4c 1 68 1 1 . . . . . . . . sbm2 24 . hb* parsed_1b4c 1 68 1 2 . . . . . . . . sbm2 24 . hn parsed_1b4c 1 69 1 1 . . . . . . . . sbm1 25 . hb* parsed_1b4c 1 69 1 2 . . . . . . . . sbm1 25 . hn parsed_1b4c 1 70 1 1 . . . . . . . . sbm2 25 . hb* parsed_1b4c 1 70 1 2 . . . . . . . . sbm2 25 . hn parsed_1b4c 1 71 1 1 . . . . . . . . sbm1 26 . ha parsed_1b4c 1 71 1 2 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 72 1 1 . . . . . . . . sbm2 26 . ha parsed_1b4c 1 72 1 2 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 73 1 1 . . . . . . . . sbm1 26 . hb* parsed_1b4c 1 73 1 2 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 74 1 1 . . . . . . . . sbm2 26 . hb* parsed_1b4c 1 74 1 2 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 75 1 1 . . . . . . . . sbm1 27 . ha parsed_1b4c 1 75 1 2 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 76 1 1 . . . . . . . . sbm2 27 . ha parsed_1b4c 1 76 1 2 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 77 1 1 . . . . . . . . sbm1 27 . hb* parsed_1b4c 1 77 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 78 1 1 . . . . . . . . sbm2 27 . hb* parsed_1b4c 1 78 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 79 1 1 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 79 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 80 1 1 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 80 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 81 1 1 . . . . . . . . sbm1 28 . hb* parsed_1b4c 1 81 1 2 . . . . . . . . sbm1 28 . hn parsed_1b4c 1 82 1 1 . . . . . . . . sbm2 28 . hb* parsed_1b4c 1 82 1 2 . . . . . . . . sbm2 28 . hn parsed_1b4c 1 83 1 1 . . . . . . . . sbm1 29 . ha parsed_1b4c 1 83 1 2 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 84 1 1 . . . . . . . . sbm2 29 . ha parsed_1b4c 1 84 1 2 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 85 1 1 . . . . . . . . sbm1 29 . hb* parsed_1b4c 1 85 1 2 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 86 1 1 . . . . . . . . sbm2 29 . hb* parsed_1b4c 1 86 1 2 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 87 1 1 . . . . . . . . sbm1 30 . ha parsed_1b4c 1 87 1 2 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 88 1 1 . . . . . . . . sbm2 30 . ha parsed_1b4c 1 88 1 2 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 89 1 1 . . . . . . . . sbm1 30 . hb* parsed_1b4c 1 89 1 2 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 90 1 1 . . . . . . . . sbm2 30 . hb* parsed_1b4c 1 90 1 2 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 91 1 1 . . . . . . . . sbm1 31 . hb* parsed_1b4c 1 91 1 2 . . . . . . . . sbm1 31 . hn parsed_1b4c 1 92 1 1 . . . . . . . . sbm2 31 . hb* parsed_1b4c 1 92 1 2 . . . . . . . . sbm2 31 . hn parsed_1b4c 1 93 1 1 . . . . . . . . sbm1 32 . ha parsed_1b4c 1 93 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 94 1 1 . . . . . . . . sbm2 32 . ha parsed_1b4c 1 94 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 95 1 1 . . . . . . . . sbm1 32 . ha parsed_1b4c 1 95 1 2 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 96 1 1 . . . . . . . . sbm2 32 . ha parsed_1b4c 1 96 1 2 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 97 1 1 . . . . . . . . sbm1 32 . hb* parsed_1b4c 1 97 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 98 1 1 . . . . . . . . sbm2 32 . hb* parsed_1b4c 1 98 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 99 1 1 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 99 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 100 1 1 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 100 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 101 1 1 . . . . . . . . sbm1 33 . ha parsed_1b4c 1 101 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 102 1 1 . . . . . . . . sbm2 33 . ha parsed_1b4c 1 102 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 103 1 1 . . . . . . . . sbm1 33 . hb* parsed_1b4c 1 103 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 104 1 1 . . . . . . . . sbm2 33 . hb* parsed_1b4c 1 104 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 105 1 1 . . . . . . . . sbm1 34 . ha parsed_1b4c 1 105 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 106 1 1 . . . . . . . . sbm2 34 . ha parsed_1b4c 1 106 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 107 1 1 . . . . . . . . sbm1 34 . hb* parsed_1b4c 1 107 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 108 1 1 . . . . . . . . sbm2 34 . hb* parsed_1b4c 1 108 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 109 1 1 . . . . . . . . sbm1 35 . ha parsed_1b4c 1 109 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 110 1 1 . . . . . . . . sbm2 35 . ha parsed_1b4c 1 110 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 111 1 1 . . . . . . . . sbm1 35 . ha parsed_1b4c 1 111 1 2 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 112 1 1 . . . . . . . . sbm2 35 . ha parsed_1b4c 1 112 1 2 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 113 1 1 . . . . . . . . sbm1 35 . hb* parsed_1b4c 1 113 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 114 1 1 . . . . . . . . sbm2 35 . hb* parsed_1b4c 1 114 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 115 1 1 . . . . . . . . sbm1 36 . ha parsed_1b4c 1 115 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 116 1 1 . . . . . . . . sbm2 36 . ha parsed_1b4c 1 116 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 117 1 1 . . . . . . . . sbm1 36 . ha parsed_1b4c 1 117 1 2 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 118 1 1 . . . . . . . . sbm2 36 . ha parsed_1b4c 1 118 1 2 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 119 1 1 . . . . . . . . sbm1 36 . hb parsed_1b4c 1 119 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 120 1 1 . . . . . . . . sbm2 36 . hb parsed_1b4c 1 120 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 121 1 1 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 121 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 122 1 1 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 122 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 123 1 1 . . . . . . . . sbm1 37 . ha parsed_1b4c 1 123 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 124 1 1 . . . . . . . . sbm2 37 . ha parsed_1b4c 1 124 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 125 1 1 . . . . . . . . sbm1 37 . hb* parsed_1b4c 1 125 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 126 1 1 . . . . . . . . sbm2 37 . hb* parsed_1b4c 1 126 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 127 1 1 . . . . . . . . sbm1 38 . ha parsed_1b4c 1 127 1 2 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 128 1 1 . . . . . . . . sbm2 38 . ha parsed_1b4c 1 128 1 2 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 129 1 1 . . . . . . . . sbm1 38 . hb* parsed_1b4c 1 129 1 2 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 130 1 1 . . . . . . . . sbm2 38 . hb* parsed_1b4c 1 130 1 2 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 131 1 1 . . . . . . . . sbm1 39 . hb* parsed_1b4c 1 131 1 2 . . . . . . . . sbm1 39 . hn parsed_1b4c 1 132 1 1 . . . . . . . . sbm2 39 . hb* parsed_1b4c 1 132 1 2 . . . . . . . . sbm2 39 . hn parsed_1b4c 1 133 1 1 . . . . . . . . sbm1 40 . ha parsed_1b4c 1 133 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 134 1 1 . . . . . . . . sbm2 40 . ha parsed_1b4c 1 134 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 135 1 1 . . . . . . . . sbm1 40 . hb* parsed_1b4c 1 135 1 2 . . . . . . . . sbm1 40 . hn parsed_1b4c 1 136 1 1 . . . . . . . . sbm2 40 . hb* parsed_1b4c 1 136 1 2 . . . . . . . . sbm2 40 . hn parsed_1b4c 1 137 1 1 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 137 1 2 . . . . . . . . sbm1 40 . hn parsed_1b4c 1 138 1 1 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 138 1 2 . . . . . . . . sbm2 40 . hn parsed_1b4c 1 139 1 1 . . . . . . . . sbm1 41 . ha parsed_1b4c 1 139 1 2 . . . . . . . . sbm1 41 . hn parsed_1b4c 1 140 1 1 . . . . . . . . sbm2 41 . ha parsed_1b4c 1 140 1 2 . . . . . . . . sbm2 41 . hn parsed_1b4c 1 141 1 1 . . . . . . . . sbm1 41 . hb* parsed_1b4c 1 141 1 2 . . . . . . . . sbm1 41 . hn parsed_1b4c 1 142 1 1 . . . . . . . . sbm2 41 . hb* parsed_1b4c 1 142 1 2 . . . . . . . . sbm2 41 . hn parsed_1b4c 1 143 1 1 . . . . . . . . sbm1 43 . hb* parsed_1b4c 1 143 1 2 . . . . . . . . sbm1 43 . hn parsed_1b4c 1 144 1 1 . . . . . . . . sbm2 43 . hb* parsed_1b4c 1 144 1 2 . . . . . . . . sbm2 43 . hn parsed_1b4c 1 145 1 1 . . . . . . . . sbm1 43 . hd* parsed_1b4c 1 145 1 2 . . . . . . . . sbm1 43 . hn parsed_1b4c 1 146 1 1 . . . . . . . . sbm2 43 . hd* parsed_1b4c 1 146 1 2 . . . . . . . . sbm2 43 . hn parsed_1b4c 1 147 1 1 . . . . . . . . sbm1 44 . ha parsed_1b4c 1 147 1 2 . . . . . . . . sbm1 44 . hn parsed_1b4c 1 148 1 1 . . . . . . . . sbm2 44 . ha parsed_1b4c 1 148 1 2 . . . . . . . . sbm2 44 . hn parsed_1b4c 1 149 1 1 . . . . . . . . sbm1 44 . hb* parsed_1b4c 1 149 1 2 . . . . . . . . sbm1 44 . hn parsed_1b4c 1 150 1 1 . . . . . . . . sbm2 44 . hb* parsed_1b4c 1 150 1 2 . . . . . . . . sbm2 44 . hn parsed_1b4c 1 151 1 1 . . . . . . . . sbm1 45 . ha parsed_1b4c 1 151 1 2 . . . . . . . . sbm1 45 . hn parsed_1b4c 1 152 1 1 . . . . . . . . sbm2 45 . ha parsed_1b4c 1 152 1 2 . . . . . . . . sbm2 45 . hn parsed_1b4c 1 153 1 1 . . . . . . . . sbm1 45 . hb* parsed_1b4c 1 153 1 2 . . . . . . . . sbm1 45 . hn parsed_1b4c 1 154 1 1 . . . . . . . . sbm2 45 . hb* parsed_1b4c 1 154 1 2 . . . . . . . . sbm2 45 . hn parsed_1b4c 1 155 1 1 . . . . . . . . sbm1 46 . hb* parsed_1b4c 1 155 1 2 . . . . . . . . sbm1 46 . hn parsed_1b4c 1 156 1 1 . . . . . . . . sbm2 46 . hb* parsed_1b4c 1 156 1 2 . . . . . . . . sbm2 46 . hn parsed_1b4c 1 157 1 1 . . . . . . . . sbm1 49 . hb* parsed_1b4c 1 157 1 2 . . . . . . . . sbm1 49 . hn parsed_1b4c 1 158 1 1 . . . . . . . . sbm2 49 . hb* parsed_1b4c 1 158 1 2 . . . . . . . . sbm2 49 . hn parsed_1b4c 1 159 1 1 . . . . . . . . sbm1 50 . ha parsed_1b4c 1 159 1 2 . . . . . . . . sbm1 50 . hn parsed_1b4c 1 160 1 1 . . . . . . . . sbm2 50 . ha parsed_1b4c 1 160 1 2 . . . . . . . . sbm2 50 . hn parsed_1b4c 1 161 1 1 . . . . . . . . sbm1 50 . hb* parsed_1b4c 1 161 1 2 . . . . . . . . sbm1 50 . hn parsed_1b4c 1 162 1 1 . . . . . . . . sbm2 50 . hb* parsed_1b4c 1 162 1 2 . . . . . . . . sbm2 50 . hn parsed_1b4c 1 163 1 1 . . . . . . . . sbm1 51 . ha parsed_1b4c 1 163 1 2 . . . . . . . . sbm1 51 . hn parsed_1b4c 1 164 1 1 . . . . . . . . sbm2 51 . ha parsed_1b4c 1 164 1 2 . . . . . . . . sbm2 51 . hn parsed_1b4c 1 165 1 1 . . . . . . . . sbm1 51 . hb* parsed_1b4c 1 165 1 2 . . . . . . . . sbm1 51 . hn parsed_1b4c 1 166 1 1 . . . . . . . . sbm2 51 . hb* parsed_1b4c 1 166 1 2 . . . . . . . . sbm2 51 . hn parsed_1b4c 1 167 1 1 . . . . . . . . sbm1 52 . ha parsed_1b4c 1 167 1 2 . . . . . . . . sbm1 52 . hn parsed_1b4c 1 168 1 1 . . . . . . . . sbm2 52 . ha parsed_1b4c 1 168 1 2 . . . . . . . . sbm2 52 . hn parsed_1b4c 1 169 1 1 . . . . . . . . sbm1 52 . hb parsed_1b4c 1 169 1 2 . . . . . . . . sbm1 52 . hn parsed_1b4c 1 170 1 1 . . . . . . . . sbm2 52 . hb parsed_1b4c 1 170 1 2 . . . . . . . . sbm2 52 . hn parsed_1b4c 1 171 1 1 . . . . . . . . sbm1 53 . ha parsed_1b4c 1 171 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 172 1 1 . . . . . . . . sbm2 53 . ha parsed_1b4c 1 172 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 173 1 1 . . . . . . . . sbm1 53 . hb parsed_1b4c 1 173 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 174 1 1 . . . . . . . . sbm2 53 . hb parsed_1b4c 1 174 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 175 1 1 . . . . . . . . sbm1 54 . ha parsed_1b4c 1 175 1 2 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 176 1 1 . . . . . . . . sbm2 54 . ha parsed_1b4c 1 176 1 2 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 177 1 1 . . . . . . . . sbm1 54 . hb* parsed_1b4c 1 177 1 2 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 178 1 1 . . . . . . . . sbm2 54 . hb* parsed_1b4c 1 178 1 2 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 179 1 1 . . . . . . . . sbm1 55 . ha parsed_1b4c 1 179 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 180 1 1 . . . . . . . . sbm2 55 . ha parsed_1b4c 1 180 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 181 1 1 . . . . . . . . sbm1 55 . hb* parsed_1b4c 1 181 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 182 1 1 . . . . . . . . sbm2 55 . hb* parsed_1b4c 1 182 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 183 1 1 . . . . . . . . sbm1 56 . ha parsed_1b4c 1 183 1 2 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 184 1 1 . . . . . . . . sbm2 56 . ha parsed_1b4c 1 184 1 2 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 185 1 1 . . . . . . . . sbm1 56 . hb parsed_1b4c 1 185 1 2 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 186 1 1 . . . . . . . . sbm2 56 . hb parsed_1b4c 1 186 1 2 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 187 1 1 . . . . . . . . sbm1 57 . ha parsed_1b4c 1 187 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 188 1 1 . . . . . . . . sbm2 57 . ha parsed_1b4c 1 188 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 189 1 1 . . . . . . . . sbm1 57 . hb* parsed_1b4c 1 189 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 190 1 1 . . . . . . . . sbm2 57 . hb* parsed_1b4c 1 190 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 191 1 1 . . . . . . . . sbm1 58 . ha parsed_1b4c 1 191 1 2 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 192 1 1 . . . . . . . . sbm2 58 . ha parsed_1b4c 1 192 1 2 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 193 1 1 . . . . . . . . sbm1 58 . hb* parsed_1b4c 1 193 1 2 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 194 1 1 . . . . . . . . sbm2 58 . hb* parsed_1b4c 1 194 1 2 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 195 1 1 . . . . . . . . sbm1 59 . ha parsed_1b4c 1 195 1 2 . . . . . . . . sbm1 59 . hn parsed_1b4c 1 196 1 1 . . . . . . . . sbm2 59 . ha parsed_1b4c 1 196 1 2 . . . . . . . . sbm2 59 . hn parsed_1b4c 1 197 1 1 . . . . . . . . sbm1 59 . hb parsed_1b4c 1 197 1 2 . . . . . . . . sbm1 59 . hn parsed_1b4c 1 198 1 1 . . . . . . . . sbm2 59 . hb parsed_1b4c 1 198 1 2 . . . . . . . . sbm2 59 . hn parsed_1b4c 1 199 1 1 . . . . . . . . sbm1 61 . ha parsed_1b4c 1 199 1 2 . . . . . . . . sbm1 61 . hn parsed_1b4c 1 200 1 1 . . . . . . . . sbm2 61 . ha parsed_1b4c 1 200 1 2 . . . . . . . . sbm2 61 . hn parsed_1b4c 1 201 1 1 . . . . . . . . sbm1 61 . hb* parsed_1b4c 1 201 1 2 . . . . . . . . sbm1 61 . hn parsed_1b4c 1 202 1 1 . . . . . . . . sbm2 61 . hb* parsed_1b4c 1 202 1 2 . . . . . . . . sbm2 61 . hn parsed_1b4c 1 203 1 1 . . . . . . . . sbm1 62 . ha parsed_1b4c 1 203 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 204 1 1 . . . . . . . . sbm2 62 . ha parsed_1b4c 1 204 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 205 1 1 . . . . . . . . sbm1 62 . hb* parsed_1b4c 1 205 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 206 1 1 . . . . . . . . sbm2 62 . hb* parsed_1b4c 1 206 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 207 1 1 . . . . . . . . sbm1 62 . hg* parsed_1b4c 1 207 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 208 1 1 . . . . . . . . sbm2 62 . hg* parsed_1b4c 1 208 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 209 1 1 . . . . . . . . sbm1 63 . ha parsed_1b4c 1 209 1 2 . . . . . . . . sbm1 63 . hn parsed_1b4c 1 210 1 1 . . . . . . . . sbm2 63 . ha parsed_1b4c 1 210 1 2 . . . . . . . . sbm2 63 . hn parsed_1b4c 1 211 1 1 . . . . . . . . sbm1 63 . hb* parsed_1b4c 1 211 1 2 . . . . . . . . sbm1 63 . hn parsed_1b4c 1 212 1 1 . . . . . . . . sbm2 63 . hb* parsed_1b4c 1 212 1 2 . . . . . . . . sbm2 63 . hn parsed_1b4c 1 213 1 1 . . . . . . . . sbm1 64 . ha* parsed_1b4c 1 213 1 2 . . . . . . . . sbm1 64 . hn parsed_1b4c 1 214 1 1 . . . . . . . . sbm2 64 . ha* parsed_1b4c 1 214 1 2 . . . . . . . . sbm2 64 . hn parsed_1b4c 1 215 1 1 . . . . . . . . sbm1 65 . ha parsed_1b4c 1 215 1 2 . . . . . . . . sbm1 65 . hn parsed_1b4c 1 216 1 1 . . . . . . . . sbm2 65 . ha parsed_1b4c 1 216 1 2 . . . . . . . . sbm2 65 . hn parsed_1b4c 1 217 1 1 . . . . . . . . sbm1 65 . hb* parsed_1b4c 1 217 1 2 . . . . . . . . sbm1 65 . hn parsed_1b4c 1 218 1 1 . . . . . . . . sbm2 65 . hb* parsed_1b4c 1 218 1 2 . . . . . . . . sbm2 65 . hn parsed_1b4c 1 219 1 1 . . . . . . . . sbm1 66 . ha* parsed_1b4c 1 219 1 2 . . . . . . . . sbm1 66 . hn parsed_1b4c 1 220 1 1 . . . . . . . . sbm2 66 . ha* parsed_1b4c 1 220 1 2 . . . . . . . . sbm2 66 . hn parsed_1b4c 1 221 1 1 . . . . . . . . sbm1 67 . ha parsed_1b4c 1 221 1 2 . . . . . . . . sbm1 67 . hn parsed_1b4c 1 222 1 1 . . . . . . . . sbm2 67 . ha parsed_1b4c 1 222 1 2 . . . . . . . . sbm2 67 . hn parsed_1b4c 1 223 1 1 . . . . . . . . sbm1 67 . hb* parsed_1b4c 1 223 1 2 . . . . . . . . sbm1 67 . hn parsed_1b4c 1 224 1 1 . . . . . . . . sbm2 67 . hb* parsed_1b4c 1 224 1 2 . . . . . . . . sbm2 67 . hn parsed_1b4c 1 225 1 1 . . . . . . . . sbm1 67 . hb* parsed_1b4c 1 225 1 2 . . . . . . . . sbm1 67 . ha parsed_1b4c 1 226 1 1 . . . . . . . . sbm2 67 . hb* parsed_1b4c 1 226 1 2 . . . . . . . . sbm2 67 . ha parsed_1b4c 1 227 1 1 . . . . . . . . sbm1 67 . hg* parsed_1b4c 1 227 1 2 . . . . . . . . sbm1 67 . ha parsed_1b4c 1 228 1 1 . . . . . . . . sbm2 67 . hg* parsed_1b4c 1 228 1 2 . . . . . . . . sbm2 67 . ha parsed_1b4c 1 229 1 1 . . . . . . . . sbm1 68 . ha parsed_1b4c 1 229 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 230 1 1 . . . . . . . . sbm2 68 . ha parsed_1b4c 1 230 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 231 1 1 . . . . . . . . sbm1 68 . hb* parsed_1b4c 1 231 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 232 1 1 . . . . . . . . sbm2 68 . hb* parsed_1b4c 1 232 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 233 1 1 . . . . . . . . sbm1 68 . hb* parsed_1b4c 1 233 1 2 . . . . . . . . sbm1 68 . ha parsed_1b4c 1 234 1 1 . . . . . . . . sbm2 68 . hb* parsed_1b4c 1 234 1 2 . . . . . . . . sbm2 68 . ha parsed_1b4c 1 235 1 1 . . . . . . . . sbm1 69 . ha parsed_1b4c 1 235 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 236 1 1 . . . . . . . . sbm2 69 . ha parsed_1b4c 1 236 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 237 1 1 . . . . . . . . sbm1 69 . hb* parsed_1b4c 1 237 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 238 1 1 . . . . . . . . sbm2 69 . hb* parsed_1b4c 1 238 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 239 1 1 . . . . . . . . sbm1 69 . hb* parsed_1b4c 1 239 1 2 . . . . . . . . sbm1 69 . ha parsed_1b4c 1 240 1 1 . . . . . . . . sbm2 69 . hb* parsed_1b4c 1 240 1 2 . . . . . . . . sbm2 69 . ha parsed_1b4c 1 241 1 1 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 241 1 2 . . . . . . . . sbm1 70 . hn parsed_1b4c 1 242 1 1 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 242 1 2 . . . . . . . . sbm2 70 . hn parsed_1b4c 1 243 1 1 . . . . . . . . sbm1 70 . hb* parsed_1b4c 1 243 1 2 . . . . . . . . sbm1 70 . hn parsed_1b4c 1 244 1 1 . . . . . . . . sbm2 70 . hb* parsed_1b4c 1 244 1 2 . . . . . . . . sbm2 70 . hn parsed_1b4c 1 245 1 1 . . . . . . . . sbm1 70 . hd* parsed_1b4c 1 245 1 2 . . . . . . . . sbm1 70 . hn parsed_1b4c 1 246 1 1 . . . . . . . . sbm2 70 . hd* parsed_1b4c 1 246 1 2 . . . . . . . . sbm2 70 . hn parsed_1b4c 1 247 1 1 . . . . . . . . sbm1 70 . hb* parsed_1b4c 1 247 1 2 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 248 1 1 . . . . . . . . sbm2 70 . hb* parsed_1b4c 1 248 1 2 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 249 1 1 . . . . . . . . sbm1 70 . hd* parsed_1b4c 1 249 1 2 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 250 1 1 . . . . . . . . sbm2 70 . hd* parsed_1b4c 1 250 1 2 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 251 1 1 . . . . . . . . sbm1 71 . ha parsed_1b4c 1 251 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 252 1 1 . . . . . . . . sbm2 71 . ha parsed_1b4c 1 252 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 253 1 1 . . . . . . . . sbm1 71 . hb* parsed_1b4c 1 253 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 254 1 1 . . . . . . . . sbm2 71 . hb* parsed_1b4c 1 254 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 255 1 1 . . . . . . . . sbm1 71 . he2* parsed_1b4c 1 255 1 2 . . . . . . . . sbm1 71 . ha parsed_1b4c 1 256 1 1 . . . . . . . . sbm2 71 . he2* parsed_1b4c 1 256 1 2 . . . . . . . . sbm2 71 . ha parsed_1b4c 1 257 1 1 . . . . . . . . sbm1 71 . hg* parsed_1b4c 1 257 1 2 . . . . . . . . sbm1 71 . ha parsed_1b4c 1 258 1 1 . . . . . . . . sbm2 71 . hg* parsed_1b4c 1 258 1 2 . . . . . . . . sbm2 71 . ha parsed_1b4c 1 259 1 1 . . . . . . . . sbm1 71 . hb* parsed_1b4c 1 259 1 2 . . . . . . . . sbm1 71 . ha parsed_1b4c 1 260 1 1 . . . . . . . . sbm2 71 . hb* parsed_1b4c 1 260 1 2 . . . . . . . . sbm2 71 . ha parsed_1b4c 1 261 1 1 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 261 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 262 1 1 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 262 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 263 1 1 . . . . . . . . sbm1 72 . hb* parsed_1b4c 1 263 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 264 1 1 . . . . . . . . sbm2 72 . hb* parsed_1b4c 1 264 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 265 1 1 . . . . . . . . sbm1 72 . hg* parsed_1b4c 1 265 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 266 1 1 . . . . . . . . sbm2 72 . hg* parsed_1b4c 1 266 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 267 1 1 . . . . . . . . sbm1 72 . hg* parsed_1b4c 1 267 1 2 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 268 1 1 . . . . . . . . sbm2 72 . hg* parsed_1b4c 1 268 1 2 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 269 1 1 . . . . . . . . sbm1 72 . hb* parsed_1b4c 1 269 1 2 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 270 1 1 . . . . . . . . sbm2 72 . hb* parsed_1b4c 1 270 1 2 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 271 1 1 . . . . . . . . sbm1 73 . hb* parsed_1b4c 1 271 1 2 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 272 1 1 . . . . . . . . sbm2 73 . hb* parsed_1b4c 1 272 1 2 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 273 1 1 . . . . . . . . sbm1 74 . ha parsed_1b4c 1 273 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 274 1 1 . . . . . . . . sbm2 74 . ha parsed_1b4c 1 274 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 275 1 1 . . . . . . . . sbm1 74 . hb* parsed_1b4c 1 275 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 276 1 1 . . . . . . . . sbm2 74 . hb* parsed_1b4c 1 276 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 277 1 1 . . . . . . . . sbm1 75 . ha parsed_1b4c 1 277 1 2 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 278 1 1 . . . . . . . . sbm2 75 . ha parsed_1b4c 1 278 1 2 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 279 1 1 . . . . . . . . sbm1 75 . hb* parsed_1b4c 1 279 1 2 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 280 1 1 . . . . . . . . sbm2 75 . hb* parsed_1b4c 1 280 1 2 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 281 1 1 . . . . . . . . sbm1 76 . hb* parsed_1b4c 1 281 1 2 . . . . . . . . sbm1 76 . hn parsed_1b4c 1 282 1 1 . . . . . . . . sbm2 76 . hb* parsed_1b4c 1 282 1 2 . . . . . . . . sbm2 76 . hn parsed_1b4c 1 283 1 1 . . . . . . . . sbm1 77 . ha parsed_1b4c 1 283 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 284 1 1 . . . . . . . . sbm2 77 . ha parsed_1b4c 1 284 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 285 1 1 . . . . . . . . sbm1 77 . hb parsed_1b4c 1 285 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 286 1 1 . . . . . . . . sbm2 77 . hb parsed_1b4c 1 286 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 287 1 1 . . . . . . . . sbm1 78 . ha parsed_1b4c 1 287 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 288 1 1 . . . . . . . . sbm2 78 . ha parsed_1b4c 1 288 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 289 1 1 . . . . . . . . sbm1 78 . hb* parsed_1b4c 1 289 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 290 1 1 . . . . . . . . sbm2 78 . hb* parsed_1b4c 1 290 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 291 1 1 . . . . . . . . sbm1 79 . ha parsed_1b4c 1 291 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 292 1 1 . . . . . . . . sbm2 79 . ha parsed_1b4c 1 292 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 293 1 1 . . . . . . . . sbm1 79 . hb* parsed_1b4c 1 293 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 294 1 1 . . . . . . . . sbm2 79 . hb* parsed_1b4c 1 294 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 295 1 1 . . . . . . . . sbm1 80 . ha parsed_1b4c 1 295 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 296 1 1 . . . . . . . . sbm2 80 . ha parsed_1b4c 1 296 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 297 1 1 . . . . . . . . sbm1 80 . hb parsed_1b4c 1 297 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 298 1 1 . . . . . . . . sbm2 80 . hb parsed_1b4c 1 298 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 299 1 1 . . . . . . . . sbm1 81 . hb parsed_1b4c 1 299 1 2 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 300 1 1 . . . . . . . . sbm2 81 . hb parsed_1b4c 1 300 1 2 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 301 1 1 . . . . . . . . sbm1 83 . ha parsed_1b4c 1 301 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 302 1 1 . . . . . . . . sbm2 83 . ha parsed_1b4c 1 302 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 303 1 1 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 303 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 304 1 1 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 304 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 305 1 1 . . . . . . . . sbm1 88 . ha parsed_1b4c 1 305 1 2 . . . . . . . . sbm1 88 . hn parsed_1b4c 1 306 1 1 . . . . . . . . sbm2 88 . ha parsed_1b4c 1 306 1 2 . . . . . . . . sbm2 88 . hn parsed_1b4c 1 307 1 1 . . . . . . . . sbm1 88 . hb* parsed_1b4c 1 307 1 2 . . . . . . . . sbm1 88 . hn parsed_1b4c 1 308 1 1 . . . . . . . . sbm2 88 . hb* parsed_1b4c 1 308 1 2 . . . . . . . . sbm2 88 . hn parsed_1b4c 1 309 1 1 . . . . . . . . sbm1 89 . ha parsed_1b4c 1 309 1 2 . . . . . . . . sbm1 89 . hn parsed_1b4c 1 310 1 1 . . . . . . . . sbm2 89 . ha parsed_1b4c 1 310 1 2 . . . . . . . . sbm2 89 . hn parsed_1b4c 1 311 1 1 . . . . . . . . sbm1 89 . hb* parsed_1b4c 1 311 1 2 . . . . . . . . sbm1 89 . hn parsed_1b4c 1 312 1 1 . . . . . . . . sbm2 89 . hb* parsed_1b4c 1 312 1 2 . . . . . . . . sbm2 89 . hn parsed_1b4c 1 313 1 1 . . . . . . . . sbm1 90 . ha parsed_1b4c 1 313 1 2 . . . . . . . . sbm1 90 . hn parsed_1b4c 1 314 1 1 . . . . . . . . sbm2 90 . ha parsed_1b4c 1 314 1 2 . . . . . . . . sbm2 90 . hn parsed_1b4c 1 315 1 1 . . . . . . . . sbm1 91 . hb* parsed_1b4c 1 315 1 2 . . . . . . . . sbm1 91 . hn parsed_1b4c 1 316 1 1 . . . . . . . . sbm2 91 . hb* parsed_1b4c 1 316 1 2 . . . . . . . . sbm2 91 . hn parsed_1b4c 1 317 1 1 . . . . . . . . sbm1 2 . hn parsed_1b4c 1 317 1 2 . . . . . . . . sbm1 1 . hn parsed_1b4c 1 318 1 1 . . . . . . . . sbm2 2 . hn parsed_1b4c 1 318 1 2 . . . . . . . . sbm2 1 . hn parsed_1b4c 1 319 1 1 . . . . . . . . sbm1 1 . ha parsed_1b4c 1 319 1 2 . . . . . . . . sbm1 2 . hn parsed_1b4c 1 320 1 1 . . . . . . . . sbm2 1 . ha parsed_1b4c 1 320 1 2 . . . . . . . . sbm2 2 . hn parsed_1b4c 1 321 1 1 . . . . . . . . sbm1 2 . hn parsed_1b4c 1 321 1 2 . . . . . . . . sbm1 3 . hn parsed_1b4c 1 322 1 1 . . . . . . . . sbm2 2 . hn parsed_1b4c 1 322 1 2 . . . . . . . . sbm2 3 . hn parsed_1b4c 1 323 1 1 . . . . . . . . sbm1 2 . ha parsed_1b4c 1 323 1 2 . . . . . . . . sbm1 3 . hn parsed_1b4c 1 324 1 1 . . . . . . . . sbm2 2 . ha parsed_1b4c 1 324 1 2 . . . . . . . . sbm2 3 . hn parsed_1b4c 1 325 1 1 . . . . . . . . sbm1 2 . hb* parsed_1b4c 1 325 1 2 . . . . . . . . sbm1 3 . hn parsed_1b4c 1 326 1 1 . . . . . . . . sbm2 2 . hb* parsed_1b4c 1 326 1 2 . . . . . . . . sbm2 3 . hn parsed_1b4c 1 327 1 1 . . . . . . . . sbm1 3 . hn parsed_1b4c 1 327 1 2 . . . . . . . . sbm1 4 . hn parsed_1b4c 1 328 1 1 . . . . . . . . sbm2 3 . hn parsed_1b4c 1 328 1 2 . . . . . . . . sbm2 4 . hn parsed_1b4c 1 329 1 1 . . . . . . . . sbm1 3 . ha parsed_1b4c 1 329 1 2 . . . . . . . . sbm1 4 . hn parsed_1b4c 1 330 1 1 . . . . . . . . sbm2 3 . ha parsed_1b4c 1 330 1 2 . . . . . . . . sbm2 4 . hn parsed_1b4c 1 331 1 1 . . . . . . . . sbm1 3 . hb* parsed_1b4c 1 331 1 2 . . . . . . . . sbm1 4 . hn parsed_1b4c 1 332 1 1 . . . . . . . . sbm2 3 . hb* parsed_1b4c 1 332 1 2 . . . . . . . . sbm2 4 . hn parsed_1b4c 1 333 1 1 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 333 1 2 . . . . . . . . sbm1 4 . hn parsed_1b4c 1 334 1 1 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 334 1 2 . . . . . . . . sbm2 4 . hn parsed_1b4c 1 335 1 1 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 335 1 2 . . . . . . . . sbm1 4 . hn parsed_1b4c 1 336 1 1 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 336 1 2 . . . . . . . . sbm2 4 . hn parsed_1b4c 1 337 1 1 . . . . . . . . sbm1 4 . ha parsed_1b4c 1 337 1 2 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 338 1 1 . . . . . . . . sbm2 4 . ha parsed_1b4c 1 338 1 2 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 339 1 1 . . . . . . . . sbm1 4 . hb* parsed_1b4c 1 339 1 2 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 340 1 1 . . . . . . . . sbm2 4 . hb* parsed_1b4c 1 340 1 2 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 341 1 1 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 341 1 2 . . . . . . . . sbm1 6 . hn parsed_1b4c 1 342 1 1 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 342 1 2 . . . . . . . . sbm2 6 . hn parsed_1b4c 1 343 1 1 . . . . . . . . sbm1 5 . ha parsed_1b4c 1 343 1 2 . . . . . . . . sbm1 6 . hn parsed_1b4c 1 344 1 1 . . . . . . . . sbm2 5 . ha parsed_1b4c 1 344 1 2 . . . . . . . . sbm2 6 . hn parsed_1b4c 1 345 1 1 . . . . . . . . sbm1 5 . hb* parsed_1b4c 1 345 1 2 . . . . . . . . sbm1 6 . hn parsed_1b4c 1 346 1 1 . . . . . . . . sbm2 5 . hb* parsed_1b4c 1 346 1 2 . . . . . . . . sbm2 6 . hn parsed_1b4c 1 347 1 1 . . . . . . . . sbm1 6 . hn parsed_1b4c 1 347 1 2 . . . . . . . . sbm1 7 . hn parsed_1b4c 1 348 1 1 . . . . . . . . sbm2 6 . hn parsed_1b4c 1 348 1 2 . . . . . . . . sbm2 7 . hn parsed_1b4c 1 349 1 1 . . . . . . . . sbm1 6 . ha parsed_1b4c 1 349 1 2 . . . . . . . . sbm1 7 . hn parsed_1b4c 1 350 1 1 . . . . . . . . sbm2 6 . ha parsed_1b4c 1 350 1 2 . . . . . . . . sbm2 7 . hn parsed_1b4c 1 351 1 1 . . . . . . . . sbm1 7 . hn parsed_1b4c 1 351 1 2 . . . . . . . . sbm1 8 . hn parsed_1b4c 1 352 1 1 . . . . . . . . sbm2 7 . hn parsed_1b4c 1 352 1 2 . . . . . . . . sbm2 8 . hn parsed_1b4c 1 353 1 1 . . . . . . . . sbm1 7 . hb* parsed_1b4c 1 353 1 2 . . . . . . . . sbm1 8 . hn parsed_1b4c 1 354 1 1 . . . . . . . . sbm2 7 . hb* parsed_1b4c 1 354 1 2 . . . . . . . . sbm2 8 . hn parsed_1b4c 1 355 1 1 . . . . . . . . sbm1 8 . hn parsed_1b4c 1 355 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 356 1 1 . . . . . . . . sbm2 8 . hn parsed_1b4c 1 356 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 357 1 1 . . . . . . . . sbm1 8 . ha parsed_1b4c 1 357 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 358 1 1 . . . . . . . . sbm2 8 . ha parsed_1b4c 1 358 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 359 1 1 . . . . . . . . sbm1 8 . hb parsed_1b4c 1 359 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 360 1 1 . . . . . . . . sbm2 8 . hb parsed_1b4c 1 360 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 361 1 1 . . . . . . . . sbm1 8 . hg2* parsed_1b4c 1 361 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 362 1 1 . . . . . . . . sbm2 8 . hg2* parsed_1b4c 1 362 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 363 1 1 . . . . . . . . sbm1 8 . hg1* parsed_1b4c 1 363 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 364 1 1 . . . . . . . . sbm2 8 . hg1* parsed_1b4c 1 364 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 365 1 1 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 365 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 366 1 1 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 366 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 367 1 1 . . . . . . . . sbm1 9 . ha parsed_1b4c 1 367 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 368 1 1 . . . . . . . . sbm2 9 . ha parsed_1b4c 1 368 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 369 1 1 . . . . . . . . sbm1 9 . hb* parsed_1b4c 1 369 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 370 1 1 . . . . . . . . sbm2 9 . hb* parsed_1b4c 1 370 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 371 1 1 . . . . . . . . sbm1 11 . hn parsed_1b4c 1 371 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 372 1 1 . . . . . . . . sbm2 11 . hn parsed_1b4c 1 372 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 373 1 1 . . . . . . . . sbm1 10 . ha parsed_1b4c 1 373 1 2 . . . . . . . . sbm1 11 . hn parsed_1b4c 1 374 1 1 . . . . . . . . sbm2 10 . ha parsed_1b4c 1 374 1 2 . . . . . . . . sbm2 11 . hn parsed_1b4c 1 375 1 1 . . . . . . . . sbm1 11 . hn parsed_1b4c 1 375 1 2 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 376 1 1 . . . . . . . . sbm2 11 . hn parsed_1b4c 1 376 1 2 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 377 1 1 . . . . . . . . sbm1 11 . ha parsed_1b4c 1 377 1 2 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 378 1 1 . . . . . . . . sbm2 11 . ha parsed_1b4c 1 378 1 2 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 379 1 1 . . . . . . . . sbm1 11 . hb parsed_1b4c 1 379 1 2 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 380 1 1 . . . . . . . . sbm2 11 . hb parsed_1b4c 1 380 1 2 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 381 1 1 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 381 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 382 1 1 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 382 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 383 1 1 . . . . . . . . sbm1 12 . ha parsed_1b4c 1 383 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 384 1 1 . . . . . . . . sbm2 12 . ha parsed_1b4c 1 384 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 385 1 1 . . . . . . . . sbm1 12 . hb* parsed_1b4c 1 385 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 386 1 1 . . . . . . . . sbm2 12 . hb* parsed_1b4c 1 386 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 387 1 1 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 387 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 388 1 1 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 388 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 389 1 1 . . . . . . . . sbm1 13 . ha parsed_1b4c 1 389 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 390 1 1 . . . . . . . . sbm2 13 . ha parsed_1b4c 1 390 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 391 1 1 . . . . . . . . sbm1 13 . hb parsed_1b4c 1 391 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 392 1 1 . . . . . . . . sbm2 13 . hb parsed_1b4c 1 392 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 393 1 1 . . . . . . . . sbm1 13 . hg1* parsed_1b4c 1 393 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 394 1 1 . . . . . . . . sbm2 13 . hg1* parsed_1b4c 1 394 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 395 1 1 . . . . . . . . sbm1 15 . hn parsed_1b4c 1 395 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 396 1 1 . . . . . . . . sbm2 15 . hn parsed_1b4c 1 396 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 397 1 1 . . . . . . . . sbm1 14 . ha parsed_1b4c 1 397 1 2 . . . . . . . . sbm1 15 . hn parsed_1b4c 1 398 1 1 . . . . . . . . sbm2 14 . ha parsed_1b4c 1 398 1 2 . . . . . . . . sbm2 15 . hn parsed_1b4c 1 399 1 1 . . . . . . . . sbm1 14 . hb* parsed_1b4c 1 399 1 2 . . . . . . . . sbm1 15 . hn parsed_1b4c 1 400 1 1 . . . . . . . . sbm2 14 . hb* parsed_1b4c 1 400 1 2 . . . . . . . . sbm2 15 . hn parsed_1b4c 1 401 1 1 . . . . . . . . sbm1 15 . hn parsed_1b4c 1 401 1 2 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 402 1 1 . . . . . . . . sbm2 15 . hn parsed_1b4c 1 402 1 2 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 403 1 1 . . . . . . . . sbm1 15 . ha parsed_1b4c 1 403 1 2 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 404 1 1 . . . . . . . . sbm2 15 . ha parsed_1b4c 1 404 1 2 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 405 1 1 . . . . . . . . sbm1 15 . hb* parsed_1b4c 1 405 1 2 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 406 1 1 . . . . . . . . sbm2 15 . hb* parsed_1b4c 1 406 1 2 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 407 1 1 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 407 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 408 1 1 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 408 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 409 1 1 . . . . . . . . sbm1 16 . ha parsed_1b4c 1 409 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 410 1 1 . . . . . . . . sbm2 16 . ha parsed_1b4c 1 410 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 411 1 1 . . . . . . . . sbm1 16 . hb* parsed_1b4c 1 411 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 412 1 1 . . . . . . . . sbm2 16 . hb* parsed_1b4c 1 412 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 413 1 1 . . . . . . . . sbm1 16 . hb* parsed_1b4c 1 413 1 2 . . . . . . . . sbm1 17 . hd* parsed_1b4c 1 414 1 1 . . . . . . . . sbm2 16 . hb* parsed_1b4c 1 414 1 2 . . . . . . . . sbm2 17 . hd* parsed_1b4c 1 415 1 1 . . . . . . . . sbm1 16 . hg* parsed_1b4c 1 415 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 416 1 1 . . . . . . . . sbm2 16 . hg* parsed_1b4c 1 416 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 417 1 1 . . . . . . . . sbm1 18 . ha parsed_1b4c 1 417 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 418 1 1 . . . . . . . . sbm2 18 . ha parsed_1b4c 1 418 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 419 1 1 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 419 1 2 . . . . . . . . sbm1 18 . hn parsed_1b4c 1 420 1 1 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 420 1 2 . . . . . . . . sbm2 18 . hn parsed_1b4c 1 421 1 1 . . . . . . . . sbm1 17 . ha parsed_1b4c 1 421 1 2 . . . . . . . . sbm1 18 . hn parsed_1b4c 1 422 1 1 . . . . . . . . sbm2 17 . ha parsed_1b4c 1 422 1 2 . . . . . . . . sbm2 18 . hn parsed_1b4c 1 423 1 1 . . . . . . . . sbm1 17 . hb* parsed_1b4c 1 423 1 2 . . . . . . . . sbm1 18 . hn parsed_1b4c 1 424 1 1 . . . . . . . . sbm2 17 . hb* parsed_1b4c 1 424 1 2 . . . . . . . . sbm2 18 . hn parsed_1b4c 1 425 1 1 . . . . . . . . sbm1 19 . hn parsed_1b4c 1 425 1 2 . . . . . . . . sbm1 20 . hn parsed_1b4c 1 426 1 1 . . . . . . . . sbm2 19 . hn parsed_1b4c 1 426 1 2 . . . . . . . . sbm2 20 . hn parsed_1b4c 1 427 1 1 . . . . . . . . sbm1 20 . hn parsed_1b4c 1 427 1 2 . . . . . . . . sbm1 21 . hn parsed_1b4c 1 428 1 1 . . . . . . . . sbm2 20 . hn parsed_1b4c 1 428 1 2 . . . . . . . . sbm2 21 . hn parsed_1b4c 1 429 1 1 . . . . . . . . sbm1 20 . ha parsed_1b4c 1 429 1 2 . . . . . . . . sbm1 21 . hn parsed_1b4c 1 430 1 1 . . . . . . . . sbm2 20 . ha parsed_1b4c 1 430 1 2 . . . . . . . . sbm2 21 . hn parsed_1b4c 1 431 1 1 . . . . . . . . sbm1 20 . hb* parsed_1b4c 1 431 1 2 . . . . . . . . sbm1 21 . hn parsed_1b4c 1 432 1 1 . . . . . . . . sbm2 20 . hb* parsed_1b4c 1 432 1 2 . . . . . . . . sbm2 21 . hn parsed_1b4c 1 433 1 1 . . . . . . . . sbm1 21 . hn parsed_1b4c 1 433 1 2 . . . . . . . . sbm1 22 . hn parsed_1b4c 1 434 1 1 . . . . . . . . sbm2 21 . hn parsed_1b4c 1 434 1 2 . . . . . . . . sbm2 22 . hn parsed_1b4c 1 435 1 1 . . . . . . . . sbm1 21 . hb* parsed_1b4c 1 435 1 2 . . . . . . . . sbm1 22 . hn parsed_1b4c 1 436 1 1 . . . . . . . . sbm2 21 . hb* parsed_1b4c 1 436 1 2 . . . . . . . . sbm2 22 . hn parsed_1b4c 1 437 1 1 . . . . . . . . sbm1 21 . hg* parsed_1b4c 1 437 1 2 . . . . . . . . sbm1 22 . hn parsed_1b4c 1 438 1 1 . . . . . . . . sbm2 21 . hg* parsed_1b4c 1 438 1 2 . . . . . . . . sbm2 22 . hn parsed_1b4c 1 439 1 1 . . . . . . . . sbm1 22 . hn parsed_1b4c 1 439 1 2 . . . . . . . . sbm1 23 . hn parsed_1b4c 1 440 1 1 . . . . . . . . sbm2 22 . hn parsed_1b4c 1 440 1 2 . . . . . . . . sbm2 23 . hn parsed_1b4c 1 441 1 1 . . . . . . . . sbm1 22 . ha* parsed_1b4c 1 441 1 2 . . . . . . . . sbm1 23 . hn parsed_1b4c 1 442 1 1 . . . . . . . . sbm2 22 . ha* parsed_1b4c 1 442 1 2 . . . . . . . . sbm2 23 . hn parsed_1b4c 1 443 1 1 . . . . . . . . sbm1 23 . ha parsed_1b4c 1 443 1 2 . . . . . . . . sbm1 24 . hn parsed_1b4c 1 444 1 1 . . . . . . . . sbm2 23 . ha parsed_1b4c 1 444 1 2 . . . . . . . . sbm2 24 . hn parsed_1b4c 1 445 1 1 . . . . . . . . sbm1 23 . hb* parsed_1b4c 1 445 1 2 . . . . . . . . sbm1 24 . hn parsed_1b4c 1 446 1 1 . . . . . . . . sbm2 23 . hb* parsed_1b4c 1 446 1 2 . . . . . . . . sbm2 24 . hn parsed_1b4c 1 447 1 1 . . . . . . . . sbm1 24 . hn parsed_1b4c 1 447 1 2 . . . . . . . . sbm1 25 . hn parsed_1b4c 1 448 1 1 . . . . . . . . sbm2 24 . hn parsed_1b4c 1 448 1 2 . . . . . . . . sbm2 25 . hn parsed_1b4c 1 449 1 1 . . . . . . . . sbm1 24 . ha parsed_1b4c 1 449 1 2 . . . . . . . . sbm1 25 . hn parsed_1b4c 1 450 1 1 . . . . . . . . sbm2 24 . ha parsed_1b4c 1 450 1 2 . . . . . . . . sbm2 25 . hn parsed_1b4c 1 451 1 1 . . . . . . . . sbm1 24 . hb* parsed_1b4c 1 451 1 2 . . . . . . . . sbm1 25 . hn parsed_1b4c 1 452 1 1 . . . . . . . . sbm2 24 . hb* parsed_1b4c 1 452 1 2 . . . . . . . . sbm2 25 . hn parsed_1b4c 1 453 1 1 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 453 1 2 . . . . . . . . sbm1 25 . hn parsed_1b4c 1 454 1 1 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 454 1 2 . . . . . . . . sbm2 25 . hn parsed_1b4c 1 455 1 1 . . . . . . . . sbm1 25 . ha parsed_1b4c 1 455 1 2 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 456 1 1 . . . . . . . . sbm2 25 . ha parsed_1b4c 1 456 1 2 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 457 1 1 . . . . . . . . sbm1 25 . hb* parsed_1b4c 1 457 1 2 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 458 1 1 . . . . . . . . sbm2 25 . hb* parsed_1b4c 1 458 1 2 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 459 1 1 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 459 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 460 1 1 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 460 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 461 1 1 . . . . . . . . sbm1 26 . ha parsed_1b4c 1 461 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 462 1 1 . . . . . . . . sbm2 26 . ha parsed_1b4c 1 462 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 463 1 1 . . . . . . . . sbm1 26 . hb* parsed_1b4c 1 463 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 464 1 1 . . . . . . . . sbm2 26 . hb* parsed_1b4c 1 464 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 465 1 1 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 465 1 2 . . . . . . . . sbm1 28 . hn parsed_1b4c 1 466 1 1 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 466 1 2 . . . . . . . . sbm2 28 . hn parsed_1b4c 1 467 1 1 . . . . . . . . sbm1 27 . ha parsed_1b4c 1 467 1 2 . . . . . . . . sbm1 28 . hn parsed_1b4c 1 468 1 1 . . . . . . . . sbm2 27 . ha parsed_1b4c 1 468 1 2 . . . . . . . . sbm2 28 . hn parsed_1b4c 1 469 1 1 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 469 1 2 . . . . . . . . sbm1 28 . hn parsed_1b4c 1 470 1 1 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 470 1 2 . . . . . . . . sbm2 28 . hn parsed_1b4c 1 471 1 1 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 471 1 2 . . . . . . . . sbm1 28 . hn parsed_1b4c 1 472 1 1 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 472 1 2 . . . . . . . . sbm2 28 . hn parsed_1b4c 1 473 1 1 . . . . . . . . sbm1 28 . ha parsed_1b4c 1 473 1 2 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 474 1 1 . . . . . . . . sbm2 28 . ha parsed_1b4c 1 474 1 2 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 475 1 1 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 475 1 2 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 476 1 1 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 476 1 2 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 477 1 1 . . . . . . . . sbm1 29 . hb* parsed_1b4c 1 477 1 2 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 478 1 1 . . . . . . . . sbm2 29 . hb* parsed_1b4c 1 478 1 2 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 479 1 1 . . . . . . . . sbm1 31 . hn parsed_1b4c 1 479 1 2 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 480 1 1 . . . . . . . . sbm2 31 . hn parsed_1b4c 1 480 1 2 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 481 1 1 . . . . . . . . sbm1 31 . hb* parsed_1b4c 1 481 1 2 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 482 1 1 . . . . . . . . sbm2 31 . hb* parsed_1b4c 1 482 1 2 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 483 1 1 . . . . . . . . sbm1 30 . ha parsed_1b4c 1 483 1 2 . . . . . . . . sbm1 31 . hn parsed_1b4c 1 484 1 1 . . . . . . . . sbm2 30 . ha parsed_1b4c 1 484 1 2 . . . . . . . . sbm2 31 . hn parsed_1b4c 1 485 1 1 . . . . . . . . sbm1 30 . hb* parsed_1b4c 1 485 1 2 . . . . . . . . sbm1 31 . hn parsed_1b4c 1 486 1 1 . . . . . . . . sbm2 30 . hb* parsed_1b4c 1 486 1 2 . . . . . . . . sbm2 31 . hn parsed_1b4c 1 487 1 1 . . . . . . . . sbm1 31 . hn parsed_1b4c 1 487 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 488 1 1 . . . . . . . . sbm2 31 . hn parsed_1b4c 1 488 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 489 1 1 . . . . . . . . sbm1 31 . hb* parsed_1b4c 1 489 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 490 1 1 . . . . . . . . sbm2 31 . hb* parsed_1b4c 1 490 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 491 1 1 . . . . . . . . sbm1 31 . hg* parsed_1b4c 1 491 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 492 1 1 . . . . . . . . sbm2 31 . hg* parsed_1b4c 1 492 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 493 1 1 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 493 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 494 1 1 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 494 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 495 1 1 . . . . . . . . sbm1 32 . ha parsed_1b4c 1 495 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 496 1 1 . . . . . . . . sbm2 32 . ha parsed_1b4c 1 496 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 497 1 1 . . . . . . . . sbm1 32 . hb* parsed_1b4c 1 497 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 498 1 1 . . . . . . . . sbm2 32 . hb* parsed_1b4c 1 498 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 499 1 1 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 499 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 500 1 1 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 500 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 501 1 1 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 501 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 502 1 1 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 502 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 503 1 1 . . . . . . . . sbm1 33 . ha parsed_1b4c 1 503 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 504 1 1 . . . . . . . . sbm2 33 . ha parsed_1b4c 1 504 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 505 1 1 . . . . . . . . sbm1 33 . hb* parsed_1b4c 1 505 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 506 1 1 . . . . . . . . sbm2 33 . hb* parsed_1b4c 1 506 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 507 1 1 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 507 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 508 1 1 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 508 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 509 1 1 . . . . . . . . sbm1 34 . ha parsed_1b4c 1 509 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 510 1 1 . . . . . . . . sbm2 34 . ha parsed_1b4c 1 510 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 511 1 1 . . . . . . . . sbm1 34 . hb* parsed_1b4c 1 511 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 512 1 1 . . . . . . . . sbm2 34 . hb* parsed_1b4c 1 512 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 513 1 1 . . . . . . . . sbm1 34 . hg* parsed_1b4c 1 513 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 514 1 1 . . . . . . . . sbm2 34 . hg* parsed_1b4c 1 514 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 515 1 1 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 515 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 516 1 1 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 516 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 517 1 1 . . . . . . . . sbm1 36 . ha parsed_1b4c 1 517 1 2 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 518 1 1 . . . . . . . . sbm2 36 . ha parsed_1b4c 1 518 1 2 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 519 1 1 . . . . . . . . sbm1 35 . ha parsed_1b4c 1 519 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 520 1 1 . . . . . . . . sbm2 35 . ha parsed_1b4c 1 520 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 521 1 1 . . . . . . . . sbm1 35 . hb* parsed_1b4c 1 521 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 522 1 1 . . . . . . . . sbm2 35 . hb* parsed_1b4c 1 522 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 523 1 1 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 523 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 524 1 1 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 524 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 525 1 1 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 525 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 526 1 1 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 526 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 527 1 1 . . . . . . . . sbm1 36 . ha parsed_1b4c 1 527 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 528 1 1 . . . . . . . . sbm2 36 . ha parsed_1b4c 1 528 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 529 1 1 . . . . . . . . sbm1 36 . hb parsed_1b4c 1 529 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 530 1 1 . . . . . . . . sbm2 36 . hb parsed_1b4c 1 530 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 531 1 1 . . . . . . . . sbm1 36 . hg2* parsed_1b4c 1 531 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 532 1 1 . . . . . . . . sbm2 36 . hg2* parsed_1b4c 1 532 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 533 1 1 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 533 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 534 1 1 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 534 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 535 1 1 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 535 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 536 1 1 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 536 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 537 1 1 . . . . . . . . sbm1 37 . ha parsed_1b4c 1 537 1 2 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 538 1 1 . . . . . . . . sbm2 37 . ha parsed_1b4c 1 538 1 2 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 539 1 1 . . . . . . . . sbm1 37 . hb* parsed_1b4c 1 539 1 2 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 540 1 1 . . . . . . . . sbm2 37 . hb* parsed_1b4c 1 540 1 2 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 541 1 1 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 541 1 2 . . . . . . . . sbm1 39 . hn parsed_1b4c 1 542 1 1 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 542 1 2 . . . . . . . . sbm2 39 . hn parsed_1b4c 1 543 1 1 . . . . . . . . sbm1 38 . hb* parsed_1b4c 1 543 1 2 . . . . . . . . sbm1 39 . hn parsed_1b4c 1 544 1 1 . . . . . . . . sbm2 38 . hb* parsed_1b4c 1 544 1 2 . . . . . . . . sbm2 39 . hn parsed_1b4c 1 545 1 1 . . . . . . . . sbm1 39 . hn parsed_1b4c 1 545 1 2 . . . . . . . . sbm1 40 . hn parsed_1b4c 1 546 1 1 . . . . . . . . sbm2 39 . hn parsed_1b4c 1 546 1 2 . . . . . . . . sbm2 40 . hn parsed_1b4c 1 547 1 1 . . . . . . . . sbm1 39 . ha parsed_1b4c 1 547 1 2 . . . . . . . . sbm1 40 . hn parsed_1b4c 1 548 1 1 . . . . . . . . sbm2 39 . ha parsed_1b4c 1 548 1 2 . . . . . . . . sbm2 40 . hn parsed_1b4c 1 549 1 1 . . . . . . . . sbm1 39 . hb* parsed_1b4c 1 549 1 2 . . . . . . . . sbm1 40 . hn parsed_1b4c 1 550 1 1 . . . . . . . . sbm2 39 . hb* parsed_1b4c 1 550 1 2 . . . . . . . . sbm2 40 . hn parsed_1b4c 1 551 1 1 . . . . . . . . sbm1 40 . hn parsed_1b4c 1 551 1 2 . . . . . . . . sbm1 41 . hn parsed_1b4c 1 552 1 1 . . . . . . . . sbm2 40 . hn parsed_1b4c 1 552 1 2 . . . . . . . . sbm2 41 . hn parsed_1b4c 1 553 1 1 . . . . . . . . sbm1 40 . ha parsed_1b4c 1 553 1 2 . . . . . . . . sbm1 41 . hn parsed_1b4c 1 554 1 1 . . . . . . . . sbm2 40 . ha parsed_1b4c 1 554 1 2 . . . . . . . . sbm2 41 . hn parsed_1b4c 1 555 1 1 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 555 1 2 . . . . . . . . sbm1 41 . hn parsed_1b4c 1 556 1 1 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 556 1 2 . . . . . . . . sbm2 41 . hn parsed_1b4c 1 557 1 1 . . . . . . . . sbm1 41 . ha parsed_1b4c 1 557 1 2 . . . . . . . . sbm1 42 . hn parsed_1b4c 1 558 1 1 . . . . . . . . sbm2 41 . ha parsed_1b4c 1 558 1 2 . . . . . . . . sbm2 42 . hn parsed_1b4c 1 559 1 1 . . . . . . . . sbm1 41 . hb* parsed_1b4c 1 559 1 2 . . . . . . . . sbm1 42 . hn parsed_1b4c 1 560 1 1 . . . . . . . . sbm2 41 . hb* parsed_1b4c 1 560 1 2 . . . . . . . . sbm2 42 . hn parsed_1b4c 1 561 1 1 . . . . . . . . sbm1 43 . hn parsed_1b4c 1 561 1 2 . . . . . . . . sbm1 42 . hn parsed_1b4c 1 562 1 1 . . . . . . . . sbm2 43 . hn parsed_1b4c 1 562 1 2 . . . . . . . . sbm2 42 . hn parsed_1b4c 1 563 1 1 . . . . . . . . sbm1 44 . ha parsed_1b4c 1 563 1 2 . . . . . . . . sbm1 45 . hn parsed_1b4c 1 564 1 1 . . . . . . . . sbm2 44 . ha parsed_1b4c 1 564 1 2 . . . . . . . . sbm2 45 . hn parsed_1b4c 1 565 1 1 . . . . . . . . sbm1 44 . hb* parsed_1b4c 1 565 1 2 . . . . . . . . sbm1 45 . hn parsed_1b4c 1 566 1 1 . . . . . . . . sbm2 44 . hb* parsed_1b4c 1 566 1 2 . . . . . . . . sbm2 45 . hn parsed_1b4c 1 567 1 1 . . . . . . . . sbm1 45 . hn parsed_1b4c 1 567 1 2 . . . . . . . . sbm1 46 . hn parsed_1b4c 1 568 1 1 . . . . . . . . sbm2 45 . hn parsed_1b4c 1 568 1 2 . . . . . . . . sbm2 46 . hn parsed_1b4c 1 569 1 1 . . . . . . . . sbm1 45 . ha parsed_1b4c 1 569 1 2 . . . . . . . . sbm1 46 . hn parsed_1b4c 1 570 1 1 . . . . . . . . sbm2 45 . ha parsed_1b4c 1 570 1 2 . . . . . . . . sbm2 46 . hn parsed_1b4c 1 571 1 1 . . . . . . . . sbm1 45 . hb* parsed_1b4c 1 571 1 2 . . . . . . . . sbm1 46 . hn parsed_1b4c 1 572 1 1 . . . . . . . . sbm2 45 . hb* parsed_1b4c 1 572 1 2 . . . . . . . . sbm2 46 . hn parsed_1b4c 1 573 1 1 . . . . . . . . sbm1 47 . hn parsed_1b4c 1 573 1 2 . . . . . . . . sbm1 46 . hn parsed_1b4c 1 574 1 1 . . . . . . . . sbm2 47 . hn parsed_1b4c 1 574 1 2 . . . . . . . . sbm2 46 . hn parsed_1b4c 1 575 1 1 . . . . . . . . sbm1 48 . hn parsed_1b4c 1 575 1 2 . . . . . . . . sbm1 49 . hn parsed_1b4c 1 576 1 1 . . . . . . . . sbm2 48 . hn parsed_1b4c 1 576 1 2 . . . . . . . . sbm2 49 . hn parsed_1b4c 1 577 1 1 . . . . . . . . sbm1 48 . ha parsed_1b4c 1 577 1 2 . . . . . . . . sbm1 49 . hn parsed_1b4c 1 578 1 1 . . . . . . . . sbm2 48 . ha parsed_1b4c 1 578 1 2 . . . . . . . . sbm2 49 . hn parsed_1b4c 1 579 1 1 . . . . . . . . sbm1 48 . hb* parsed_1b4c 1 579 1 2 . . . . . . . . sbm1 49 . hn parsed_1b4c 1 580 1 1 . . . . . . . . sbm2 48 . hb* parsed_1b4c 1 580 1 2 . . . . . . . . sbm2 49 . hn parsed_1b4c 1 581 1 1 . . . . . . . . sbm1 48 . hg* parsed_1b4c 1 581 1 2 . . . . . . . . sbm1 49 . hn parsed_1b4c 1 582 1 1 . . . . . . . . sbm2 48 . hg* parsed_1b4c 1 582 1 2 . . . . . . . . sbm2 49 . hn parsed_1b4c 1 583 1 1 . . . . . . . . sbm1 49 . ha parsed_1b4c 1 583 1 2 . . . . . . . . sbm1 50 . hn parsed_1b4c 1 584 1 1 . . . . . . . . sbm2 49 . ha parsed_1b4c 1 584 1 2 . . . . . . . . sbm2 50 . hn parsed_1b4c 1 585 1 1 . . . . . . . . sbm1 51 . hn parsed_1b4c 1 585 1 2 . . . . . . . . sbm1 50 . hn parsed_1b4c 1 586 1 1 . . . . . . . . sbm2 51 . hn parsed_1b4c 1 586 1 2 . . . . . . . . sbm2 50 . hn parsed_1b4c 1 587 1 1 . . . . . . . . sbm1 50 . ha parsed_1b4c 1 587 1 2 . . . . . . . . sbm1 51 . hn parsed_1b4c 1 588 1 1 . . . . . . . . sbm2 50 . ha parsed_1b4c 1 588 1 2 . . . . . . . . sbm2 51 . hn parsed_1b4c 1 589 1 1 . . . . . . . . sbm1 52 . hn parsed_1b4c 1 589 1 2 . . . . . . . . sbm1 51 . hn parsed_1b4c 1 590 1 1 . . . . . . . . sbm2 52 . hn parsed_1b4c 1 590 1 2 . . . . . . . . sbm2 51 . hn parsed_1b4c 1 591 1 1 . . . . . . . . sbm1 51 . ha parsed_1b4c 1 591 1 2 . . . . . . . . sbm1 52 . hn parsed_1b4c 1 592 1 1 . . . . . . . . sbm2 51 . ha parsed_1b4c 1 592 1 2 . . . . . . . . sbm2 52 . hn parsed_1b4c 1 593 1 1 . . . . . . . . sbm1 52 . hn parsed_1b4c 1 593 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 594 1 1 . . . . . . . . sbm2 52 . hn parsed_1b4c 1 594 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 595 1 1 . . . . . . . . sbm1 52 . ha parsed_1b4c 1 595 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 596 1 1 . . . . . . . . sbm2 52 . ha parsed_1b4c 1 596 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 597 1 1 . . . . . . . . sbm1 52 . hb parsed_1b4c 1 597 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 598 1 1 . . . . . . . . sbm2 52 . hb parsed_1b4c 1 598 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 599 1 1 . . . . . . . . sbm1 52 . hg1* parsed_1b4c 1 599 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 600 1 1 . . . . . . . . sbm2 52 . hg1* parsed_1b4c 1 600 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 601 1 1 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 601 1 2 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 602 1 1 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 602 1 2 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 603 1 1 . . . . . . . . sbm1 53 . ha parsed_1b4c 1 603 1 2 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 604 1 1 . . . . . . . . sbm2 53 . ha parsed_1b4c 1 604 1 2 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 605 1 1 . . . . . . . . sbm1 53 . hb parsed_1b4c 1 605 1 2 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 606 1 1 . . . . . . . . sbm2 53 . hb parsed_1b4c 1 606 1 2 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 607 1 1 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 607 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 608 1 1 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 608 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 609 1 1 . . . . . . . . sbm1 54 . ha parsed_1b4c 1 609 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 610 1 1 . . . . . . . . sbm2 54 . ha parsed_1b4c 1 610 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 611 1 1 . . . . . . . . sbm1 54 . hb* parsed_1b4c 1 611 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 612 1 1 . . . . . . . . sbm2 54 . hb* parsed_1b4c 1 612 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 613 1 1 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 613 1 2 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 614 1 1 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 614 1 2 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 615 1 1 . . . . . . . . sbm1 55 . ha parsed_1b4c 1 615 1 2 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 616 1 1 . . . . . . . . sbm2 55 . ha parsed_1b4c 1 616 1 2 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 617 1 1 . . . . . . . . sbm1 55 . hb* parsed_1b4c 1 617 1 2 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 618 1 1 . . . . . . . . sbm2 55 . hb* parsed_1b4c 1 618 1 2 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 619 1 1 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 619 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 620 1 1 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 620 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 621 1 1 . . . . . . . . sbm1 56 . ha parsed_1b4c 1 621 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 622 1 1 . . . . . . . . sbm2 56 . ha parsed_1b4c 1 622 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 623 1 1 . . . . . . . . sbm1 56 . hb parsed_1b4c 1 623 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 624 1 1 . . . . . . . . sbm2 56 . hb parsed_1b4c 1 624 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 625 1 1 . . . . . . . . sbm1 56 . hg2* parsed_1b4c 1 625 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 626 1 1 . . . . . . . . sbm2 56 . hg2* parsed_1b4c 1 626 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 627 1 1 . . . . . . . . sbm1 56 . hg1* parsed_1b4c 1 627 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 628 1 1 . . . . . . . . sbm2 56 . hg1* parsed_1b4c 1 628 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 629 1 1 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 629 1 2 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 630 1 1 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 630 1 2 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 631 1 1 . . . . . . . . sbm1 57 . ha parsed_1b4c 1 631 1 2 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 632 1 1 . . . . . . . . sbm2 57 . ha parsed_1b4c 1 632 1 2 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 633 1 1 . . . . . . . . sbm1 57 . hb* parsed_1b4c 1 633 1 2 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 634 1 1 . . . . . . . . sbm2 57 . hb* parsed_1b4c 1 634 1 2 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 635 1 1 . . . . . . . . sbm1 57 . hg* parsed_1b4c 1 635 1 2 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 636 1 1 . . . . . . . . sbm2 57 . hg* parsed_1b4c 1 636 1 2 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 637 1 1 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 637 1 2 . . . . . . . . sbm1 59 . hn parsed_1b4c 1 638 1 1 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 638 1 2 . . . . . . . . sbm2 59 . hn parsed_1b4c 1 639 1 1 . . . . . . . . sbm1 58 . ha parsed_1b4c 1 639 1 2 . . . . . . . . sbm1 59 . hn parsed_1b4c 1 640 1 1 . . . . . . . . sbm2 58 . ha parsed_1b4c 1 640 1 2 . . . . . . . . sbm2 59 . hn parsed_1b4c 1 641 1 1 . . . . . . . . sbm1 58 . hb* parsed_1b4c 1 641 1 2 . . . . . . . . sbm1 59 . hn parsed_1b4c 1 642 1 1 . . . . . . . . sbm2 58 . hb* parsed_1b4c 1 642 1 2 . . . . . . . . sbm2 59 . hn parsed_1b4c 1 643 1 1 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 643 1 2 . . . . . . . . sbm1 59 . hn parsed_1b4c 1 644 1 1 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 644 1 2 . . . . . . . . sbm2 59 . hn parsed_1b4c 1 645 1 1 . . . . . . . . sbm1 59 . ha parsed_1b4c 1 645 1 2 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 646 1 1 . . . . . . . . sbm2 59 . ha parsed_1b4c 1 646 1 2 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 647 1 1 . . . . . . . . sbm1 59 . hb parsed_1b4c 1 647 1 2 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 648 1 1 . . . . . . . . sbm2 59 . hb parsed_1b4c 1 648 1 2 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 649 1 1 . . . . . . . . sbm1 59 . hg2* parsed_1b4c 1 649 1 2 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 650 1 1 . . . . . . . . sbm2 59 . hg2* parsed_1b4c 1 650 1 2 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 651 1 1 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 651 1 2 . . . . . . . . sbm1 61 . hn parsed_1b4c 1 652 1 1 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 652 1 2 . . . . . . . . sbm2 61 . hn parsed_1b4c 1 653 1 1 . . . . . . . . sbm1 60 . ha parsed_1b4c 1 653 1 2 . . . . . . . . sbm1 61 . hn parsed_1b4c 1 654 1 1 . . . . . . . . sbm2 60 . ha parsed_1b4c 1 654 1 2 . . . . . . . . sbm2 61 . hn parsed_1b4c 1 655 1 1 . . . . . . . . sbm1 60 . hb* parsed_1b4c 1 655 1 2 . . . . . . . . sbm1 61 . hn parsed_1b4c 1 656 1 1 . . . . . . . . sbm2 60 . hb* parsed_1b4c 1 656 1 2 . . . . . . . . sbm2 61 . hn parsed_1b4c 1 657 1 1 . . . . . . . . sbm1 61 . hn parsed_1b4c 1 657 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 658 1 1 . . . . . . . . sbm2 61 . hn parsed_1b4c 1 658 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 659 1 1 . . . . . . . . sbm1 61 . ha parsed_1b4c 1 659 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 660 1 1 . . . . . . . . sbm2 61 . ha parsed_1b4c 1 660 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 661 1 1 . . . . . . . . sbm1 61 . hb* parsed_1b4c 1 661 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 662 1 1 . . . . . . . . sbm2 61 . hb* parsed_1b4c 1 662 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 663 1 1 . . . . . . . . sbm1 63 . hn parsed_1b4c 1 663 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 664 1 1 . . . . . . . . sbm2 63 . hn parsed_1b4c 1 664 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 665 1 1 . . . . . . . . sbm1 62 . ha parsed_1b4c 1 665 1 2 . . . . . . . . sbm1 63 . hn parsed_1b4c 1 666 1 1 . . . . . . . . sbm2 62 . ha parsed_1b4c 1 666 1 2 . . . . . . . . sbm2 63 . hn parsed_1b4c 1 667 1 1 . . . . . . . . sbm1 62 . hb* parsed_1b4c 1 667 1 2 . . . . . . . . sbm1 63 . hn parsed_1b4c 1 668 1 1 . . . . . . . . sbm2 62 . hb* parsed_1b4c 1 668 1 2 . . . . . . . . sbm2 63 . hn parsed_1b4c 1 669 1 1 . . . . . . . . sbm1 62 . hg* parsed_1b4c 1 669 1 2 . . . . . . . . sbm1 63 . hn parsed_1b4c 1 670 1 1 . . . . . . . . sbm2 62 . hg* parsed_1b4c 1 670 1 2 . . . . . . . . sbm2 63 . hn parsed_1b4c 1 671 1 1 . . . . . . . . sbm1 63 . hn parsed_1b4c 1 671 1 2 . . . . . . . . sbm1 64 . hn parsed_1b4c 1 672 1 1 . . . . . . . . sbm2 63 . hn parsed_1b4c 1 672 1 2 . . . . . . . . sbm2 64 . hn parsed_1b4c 1 673 1 1 . . . . . . . . sbm1 63 . ha parsed_1b4c 1 673 1 2 . . . . . . . . sbm1 64 . hn parsed_1b4c 1 674 1 1 . . . . . . . . sbm2 63 . ha parsed_1b4c 1 674 1 2 . . . . . . . . sbm2 64 . hn parsed_1b4c 1 675 1 1 . . . . . . . . sbm1 63 . hb* parsed_1b4c 1 675 1 2 . . . . . . . . sbm1 64 . hn parsed_1b4c 1 676 1 1 . . . . . . . . sbm2 63 . hb* parsed_1b4c 1 676 1 2 . . . . . . . . sbm2 64 . hn parsed_1b4c 1 677 1 1 . . . . . . . . sbm1 64 . hn parsed_1b4c 1 677 1 2 . . . . . . . . sbm1 65 . hn parsed_1b4c 1 678 1 1 . . . . . . . . sbm2 64 . hn parsed_1b4c 1 678 1 2 . . . . . . . . sbm2 65 . hn parsed_1b4c 1 679 1 1 . . . . . . . . sbm1 64 . ha* parsed_1b4c 1 679 1 2 . . . . . . . . sbm1 65 . hn parsed_1b4c 1 680 1 1 . . . . . . . . sbm2 64 . ha* parsed_1b4c 1 680 1 2 . . . . . . . . sbm2 65 . hn parsed_1b4c 1 681 1 1 . . . . . . . . sbm1 65 . hn parsed_1b4c 1 681 1 2 . . . . . . . . sbm1 66 . hn parsed_1b4c 1 682 1 1 . . . . . . . . sbm2 65 . hn parsed_1b4c 1 682 1 2 . . . . . . . . sbm2 66 . hn parsed_1b4c 1 683 1 1 . . . . . . . . sbm1 65 . ha parsed_1b4c 1 683 1 2 . . . . . . . . sbm1 66 . hn parsed_1b4c 1 684 1 1 . . . . . . . . sbm2 65 . ha parsed_1b4c 1 684 1 2 . . . . . . . . sbm2 66 . hn parsed_1b4c 1 685 1 1 . . . . . . . . sbm1 65 . hb* parsed_1b4c 1 685 1 2 . . . . . . . . sbm1 66 . hn parsed_1b4c 1 686 1 1 . . . . . . . . sbm2 65 . hb* parsed_1b4c 1 686 1 2 . . . . . . . . sbm2 66 . hn parsed_1b4c 1 687 1 1 . . . . . . . . sbm1 66 . hn parsed_1b4c 1 687 1 2 . . . . . . . . sbm1 67 . hn parsed_1b4c 1 688 1 1 . . . . . . . . sbm2 66 . hn parsed_1b4c 1 688 1 2 . . . . . . . . sbm2 67 . hn parsed_1b4c 1 689 1 1 . . . . . . . . sbm1 66 . ha* parsed_1b4c 1 689 1 2 . . . . . . . . sbm1 67 . hn parsed_1b4c 1 690 1 1 . . . . . . . . sbm2 66 . ha* parsed_1b4c 1 690 1 2 . . . . . . . . sbm2 67 . hn parsed_1b4c 1 691 1 1 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 691 1 2 . . . . . . . . sbm1 67 . hn parsed_1b4c 1 692 1 1 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 692 1 2 . . . . . . . . sbm2 67 . hn parsed_1b4c 1 693 1 1 . . . . . . . . sbm1 67 . ha parsed_1b4c 1 693 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 694 1 1 . . . . . . . . sbm2 67 . ha parsed_1b4c 1 694 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 695 1 1 . . . . . . . . sbm1 67 . hb* parsed_1b4c 1 695 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 696 1 1 . . . . . . . . sbm2 67 . hb* parsed_1b4c 1 696 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 697 1 1 . . . . . . . . sbm1 72 . hb* parsed_1b4c 1 697 1 2 . . . . . . . . sbm1 68 . ha parsed_1b4c 1 698 1 1 . . . . . . . . sbm2 72 . hb* parsed_1b4c 1 698 1 2 . . . . . . . . sbm2 68 . ha parsed_1b4c 1 699 1 1 . . . . . . . . sbm1 67 . hg* parsed_1b4c 1 699 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 700 1 1 . . . . . . . . sbm2 67 . hg* parsed_1b4c 1 700 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 701 1 1 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 701 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 702 1 1 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 702 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 703 1 1 . . . . . . . . sbm1 68 . ha parsed_1b4c 1 703 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 704 1 1 . . . . . . . . sbm2 68 . ha parsed_1b4c 1 704 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 705 1 1 . . . . . . . . sbm1 68 . hb* parsed_1b4c 1 705 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 706 1 1 . . . . . . . . sbm2 68 . hb* parsed_1b4c 1 706 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 707 1 1 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 707 1 2 . . . . . . . . sbm1 70 . hn parsed_1b4c 1 708 1 1 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 708 1 2 . . . . . . . . sbm2 70 . hn parsed_1b4c 1 709 1 1 . . . . . . . . sbm1 69 . ha parsed_1b4c 1 709 1 2 . . . . . . . . sbm1 70 . hn parsed_1b4c 1 710 1 1 . . . . . . . . sbm2 69 . ha parsed_1b4c 1 710 1 2 . . . . . . . . sbm2 70 . hn parsed_1b4c 1 711 1 1 . . . . . . . . sbm1 69 . hb* parsed_1b4c 1 711 1 2 . . . . . . . . sbm1 70 . hn parsed_1b4c 1 712 1 1 . . . . . . . . sbm2 69 . hb* parsed_1b4c 1 712 1 2 . . . . . . . . sbm2 70 . hn parsed_1b4c 1 713 1 1 . . . . . . . . sbm1 70 . hn parsed_1b4c 1 713 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 714 1 1 . . . . . . . . sbm2 70 . hn parsed_1b4c 1 714 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 715 1 1 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 715 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 716 1 1 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 716 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 717 1 1 . . . . . . . . sbm1 69 . ha parsed_1b4c 1 717 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 718 1 1 . . . . . . . . sbm2 69 . ha parsed_1b4c 1 718 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 719 1 1 . . . . . . . . sbm1 70 . hb* parsed_1b4c 1 719 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 720 1 1 . . . . . . . . sbm2 70 . hb* parsed_1b4c 1 720 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 721 1 1 . . . . . . . . sbm1 70 . hd* parsed_1b4c 1 721 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 722 1 1 . . . . . . . . sbm2 70 . hd* parsed_1b4c 1 722 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 723 1 1 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 723 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 724 1 1 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 724 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 725 1 1 . . . . . . . . sbm1 71 . ha parsed_1b4c 1 725 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 726 1 1 . . . . . . . . sbm2 71 . ha parsed_1b4c 1 726 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 727 1 1 . . . . . . . . sbm1 71 . hb* parsed_1b4c 1 727 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 728 1 1 . . . . . . . . sbm2 71 . hb* parsed_1b4c 1 728 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 729 1 1 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 729 1 2 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 730 1 1 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 730 1 2 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 731 1 1 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 731 1 2 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 732 1 1 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 732 1 2 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 733 1 1 . . . . . . . . sbm1 72 . hb* parsed_1b4c 1 733 1 2 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 734 1 1 . . . . . . . . sbm2 72 . hb* parsed_1b4c 1 734 1 2 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 735 1 1 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 735 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 736 1 1 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 736 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 737 1 1 . . . . . . . . sbm1 73 . ha parsed_1b4c 1 737 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 738 1 1 . . . . . . . . sbm2 73 . ha parsed_1b4c 1 738 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 739 1 1 . . . . . . . . sbm1 73 . hb* parsed_1b4c 1 739 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 740 1 1 . . . . . . . . sbm2 73 . hb* parsed_1b4c 1 740 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 741 1 1 . . . . . . . . sbm1 73 . hd* parsed_1b4c 1 741 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 742 1 1 . . . . . . . . sbm2 73 . hd* parsed_1b4c 1 742 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 743 1 1 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 743 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 744 1 1 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 744 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 745 1 1 . . . . . . . . sbm1 74 . ha parsed_1b4c 1 745 1 2 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 746 1 1 . . . . . . . . sbm2 74 . ha parsed_1b4c 1 746 1 2 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 747 1 1 . . . . . . . . sbm1 74 . hb* parsed_1b4c 1 747 1 2 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 748 1 1 . . . . . . . . sbm2 74 . hb* parsed_1b4c 1 748 1 2 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 749 1 1 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 749 1 2 . . . . . . . . sbm1 76 . hn parsed_1b4c 1 750 1 1 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 750 1 2 . . . . . . . . sbm2 76 . hn parsed_1b4c 1 751 1 1 . . . . . . . . sbm1 75 . ha parsed_1b4c 1 751 1 2 . . . . . . . . sbm1 76 . hn parsed_1b4c 1 752 1 1 . . . . . . . . sbm2 75 . ha parsed_1b4c 1 752 1 2 . . . . . . . . sbm2 76 . hn parsed_1b4c 1 753 1 1 . . . . . . . . sbm1 75 . hb* parsed_1b4c 1 753 1 2 . . . . . . . . sbm1 76 . hn parsed_1b4c 1 754 1 1 . . . . . . . . sbm2 75 . hb* parsed_1b4c 1 754 1 2 . . . . . . . . sbm2 76 . hn parsed_1b4c 1 755 1 1 . . . . . . . . sbm1 76 . hn parsed_1b4c 1 755 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 756 1 1 . . . . . . . . sbm2 76 . hn parsed_1b4c 1 756 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 757 1 1 . . . . . . . . sbm1 76 . ha parsed_1b4c 1 757 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 758 1 1 . . . . . . . . sbm2 76 . ha parsed_1b4c 1 758 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 759 1 1 . . . . . . . . sbm1 76 . hb* parsed_1b4c 1 759 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 760 1 1 . . . . . . . . sbm2 76 . hb* parsed_1b4c 1 760 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 761 1 1 . . . . . . . . sbm1 76 . hd* parsed_1b4c 1 761 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 762 1 1 . . . . . . . . sbm2 76 . hd* parsed_1b4c 1 762 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 763 1 1 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 763 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 764 1 1 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 764 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 765 1 1 . . . . . . . . sbm1 77 . ha parsed_1b4c 1 765 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 766 1 1 . . . . . . . . sbm2 77 . ha parsed_1b4c 1 766 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 767 1 1 . . . . . . . . sbm1 77 . hb parsed_1b4c 1 767 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 768 1 1 . . . . . . . . sbm2 77 . hb parsed_1b4c 1 768 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 769 1 1 . . . . . . . . sbm1 77 . hg1* parsed_1b4c 1 769 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 770 1 1 . . . . . . . . sbm2 77 . hg1* parsed_1b4c 1 770 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 771 1 1 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 771 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 772 1 1 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 772 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 773 1 1 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 773 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 774 1 1 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 774 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 775 1 1 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 775 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 776 1 1 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 776 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 777 1 1 . . . . . . . . sbm1 78 . ha parsed_1b4c 1 777 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 778 1 1 . . . . . . . . sbm2 78 . ha parsed_1b4c 1 778 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 779 1 1 . . . . . . . . sbm1 78 . hb* parsed_1b4c 1 779 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 780 1 1 . . . . . . . . sbm2 78 . hb* parsed_1b4c 1 780 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 781 1 1 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 781 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 782 1 1 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 782 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 783 1 1 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 783 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 784 1 1 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 784 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 785 1 1 . . . . . . . . sbm1 79 . ha parsed_1b4c 1 785 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 786 1 1 . . . . . . . . sbm2 79 . ha parsed_1b4c 1 786 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 787 1 1 . . . . . . . . sbm1 79 . hb* parsed_1b4c 1 787 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 788 1 1 . . . . . . . . sbm2 79 . hb* parsed_1b4c 1 788 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 789 1 1 . . . . . . . . sbm1 79 . hb* parsed_1b4c 1 789 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 790 1 1 . . . . . . . . sbm2 79 . hb* parsed_1b4c 1 790 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 791 1 1 . . . . . . . . sbm1 79 . hb* parsed_1b4c 1 791 1 2 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 792 1 1 . . . . . . . . sbm2 79 . hb* parsed_1b4c 1 792 1 2 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 793 1 1 . . . . . . . . sbm1 79 . hg* parsed_1b4c 1 793 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 794 1 1 . . . . . . . . sbm2 79 . hg* parsed_1b4c 1 794 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 795 1 1 . . . . . . . . sbm1 79 . hg* parsed_1b4c 1 795 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 796 1 1 . . . . . . . . sbm2 79 . hg* parsed_1b4c 1 796 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 797 1 1 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 797 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 798 1 1 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 798 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 799 1 1 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 799 1 2 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 800 1 1 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 800 1 2 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 801 1 1 . . . . . . . . sbm1 80 . ha parsed_1b4c 1 801 1 2 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 802 1 1 . . . . . . . . sbm2 80 . ha parsed_1b4c 1 802 1 2 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 803 1 1 . . . . . . . . sbm1 80 . hb parsed_1b4c 1 803 1 2 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 804 1 1 . . . . . . . . sbm2 80 . hb parsed_1b4c 1 804 1 2 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 805 1 1 . . . . . . . . sbm1 80 . hg1* parsed_1b4c 1 805 1 2 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 806 1 1 . . . . . . . . sbm2 80 . hg1* parsed_1b4c 1 806 1 2 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 807 1 1 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 807 1 2 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 808 1 1 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 808 1 2 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 809 1 1 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 809 1 2 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 810 1 1 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 810 1 2 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 811 1 1 . . . . . . . . sbm1 81 . hb parsed_1b4c 1 811 1 2 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 812 1 1 . . . . . . . . sbm2 81 . hb parsed_1b4c 1 812 1 2 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 813 1 1 . . . . . . . . sbm1 81 . ha parsed_1b4c 1 813 1 2 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 814 1 1 . . . . . . . . sbm2 81 . ha parsed_1b4c 1 814 1 2 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 815 1 1 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 815 1 2 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 816 1 1 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 816 1 2 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 817 1 1 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 817 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 818 1 1 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 818 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 819 1 1 . . . . . . . . sbm1 82 . ha parsed_1b4c 1 819 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 820 1 1 . . . . . . . . sbm2 82 . ha parsed_1b4c 1 820 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 821 1 1 . . . . . . . . sbm1 82 . hb parsed_1b4c 1 821 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 822 1 1 . . . . . . . . sbm2 82 . hb parsed_1b4c 1 822 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 823 1 1 . . . . . . . . sbm1 82 . hg2* parsed_1b4c 1 823 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 824 1 1 . . . . . . . . sbm2 82 . hg2* parsed_1b4c 1 824 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 825 1 1 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 825 1 2 . . . . . . . . sbm1 84 . hn parsed_1b4c 1 826 1 1 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 826 1 2 . . . . . . . . sbm2 84 . hn parsed_1b4c 1 827 1 1 . . . . . . . . sbm1 83 . ha parsed_1b4c 1 827 1 2 . . . . . . . . sbm1 84 . hn parsed_1b4c 1 828 1 1 . . . . . . . . sbm2 83 . ha parsed_1b4c 1 828 1 2 . . . . . . . . sbm2 84 . hn parsed_1b4c 1 829 1 1 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 829 1 2 . . . . . . . . sbm1 84 . hn parsed_1b4c 1 830 1 1 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 830 1 2 . . . . . . . . sbm2 84 . hn parsed_1b4c 1 831 1 1 . . . . . . . . sbm1 87 . ha parsed_1b4c 1 831 1 2 . . . . . . . . sbm1 88 . hn parsed_1b4c 1 832 1 1 . . . . . . . . sbm2 87 . ha parsed_1b4c 1 832 1 2 . . . . . . . . sbm2 88 . hn parsed_1b4c 1 833 1 1 . . . . . . . . sbm1 87 . hb* parsed_1b4c 1 833 1 2 . . . . . . . . sbm1 88 . hn parsed_1b4c 1 834 1 1 . . . . . . . . sbm2 87 . hb* parsed_1b4c 1 834 1 2 . . . . . . . . sbm2 88 . hn parsed_1b4c 1 835 1 1 . . . . . . . . sbm1 87 . hd* parsed_1b4c 1 835 1 2 . . . . . . . . sbm1 88 . hn parsed_1b4c 1 836 1 1 . . . . . . . . sbm2 87 . hd* parsed_1b4c 1 836 1 2 . . . . . . . . sbm2 88 . hn parsed_1b4c 1 837 1 1 . . . . . . . . sbm1 87 . he* parsed_1b4c 1 837 1 2 . . . . . . . . sbm1 88 . he* parsed_1b4c 1 838 1 1 . . . . . . . . sbm2 87 . he* parsed_1b4c 1 838 1 2 . . . . . . . . sbm2 88 . he* parsed_1b4c 1 839 1 1 . . . . . . . . sbm1 88 . hn parsed_1b4c 1 839 1 2 . . . . . . . . sbm1 89 . hn parsed_1b4c 1 840 1 1 . . . . . . . . sbm2 88 . hn parsed_1b4c 1 840 1 2 . . . . . . . . sbm2 89 . hn parsed_1b4c 1 841 1 1 . . . . . . . . sbm1 88 . ha parsed_1b4c 1 841 1 2 . . . . . . . . sbm1 89 . hn parsed_1b4c 1 842 1 1 . . . . . . . . sbm2 88 . ha parsed_1b4c 1 842 1 2 . . . . . . . . sbm2 89 . hn parsed_1b4c 1 843 1 1 . . . . . . . . sbm1 88 . hb* parsed_1b4c 1 843 1 2 . . . . . . . . sbm1 89 . hn parsed_1b4c 1 844 1 1 . . . . . . . . sbm2 88 . hb* parsed_1b4c 1 844 1 2 . . . . . . . . sbm2 89 . hn parsed_1b4c 1 845 1 1 . . . . . . . . sbm1 88 . hd* parsed_1b4c 1 845 1 2 . . . . . . . . sbm1 89 . hn parsed_1b4c 1 846 1 1 . . . . . . . . sbm2 88 . hd* parsed_1b4c 1 846 1 2 . . . . . . . . sbm2 89 . hn parsed_1b4c 1 847 1 1 . . . . . . . . sbm1 90 . hn parsed_1b4c 1 847 1 2 . . . . . . . . sbm1 89 . hn parsed_1b4c 1 848 1 1 . . . . . . . . sbm2 90 . hn parsed_1b4c 1 848 1 2 . . . . . . . . sbm2 89 . hn parsed_1b4c 1 849 1 1 . . . . . . . . sbm1 89 . ha parsed_1b4c 1 849 1 2 . . . . . . . . sbm1 90 . hn parsed_1b4c 1 850 1 1 . . . . . . . . sbm2 89 . ha parsed_1b4c 1 850 1 2 . . . . . . . . sbm2 90 . hn parsed_1b4c 1 851 1 1 . . . . . . . . sbm1 90 . ha parsed_1b4c 1 851 1 2 . . . . . . . . sbm1 91 . hn parsed_1b4c 1 852 1 1 . . . . . . . . sbm2 90 . ha parsed_1b4c 1 852 1 2 . . . . . . . . sbm2 91 . hn parsed_1b4c 1 853 1 1 . . . . . . . . sbm1 90 . hb* parsed_1b4c 1 853 1 2 . . . . . . . . sbm1 91 . hn parsed_1b4c 1 854 1 1 . . . . . . . . sbm2 90 . hb* parsed_1b4c 1 854 1 2 . . . . . . . . sbm2 91 . hn parsed_1b4c 1 855 1 1 . . . . . . . . sbm1 3 . hn parsed_1b4c 1 855 1 2 . . . . . . . . sbm1 1 . hn parsed_1b4c 1 856 1 1 . . . . . . . . sbm2 3 . hn parsed_1b4c 1 856 1 2 . . . . . . . . sbm2 1 . hn parsed_1b4c 1 857 1 1 . . . . . . . . sbm1 4 . hn parsed_1b4c 1 857 1 2 . . . . . . . . sbm1 2 . hn parsed_1b4c 1 858 1 1 . . . . . . . . sbm2 4 . hn parsed_1b4c 1 858 1 2 . . . . . . . . sbm2 2 . hn parsed_1b4c 1 859 1 1 . . . . . . . . sbm1 5 . hb* parsed_1b4c 1 859 1 2 . . . . . . . . sbm1 2 . ha parsed_1b4c 1 860 1 1 . . . . . . . . sbm2 5 . hb* parsed_1b4c 1 860 1 2 . . . . . . . . sbm2 2 . ha parsed_1b4c 1 861 1 1 . . . . . . . . sbm1 6 . hb* parsed_1b4c 1 861 1 2 . . . . . . . . sbm1 3 . ha parsed_1b4c 1 862 1 1 . . . . . . . . sbm2 6 . hb* parsed_1b4c 1 862 1 2 . . . . . . . . sbm2 3 . ha parsed_1b4c 1 863 1 1 . . . . . . . . sbm1 2 . ha parsed_1b4c 1 863 1 2 . . . . . . . . sbm1 4 . hn parsed_1b4c 1 864 1 1 . . . . . . . . sbm2 2 . ha parsed_1b4c 1 864 1 2 . . . . . . . . sbm2 4 . hn parsed_1b4c 1 865 1 1 . . . . . . . . sbm1 7 . hb* parsed_1b4c 1 865 1 2 . . . . . . . . sbm1 4 . ha parsed_1b4c 1 866 1 1 . . . . . . . . sbm2 7 . hb* parsed_1b4c 1 866 1 2 . . . . . . . . sbm2 4 . ha parsed_1b4c 1 867 1 1 . . . . . . . . sbm1 2 . ha parsed_1b4c 1 867 1 2 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 868 1 1 . . . . . . . . sbm2 2 . ha parsed_1b4c 1 868 1 2 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 869 1 1 . . . . . . . . sbm1 3 . ha parsed_1b4c 1 869 1 2 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 870 1 1 . . . . . . . . sbm2 3 . ha parsed_1b4c 1 870 1 2 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 871 1 1 . . . . . . . . sbm1 8 . hb parsed_1b4c 1 871 1 2 . . . . . . . . sbm1 5 . ha parsed_1b4c 1 872 1 1 . . . . . . . . sbm2 8 . hb parsed_1b4c 1 872 1 2 . . . . . . . . sbm2 5 . ha parsed_1b4c 1 873 1 1 . . . . . . . . sbm1 2 . ha parsed_1b4c 1 873 1 2 . . . . . . . . sbm1 6 . hn parsed_1b4c 1 874 1 1 . . . . . . . . sbm2 2 . ha parsed_1b4c 1 874 1 2 . . . . . . . . sbm2 6 . hn parsed_1b4c 1 875 1 1 . . . . . . . . sbm1 3 . ha parsed_1b4c 1 875 1 2 . . . . . . . . sbm1 6 . hn parsed_1b4c 1 876 1 1 . . . . . . . . sbm2 3 . ha parsed_1b4c 1 876 1 2 . . . . . . . . sbm2 6 . hn parsed_1b4c 1 877 1 1 . . . . . . . . sbm1 4 . hn parsed_1b4c 1 877 1 2 . . . . . . . . sbm1 6 . hn parsed_1b4c 1 878 1 1 . . . . . . . . sbm2 4 . hn parsed_1b4c 1 878 1 2 . . . . . . . . sbm2 6 . hn parsed_1b4c 1 879 1 1 . . . . . . . . sbm1 9 . hb* parsed_1b4c 1 879 1 2 . . . . . . . . sbm1 6 . ha parsed_1b4c 1 880 1 1 . . . . . . . . sbm2 9 . hb* parsed_1b4c 1 880 1 2 . . . . . . . . sbm2 6 . ha parsed_1b4c 1 881 1 1 . . . . . . . . sbm1 3 . ha parsed_1b4c 1 881 1 2 . . . . . . . . sbm1 7 . hn parsed_1b4c 1 882 1 1 . . . . . . . . sbm2 3 . ha parsed_1b4c 1 882 1 2 . . . . . . . . sbm2 7 . hn parsed_1b4c 1 883 1 1 . . . . . . . . sbm1 4 . ha parsed_1b4c 1 883 1 2 . . . . . . . . sbm1 7 . hn parsed_1b4c 1 884 1 1 . . . . . . . . sbm2 4 . ha parsed_1b4c 1 884 1 2 . . . . . . . . sbm2 7 . hn parsed_1b4c 1 885 1 1 . . . . . . . . sbm1 5 . hn parsed_1b4c 1 885 1 2 . . . . . . . . sbm1 7 . hn parsed_1b4c 1 886 1 1 . . . . . . . . sbm2 5 . hn parsed_1b4c 1 886 1 2 . . . . . . . . sbm2 7 . hn parsed_1b4c 1 887 1 1 . . . . . . . . sbm1 5 . ha parsed_1b4c 1 887 1 2 . . . . . . . . sbm1 7 . hn parsed_1b4c 1 888 1 1 . . . . . . . . sbm2 5 . ha parsed_1b4c 1 888 1 2 . . . . . . . . sbm2 7 . hn parsed_1b4c 1 889 1 1 . . . . . . . . sbm1 5 . ha parsed_1b4c 1 889 1 2 . . . . . . . . sbm1 8 . hn parsed_1b4c 1 890 1 1 . . . . . . . . sbm2 5 . ha parsed_1b4c 1 890 1 2 . . . . . . . . sbm2 8 . hn parsed_1b4c 1 891 1 1 . . . . . . . . sbm1 11 . hb parsed_1b4c 1 891 1 2 . . . . . . . . sbm1 8 . ha parsed_1b4c 1 892 1 1 . . . . . . . . sbm2 11 . hb parsed_1b4c 1 892 1 2 . . . . . . . . sbm2 8 . ha parsed_1b4c 1 893 1 1 . . . . . . . . sbm1 5 . ha parsed_1b4c 1 893 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 894 1 1 . . . . . . . . sbm2 5 . ha parsed_1b4c 1 894 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 895 1 1 . . . . . . . . sbm1 6 . ha parsed_1b4c 1 895 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 896 1 1 . . . . . . . . sbm2 6 . ha parsed_1b4c 1 896 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 897 1 1 . . . . . . . . sbm1 7 . hn parsed_1b4c 1 897 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 898 1 1 . . . . . . . . sbm2 7 . hn parsed_1b4c 1 898 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 899 1 1 . . . . . . . . sbm1 11 . hn parsed_1b4c 1 899 1 2 . . . . . . . . sbm1 9 . hn parsed_1b4c 1 900 1 1 . . . . . . . . sbm2 11 . hn parsed_1b4c 1 900 1 2 . . . . . . . . sbm2 9 . hn parsed_1b4c 1 901 1 1 . . . . . . . . sbm1 12 . hb* parsed_1b4c 1 901 1 2 . . . . . . . . sbm1 9 . ha parsed_1b4c 1 902 1 1 . . . . . . . . sbm2 12 . hb* parsed_1b4c 1 902 1 2 . . . . . . . . sbm2 9 . ha parsed_1b4c 1 903 1 1 . . . . . . . . sbm1 6 . ha parsed_1b4c 1 903 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 904 1 1 . . . . . . . . sbm2 6 . ha parsed_1b4c 1 904 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 905 1 1 . . . . . . . . sbm1 7 . ha parsed_1b4c 1 905 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 906 1 1 . . . . . . . . sbm2 7 . ha parsed_1b4c 1 906 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 907 1 1 . . . . . . . . sbm1 7 . ha parsed_1b4c 1 907 1 2 . . . . . . . . sbm1 10 . hb* parsed_1b4c 1 908 1 1 . . . . . . . . sbm2 7 . ha parsed_1b4c 1 908 1 2 . . . . . . . . sbm2 10 . hb* parsed_1b4c 1 909 1 1 . . . . . . . . sbm1 7 . ha parsed_1b4c 1 909 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 910 1 1 . . . . . . . . sbm2 7 . ha parsed_1b4c 1 910 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 911 1 1 . . . . . . . . sbm1 8 . ha parsed_1b4c 1 911 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 912 1 1 . . . . . . . . sbm2 8 . ha parsed_1b4c 1 912 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 913 1 1 . . . . . . . . sbm1 8 . hn parsed_1b4c 1 913 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 914 1 1 . . . . . . . . sbm2 8 . hn parsed_1b4c 1 914 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 915 1 1 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 915 1 2 . . . . . . . . sbm1 10 . hn parsed_1b4c 1 916 1 1 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 916 1 2 . . . . . . . . sbm2 10 . hn parsed_1b4c 1 917 1 1 . . . . . . . . sbm1 13 . hb parsed_1b4c 1 917 1 2 . . . . . . . . sbm1 10 . ha parsed_1b4c 1 918 1 1 . . . . . . . . sbm2 13 . hb parsed_1b4c 1 918 1 2 . . . . . . . . sbm2 10 . ha parsed_1b4c 1 919 1 1 . . . . . . . . sbm1 13 . hb parsed_1b4c 1 919 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 920 1 1 . . . . . . . . sbm2 13 . hb parsed_1b4c 1 920 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 921 1 1 . . . . . . . . sbm1 13 . hg* parsed_1b4c 1 921 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 922 1 1 . . . . . . . . sbm2 13 . hg* parsed_1b4c 1 922 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 923 1 1 . . . . . . . . sbm1 8 . ha parsed_1b4c 1 923 1 2 . . . . . . . . sbm1 11 . hn parsed_1b4c 1 924 1 1 . . . . . . . . sbm2 8 . ha parsed_1b4c 1 924 1 2 . . . . . . . . sbm2 11 . hn parsed_1b4c 1 925 1 1 . . . . . . . . sbm1 9 . ha parsed_1b4c 1 925 1 2 . . . . . . . . sbm1 11 . hn parsed_1b4c 1 926 1 1 . . . . . . . . sbm2 9 . ha parsed_1b4c 1 926 1 2 . . . . . . . . sbm2 11 . hn parsed_1b4c 1 927 1 1 . . . . . . . . sbm1 8 . ha parsed_1b4c 1 927 1 2 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 928 1 1 . . . . . . . . sbm2 8 . ha parsed_1b4c 1 928 1 2 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 929 1 1 . . . . . . . . sbm1 9 . ha parsed_1b4c 1 929 1 2 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 930 1 1 . . . . . . . . sbm2 9 . ha parsed_1b4c 1 930 1 2 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 931 1 1 . . . . . . . . sbm1 10 . ha parsed_1b4c 1 931 1 2 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 932 1 1 . . . . . . . . sbm2 10 . ha parsed_1b4c 1 932 1 2 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 933 1 1 . . . . . . . . sbm1 15 . hb* parsed_1b4c 1 933 1 2 . . . . . . . . sbm1 12 . ha parsed_1b4c 1 934 1 1 . . . . . . . . sbm2 15 . hb* parsed_1b4c 1 934 1 2 . . . . . . . . sbm2 12 . ha parsed_1b4c 1 935 1 1 . . . . . . . . sbm1 9 . ha parsed_1b4c 1 935 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 936 1 1 . . . . . . . . sbm2 9 . ha parsed_1b4c 1 936 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 937 1 1 . . . . . . . . sbm1 10 . ha parsed_1b4c 1 937 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 938 1 1 . . . . . . . . sbm2 10 . ha parsed_1b4c 1 938 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 939 1 1 . . . . . . . . sbm1 11 . hn parsed_1b4c 1 939 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 940 1 1 . . . . . . . . sbm2 11 . hn parsed_1b4c 1 940 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 941 1 1 . . . . . . . . sbm1 11 . ha parsed_1b4c 1 941 1 2 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 942 1 1 . . . . . . . . sbm2 11 . ha parsed_1b4c 1 942 1 2 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 943 1 1 . . . . . . . . sbm1 16 . hb* parsed_1b4c 1 943 1 2 . . . . . . . . sbm1 13 . ha parsed_1b4c 1 944 1 1 . . . . . . . . sbm2 16 . hb* parsed_1b4c 1 944 1 2 . . . . . . . . sbm2 13 . ha parsed_1b4c 1 945 1 1 . . . . . . . . sbm1 16 . hg* parsed_1b4c 1 945 1 2 . . . . . . . . sbm1 13 . hg1* parsed_1b4c 1 946 1 1 . . . . . . . . sbm2 16 . hg* parsed_1b4c 1 946 1 2 . . . . . . . . sbm2 13 . hg1* parsed_1b4c 1 947 1 1 . . . . . . . . sbm1 17 . hd* parsed_1b4c 1 947 1 2 . . . . . . . . sbm1 13 . hg1* parsed_1b4c 1 948 1 1 . . . . . . . . sbm2 17 . hd* parsed_1b4c 1 948 1 2 . . . . . . . . sbm2 13 . hg1* parsed_1b4c 1 949 1 1 . . . . . . . . sbm1 10 . ha parsed_1b4c 1 949 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 950 1 1 . . . . . . . . sbm2 10 . ha parsed_1b4c 1 950 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 951 1 1 . . . . . . . . sbm1 11 . ha parsed_1b4c 1 951 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 952 1 1 . . . . . . . . sbm2 11 . ha parsed_1b4c 1 952 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 953 1 1 . . . . . . . . sbm1 11 . ha parsed_1b4c 1 953 1 2 . . . . . . . . sbm1 14 . hb* parsed_1b4c 1 954 1 1 . . . . . . . . sbm2 11 . ha parsed_1b4c 1 954 1 2 . . . . . . . . sbm2 14 . hb* parsed_1b4c 1 955 1 1 . . . . . . . . sbm1 12 . hn parsed_1b4c 1 955 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 956 1 1 . . . . . . . . sbm2 12 . hn parsed_1b4c 1 956 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 957 1 1 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 957 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 958 1 1 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 958 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 959 1 1 . . . . . . . . sbm1 17 . hb* parsed_1b4c 1 959 1 2 . . . . . . . . sbm1 14 . ha parsed_1b4c 1 960 1 1 . . . . . . . . sbm2 17 . hb* parsed_1b4c 1 960 1 2 . . . . . . . . sbm2 14 . ha parsed_1b4c 1 961 1 1 . . . . . . . . sbm1 11 . ha parsed_1b4c 1 961 1 2 . . . . . . . . sbm1 15 . hn parsed_1b4c 1 962 1 1 . . . . . . . . sbm2 11 . ha parsed_1b4c 1 962 1 2 . . . . . . . . sbm2 15 . hn parsed_1b4c 1 963 1 1 . . . . . . . . sbm1 13 . hn parsed_1b4c 1 963 1 2 . . . . . . . . sbm1 15 . hn parsed_1b4c 1 964 1 1 . . . . . . . . sbm2 13 . hn parsed_1b4c 1 964 1 2 . . . . . . . . sbm2 15 . hn parsed_1b4c 1 965 1 1 . . . . . . . . sbm1 13 . ha parsed_1b4c 1 965 1 2 . . . . . . . . sbm1 15 . hn parsed_1b4c 1 966 1 1 . . . . . . . . sbm2 13 . ha parsed_1b4c 1 966 1 2 . . . . . . . . sbm2 15 . hn parsed_1b4c 1 967 1 1 . . . . . . . . sbm1 13 . ha parsed_1b4c 1 967 1 2 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 968 1 1 . . . . . . . . sbm2 13 . ha parsed_1b4c 1 968 1 2 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 969 1 1 . . . . . . . . sbm1 13 . hg1* parsed_1b4c 1 969 1 2 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 970 1 1 . . . . . . . . sbm2 13 . hg1* parsed_1b4c 1 970 1 2 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 971 1 1 . . . . . . . . sbm1 13 . ha parsed_1b4c 1 971 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 972 1 1 . . . . . . . . sbm2 13 . ha parsed_1b4c 1 972 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 973 1 1 . . . . . . . . sbm1 15 . ha parsed_1b4c 1 973 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 974 1 1 . . . . . . . . sbm2 15 . ha parsed_1b4c 1 974 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 975 1 1 . . . . . . . . sbm1 15 . ha parsed_1b4c 1 975 1 2 . . . . . . . . sbm1 18 . hn parsed_1b4c 1 976 1 1 . . . . . . . . sbm2 15 . ha parsed_1b4c 1 976 1 2 . . . . . . . . sbm2 18 . hn parsed_1b4c 1 977 1 1 . . . . . . . . sbm1 16 . hn parsed_1b4c 1 977 1 2 . . . . . . . . sbm1 18 . hn parsed_1b4c 1 978 1 1 . . . . . . . . sbm2 16 . hn parsed_1b4c 1 978 1 2 . . . . . . . . sbm2 18 . hn parsed_1b4c 1 979 1 1 . . . . . . . . sbm1 24 . ha parsed_1b4c 1 979 1 2 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 980 1 1 . . . . . . . . sbm2 24 . ha parsed_1b4c 1 980 1 2 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 981 1 1 . . . . . . . . sbm1 31 . hb* parsed_1b4c 1 981 1 2 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 982 1 1 . . . . . . . . sbm2 31 . hb* parsed_1b4c 1 982 1 2 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 983 1 1 . . . . . . . . sbm1 32 . ha parsed_1b4c 1 983 1 2 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 984 1 1 . . . . . . . . sbm2 32 . ha parsed_1b4c 1 984 1 2 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 985 1 1 . . . . . . . . sbm1 31 . hn parsed_1b4c 1 985 1 2 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 986 1 1 . . . . . . . . sbm2 31 . hn parsed_1b4c 1 986 1 2 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 987 1 1 . . . . . . . . sbm1 28 . ha parsed_1b4c 1 987 1 2 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 988 1 1 . . . . . . . . sbm2 28 . ha parsed_1b4c 1 988 1 2 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 989 1 1 . . . . . . . . sbm1 28 . hb* parsed_1b4c 1 989 1 2 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 990 1 1 . . . . . . . . sbm2 28 . hb* parsed_1b4c 1 990 1 2 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 991 1 1 . . . . . . . . sbm1 28 . hn parsed_1b4c 1 991 1 2 . . . . . . . . sbm1 31 . hn parsed_1b4c 1 992 1 1 . . . . . . . . sbm2 28 . hn parsed_1b4c 1 992 1 2 . . . . . . . . sbm2 31 . hn parsed_1b4c 1 993 1 1 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 993 1 2 . . . . . . . . sbm1 31 . hn parsed_1b4c 1 994 1 1 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 994 1 2 . . . . . . . . sbm2 31 . hn parsed_1b4c 1 995 1 1 . . . . . . . . sbm1 34 . hb* parsed_1b4c 1 995 1 2 . . . . . . . . sbm1 31 . ha parsed_1b4c 1 996 1 1 . . . . . . . . sbm2 34 . hb* parsed_1b4c 1 996 1 2 . . . . . . . . sbm2 31 . ha parsed_1b4c 1 997 1 1 . . . . . . . . sbm1 29 . ha parsed_1b4c 1 997 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 998 1 1 . . . . . . . . sbm2 29 . ha parsed_1b4c 1 998 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 999 1 1 . . . . . . . . sbm1 29 . ha parsed_1b4c 1 999 1 2 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1000 1 1 . . . . . . . . sbm2 29 . ha parsed_1b4c 1 1000 1 2 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1001 1 1 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 1001 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 1002 1 1 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 1002 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 1003 1 1 . . . . . . . . sbm1 30 . ha parsed_1b4c 1 1003 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 1004 1 1 . . . . . . . . sbm2 30 . ha parsed_1b4c 1 1004 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 1005 1 1 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1005 1 2 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1006 1 1 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1006 1 2 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1007 1 1 . . . . . . . . sbm1 29 . ha parsed_1b4c 1 1007 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 1008 1 1 . . . . . . . . sbm2 29 . ha parsed_1b4c 1 1008 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 1009 1 1 . . . . . . . . sbm1 30 . ha parsed_1b4c 1 1009 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 1010 1 1 . . . . . . . . sbm2 30 . ha parsed_1b4c 1 1010 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 1011 1 1 . . . . . . . . sbm1 30 . ha parsed_1b4c 1 1011 1 2 . . . . . . . . sbm1 33 . hb* parsed_1b4c 1 1012 1 1 . . . . . . . . sbm2 30 . ha parsed_1b4c 1 1012 1 2 . . . . . . . . sbm2 33 . hb* parsed_1b4c 1 1013 1 1 . . . . . . . . sbm1 31 . hn parsed_1b4c 1 1013 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 1014 1 1 . . . . . . . . sbm2 31 . hn parsed_1b4c 1 1014 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 1015 1 1 . . . . . . . . sbm1 30 . ha parsed_1b4c 1 1015 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 1016 1 1 . . . . . . . . sbm2 30 . ha parsed_1b4c 1 1016 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 1017 1 1 . . . . . . . . sbm1 31 . ha parsed_1b4c 1 1017 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 1018 1 1 . . . . . . . . sbm2 31 . ha parsed_1b4c 1 1018 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 1019 1 1 . . . . . . . . sbm1 31 . ha parsed_1b4c 1 1019 1 2 . . . . . . . . sbm1 34 . hb* parsed_1b4c 1 1020 1 1 . . . . . . . . sbm2 31 . ha parsed_1b4c 1 1020 1 2 . . . . . . . . sbm2 34 . hb* parsed_1b4c 1 1021 1 1 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 1021 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 1022 1 1 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 1022 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 1023 1 1 . . . . . . . . sbm1 32 . ha parsed_1b4c 1 1023 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 1024 1 1 . . . . . . . . sbm2 32 . ha parsed_1b4c 1 1024 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 1025 1 1 . . . . . . . . sbm1 32 . ha parsed_1b4c 1 1025 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 1026 1 1 . . . . . . . . sbm2 32 . ha parsed_1b4c 1 1026 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 1027 1 1 . . . . . . . . sbm1 32 . ha parsed_1b4c 1 1027 1 2 . . . . . . . . sbm1 35 . hb* parsed_1b4c 1 1028 1 1 . . . . . . . . sbm2 32 . ha parsed_1b4c 1 1028 1 2 . . . . . . . . sbm2 35 . hb* parsed_1b4c 1 1029 1 1 . . . . . . . . sbm1 32 . ha parsed_1b4c 1 1029 1 2 . . . . . . . . sbm1 35 . hb* parsed_1b4c 1 1030 1 1 . . . . . . . . sbm2 32 . ha parsed_1b4c 1 1030 1 2 . . . . . . . . sbm2 35 . hb* parsed_1b4c 1 1031 1 1 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1031 1 2 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1032 1 1 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1032 1 2 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1033 1 1 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 1033 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 1034 1 1 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 1034 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 1035 1 1 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 1035 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 1036 1 1 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 1036 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 1037 1 1 . . . . . . . . sbm1 38 . hb* parsed_1b4c 1 1037 1 2 . . . . . . . . sbm1 35 . ha parsed_1b4c 1 1038 1 1 . . . . . . . . sbm2 38 . hb* parsed_1b4c 1 1038 1 2 . . . . . . . . sbm2 35 . ha parsed_1b4c 1 1039 1 1 . . . . . . . . sbm1 32 . ha parsed_1b4c 1 1039 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 1040 1 1 . . . . . . . . sbm2 32 . ha parsed_1b4c 1 1040 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 1041 1 1 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1041 1 2 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1042 1 1 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1042 1 2 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1043 1 1 . . . . . . . . sbm1 33 . ha parsed_1b4c 1 1043 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 1044 1 1 . . . . . . . . sbm2 33 . ha parsed_1b4c 1 1044 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 1045 1 1 . . . . . . . . sbm1 33 . ha parsed_1b4c 1 1045 1 2 . . . . . . . . sbm1 36 . hb parsed_1b4c 1 1046 1 1 . . . . . . . . sbm2 33 . ha parsed_1b4c 1 1046 1 2 . . . . . . . . sbm2 36 . hb parsed_1b4c 1 1047 1 1 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 1047 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 1048 1 1 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 1048 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 1049 1 1 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 1049 1 2 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 1050 1 1 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 1050 1 2 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 1051 1 1 . . . . . . . . sbm1 33 . ha parsed_1b4c 1 1051 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 1052 1 1 . . . . . . . . sbm2 33 . ha parsed_1b4c 1 1052 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 1053 1 1 . . . . . . . . sbm1 34 . ha parsed_1b4c 1 1053 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 1054 1 1 . . . . . . . . sbm2 34 . ha parsed_1b4c 1 1054 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 1055 1 1 . . . . . . . . sbm1 34 . ha parsed_1b4c 1 1055 1 2 . . . . . . . . sbm1 37 . hb* parsed_1b4c 1 1056 1 1 . . . . . . . . sbm2 34 . ha parsed_1b4c 1 1056 1 2 . . . . . . . . sbm2 37 . hb* parsed_1b4c 1 1057 1 1 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 1057 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 1058 1 1 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 1058 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 1059 1 1 . . . . . . . . sbm1 39 . hn parsed_1b4c 1 1059 1 2 . . . . . . . . sbm1 37 . hn parsed_1b4c 1 1060 1 1 . . . . . . . . sbm2 39 . hn parsed_1b4c 1 1060 1 2 . . . . . . . . sbm2 37 . hn parsed_1b4c 1 1061 1 1 . . . . . . . . sbm1 34 . ha parsed_1b4c 1 1061 1 2 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 1062 1 1 . . . . . . . . sbm2 34 . ha parsed_1b4c 1 1062 1 2 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 1063 1 1 . . . . . . . . sbm1 35 . ha parsed_1b4c 1 1063 1 2 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 1064 1 1 . . . . . . . . sbm2 35 . ha parsed_1b4c 1 1064 1 2 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 1065 1 1 . . . . . . . . sbm1 36 . hn parsed_1b4c 1 1065 1 2 . . . . . . . . sbm1 38 . hn parsed_1b4c 1 1066 1 1 . . . . . . . . sbm2 36 . hn parsed_1b4c 1 1066 1 2 . . . . . . . . sbm2 38 . hn parsed_1b4c 1 1067 1 1 . . . . . . . . sbm1 35 . ha parsed_1b4c 1 1067 1 2 . . . . . . . . sbm1 39 . hn parsed_1b4c 1 1068 1 1 . . . . . . . . sbm2 35 . ha parsed_1b4c 1 1068 1 2 . . . . . . . . sbm2 39 . hn parsed_1b4c 1 1069 1 1 . . . . . . . . sbm1 36 . ha parsed_1b4c 1 1069 1 2 . . . . . . . . sbm1 39 . hn parsed_1b4c 1 1070 1 1 . . . . . . . . sbm2 36 . ha parsed_1b4c 1 1070 1 2 . . . . . . . . sbm2 39 . hn parsed_1b4c 1 1071 1 1 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1071 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1072 1 1 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1072 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1073 1 1 . . . . . . . . sbm1 36 . ha parsed_1b4c 1 1073 1 2 . . . . . . . . sbm1 40 . hn parsed_1b4c 1 1074 1 1 . . . . . . . . sbm2 36 . ha parsed_1b4c 1 1074 1 2 . . . . . . . . sbm2 40 . hn parsed_1b4c 1 1075 1 1 . . . . . . . . sbm1 36 . ha parsed_1b4c 1 1075 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1076 1 1 . . . . . . . . sbm2 36 . ha parsed_1b4c 1 1076 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1077 1 1 . . . . . . . . sbm1 37 . ha parsed_1b4c 1 1077 1 2 . . . . . . . . sbm1 40 . hn parsed_1b4c 1 1078 1 1 . . . . . . . . sbm2 37 . ha parsed_1b4c 1 1078 1 2 . . . . . . . . sbm2 40 . hn parsed_1b4c 1 1079 1 1 . . . . . . . . sbm1 43 . he* parsed_1b4c 1 1079 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1080 1 1 . . . . . . . . sbm2 43 . he* parsed_1b4c 1 1080 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1081 1 1 . . . . . . . . sbm1 37 . ha parsed_1b4c 1 1081 1 2 . . . . . . . . sbm1 41 . hn parsed_1b4c 1 1082 1 1 . . . . . . . . sbm2 37 . ha parsed_1b4c 1 1082 1 2 . . . . . . . . sbm2 41 . hn parsed_1b4c 1 1083 1 1 . . . . . . . . sbm1 39 . hn parsed_1b4c 1 1083 1 2 . . . . . . . . sbm1 41 . hn parsed_1b4c 1 1084 1 1 . . . . . . . . sbm2 39 . hn parsed_1b4c 1 1084 1 2 . . . . . . . . sbm2 41 . hn parsed_1b4c 1 1085 1 1 . . . . . . . . sbm1 40 . ha parsed_1b4c 1 1085 1 2 . . . . . . . . sbm1 42 . hn parsed_1b4c 1 1086 1 1 . . . . . . . . sbm2 40 . ha parsed_1b4c 1 1086 1 2 . . . . . . . . sbm2 42 . hn parsed_1b4c 1 1087 1 1 . . . . . . . . sbm1 40 . ha parsed_1b4c 1 1087 1 2 . . . . . . . . sbm1 43 . hn parsed_1b4c 1 1088 1 1 . . . . . . . . sbm2 40 . ha parsed_1b4c 1 1088 1 2 . . . . . . . . sbm2 43 . hn parsed_1b4c 1 1089 1 1 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1089 1 2 . . . . . . . . sbm1 43 . hn parsed_1b4c 1 1090 1 1 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1090 1 2 . . . . . . . . sbm2 43 . hn parsed_1b4c 1 1091 1 1 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1091 1 2 . . . . . . . . sbm1 43 . hd* parsed_1b4c 1 1092 1 1 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1092 1 2 . . . . . . . . sbm2 43 . hd* parsed_1b4c 1 1093 1 1 . . . . . . . . sbm1 47 . hd* parsed_1b4c 1 1093 1 2 . . . . . . . . sbm1 44 . hd* parsed_1b4c 1 1094 1 1 . . . . . . . . sbm2 47 . hd* parsed_1b4c 1 1094 1 2 . . . . . . . . sbm2 44 . hd* parsed_1b4c 1 1095 1 1 . . . . . . . . sbm1 47 . hg1* parsed_1b4c 1 1095 1 2 . . . . . . . . sbm1 44 . hd* parsed_1b4c 1 1096 1 1 . . . . . . . . sbm2 47 . hg1* parsed_1b4c 1 1096 1 2 . . . . . . . . sbm2 44 . hd* parsed_1b4c 1 1097 1 1 . . . . . . . . sbm1 44 . ha parsed_1b4c 1 1097 1 2 . . . . . . . . sbm1 46 . hn parsed_1b4c 1 1098 1 1 . . . . . . . . sbm2 44 . ha parsed_1b4c 1 1098 1 2 . . . . . . . . sbm2 46 . hn parsed_1b4c 1 1099 1 1 . . . . . . . . sbm1 44 . hd* parsed_1b4c 1 1099 1 2 . . . . . . . . sbm1 46 . hn parsed_1b4c 1 1100 1 1 . . . . . . . . sbm2 44 . hd* parsed_1b4c 1 1100 1 2 . . . . . . . . sbm2 46 . hn parsed_1b4c 1 1101 1 1 . . . . . . . . sbm1 44 . ha parsed_1b4c 1 1101 1 2 . . . . . . . . sbm1 47 . hd* parsed_1b4c 1 1102 1 1 . . . . . . . . sbm2 44 . ha parsed_1b4c 1 1102 1 2 . . . . . . . . sbm2 47 . hd* parsed_1b4c 1 1103 1 1 . . . . . . . . sbm1 44 . hd* parsed_1b4c 1 1103 1 2 . . . . . . . . sbm1 47 . hg2* parsed_1b4c 1 1104 1 1 . . . . . . . . sbm2 44 . hd* parsed_1b4c 1 1104 1 2 . . . . . . . . sbm2 47 . hg2* parsed_1b4c 1 1105 1 1 . . . . . . . . sbm1 50 . ha parsed_1b4c 1 1105 1 2 . . . . . . . . sbm1 47 . hg2* parsed_1b4c 1 1106 1 1 . . . . . . . . sbm2 50 . ha parsed_1b4c 1 1106 1 2 . . . . . . . . sbm2 47 . hg2* parsed_1b4c 1 1107 1 1 . . . . . . . . sbm1 50 . hb* parsed_1b4c 1 1107 1 2 . . . . . . . . sbm1 47 . hg2* parsed_1b4c 1 1108 1 1 . . . . . . . . sbm2 50 . hb* parsed_1b4c 1 1108 1 2 . . . . . . . . sbm2 47 . hg2* parsed_1b4c 1 1109 1 1 . . . . . . . . sbm1 47 . ha parsed_1b4c 1 1109 1 2 . . . . . . . . sbm1 49 . hn parsed_1b4c 1 1110 1 1 . . . . . . . . sbm2 47 . ha parsed_1b4c 1 1110 1 2 . . . . . . . . sbm2 49 . hn parsed_1b4c 1 1111 1 1 . . . . . . . . sbm1 47 . hg2* parsed_1b4c 1 1111 1 2 . . . . . . . . sbm1 49 . hn parsed_1b4c 1 1112 1 1 . . . . . . . . sbm2 47 . hg2* parsed_1b4c 1 1112 1 2 . . . . . . . . sbm2 49 . hn parsed_1b4c 1 1113 1 1 . . . . . . . . sbm1 53 . hb parsed_1b4c 1 1113 1 2 . . . . . . . . sbm1 50 . ha parsed_1b4c 1 1114 1 1 . . . . . . . . sbm2 53 . hb parsed_1b4c 1 1114 1 2 . . . . . . . . sbm2 50 . ha parsed_1b4c 1 1115 1 1 . . . . . . . . sbm1 52 . hn parsed_1b4c 1 1115 1 2 . . . . . . . . sbm1 50 . hn parsed_1b4c 1 1116 1 1 . . . . . . . . sbm2 52 . hn parsed_1b4c 1 1116 1 2 . . . . . . . . sbm2 50 . hn parsed_1b4c 1 1117 1 1 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 1117 1 2 . . . . . . . . sbm1 51 . hn parsed_1b4c 1 1118 1 1 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 1118 1 2 . . . . . . . . sbm2 51 . hn parsed_1b4c 1 1119 1 1 . . . . . . . . sbm1 54 . hb* parsed_1b4c 1 1119 1 2 . . . . . . . . sbm1 51 . ha parsed_1b4c 1 1120 1 1 . . . . . . . . sbm2 54 . hb* parsed_1b4c 1 1120 1 2 . . . . . . . . sbm2 51 . ha parsed_1b4c 1 1121 1 1 . . . . . . . . sbm1 50 . hn parsed_1b4c 1 1121 1 2 . . . . . . . . sbm1 52 . hn parsed_1b4c 1 1122 1 1 . . . . . . . . sbm2 50 . hn parsed_1b4c 1 1122 1 2 . . . . . . . . sbm2 52 . hn parsed_1b4c 1 1123 1 1 . . . . . . . . sbm1 55 . hb* parsed_1b4c 1 1123 1 2 . . . . . . . . sbm1 52 . ha parsed_1b4c 1 1124 1 1 . . . . . . . . sbm2 55 . hb* parsed_1b4c 1 1124 1 2 . . . . . . . . sbm2 52 . ha parsed_1b4c 1 1125 1 1 . . . . . . . . sbm1 50 . ha parsed_1b4c 1 1125 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 1126 1 1 . . . . . . . . sbm2 50 . ha parsed_1b4c 1 1126 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 1127 1 1 . . . . . . . . sbm1 50 . ha parsed_1b4c 1 1127 1 2 . . . . . . . . sbm1 53 . hg2* parsed_1b4c 1 1128 1 1 . . . . . . . . sbm2 50 . ha parsed_1b4c 1 1128 1 2 . . . . . . . . sbm2 53 . hg2* parsed_1b4c 1 1129 1 1 . . . . . . . . sbm1 51 . hn parsed_1b4c 1 1129 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 1130 1 1 . . . . . . . . sbm2 51 . hn parsed_1b4c 1 1130 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 1131 1 1 . . . . . . . . sbm1 51 . ha parsed_1b4c 1 1131 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 1132 1 1 . . . . . . . . sbm2 51 . ha parsed_1b4c 1 1132 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 1133 1 1 . . . . . . . . sbm1 56 . hb parsed_1b4c 1 1133 1 2 . . . . . . . . sbm1 53 . ha parsed_1b4c 1 1134 1 1 . . . . . . . . sbm2 56 . hb parsed_1b4c 1 1134 1 2 . . . . . . . . sbm2 53 . ha parsed_1b4c 1 1135 1 1 . . . . . . . . sbm1 56 . hg2* parsed_1b4c 1 1135 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 1136 1 1 . . . . . . . . sbm2 56 . hg2* parsed_1b4c 1 1136 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 1137 1 1 . . . . . . . . sbm1 50 . ha parsed_1b4c 1 1137 1 2 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 1138 1 1 . . . . . . . . sbm2 50 . ha parsed_1b4c 1 1138 1 2 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 1139 1 1 . . . . . . . . sbm1 51 . ha parsed_1b4c 1 1139 1 2 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 1140 1 1 . . . . . . . . sbm2 51 . ha parsed_1b4c 1 1140 1 2 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 1141 1 1 . . . . . . . . sbm1 52 . hn parsed_1b4c 1 1141 1 2 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 1142 1 1 . . . . . . . . sbm2 52 . hn parsed_1b4c 1 1142 1 2 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 1143 1 1 . . . . . . . . sbm1 52 . ha parsed_1b4c 1 1143 1 2 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 1144 1 1 . . . . . . . . sbm2 52 . ha parsed_1b4c 1 1144 1 2 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 1145 1 1 . . . . . . . . sbm1 57 . hb* parsed_1b4c 1 1145 1 2 . . . . . . . . sbm1 54 . ha parsed_1b4c 1 1146 1 1 . . . . . . . . sbm2 57 . hb* parsed_1b4c 1 1146 1 2 . . . . . . . . sbm2 54 . ha parsed_1b4c 1 1147 1 1 . . . . . . . . sbm1 51 . ha parsed_1b4c 1 1147 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 1148 1 1 . . . . . . . . sbm2 51 . ha parsed_1b4c 1 1148 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 1149 1 1 . . . . . . . . sbm1 52 . ha parsed_1b4c 1 1149 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 1150 1 1 . . . . . . . . sbm2 52 . ha parsed_1b4c 1 1150 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 1151 1 1 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 1151 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 1152 1 1 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 1152 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 1153 1 1 . . . . . . . . sbm1 53 . ha parsed_1b4c 1 1153 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 1154 1 1 . . . . . . . . sbm2 53 . ha parsed_1b4c 1 1154 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 1155 1 1 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 1155 1 2 . . . . . . . . sbm1 55 . hn parsed_1b4c 1 1156 1 1 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 1156 1 2 . . . . . . . . sbm2 55 . hn parsed_1b4c 1 1157 1 1 . . . . . . . . sbm1 58 . hb* parsed_1b4c 1 1157 1 2 . . . . . . . . sbm1 55 . ha parsed_1b4c 1 1158 1 1 . . . . . . . . sbm2 58 . hb* parsed_1b4c 1 1158 1 2 . . . . . . . . sbm2 55 . ha parsed_1b4c 1 1159 1 1 . . . . . . . . sbm1 52 . ha parsed_1b4c 1 1159 1 2 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 1160 1 1 . . . . . . . . sbm2 52 . ha parsed_1b4c 1 1160 1 2 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 1161 1 1 . . . . . . . . sbm1 53 . ha parsed_1b4c 1 1161 1 2 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 1162 1 1 . . . . . . . . sbm2 53 . ha parsed_1b4c 1 1162 1 2 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 1163 1 1 . . . . . . . . sbm1 53 . ha parsed_1b4c 1 1163 1 2 . . . . . . . . sbm1 56 . hg2* parsed_1b4c 1 1164 1 1 . . . . . . . . sbm2 53 . ha parsed_1b4c 1 1164 1 2 . . . . . . . . sbm2 56 . hg2* parsed_1b4c 1 1165 1 1 . . . . . . . . sbm1 54 . hn parsed_1b4c 1 1165 1 2 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 1166 1 1 . . . . . . . . sbm2 54 . hn parsed_1b4c 1 1166 1 2 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 1167 1 1 . . . . . . . . sbm1 59 . hb parsed_1b4c 1 1167 1 2 . . . . . . . . sbm1 56 . ha parsed_1b4c 1 1168 1 1 . . . . . . . . sbm2 59 . hb parsed_1b4c 1 1168 1 2 . . . . . . . . sbm2 56 . ha parsed_1b4c 1 1169 1 1 . . . . . . . . sbm1 53 . ha parsed_1b4c 1 1169 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 1170 1 1 . . . . . . . . sbm2 53 . ha parsed_1b4c 1 1170 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 1171 1 1 . . . . . . . . sbm1 54 . ha parsed_1b4c 1 1171 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 1172 1 1 . . . . . . . . sbm2 54 . ha parsed_1b4c 1 1172 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 1173 1 1 . . . . . . . . sbm1 60 . hb* parsed_1b4c 1 1173 1 2 . . . . . . . . sbm1 57 . ha parsed_1b4c 1 1174 1 1 . . . . . . . . sbm2 60 . hb* parsed_1b4c 1 1174 1 2 . . . . . . . . sbm2 57 . ha parsed_1b4c 1 1175 1 1 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1175 1 2 . . . . . . . . sbm1 57 . he* parsed_1b4c 1 1176 1 1 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1176 1 2 . . . . . . . . sbm2 57 . he* parsed_1b4c 1 1177 1 1 . . . . . . . . sbm1 54 . ha parsed_1b4c 1 1177 1 2 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 1178 1 1 . . . . . . . . sbm2 54 . ha parsed_1b4c 1 1178 1 2 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 1179 1 1 . . . . . . . . sbm1 55 . ha parsed_1b4c 1 1179 1 2 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 1180 1 1 . . . . . . . . sbm2 55 . ha parsed_1b4c 1 1180 1 2 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 1181 1 1 . . . . . . . . sbm1 56 . ha parsed_1b4c 1 1181 1 2 . . . . . . . . sbm1 58 . hn parsed_1b4c 1 1182 1 1 . . . . . . . . sbm2 56 . ha parsed_1b4c 1 1182 1 2 . . . . . . . . sbm2 58 . hn parsed_1b4c 1 1183 1 1 . . . . . . . . sbm1 61 . hb* parsed_1b4c 1 1183 1 2 . . . . . . . . sbm1 58 . ha parsed_1b4c 1 1184 1 1 . . . . . . . . sbm2 61 . hb* parsed_1b4c 1 1184 1 2 . . . . . . . . sbm2 58 . ha parsed_1b4c 1 1185 1 1 . . . . . . . . sbm1 55 . ha parsed_1b4c 1 1185 1 2 . . . . . . . . sbm1 59 . hn parsed_1b4c 1 1186 1 1 . . . . . . . . sbm2 55 . ha parsed_1b4c 1 1186 1 2 . . . . . . . . sbm2 59 . hn parsed_1b4c 1 1187 1 1 . . . . . . . . sbm1 56 . ha parsed_1b4c 1 1187 1 2 . . . . . . . . sbm1 59 . hn parsed_1b4c 1 1188 1 1 . . . . . . . . sbm2 56 . ha parsed_1b4c 1 1188 1 2 . . . . . . . . sbm2 59 . hn parsed_1b4c 1 1189 1 1 . . . . . . . . sbm1 62 . hb* parsed_1b4c 1 1189 1 2 . . . . . . . . sbm1 59 . ha parsed_1b4c 1 1190 1 1 . . . . . . . . sbm2 62 . hb* parsed_1b4c 1 1190 1 2 . . . . . . . . sbm2 59 . ha parsed_1b4c 1 1191 1 1 . . . . . . . . sbm1 56 . ha parsed_1b4c 1 1191 1 2 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 1192 1 1 . . . . . . . . sbm2 56 . ha parsed_1b4c 1 1192 1 2 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 1193 1 1 . . . . . . . . sbm1 57 . ha parsed_1b4c 1 1193 1 2 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 1194 1 1 . . . . . . . . sbm2 57 . ha parsed_1b4c 1 1194 1 2 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 1195 1 1 . . . . . . . . sbm1 57 . ha parsed_1b4c 1 1195 1 2 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1196 1 1 . . . . . . . . sbm2 57 . ha parsed_1b4c 1 1196 1 2 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1197 1 1 . . . . . . . . sbm1 58 . ha parsed_1b4c 1 1197 1 2 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 1198 1 1 . . . . . . . . sbm2 58 . ha parsed_1b4c 1 1198 1 2 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 1199 1 1 . . . . . . . . sbm1 57 . ha parsed_1b4c 1 1199 1 2 . . . . . . . . sbm1 61 . hn parsed_1b4c 1 1200 1 1 . . . . . . . . sbm2 57 . ha parsed_1b4c 1 1200 1 2 . . . . . . . . sbm2 61 . hn parsed_1b4c 1 1201 1 1 . . . . . . . . sbm1 58 . ha parsed_1b4c 1 1201 1 2 . . . . . . . . sbm1 61 . hn parsed_1b4c 1 1202 1 1 . . . . . . . . sbm2 58 . ha parsed_1b4c 1 1202 1 2 . . . . . . . . sbm2 61 . hn parsed_1b4c 1 1203 1 1 . . . . . . . . sbm1 59 . hn parsed_1b4c 1 1203 1 2 . . . . . . . . sbm1 61 . hn parsed_1b4c 1 1204 1 1 . . . . . . . . sbm2 59 . hn parsed_1b4c 1 1204 1 2 . . . . . . . . sbm2 61 . hn parsed_1b4c 1 1205 1 1 . . . . . . . . sbm1 58 . ha parsed_1b4c 1 1205 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 1206 1 1 . . . . . . . . sbm2 58 . ha parsed_1b4c 1 1206 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 1207 1 1 . . . . . . . . sbm1 59 . ha parsed_1b4c 1 1207 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 1208 1 1 . . . . . . . . sbm2 59 . ha parsed_1b4c 1 1208 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 1209 1 1 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 1209 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 1210 1 1 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 1210 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 1211 1 1 . . . . . . . . sbm1 60 . ha parsed_1b4c 1 1211 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 1212 1 1 . . . . . . . . sbm2 60 . ha parsed_1b4c 1 1212 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 1213 1 1 . . . . . . . . sbm1 60 . hb* parsed_1b4c 1 1213 1 2 . . . . . . . . sbm1 62 . hn parsed_1b4c 1 1214 1 1 . . . . . . . . sbm2 60 . hb* parsed_1b4c 1 1214 1 2 . . . . . . . . sbm2 62 . hn parsed_1b4c 1 1215 1 1 . . . . . . . . sbm1 60 . ha parsed_1b4c 1 1215 1 2 . . . . . . . . sbm1 63 . hn parsed_1b4c 1 1216 1 1 . . . . . . . . sbm2 60 . ha parsed_1b4c 1 1216 1 2 . . . . . . . . sbm2 63 . hn parsed_1b4c 1 1217 1 1 . . . . . . . . sbm1 62 . ha parsed_1b4c 1 1217 1 2 . . . . . . . . sbm1 64 . hn parsed_1b4c 1 1218 1 1 . . . . . . . . sbm2 62 . ha parsed_1b4c 1 1218 1 2 . . . . . . . . sbm2 64 . hn parsed_1b4c 1 1219 1 1 . . . . . . . . sbm1 62 . hb* parsed_1b4c 1 1219 1 2 . . . . . . . . sbm1 64 . hn parsed_1b4c 1 1220 1 1 . . . . . . . . sbm2 62 . hb* parsed_1b4c 1 1220 1 2 . . . . . . . . sbm2 64 . hn parsed_1b4c 1 1221 1 1 . . . . . . . . sbm1 63 . hn parsed_1b4c 1 1221 1 2 . . . . . . . . sbm1 65 . hn parsed_1b4c 1 1222 1 1 . . . . . . . . sbm2 63 . hn parsed_1b4c 1 1222 1 2 . . . . . . . . sbm2 65 . hn parsed_1b4c 1 1223 1 1 . . . . . . . . sbm1 63 . ha parsed_1b4c 1 1223 1 2 . . . . . . . . sbm1 65 . hn parsed_1b4c 1 1224 1 1 . . . . . . . . sbm2 63 . ha parsed_1b4c 1 1224 1 2 . . . . . . . . sbm2 65 . hn parsed_1b4c 1 1225 1 1 . . . . . . . . sbm1 63 . hb* parsed_1b4c 1 1225 1 2 . . . . . . . . sbm1 65 . hn parsed_1b4c 1 1226 1 1 . . . . . . . . sbm2 63 . hb* parsed_1b4c 1 1226 1 2 . . . . . . . . sbm2 65 . hn parsed_1b4c 1 1227 1 1 . . . . . . . . sbm1 63 . ha parsed_1b4c 1 1227 1 2 . . . . . . . . sbm1 66 . hn parsed_1b4c 1 1228 1 1 . . . . . . . . sbm2 63 . ha parsed_1b4c 1 1228 1 2 . . . . . . . . sbm2 66 . hn parsed_1b4c 1 1229 1 1 . . . . . . . . sbm1 64 . hn parsed_1b4c 1 1229 1 2 . . . . . . . . sbm1 66 . hn parsed_1b4c 1 1230 1 1 . . . . . . . . sbm2 64 . hn parsed_1b4c 1 1230 1 2 . . . . . . . . sbm2 66 . hn parsed_1b4c 1 1231 1 1 . . . . . . . . sbm1 65 . hn parsed_1b4c 1 1231 1 2 . . . . . . . . sbm1 67 . hn parsed_1b4c 1 1232 1 1 . . . . . . . . sbm2 65 . hn parsed_1b4c 1 1232 1 2 . . . . . . . . sbm2 67 . hn parsed_1b4c 1 1233 1 1 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 1233 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 1234 1 1 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 1234 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 1235 1 1 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 1235 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 1236 1 1 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 1236 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 1237 1 1 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 1237 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 1238 1 1 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 1238 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 1239 1 1 . . . . . . . . sbm1 72 . hb* parsed_1b4c 1 1239 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 1240 1 1 . . . . . . . . sbm2 72 . hb* parsed_1b4c 1 1240 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 1241 1 1 . . . . . . . . sbm1 72 . hg* parsed_1b4c 1 1241 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 1242 1 1 . . . . . . . . sbm2 72 . hg* parsed_1b4c 1 1242 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 1243 1 1 . . . . . . . . sbm1 73 . hb* parsed_1b4c 1 1243 1 2 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 1244 1 1 . . . . . . . . sbm2 73 . hb* parsed_1b4c 1 1244 1 2 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 1245 1 1 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 1245 1 2 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 1246 1 1 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 1246 1 2 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 1247 1 1 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 1247 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 1248 1 1 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 1248 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 1249 1 1 . . . . . . . . sbm1 69 . ha parsed_1b4c 1 1249 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 1250 1 1 . . . . . . . . sbm2 69 . ha parsed_1b4c 1 1250 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 1251 1 1 . . . . . . . . sbm1 69 . hb* parsed_1b4c 1 1251 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 1252 1 1 . . . . . . . . sbm2 69 . hb* parsed_1b4c 1 1252 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 1253 1 1 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 1253 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 1254 1 1 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 1254 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 1255 1 1 . . . . . . . . sbm1 74 . hb* parsed_1b4c 1 1255 1 2 . . . . . . . . sbm1 71 . ha parsed_1b4c 1 1256 1 1 . . . . . . . . sbm2 74 . hb* parsed_1b4c 1 1256 1 2 . . . . . . . . sbm2 71 . ha parsed_1b4c 1 1257 1 1 . . . . . . . . sbm1 68 . ha parsed_1b4c 1 1257 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 1258 1 1 . . . . . . . . sbm2 68 . ha parsed_1b4c 1 1258 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 1259 1 1 . . . . . . . . sbm1 68 . hb* parsed_1b4c 1 1259 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 1260 1 1 . . . . . . . . sbm2 68 . hb* parsed_1b4c 1 1260 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 1261 1 1 . . . . . . . . sbm1 69 . hb* parsed_1b4c 1 1261 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 1262 1 1 . . . . . . . . sbm2 69 . hb* parsed_1b4c 1 1262 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 1263 1 1 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 1263 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 1264 1 1 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 1264 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 1265 1 1 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 1265 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 1266 1 1 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 1266 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 1267 1 1 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 1267 1 2 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 1268 1 1 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 1268 1 2 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 1269 1 1 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 1269 1 2 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 1270 1 1 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 1270 1 2 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 1271 1 1 . . . . . . . . sbm1 71 . ha parsed_1b4c 1 1271 1 2 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 1272 1 1 . . . . . . . . sbm2 71 . ha parsed_1b4c 1 1272 1 2 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 1273 1 1 . . . . . . . . sbm1 76 . hb* parsed_1b4c 1 1273 1 2 . . . . . . . . sbm1 73 . ha parsed_1b4c 1 1274 1 1 . . . . . . . . sbm2 76 . hb* parsed_1b4c 1 1274 1 2 . . . . . . . . sbm2 73 . ha parsed_1b4c 1 1275 1 1 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 1275 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 1276 1 1 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 1276 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 1277 1 1 . . . . . . . . sbm1 71 . ha parsed_1b4c 1 1277 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 1278 1 1 . . . . . . . . sbm2 71 . ha parsed_1b4c 1 1278 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 1279 1 1 . . . . . . . . sbm1 72 . hn parsed_1b4c 1 1279 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 1280 1 1 . . . . . . . . sbm2 72 . hn parsed_1b4c 1 1280 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 1281 1 1 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 1281 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 1282 1 1 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 1282 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 1283 1 1 . . . . . . . . sbm1 76 . hn parsed_1b4c 1 1283 1 2 . . . . . . . . sbm1 74 . hn parsed_1b4c 1 1284 1 1 . . . . . . . . sbm2 76 . hn parsed_1b4c 1 1284 1 2 . . . . . . . . sbm2 74 . hn parsed_1b4c 1 1285 1 1 . . . . . . . . sbm1 77 . hb parsed_1b4c 1 1285 1 2 . . . . . . . . sbm1 74 . ha parsed_1b4c 1 1286 1 1 . . . . . . . . sbm2 77 . hb parsed_1b4c 1 1286 1 2 . . . . . . . . sbm2 74 . ha parsed_1b4c 1 1287 1 1 . . . . . . . . sbm1 77 . hg1* parsed_1b4c 1 1287 1 2 . . . . . . . . sbm1 74 . he* parsed_1b4c 1 1288 1 1 . . . . . . . . sbm2 77 . hg1* parsed_1b4c 1 1288 1 2 . . . . . . . . sbm2 74 . he* parsed_1b4c 1 1289 1 1 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1289 1 2 . . . . . . . . sbm1 74 . he* parsed_1b4c 1 1290 1 1 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1290 1 2 . . . . . . . . sbm2 74 . he* parsed_1b4c 1 1291 1 1 . . . . . . . . sbm1 71 . ha parsed_1b4c 1 1291 1 2 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 1292 1 1 . . . . . . . . sbm2 71 . ha parsed_1b4c 1 1292 1 2 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 1293 1 1 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 1293 1 2 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 1294 1 1 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 1294 1 2 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 1295 1 1 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 1295 1 2 . . . . . . . . sbm1 75 . hb* parsed_1b4c 1 1296 1 1 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 1296 1 2 . . . . . . . . sbm2 75 . hb* parsed_1b4c 1 1297 1 1 . . . . . . . . sbm1 73 . hn parsed_1b4c 1 1297 1 2 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 1298 1 1 . . . . . . . . sbm2 73 . hn parsed_1b4c 1 1298 1 2 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 1299 1 1 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 1299 1 2 . . . . . . . . sbm1 75 . hn parsed_1b4c 1 1300 1 1 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 1300 1 2 . . . . . . . . sbm2 75 . hn parsed_1b4c 1 1301 1 1 . . . . . . . . sbm1 78 . hb* parsed_1b4c 1 1301 1 2 . . . . . . . . sbm1 75 . ha parsed_1b4c 1 1302 1 1 . . . . . . . . sbm2 78 . hb* parsed_1b4c 1 1302 1 2 . . . . . . . . sbm2 75 . ha parsed_1b4c 1 1303 1 1 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 1303 1 2 . . . . . . . . sbm1 76 . hn parsed_1b4c 1 1304 1 1 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 1304 1 2 . . . . . . . . sbm2 76 . hn parsed_1b4c 1 1305 1 1 . . . . . . . . sbm1 73 . ha parsed_1b4c 1 1305 1 2 . . . . . . . . sbm1 76 . hn parsed_1b4c 1 1306 1 1 . . . . . . . . sbm2 73 . ha parsed_1b4c 1 1306 1 2 . . . . . . . . sbm2 76 . hn parsed_1b4c 1 1307 1 1 . . . . . . . . sbm1 79 . hb* parsed_1b4c 1 1307 1 2 . . . . . . . . sbm1 76 . ha parsed_1b4c 1 1308 1 1 . . . . . . . . sbm2 79 . hb* parsed_1b4c 1 1308 1 2 . . . . . . . . sbm2 76 . ha parsed_1b4c 1 1309 1 1 . . . . . . . . sbm1 76 . hb* parsed_1b4c 1 1309 1 2 . . . . . . . . sbm1 72 . ha parsed_1b4c 1 1310 1 1 . . . . . . . . sbm2 76 . hb* parsed_1b4c 1 1310 1 2 . . . . . . . . sbm2 72 . ha parsed_1b4c 1 1311 1 1 . . . . . . . . sbm1 73 . ha parsed_1b4c 1 1311 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 1312 1 1 . . . . . . . . sbm2 73 . ha parsed_1b4c 1 1312 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 1313 1 1 . . . . . . . . sbm1 73 . hd* parsed_1b4c 1 1313 1 2 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1314 1 1 . . . . . . . . sbm2 73 . hd* parsed_1b4c 1 1314 1 2 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1315 1 1 . . . . . . . . sbm1 73 . he* parsed_1b4c 1 1315 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 1316 1 1 . . . . . . . . sbm2 73 . he* parsed_1b4c 1 1316 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 1317 1 1 . . . . . . . . sbm1 73 . he* parsed_1b4c 1 1317 1 2 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1318 1 1 . . . . . . . . sbm2 73 . he* parsed_1b4c 1 1318 1 2 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1319 1 1 . . . . . . . . sbm1 73 . hz parsed_1b4c 1 1319 1 2 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1320 1 1 . . . . . . . . sbm2 73 . hz parsed_1b4c 1 1320 1 2 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1321 1 1 . . . . . . . . sbm1 74 . ha parsed_1b4c 1 1321 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 1322 1 1 . . . . . . . . sbm2 74 . ha parsed_1b4c 1 1322 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 1323 1 1 . . . . . . . . sbm1 74 . ha parsed_1b4c 1 1323 1 2 . . . . . . . . sbm1 77 . hg1* parsed_1b4c 1 1324 1 1 . . . . . . . . sbm2 74 . ha parsed_1b4c 1 1324 1 2 . . . . . . . . sbm2 77 . hg1* parsed_1b4c 1 1325 1 1 . . . . . . . . sbm1 74 . ha parsed_1b4c 1 1325 1 2 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1326 1 1 . . . . . . . . sbm2 74 . ha parsed_1b4c 1 1326 1 2 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1327 1 1 . . . . . . . . sbm1 80 . hb parsed_1b4c 1 1327 1 2 . . . . . . . . sbm1 77 . ha parsed_1b4c 1 1328 1 1 . . . . . . . . sbm2 80 . hb parsed_1b4c 1 1328 1 2 . . . . . . . . sbm2 77 . ha parsed_1b4c 1 1329 1 1 . . . . . . . . sbm1 74 . ha parsed_1b4c 1 1329 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 1330 1 1 . . . . . . . . sbm2 74 . ha parsed_1b4c 1 1330 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 1331 1 1 . . . . . . . . sbm1 74 . he* parsed_1b4c 1 1331 1 1 . . . . . . . . sbm2 74 . he* parsed_1b4c 1 1331 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 1332 1 1 . . . . . . . . sbm1 74 . he* parsed_1b4c 1 1332 1 1 . . . . . . . . sbm2 74 . he* parsed_1b4c 1 1332 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 1333 1 1 . . . . . . . . sbm1 75 . ha parsed_1b4c 1 1333 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 1334 1 1 . . . . . . . . sbm2 75 . ha parsed_1b4c 1 1334 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 1335 1 1 . . . . . . . . sbm1 76 . hn parsed_1b4c 1 1335 1 2 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 1336 1 1 . . . . . . . . sbm2 76 . hn parsed_1b4c 1 1336 1 2 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 1337 1 1 . . . . . . . . sbm1 75 . ha parsed_1b4c 1 1337 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 1338 1 1 . . . . . . . . sbm2 75 . ha parsed_1b4c 1 1338 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 1339 1 1 . . . . . . . . sbm1 76 . ha parsed_1b4c 1 1339 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 1340 1 1 . . . . . . . . sbm2 76 . ha parsed_1b4c 1 1340 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 1341 1 1 . . . . . . . . sbm1 76 . ha parsed_1b4c 1 1341 1 2 . . . . . . . . sbm1 79 . he* parsed_1b4c 1 1342 1 1 . . . . . . . . sbm2 76 . ha parsed_1b4c 1 1342 1 2 . . . . . . . . sbm2 79 . he* parsed_1b4c 1 1343 1 1 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 1343 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 1344 1 1 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 1344 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 1345 1 1 . . . . . . . . sbm1 77 . ha parsed_1b4c 1 1345 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 1346 1 1 . . . . . . . . sbm2 77 . ha parsed_1b4c 1 1346 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 1347 1 1 . . . . . . . . sbm1 82 . hb parsed_1b4c 1 1347 1 2 . . . . . . . . sbm1 79 . ha parsed_1b4c 1 1348 1 1 . . . . . . . . sbm2 82 . hb parsed_1b4c 1 1348 1 2 . . . . . . . . sbm2 79 . ha parsed_1b4c 1 1349 1 1 . . . . . . . . sbm1 76 . ha parsed_1b4c 1 1349 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 1350 1 1 . . . . . . . . sbm2 76 . ha parsed_1b4c 1 1350 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 1351 1 1 . . . . . . . . sbm1 77 . ha parsed_1b4c 1 1351 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 1352 1 1 . . . . . . . . sbm2 77 . ha parsed_1b4c 1 1352 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 1353 1 1 . . . . . . . . sbm1 78 . hn parsed_1b4c 1 1353 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 1354 1 1 . . . . . . . . sbm2 78 . hn parsed_1b4c 1 1354 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 1355 1 1 . . . . . . . . sbm1 78 . ha parsed_1b4c 1 1355 1 2 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 1356 1 1 . . . . . . . . sbm2 78 . ha parsed_1b4c 1 1356 1 2 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 1357 1 1 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1357 1 2 . . . . . . . . sbm1 80 . ha parsed_1b4c 1 1358 1 1 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1358 1 2 . . . . . . . . sbm2 80 . ha parsed_1b4c 1 1359 1 1 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1359 1 2 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 1360 1 1 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1360 1 2 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 1361 1 1 . . . . . . . . sbm1 77 . ha parsed_1b4c 1 1361 1 2 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 1362 1 1 . . . . . . . . sbm2 77 . ha parsed_1b4c 1 1362 1 2 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 1363 1 1 . . . . . . . . sbm1 78 . ha parsed_1b4c 1 1363 1 2 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 1364 1 1 . . . . . . . . sbm2 78 . ha parsed_1b4c 1 1364 1 2 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 1365 1 1 . . . . . . . . sbm1 78 . ha parsed_1b4c 1 1365 1 2 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 1366 1 1 . . . . . . . . sbm2 78 . ha parsed_1b4c 1 1366 1 2 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 1367 1 1 . . . . . . . . sbm1 79 . ha parsed_1b4c 1 1367 1 2 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 1368 1 1 . . . . . . . . sbm2 79 . ha parsed_1b4c 1 1368 1 2 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 1369 1 1 . . . . . . . . sbm1 80 . hn parsed_1b4c 1 1369 1 2 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 1370 1 1 . . . . . . . . sbm2 80 . hn parsed_1b4c 1 1370 1 2 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 1371 1 1 . . . . . . . . sbm1 80 . ha parsed_1b4c 1 1371 1 2 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 1372 1 1 . . . . . . . . sbm2 80 . ha parsed_1b4c 1 1372 1 2 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 1373 1 1 . . . . . . . . sbm1 79 . ha parsed_1b4c 1 1373 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 1374 1 1 . . . . . . . . sbm2 79 . ha parsed_1b4c 1 1374 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 1375 1 1 . . . . . . . . sbm1 80 . ha parsed_1b4c 1 1375 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 1376 1 1 . . . . . . . . sbm2 80 . ha parsed_1b4c 1 1376 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 1377 1 1 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 1377 1 2 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1378 1 1 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 1378 1 2 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1379 1 1 . . . . . . . . sbm1 81 . hn parsed_1b4c 1 1379 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 1380 1 1 . . . . . . . . sbm2 81 . hn parsed_1b4c 1 1380 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 1381 1 1 . . . . . . . . sbm1 81 . ha parsed_1b4c 1 1381 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 1382 1 1 . . . . . . . . sbm2 81 . ha parsed_1b4c 1 1382 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 1383 1 1 . . . . . . . . sbm1 81 . ha parsed_1b4c 1 1383 1 2 . . . . . . . . sbm1 84 . hn parsed_1b4c 1 1384 1 1 . . . . . . . . sbm2 81 . ha parsed_1b4c 1 1384 1 2 . . . . . . . . sbm2 84 . hn parsed_1b4c 1 1385 1 1 . . . . . . . . sbm1 80 . ha parsed_1b4c 1 1385 1 2 . . . . . . . . sbm1 84 . hn parsed_1b4c 1 1386 1 1 . . . . . . . . sbm2 80 . ha parsed_1b4c 1 1386 1 2 . . . . . . . . sbm2 84 . hn parsed_1b4c 1 1387 1 1 . . . . . . . . sbm1 82 . hn parsed_1b4c 1 1387 1 2 . . . . . . . . sbm1 84 . hn parsed_1b4c 1 1388 1 1 . . . . . . . . sbm2 82 . hn parsed_1b4c 1 1388 1 2 . . . . . . . . sbm2 84 . hn parsed_1b4c 1 1389 1 1 . . . . . . . . sbm1 87 . hd* parsed_1b4c 1 1389 1 2 . . . . . . . . sbm1 89 . hn parsed_1b4c 1 1390 1 1 . . . . . . . . sbm2 87 . hd* parsed_1b4c 1 1390 1 2 . . . . . . . . sbm2 89 . hn parsed_1b4c 1 1391 1 1 . . . . . . . . sbm1 88 . hd* parsed_1b4c 1 1391 1 2 . . . . . . . . sbm1 90 . hn parsed_1b4c 1 1392 1 1 . . . . . . . . sbm2 88 . hd* parsed_1b4c 1 1392 1 2 . . . . . . . . sbm2 90 . hn parsed_1b4c 1 1393 1 1 . . . . . . . . sbm1 70 . he* parsed_1b4c 1 1393 1 2 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 1394 1 1 . . . . . . . . sbm2 70 . he* parsed_1b4c 1 1394 1 2 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 1395 1 1 . . . . . . . . sbm1 73 . he* parsed_1b4c 1 1395 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1396 1 1 . . . . . . . . sbm2 73 . he* parsed_1b4c 1 1396 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1397 1 1 . . . . . . . . sbm1 73 . hz parsed_1b4c 1 1397 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1398 1 1 . . . . . . . . sbm2 73 . hz parsed_1b4c 1 1398 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1399 1 1 . . . . . . . . sbm1 77 . hg1* parsed_1b4c 1 1399 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1400 1 1 . . . . . . . . sbm2 77 . hg1* parsed_1b4c 1 1400 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1401 1 1 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1401 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1402 1 1 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1402 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1403 1 1 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1403 1 2 . . . . . . . . sbm1 13 . hg* parsed_1b4c 1 1404 1 1 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1404 1 2 . . . . . . . . sbm2 13 . hg* parsed_1b4c 1 1405 1 1 . . . . . . . . sbm1 73 . hz parsed_1b4c 1 1405 1 2 . . . . . . . . sbm1 13 . hg1* parsed_1b4c 1 1406 1 1 . . . . . . . . sbm2 73 . hz parsed_1b4c 1 1406 1 2 . . . . . . . . sbm2 13 . hg1* parsed_1b4c 1 1407 1 1 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1407 1 2 . . . . . . . . sbm1 14 . hd* parsed_1b4c 1 1408 1 1 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1408 1 2 . . . . . . . . sbm2 14 . hd* parsed_1b4c 1 1409 1 1 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1409 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 1410 1 1 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1410 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 1411 1 1 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1411 1 2 . . . . . . . . sbm1 14 . ha parsed_1b4c 1 1412 1 1 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1412 1 2 . . . . . . . . sbm2 14 . ha parsed_1b4c 1 1413 1 1 . . . . . . . . sbm1 70 . hb* parsed_1b4c 1 1413 1 2 . . . . . . . . sbm1 14 . hd* parsed_1b4c 1 1414 1 1 . . . . . . . . sbm2 70 . hb* parsed_1b4c 1 1414 1 2 . . . . . . . . sbm2 14 . hd* parsed_1b4c 1 1415 1 1 . . . . . . . . sbm1 70 . hd* parsed_1b4c 1 1415 1 2 . . . . . . . . sbm1 14 . hd* parsed_1b4c 1 1416 1 1 . . . . . . . . sbm2 70 . hd* parsed_1b4c 1 1416 1 2 . . . . . . . . sbm2 14 . hd* parsed_1b4c 1 1417 1 1 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1417 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 1418 1 1 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1418 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 1419 1 1 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 1419 1 2 . . . . . . . . sbm1 17 . hb* parsed_1b4c 1 1420 1 1 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 1420 1 2 . . . . . . . . sbm2 17 . hb* parsed_1b4c 1 1421 1 1 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1421 1 2 . . . . . . . . sbm1 17 . hn parsed_1b4c 1 1422 1 1 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1422 1 2 . . . . . . . . sbm2 17 . hn parsed_1b4c 1 1423 1 1 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1423 1 2 . . . . . . . . sbm1 17 . hb* parsed_1b4c 1 1424 1 1 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1424 1 2 . . . . . . . . sbm2 17 . hb* parsed_1b4c 1 1425 1 1 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 1425 1 2 . . . . . . . . sbm1 18 . hn parsed_1b4c 1 1426 1 1 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 1426 1 2 . . . . . . . . sbm2 18 . hn parsed_1b4c 1 1427 1 1 . . . . . . . . sbm1 14 . hz parsed_1b4c 1 1427 1 2 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 1428 1 1 . . . . . . . . sbm2 14 . hz parsed_1b4c 1 1428 1 2 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 1429 1 1 . . . . . . . . sbm1 14 . he* parsed_1b4c 1 1429 1 2 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 1430 1 1 . . . . . . . . sbm2 14 . he* parsed_1b4c 1 1430 1 2 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 1431 1 1 . . . . . . . . sbm1 18 . hb* parsed_1b4c 1 1431 1 2 . . . . . . . . sbm1 26 . hn parsed_1b4c 1 1432 1 1 . . . . . . . . sbm2 18 . hb* parsed_1b4c 1 1432 1 2 . . . . . . . . sbm2 26 . hn parsed_1b4c 1 1433 1 1 . . . . . . . . sbm1 69 . ha parsed_1b4c 1 1433 1 2 . . . . . . . . sbm1 26 . ha parsed_1b4c 1 1434 1 1 . . . . . . . . sbm2 69 . ha parsed_1b4c 1 1434 1 2 . . . . . . . . sbm2 26 . ha parsed_1b4c 1 1435 1 1 . . . . . . . . sbm1 14 . hz parsed_1b4c 1 1435 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 1436 1 1 . . . . . . . . sbm2 14 . hz parsed_1b4c 1 1436 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 1437 1 1 . . . . . . . . sbm1 17 . hd* parsed_1b4c 1 1437 1 2 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 1438 1 1 . . . . . . . . sbm2 17 . hd* parsed_1b4c 1 1438 1 2 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 1439 1 1 . . . . . . . . sbm1 18 . ha parsed_1b4c 1 1439 1 2 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 1440 1 1 . . . . . . . . sbm2 18 . ha parsed_1b4c 1 1440 1 2 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 1441 1 1 . . . . . . . . sbm1 67 . ha parsed_1b4c 1 1441 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 1442 1 1 . . . . . . . . sbm2 67 . ha parsed_1b4c 1 1442 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 1443 1 1 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1443 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 1444 1 1 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1444 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 1445 1 1 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1445 1 2 . . . . . . . . sbm1 27 . ha parsed_1b4c 1 1446 1 1 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1446 1 2 . . . . . . . . sbm2 27 . ha parsed_1b4c 1 1447 1 1 . . . . . . . . sbm1 68 . ha parsed_1b4c 1 1447 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 1448 1 1 . . . . . . . . sbm2 68 . ha parsed_1b4c 1 1448 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 1449 1 1 . . . . . . . . sbm1 68 . hb* parsed_1b4c 1 1449 1 2 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 1450 1 1 . . . . . . . . sbm2 68 . hb* parsed_1b4c 1 1450 1 2 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 1451 1 1 . . . . . . . . sbm1 69 . ha parsed_1b4c 1 1451 1 2 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 1452 1 1 . . . . . . . . sbm2 69 . ha parsed_1b4c 1 1452 1 2 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 1453 1 1 . . . . . . . . sbm1 67 . ha parsed_1b4c 1 1453 1 2 . . . . . . . . sbm1 28 . ha parsed_1b4c 1 1454 1 1 . . . . . . . . sbm2 67 . ha parsed_1b4c 1 1454 1 2 . . . . . . . . sbm2 28 . ha parsed_1b4c 1 1455 1 1 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1455 1 2 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 1456 1 1 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1456 1 2 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 1457 1 1 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1457 1 2 . . . . . . . . sbm1 29 . ha parsed_1b4c 1 1458 1 1 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1458 1 2 . . . . . . . . sbm2 29 . ha parsed_1b4c 1 1459 1 1 . . . . . . . . sbm1 67 . hn parsed_1b4c 1 1459 1 2 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 1460 1 1 . . . . . . . . sbm2 67 . hn parsed_1b4c 1 1460 1 2 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 1461 1 1 . . . . . . . . sbm1 67 . ha parsed_1b4c 1 1461 1 2 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 1462 1 1 . . . . . . . . sbm2 67 . ha parsed_1b4c 1 1462 1 2 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 1463 1 1 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1463 1 2 . . . . . . . . sbm1 30 . hn parsed_1b4c 1 1464 1 1 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1464 1 2 . . . . . . . . sbm2 30 . hn parsed_1b4c 1 1465 1 1 . . . . . . . . sbm1 60 . hg parsed_1b4c 1 1465 1 2 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1466 1 1 . . . . . . . . sbm2 60 . hg parsed_1b4c 1 1466 1 2 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1467 1 1 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1467 1 2 . . . . . . . . sbm1 32 . hn parsed_1b4c 1 1468 1 1 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1468 1 2 . . . . . . . . sbm2 32 . hn parsed_1b4c 1 1469 1 1 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1469 1 2 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1470 1 1 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1470 1 2 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1471 1 1 . . . . . . . . sbm1 73 . ha parsed_1b4c 1 1471 1 2 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1472 1 1 . . . . . . . . sbm2 73 . ha parsed_1b4c 1 1472 1 2 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1473 1 1 . . . . . . . . sbm1 73 . hd* parsed_1b4c 1 1473 1 2 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1474 1 1 . . . . . . . . sbm2 73 . hd* parsed_1b4c 1 1474 1 2 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1475 1 1 . . . . . . . . sbm1 76 . hb* parsed_1b4c 1 1475 1 2 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1476 1 1 . . . . . . . . sbm2 76 . hb* parsed_1b4c 1 1476 1 2 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1477 1 1 . . . . . . . . sbm1 76 . hd* parsed_1b4c 1 1477 1 2 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1478 1 1 . . . . . . . . sbm2 76 . hd* parsed_1b4c 1 1478 1 2 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1479 1 1 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1479 1 2 . . . . . . . . sbm1 33 . hn parsed_1b4c 1 1480 1 1 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1480 1 2 . . . . . . . . sbm2 33 . hn parsed_1b4c 1 1481 1 1 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1481 1 2 . . . . . . . . sbm1 33 . ha parsed_1b4c 1 1482 1 1 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1482 1 2 . . . . . . . . sbm2 33 . ha parsed_1b4c 1 1483 1 1 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1483 1 2 . . . . . . . . sbm1 34 . hn parsed_1b4c 1 1484 1 1 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1484 1 2 . . . . . . . . sbm2 34 . hn parsed_1b4c 1 1485 1 1 . . . . . . . . sbm1 17 . hd* parsed_1b4c 1 1485 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 1486 1 1 . . . . . . . . sbm2 17 . hd* parsed_1b4c 1 1486 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 1487 1 1 . . . . . . . . sbm1 17 . hd* parsed_1b4c 1 1487 1 2 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1488 1 1 . . . . . . . . sbm2 17 . hd* parsed_1b4c 1 1488 1 2 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1489 1 1 . . . . . . . . sbm1 17 . he* parsed_1b4c 1 1489 1 2 . . . . . . . . sbm1 35 . hn parsed_1b4c 1 1490 1 1 . . . . . . . . sbm2 17 . he* parsed_1b4c 1 1490 1 2 . . . . . . . . sbm2 35 . hn parsed_1b4c 1 1491 1 1 . . . . . . . . sbm1 17 . he* parsed_1b4c 1 1491 1 2 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1492 1 1 . . . . . . . . sbm2 17 . he* parsed_1b4c 1 1492 1 2 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1493 1 1 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 1493 1 2 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1494 1 1 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 1494 1 2 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1495 1 1 . . . . . . . . sbm1 73 . he* parsed_1b4c 1 1495 1 2 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1496 1 1 . . . . . . . . sbm2 73 . he* parsed_1b4c 1 1496 1 2 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1497 1 1 . . . . . . . . sbm1 73 . hz parsed_1b4c 1 1497 1 2 . . . . . . . . sbm1 35 . hd* parsed_1b4c 1 1498 1 1 . . . . . . . . sbm2 73 . hz parsed_1b4c 1 1498 1 2 . . . . . . . . sbm2 35 . hd* parsed_1b4c 1 1499 1 1 . . . . . . . . sbm1 56 . hg1* parsed_1b4c 1 1499 1 2 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1500 1 1 . . . . . . . . sbm2 56 . hg1* parsed_1b4c 1 1500 1 2 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1501 1 1 . . . . . . . . sbm1 76 . hb* parsed_1b4c 1 1501 1 2 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1502 1 1 . . . . . . . . sbm2 76 . hb* parsed_1b4c 1 1502 1 2 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1503 1 1 . . . . . . . . sbm1 77 . ha parsed_1b4c 1 1503 1 2 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1504 1 1 . . . . . . . . sbm2 77 . ha parsed_1b4c 1 1504 1 2 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1505 1 1 . . . . . . . . sbm1 80 . hg1* parsed_1b4c 1 1505 1 2 . . . . . . . . sbm1 36 . hg2* parsed_1b4c 1 1506 1 1 . . . . . . . . sbm2 80 . hg1* parsed_1b4c 1 1506 1 2 . . . . . . . . sbm2 36 . hg2* parsed_1b4c 1 1507 1 1 . . . . . . . . sbm1 77 . ha parsed_1b4c 1 1507 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1508 1 1 . . . . . . . . sbm2 77 . ha parsed_1b4c 1 1508 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1509 1 1 . . . . . . . . sbm1 77 . hb parsed_1b4c 1 1509 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1510 1 1 . . . . . . . . sbm2 77 . hb parsed_1b4c 1 1510 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1511 1 1 . . . . . . . . sbm1 77 . hg1* parsed_1b4c 1 1511 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1512 1 1 . . . . . . . . sbm2 77 . hg1* parsed_1b4c 1 1512 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1513 1 1 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1513 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1514 1 1 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1514 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1515 1 1 . . . . . . . . sbm1 80 . hg1* parsed_1b4c 1 1515 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1516 1 1 . . . . . . . . sbm2 80 . hg1* parsed_1b4c 1 1516 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1517 1 1 . . . . . . . . sbm1 80 . hb parsed_1b4c 1 1517 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1518 1 1 . . . . . . . . sbm2 80 . hb parsed_1b4c 1 1518 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1519 1 1 . . . . . . . . sbm1 53 . hg1* parsed_1b4c 1 1519 1 2 . . . . . . . . sbm1 44 . hd* parsed_1b4c 1 1520 1 1 . . . . . . . . sbm2 53 . hg1* parsed_1b4c 1 1520 1 2 . . . . . . . . sbm2 44 . hd* parsed_1b4c 1 1521 1 1 . . . . . . . . sbm1 57 . he* parsed_1b4c 1 1521 1 2 . . . . . . . . sbm1 44 . hd* parsed_1b4c 1 1522 1 1 . . . . . . . . sbm2 57 . he* parsed_1b4c 1 1522 1 2 . . . . . . . . sbm2 44 . hd* parsed_1b4c 1 1523 1 1 . . . . . . . . sbm1 80 . hg1* parsed_1b4c 1 1523 1 2 . . . . . . . . sbm1 44 . hd* parsed_1b4c 1 1524 1 1 . . . . . . . . sbm2 80 . hg1* parsed_1b4c 1 1524 1 2 . . . . . . . . sbm2 44 . hd* parsed_1b4c 1 1525 1 1 . . . . . . . . sbm1 53 . hb parsed_1b4c 1 1525 1 2 . . . . . . . . sbm1 47 . hg2* parsed_1b4c 1 1526 1 1 . . . . . . . . sbm2 53 . hb parsed_1b4c 1 1526 1 2 . . . . . . . . sbm2 47 . hg2* parsed_1b4c 1 1527 1 1 . . . . . . . . sbm1 53 . hb parsed_1b4c 1 1527 1 2 . . . . . . . . sbm1 47 . hd* parsed_1b4c 1 1528 1 1 . . . . . . . . sbm2 53 . hb parsed_1b4c 1 1528 1 2 . . . . . . . . sbm2 47 . hd* parsed_1b4c 1 1529 1 1 . . . . . . . . sbm1 53 . hg1* parsed_1b4c 1 1529 1 2 . . . . . . . . sbm1 47 . hg2* parsed_1b4c 1 1530 1 1 . . . . . . . . sbm2 53 . hg1* parsed_1b4c 1 1530 1 2 . . . . . . . . sbm2 47 . hg2* parsed_1b4c 1 1531 1 1 . . . . . . . . sbm1 53 . hg2* parsed_1b4c 1 1531 1 2 . . . . . . . . sbm1 47 . hg2* parsed_1b4c 1 1532 1 1 . . . . . . . . sbm2 53 . hg2* parsed_1b4c 1 1532 1 2 . . . . . . . . sbm2 47 . hg2* parsed_1b4c 1 1533 1 1 . . . . . . . . sbm1 53 . hg2* parsed_1b4c 1 1533 1 2 . . . . . . . . sbm1 47 . hd* parsed_1b4c 1 1534 1 1 . . . . . . . . sbm2 53 . hg2* parsed_1b4c 1 1534 1 2 . . . . . . . . sbm2 47 . hd* parsed_1b4c 1 1535 1 1 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1535 1 2 . . . . . . . . sbm1 47 . hg2* parsed_1b4c 1 1536 1 1 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1536 1 2 . . . . . . . . sbm2 47 . hg2* parsed_1b4c 1 1537 1 1 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1537 1 2 . . . . . . . . sbm1 49 . hn parsed_1b4c 1 1538 1 1 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1538 1 2 . . . . . . . . sbm2 49 . hn parsed_1b4c 1 1539 1 1 . . . . . . . . sbm1 80 . ha parsed_1b4c 1 1539 1 2 . . . . . . . . sbm1 52 . hg2* parsed_1b4c 1 1540 1 1 . . . . . . . . sbm2 80 . ha parsed_1b4c 1 1540 1 2 . . . . . . . . sbm2 52 . hg2* parsed_1b4c 1 1541 1 1 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1541 1 2 . . . . . . . . sbm1 52 . hg2* parsed_1b4c 1 1542 1 1 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1542 1 2 . . . . . . . . sbm2 52 . hg2* parsed_1b4c 1 1543 1 1 . . . . . . . . sbm1 47 . hg1* parsed_1b4c 1 1543 1 2 . . . . . . . . sbm1 53 . hg2* parsed_1b4c 1 1544 1 1 . . . . . . . . sbm2 47 . hg1* parsed_1b4c 1 1544 1 2 . . . . . . . . sbm2 53 . hg2* parsed_1b4c 1 1545 1 1 . . . . . . . . sbm1 47 . hd* parsed_1b4c 1 1545 1 2 . . . . . . . . sbm1 53 . hg2* parsed_1b4c 1 1546 1 1 . . . . . . . . sbm2 47 . hd* parsed_1b4c 1 1546 1 2 . . . . . . . . sbm2 53 . hg2* parsed_1b4c 1 1547 1 1 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1547 1 2 . . . . . . . . sbm1 53 . hn parsed_1b4c 1 1548 1 1 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1548 1 2 . . . . . . . . sbm2 53 . hn parsed_1b4c 1 1549 1 1 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1549 1 2 . . . . . . . . sbm1 53 . hg2* parsed_1b4c 1 1550 1 1 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1550 1 2 . . . . . . . . sbm2 53 . hg2* parsed_1b4c 1 1551 1 1 . . . . . . . . sbm1 76 . ha parsed_1b4c 1 1551 1 2 . . . . . . . . sbm1 56 . hg2* parsed_1b4c 1 1552 1 1 . . . . . . . . sbm2 76 . ha parsed_1b4c 1 1552 1 2 . . . . . . . . sbm2 56 . hg2* parsed_1b4c 1 1553 1 1 . . . . . . . . sbm1 76 . he* parsed_1b4c 1 1553 1 2 . . . . . . . . sbm1 56 . hg2* parsed_1b4c 1 1554 1 1 . . . . . . . . sbm2 76 . he* parsed_1b4c 1 1554 1 2 . . . . . . . . sbm2 56 . hg2* parsed_1b4c 1 1555 1 1 . . . . . . . . sbm1 79 . ha parsed_1b4c 1 1555 1 2 . . . . . . . . sbm1 56 . hg2* parsed_1b4c 1 1556 1 1 . . . . . . . . sbm2 79 . ha parsed_1b4c 1 1556 1 2 . . . . . . . . sbm2 56 . hg2* parsed_1b4c 1 1557 1 1 . . . . . . . . sbm1 79 . hb* parsed_1b4c 1 1557 1 2 . . . . . . . . sbm1 56 . hg2* parsed_1b4c 1 1558 1 1 . . . . . . . . sbm2 79 . hb* parsed_1b4c 1 1558 1 2 . . . . . . . . sbm2 56 . hg2* parsed_1b4c 1 1559 1 1 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 1559 1 2 . . . . . . . . sbm1 56 . hn parsed_1b4c 1 1560 1 1 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 1560 1 2 . . . . . . . . sbm2 56 . hn parsed_1b4c 1 1561 1 1 . . . . . . . . sbm1 33 . ha parsed_1b4c 1 1561 1 2 . . . . . . . . sbm1 57 . he* parsed_1b4c 1 1562 1 1 . . . . . . . . sbm2 33 . ha parsed_1b4c 1 1562 1 2 . . . . . . . . sbm2 57 . he* parsed_1b4c 1 1563 1 1 . . . . . . . . sbm1 33 . hg* parsed_1b4c 1 1563 1 2 . . . . . . . . sbm1 57 . he* parsed_1b4c 1 1564 1 1 . . . . . . . . sbm2 33 . hg* parsed_1b4c 1 1564 1 2 . . . . . . . . sbm2 57 . he* parsed_1b4c 1 1565 1 1 . . . . . . . . sbm1 36 . hb parsed_1b4c 1 1565 1 2 . . . . . . . . sbm1 57 . he* parsed_1b4c 1 1566 1 1 . . . . . . . . sbm2 36 . hb parsed_1b4c 1 1566 1 2 . . . . . . . . sbm2 57 . he* parsed_1b4c 1 1567 1 1 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1567 1 2 . . . . . . . . sbm1 57 . he* parsed_1b4c 1 1568 1 1 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1568 1 2 . . . . . . . . sbm2 57 . he* parsed_1b4c 1 1569 1 1 . . . . . . . . sbm1 36 . hg2* parsed_1b4c 1 1569 1 2 . . . . . . . . sbm1 57 . he* parsed_1b4c 1 1570 1 1 . . . . . . . . sbm2 36 . hg2* parsed_1b4c 1 1570 1 2 . . . . . . . . sbm2 57 . he* parsed_1b4c 1 1571 1 1 . . . . . . . . sbm1 37 . ha parsed_1b4c 1 1571 1 2 . . . . . . . . sbm1 57 . he* parsed_1b4c 1 1572 1 1 . . . . . . . . sbm2 37 . ha parsed_1b4c 1 1572 1 2 . . . . . . . . sbm2 57 . he* parsed_1b4c 1 1573 1 1 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 1573 1 2 . . . . . . . . sbm1 57 . hn parsed_1b4c 1 1574 1 1 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 1574 1 2 . . . . . . . . sbm2 57 . hn parsed_1b4c 1 1575 1 1 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 1575 1 2 . . . . . . . . sbm1 57 . he* parsed_1b4c 1 1576 1 1 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 1576 1 2 . . . . . . . . sbm2 57 . he* parsed_1b4c 1 1577 1 1 . . . . . . . . sbm1 76 . hz parsed_1b4c 1 1577 1 2 . . . . . . . . sbm1 59 . hg2* parsed_1b4c 1 1578 1 1 . . . . . . . . sbm2 76 . hz parsed_1b4c 1 1578 1 2 . . . . . . . . sbm2 59 . hg2* parsed_1b4c 1 1579 1 1 . . . . . . . . sbm1 33 . hb* parsed_1b4c 1 1579 1 2 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1580 1 1 . . . . . . . . sbm2 33 . hb* parsed_1b4c 1 1580 1 2 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1581 1 1 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1581 1 2 . . . . . . . . sbm1 60 . hd* parsed_1b4c 1 1582 1 1 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1582 1 2 . . . . . . . . sbm2 60 . hd* parsed_1b4c 1 1583 1 1 . . . . . . . . sbm1 76 . hz parsed_1b4c 1 1583 1 2 . . . . . . . . sbm1 60 . hn parsed_1b4c 1 1584 1 1 . . . . . . . . sbm2 76 . hz parsed_1b4c 1 1584 1 2 . . . . . . . . sbm2 60 . hn parsed_1b4c 1 1585 1 1 . . . . . . . . sbm1 29 . hb* parsed_1b4c 1 1585 1 2 . . . . . . . . sbm1 63 . ha parsed_1b4c 1 1586 1 1 . . . . . . . . sbm2 29 . hb* parsed_1b4c 1 1586 1 2 . . . . . . . . sbm2 63 . ha parsed_1b4c 1 1587 1 1 . . . . . . . . sbm1 29 . hb* parsed_1b4c 1 1587 1 2 . . . . . . . . sbm1 66 . hn parsed_1b4c 1 1588 1 1 . . . . . . . . sbm2 29 . hb* parsed_1b4c 1 1588 1 2 . . . . . . . . sbm2 66 . hn parsed_1b4c 1 1589 1 1 . . . . . . . . sbm1 29 . he* parsed_1b4c 1 1589 1 2 . . . . . . . . sbm1 66 . ha parsed_1b4c 1 1590 1 1 . . . . . . . . sbm2 29 . he* parsed_1b4c 1 1590 1 2 . . . . . . . . sbm2 66 . ha parsed_1b4c 1 1591 1 1 . . . . . . . . sbm1 29 . he* parsed_1b4c 1 1591 1 2 . . . . . . . . sbm1 66 . hn parsed_1b4c 1 1592 1 1 . . . . . . . . sbm2 29 . he* parsed_1b4c 1 1592 1 2 . . . . . . . . sbm2 66 . hn parsed_1b4c 1 1593 1 1 . . . . . . . . sbm1 28 . ha parsed_1b4c 1 1593 1 2 . . . . . . . . sbm1 67 . hn parsed_1b4c 1 1594 1 1 . . . . . . . . sbm2 28 . ha parsed_1b4c 1 1594 1 2 . . . . . . . . sbm2 67 . hn parsed_1b4c 1 1595 1 1 . . . . . . . . sbm1 28 . hg* parsed_1b4c 1 1595 1 2 . . . . . . . . sbm1 67 . ha parsed_1b4c 1 1596 1 1 . . . . . . . . sbm2 28 . hg* parsed_1b4c 1 1596 1 2 . . . . . . . . sbm2 67 . ha parsed_1b4c 1 1597 1 1 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 1597 1 2 . . . . . . . . sbm1 67 . hn parsed_1b4c 1 1598 1 1 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 1598 1 2 . . . . . . . . sbm2 67 . hn parsed_1b4c 1 1599 1 1 . . . . . . . . sbm1 26 . ha parsed_1b4c 1 1599 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1600 1 1 . . . . . . . . sbm2 26 . ha parsed_1b4c 1 1600 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1601 1 1 . . . . . . . . sbm1 26 . hb* parsed_1b4c 1 1601 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1602 1 1 . . . . . . . . sbm2 26 . hb* parsed_1b4c 1 1602 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1603 1 1 . . . . . . . . sbm1 27 . hn parsed_1b4c 1 1603 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1604 1 1 . . . . . . . . sbm2 27 . hn parsed_1b4c 1 1604 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1605 1 1 . . . . . . . . sbm1 27 . hb* parsed_1b4c 1 1605 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1606 1 1 . . . . . . . . sbm2 27 . hb* parsed_1b4c 1 1606 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1607 1 1 . . . . . . . . sbm1 27 . hd* parsed_1b4c 1 1607 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1608 1 1 . . . . . . . . sbm2 27 . hd* parsed_1b4c 1 1608 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1609 1 1 . . . . . . . . sbm1 28 . hn parsed_1b4c 1 1609 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1610 1 1 . . . . . . . . sbm2 28 . hn parsed_1b4c 1 1610 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1611 1 1 . . . . . . . . sbm1 28 . ha parsed_1b4c 1 1611 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1612 1 1 . . . . . . . . sbm2 28 . ha parsed_1b4c 1 1612 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1613 1 1 . . . . . . . . sbm1 28 . hb* parsed_1b4c 1 1613 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1614 1 1 . . . . . . . . sbm2 28 . hb* parsed_1b4c 1 1614 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1615 1 1 . . . . . . . . sbm1 29 . hn parsed_1b4c 1 1615 1 2 . . . . . . . . sbm1 68 . hn parsed_1b4c 1 1616 1 1 . . . . . . . . sbm2 29 . hn parsed_1b4c 1 1616 1 2 . . . . . . . . sbm2 68 . hn parsed_1b4c 1 1617 1 1 . . . . . . . . sbm1 26 . hb* parsed_1b4c 1 1617 1 2 . . . . . . . . sbm1 69 . hn parsed_1b4c 1 1618 1 1 . . . . . . . . sbm2 26 . hb* parsed_1b4c 1 1618 1 2 . . . . . . . . sbm2 69 . hn parsed_1b4c 1 1619 1 1 . . . . . . . . sbm1 14 . he* parsed_1b4c 1 1619 1 2 . . . . . . . . sbm1 70 . hn parsed_1b4c 1 1620 1 1 . . . . . . . . sbm2 14 . he* parsed_1b4c 1 1620 1 2 . . . . . . . . sbm2 70 . hn parsed_1b4c 1 1621 1 1 . . . . . . . . sbm1 14 . he* parsed_1b4c 1 1621 1 2 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 1622 1 1 . . . . . . . . sbm2 14 . he* parsed_1b4c 1 1622 1 2 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 1623 1 1 . . . . . . . . sbm1 14 . hz parsed_1b4c 1 1623 1 2 . . . . . . . . sbm1 70 . hn parsed_1b4c 1 1624 1 1 . . . . . . . . sbm2 14 . hz parsed_1b4c 1 1624 1 2 . . . . . . . . sbm2 70 . hn parsed_1b4c 1 1625 1 1 . . . . . . . . sbm1 14 . hz parsed_1b4c 1 1625 1 2 . . . . . . . . sbm1 70 . ha parsed_1b4c 1 1626 1 1 . . . . . . . . sbm2 14 . hz parsed_1b4c 1 1626 1 2 . . . . . . . . sbm2 70 . ha parsed_1b4c 1 1627 1 1 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 1627 1 2 . . . . . . . . sbm2 74 . he* parsed_1b4c 1 1628 1 1 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 1628 1 2 . . . . . . . . sbm1 74 . he* parsed_1b4c 1 1629 1 1 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1629 1 2 . . . . . . . . sbm1 74 . he* parsed_1b4c 1 1630 1 1 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1630 1 2 . . . . . . . . sbm2 74 . he* parsed_1b4c 1 1631 1 1 . . . . . . . . sbm1 32 . hd* parsed_1b4c 1 1631 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 1632 1 1 . . . . . . . . sbm2 32 . hd* parsed_1b4c 1 1632 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 1633 1 1 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1633 1 2 . . . . . . . . sbm1 77 . hn parsed_1b4c 1 1634 1 1 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1634 1 2 . . . . . . . . sbm2 77 . hn parsed_1b4c 1 1635 1 1 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1635 1 2 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1636 1 1 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1636 1 2 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1637 1 1 . . . . . . . . sbm1 52 . hg1* parsed_1b4c 1 1637 1 2 . . . . . . . . sbm1 79 . he* parsed_1b4c 1 1638 1 1 . . . . . . . . sbm2 52 . hg1* parsed_1b4c 1 1638 1 2 . . . . . . . . sbm2 79 . he* parsed_1b4c 1 1639 1 1 . . . . . . . . sbm1 56 . hg2* parsed_1b4c 1 1639 1 2 . . . . . . . . sbm1 79 . he* parsed_1b4c 1 1640 1 1 . . . . . . . . sbm2 56 . hg2* parsed_1b4c 1 1640 1 2 . . . . . . . . sbm2 79 . he* parsed_1b4c 1 1641 1 1 . . . . . . . . sbm1 56 . hg1* parsed_1b4c 1 1641 1 2 . . . . . . . . sbm1 79 . he* parsed_1b4c 1 1642 1 1 . . . . . . . . sbm2 56 . hg1* parsed_1b4c 1 1642 1 2 . . . . . . . . sbm2 79 . he* parsed_1b4c 1 1643 1 1 . . . . . . . . sbm1 36 . hg2* parsed_1b4c 1 1643 1 2 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 1644 1 1 . . . . . . . . sbm2 36 . hg2* parsed_1b4c 1 1644 1 2 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 1645 1 1 . . . . . . . . sbm1 36 . hd* parsed_1b4c 1 1645 1 2 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 1646 1 1 . . . . . . . . sbm2 36 . hd* parsed_1b4c 1 1646 1 2 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 1647 1 1 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1647 1 2 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 1648 1 1 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1648 1 2 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 1649 1 1 . . . . . . . . sbm1 56 . hg1* parsed_1b4c 1 1649 1 2 . . . . . . . . sbm1 80 . hg2* parsed_1b4c 1 1650 1 1 . . . . . . . . sbm2 56 . hg1* parsed_1b4c 1 1650 1 2 . . . . . . . . sbm2 80 . hg2* parsed_1b4c 1 1651 1 1 . . . . . . . . sbm1 43 . he* parsed_1b4c 1 1651 1 2 . . . . . . . . sbm1 81 . hg2* parsed_1b4c 1 1652 1 1 . . . . . . . . sbm2 43 . he* parsed_1b4c 1 1652 1 2 . . . . . . . . sbm2 81 . hg2* parsed_1b4c 1 1653 1 1 . . . . . . . . sbm1 49 . hb* parsed_1b4c 1 1653 1 2 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1654 1 1 . . . . . . . . sbm2 49 . hb* parsed_1b4c 1 1654 1 2 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1655 1 1 . . . . . . . . sbm1 49 . hg* parsed_1b4c 1 1655 1 2 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1656 1 1 . . . . . . . . sbm2 49 . hg* parsed_1b4c 1 1656 1 2 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1657 1 1 . . . . . . . . sbm1 52 . ha parsed_1b4c 1 1657 1 2 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1658 1 1 . . . . . . . . sbm2 52 . ha parsed_1b4c 1 1658 1 2 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1659 1 1 . . . . . . . . sbm1 52 . hb parsed_1b4c 1 1659 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 1660 1 1 . . . . . . . . sbm2 52 . hb parsed_1b4c 1 1660 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 1661 1 1 . . . . . . . . sbm1 52 . hb parsed_1b4c 1 1661 1 2 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1662 1 1 . . . . . . . . sbm2 52 . hb parsed_1b4c 1 1662 1 2 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1663 1 1 . . . . . . . . sbm1 52 . hg1* parsed_1b4c 1 1663 1 2 . . . . . . . . sbm1 83 . hn parsed_1b4c 1 1664 1 1 . . . . . . . . sbm2 52 . hg1* parsed_1b4c 1 1664 1 2 . . . . . . . . sbm2 83 . hn parsed_1b4c 1 1665 1 1 . . . . . . . . sbm1 52 . hg1* parsed_1b4c 1 1665 1 2 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1666 1 1 . . . . . . . . sbm2 52 . hg1* parsed_1b4c 1 1666 1 2 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1667 1 1 . . . . . . . . sbm1 53 . ha parsed_1b4c 1 1667 1 2 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1668 1 1 . . . . . . . . sbm2 53 . ha parsed_1b4c 1 1668 1 2 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1669 1 1 . . . . . . . . sbm1 53 . hb parsed_1b4c 1 1669 1 2 . . . . . . . . sbm1 83 . hb* parsed_1b4c 1 1670 1 1 . . . . . . . . sbm2 53 . hb parsed_1b4c 1 1670 1 2 . . . . . . . . sbm2 83 . hb* parsed_1b4c 1 1671 1 1 . . . . . . . . sbm1 82 . hg2* parsed_1b4c 1 1671 1 2 . . . . . . . . sbm1 87 . hd* parsed_1b4c 1 1672 1 1 . . . . . . . . sbm2 82 . hg2* parsed_1b4c 1 1672 1 2 . . . . . . . . sbm2 87 . hd* parsed_1b4c 1 1673 1 1 . . . . . . . . sbm1 13 . hg* parsed_1b4c 1 1673 1 2 . . . . . . . . sbm2 2 . hn parsed_1b4c 1 1674 1 1 . . . . . . . . sbm2 13 . hg* parsed_1b4c 1 1674 1 2 . . . . . . . . sbm1 2 . hn parsed_1b4c 1 1675 1 1 . . . . . . . . sbm1 10 . ha parsed_1b4c 1 1675 1 2 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1676 1 1 . . . . . . . . sbm2 10 . ha parsed_1b4c 1 1676 1 2 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1677 1 1 . . . . . . . . sbm1 10 . hg parsed_1b4c 1 1677 1 2 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1678 1 1 . . . . . . . . sbm2 10 . hg parsed_1b4c 1 1678 1 2 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1679 1 1 . . . . . . . . sbm1 13 . hg* parsed_1b4c 1 1679 1 2 . . . . . . . . sbm2 3 . hn parsed_1b4c 1 1680 1 1 . . . . . . . . sbm2 13 . hg* parsed_1b4c 1 1680 1 2 . . . . . . . . sbm1 3 . hn parsed_1b4c 1 1681 1 1 . . . . . . . . sbm1 13 . hb parsed_1b4c 1 1681 1 2 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1682 1 1 . . . . . . . . sbm2 13 . hb parsed_1b4c 1 1682 1 2 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1683 1 1 . . . . . . . . sbm1 39 . hb* parsed_1b4c 1 1683 1 2 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1684 1 1 . . . . . . . . sbm2 39 . hb* parsed_1b4c 1 1684 1 2 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1685 1 1 . . . . . . . . sbm1 73 . he* parsed_1b4c 1 1685 1 2 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1686 1 1 . . . . . . . . sbm2 73 . he* parsed_1b4c 1 1686 1 2 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1687 1 1 . . . . . . . . sbm1 73 . hz parsed_1b4c 1 1687 1 2 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1688 1 1 . . . . . . . . sbm2 73 . hz parsed_1b4c 1 1688 1 2 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1689 1 1 . . . . . . . . sbm1 6 . ha parsed_1b4c 1 1689 1 2 . . . . . . . . sbm2 6 . hb* parsed_1b4c 1 1690 1 1 . . . . . . . . sbm2 6 . ha parsed_1b4c 1 1690 1 2 . . . . . . . . sbm1 6 . hb* parsed_1b4c 1 1691 1 1 . . . . . . . . sbm1 10 . ha parsed_1b4c 1 1691 1 2 . . . . . . . . sbm2 6 . hb* parsed_1b4c 1 1692 1 1 . . . . . . . . sbm2 10 . ha parsed_1b4c 1 1692 1 2 . . . . . . . . sbm1 6 . hb* parsed_1b4c 1 1693 1 1 . . . . . . . . sbm1 10 . hb* parsed_1b4c 1 1693 1 2 . . . . . . . . sbm2 6 . hb* parsed_1b4c 1 1694 1 1 . . . . . . . . sbm2 10 . hb* parsed_1b4c 1 1694 1 2 . . . . . . . . sbm1 6 . hb* parsed_1b4c 1 1695 1 1 . . . . . . . . sbm1 10 . hg parsed_1b4c 1 1695 1 2 . . . . . . . . sbm2 6 . hb* parsed_1b4c 1 1696 1 1 . . . . . . . . sbm2 10 . hg parsed_1b4c 1 1696 1 2 . . . . . . . . sbm1 6 . hb* parsed_1b4c 1 1697 1 1 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1697 1 2 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 1698 1 1 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1698 1 2 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 1699 1 1 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1699 1 2 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 1700 1 1 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1700 1 2 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 1701 1 1 . . . . . . . . sbm1 78 . ha parsed_1b4c 1 1701 1 2 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 1702 1 1 . . . . . . . . sbm2 78 . ha parsed_1b4c 1 1702 1 2 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 1703 1 1 . . . . . . . . sbm1 81 . hb* parsed_1b4c 1 1703 1 2 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 1704 1 1 . . . . . . . . sbm2 81 . hb* parsed_1b4c 1 1704 1 2 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 1705 1 1 . . . . . . . . sbm1 43 . hz parsed_1b4c 1 1705 1 2 . . . . . . . . sbm2 8 . hg2* parsed_1b4c 1 1706 1 1 . . . . . . . . sbm2 43 . hz parsed_1b4c 1 1706 1 2 . . . . . . . . sbm1 8 . hg2* parsed_1b4c 1 1707 1 1 . . . . . . . . sbm1 43 . he* parsed_1b4c 1 1707 1 2 . . . . . . . . sbm2 8 . hg2* parsed_1b4c 1 1708 1 1 . . . . . . . . sbm2 43 . he* parsed_1b4c 1 1708 1 2 . . . . . . . . sbm1 8 . hg2* parsed_1b4c 1 1709 1 1 . . . . . . . . sbm1 43 . hz parsed_1b4c 1 1709 1 2 . . . . . . . . sbm2 8 . hn parsed_1b4c 1 1710 1 1 . . . . . . . . sbm2 43 . hz parsed_1b4c 1 1710 1 2 . . . . . . . . sbm1 8 . hn parsed_1b4c 1 1711 1 1 . . . . . . . . sbm1 3 . ha parsed_1b4c 1 1711 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1712 1 1 . . . . . . . . sbm2 3 . ha parsed_1b4c 1 1712 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1713 1 1 . . . . . . . . sbm1 6 . hb* parsed_1b4c 1 1713 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1714 1 1 . . . . . . . . sbm2 6 . hb* parsed_1b4c 1 1714 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1715 1 1 . . . . . . . . sbm1 10 . hg parsed_1b4c 1 1715 1 2 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1716 1 1 . . . . . . . . sbm2 10 . hg parsed_1b4c 1 1716 1 2 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1717 1 1 . . . . . . . . sbm1 2 . hb* parsed_1b4c 1 1717 1 2 . . . . . . . . sbm2 13 . hg2* parsed_1b4c 1 1718 1 1 . . . . . . . . sbm2 2 . hb* parsed_1b4c 1 1718 1 2 . . . . . . . . sbm1 13 . hg2* parsed_1b4c 1 1719 1 1 . . . . . . . . sbm1 2 . hb* parsed_1b4c 1 1719 1 2 . . . . . . . . sbm2 13 . hg1* parsed_1b4c 1 1720 1 1 . . . . . . . . sbm2 2 . hb* parsed_1b4c 1 1720 1 2 . . . . . . . . sbm1 13 . hg1* parsed_1b4c 1 1721 1 1 . . . . . . . . sbm1 2 . hg* parsed_1b4c 1 1721 1 2 . . . . . . . . sbm2 13 . hg2* parsed_1b4c 1 1722 1 1 . . . . . . . . sbm2 2 . hg* parsed_1b4c 1 1722 1 2 . . . . . . . . sbm1 13 . hg2* parsed_1b4c 1 1723 1 1 . . . . . . . . sbm1 2 . hg* parsed_1b4c 1 1723 1 2 . . . . . . . . sbm2 13 . hg1* parsed_1b4c 1 1724 1 1 . . . . . . . . sbm2 2 . hg* parsed_1b4c 1 1724 1 2 . . . . . . . . sbm1 13 . hg1* parsed_1b4c 1 1725 1 1 . . . . . . . . sbm1 3 . ha parsed_1b4c 1 1725 1 2 . . . . . . . . sbm2 13 . hg2* parsed_1b4c 1 1726 1 1 . . . . . . . . sbm2 3 . ha parsed_1b4c 1 1726 1 2 . . . . . . . . sbm1 13 . hg2* parsed_1b4c 1 1727 1 1 . . . . . . . . sbm1 3 . hb* parsed_1b4c 1 1727 1 2 . . . . . . . . sbm2 13 . hg1* parsed_1b4c 1 1728 1 1 . . . . . . . . sbm2 3 . hb* parsed_1b4c 1 1728 1 2 . . . . . . . . sbm1 13 . hg1* parsed_1b4c 1 1729 1 1 . . . . . . . . sbm1 3 . hb* parsed_1b4c 1 1729 1 2 . . . . . . . . sbm2 13 . hg2* parsed_1b4c 1 1730 1 1 . . . . . . . . sbm2 3 . hb* parsed_1b4c 1 1730 1 2 . . . . . . . . sbm1 13 . hg2* parsed_1b4c 1 1731 1 1 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1731 1 2 . . . . . . . . sbm2 13 . hg1* parsed_1b4c 1 1732 1 1 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1732 1 2 . . . . . . . . sbm1 13 . hg1* parsed_1b4c 1 1733 1 1 . . . . . . . . sbm1 6 . hb* parsed_1b4c 1 1733 1 2 . . . . . . . . sbm2 13 . hg2* parsed_1b4c 1 1734 1 1 . . . . . . . . sbm2 6 . hb* parsed_1b4c 1 1734 1 2 . . . . . . . . sbm1 13 . hg2* parsed_1b4c 1 1735 1 1 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1735 1 2 . . . . . . . . sbm2 14 . hn parsed_1b4c 1 1736 1 1 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1736 1 2 . . . . . . . . sbm1 14 . hn parsed_1b4c 1 1737 1 1 . . . . . . . . sbm1 87 . hz parsed_1b4c 1 1737 1 2 . . . . . . . . sbm2 14 . hd* parsed_1b4c 1 1738 1 1 . . . . . . . . sbm2 87 . hz parsed_1b4c 1 1738 1 2 . . . . . . . . sbm1 14 . hd* parsed_1b4c 1 1739 1 1 . . . . . . . . sbm1 8 . hg2* parsed_1b4c 1 1739 1 2 . . . . . . . . sbm2 40 . hd* parsed_1b4c 1 1740 1 1 . . . . . . . . sbm2 8 . hg2* parsed_1b4c 1 1740 1 2 . . . . . . . . sbm1 40 . hd* parsed_1b4c 1 1741 1 1 . . . . . . . . sbm1 8 . hg1* parsed_1b4c 1 1741 1 2 . . . . . . . . sbm2 43 . hd* parsed_1b4c 1 1742 1 1 . . . . . . . . sbm2 8 . hg1* parsed_1b4c 1 1742 1 2 . . . . . . . . sbm1 43 . hd* parsed_1b4c 1 1743 1 1 . . . . . . . . sbm1 82 . hg2* parsed_1b4c 1 1743 1 2 . . . . . . . . sbm2 71 . hn parsed_1b4c 1 1744 1 1 . . . . . . . . sbm2 82 . hg2* parsed_1b4c 1 1744 1 2 . . . . . . . . sbm1 71 . hn parsed_1b4c 1 1745 1 1 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 1745 1 2 . . . . . . . . sbm2 74 . he* parsed_1b4c 1 1746 1 1 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 1746 1 2 . . . . . . . . sbm1 74 . he* parsed_1b4c 1 1747 1 1 . . . . . . . . sbm1 10 . hd* parsed_1b4c 1 1747 1 2 . . . . . . . . sbm2 74 . he* parsed_1b4c 1 1748 1 1 . . . . . . . . sbm2 10 . hd* parsed_1b4c 1 1748 1 2 . . . . . . . . sbm1 74 . he* parsed_1b4c 1 1749 1 1 . . . . . . . . sbm1 78 . hb* parsed_1b4c 1 1749 1 2 . . . . . . . . sbm2 74 . he* parsed_1b4c 1 1750 1 1 . . . . . . . . sbm2 78 . hb* parsed_1b4c 1 1750 1 2 . . . . . . . . sbm1 74 . he* parsed_1b4c 1 1751 1 1 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1751 1 2 . . . . . . . . sbm2 77 . hg1* parsed_1b4c 1 1752 1 1 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1752 1 2 . . . . . . . . sbm1 77 . hg1* parsed_1b4c 1 1753 1 1 . . . . . . . . sbm1 3 . hd* parsed_1b4c 1 1753 1 2 . . . . . . . . sbm2 77 . hg2* parsed_1b4c 1 1754 1 1 . . . . . . . . sbm2 3 . hd* parsed_1b4c 1 1754 1 2 . . . . . . . . sbm1 77 . hg2* parsed_1b4c 1 1755 1 1 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 1755 1 2 . . . . . . . . sbm2 77 . hg1* parsed_1b4c 1 1756 1 1 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 1756 1 2 . . . . . . . . sbm1 77 . hg1* parsed_1b4c 1 1757 1 1 . . . . . . . . sbm1 71 . he2# parsed_1b4c 1 1757 1 2 . . . . . . . . sbm2 79 . hn parsed_1b4c 1 1758 1 1 . . . . . . . . sbm2 71 . he2# parsed_1b4c 1 1758 1 2 . . . . . . . . sbm1 79 . hn parsed_1b4c 1 1759 1 1 . . . . . . . . sbm1 7 . he* parsed_1b4c 1 1759 1 2 . . . . . . . . sbm2 81 . hg2* parsed_1b4c 1 1760 1 1 . . . . . . . . sbm2 7 . he* parsed_1b4c 1 1760 1 2 . . . . . . . . sbm1 81 . hg2* parsed_1b4c 1 1761 1 1 . . . . . . . . sbm1 11 . hd* parsed_1b4c 1 1761 1 2 . . . . . . . . sbm2 81 . hg2* parsed_1b4c 1 1762 1 1 . . . . . . . . sbm2 11 . hd* parsed_1b4c 1 1762 1 2 . . . . . . . . sbm1 81 . hg2* parsed_1b4c 1 1763 1 1 . . . . . . . . sbm1 70 . hd* parsed_1b4c 1 1763 1 2 . . . . . . . . sbm2 82 . hg2* parsed_1b4c 1 1764 1 1 . . . . . . . . sbm2 70 . hd* parsed_1b4c 1 1764 1 2 . . . . . . . . sbm1 82 . hg2* parsed_1b4c 1 1765 1 1 . . . . . . . . sbm1 14 . hd* parsed_1b4c 1 1765 1 2 . . . . . . . . sbm2 87 . he* parsed_1b4c 1 1766 1 1 . . . . . . . . sbm2 14 . hd* parsed_1b4c 1 1766 1 2 . . . . . . . . sbm1 87 . he* parsed_1b4c 1 1767 1 1 . . . . . . . . sbm1 70 . hb* parsed_1b4c 1 1767 1 2 . . . . . . . . sbm2 87 . he* parsed_1b4c 1 1768 1 1 . . . . . . . . sbm2 70 . hb* parsed_1b4c 1 1768 1 2 . . . . . . . . sbm1 87 . he* parsed_1b4c 1 1769 1 1 . . . . . . . . sbm1 70 . hd* parsed_1b4c 1 1769 1 2 . . . . . . . . sbm2 87 . hd* parsed_1b4c 1 1770 1 1 . . . . . . . . sbm2 70 . hd* parsed_1b4c 1 1770 1 2 . . . . . . . . sbm1 87 . hd* parsed_1b4c 1 1771 1 1 . . . . . . . . sbm1 70 . hd* parsed_1b4c 1 1771 1 2 . . . . . . . . sbm2 87 . he* parsed_1b4c 1 1772 1 1 . . . . . . . . sbm2 70 . hd* parsed_1b4c 1 1772 1 2 . . . . . . . . sbm1 87 . he* parsed_1b4c 1 1773 1 1 . . . . . . . . sbm1 70 . he* parsed_1b4c 1 1773 1 2 . . . . . . . . sbm2 87 . hd* parsed_1b4c 1 1774 1 1 . . . . . . . . sbm2 70 . he* parsed_1b4c 1 1774 1 2 . . . . . . . . sbm1 87 . hd* parsed_1b4c 1 1775 1 1 . . . . . . . . sbm1 11 . hg2* parsed_1b4c 1 1775 1 2 . . . . . . . . sbm2 88 . hn parsed_1b4c 1 1776 1 1 . . . . . . . . sbm2 11 . hg2* parsed_1b4c 1 1776 1 2 . . . . . . . . sbm1 88 . hn parsed_1b4c 1 1777 1 1 . . . . . . . . sbm1 14 . hd* parsed_1b4c 1 1777 1 2 . . . . . . . . sbm2 88 . he* parsed_1b4c 1 1778 1 1 . . . . . . . . sbm2 14 . hd* parsed_1b4c 1 1778 1 2 . . . . . . . . sbm1 88 . he* parsed_1b4c 1 1779 1 1 . . . . . . . . sbm1 70 . he* parsed_1b4c 1 1779 1 2 . . . . . . . . sbm2 88 . he* parsed_1b4c 1 1780 1 1 . . . . . . . . sbm2 70 . he* parsed_1b4c 1 1780 1 2 . . . . . . . . sbm1 88 . he* parsed_1b4c 1 stop_ loop_ _Dist_constraint_value.Constraint_ID _Dist_constraint_value.Tree_node_ID _Dist_constraint_value.Source_experiment_ID _Dist_constraint_value.Spectral_peak_ID _Dist_constraint_value.Intensity_val _Dist_constraint_value.Intensity_lower_val_err _Dist_constraint_value.Intensity_upper_val_err _Dist_constraint_value.Distance_val _Dist_constraint_value.Distance_lower_bound_val _Dist_constraint_value.Distance_upper_bound_val _Dist_constraint_value.Entry_ID _Dist_constraint_value.Distance_constraint_list_ID 1 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 2 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 3 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 4 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 5 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 6 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 7 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 8 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 9 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 10 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 11 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 12 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 13 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 14 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 15 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 16 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 17 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 18 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 19 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 20 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 21 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 22 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 23 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 24 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 25 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 26 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 27 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 28 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 29 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 30 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 31 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 32 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 33 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 34 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 35 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 36 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 37 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 38 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 39 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 40 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 41 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 42 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 43 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 44 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 45 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 46 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 47 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 48 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 49 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 50 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 51 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 52 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 53 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 54 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 55 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 56 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 57 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 58 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 59 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 60 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 61 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 62 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 63 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 64 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 65 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 66 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 67 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 68 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 69 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 70 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 71 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 72 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 73 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 74 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 75 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 76 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 77 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 78 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 79 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 80 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 81 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 82 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 83 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 84 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 85 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 86 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 87 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 88 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 89 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 90 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 91 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 92 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 93 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 94 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 95 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 96 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 97 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 98 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 99 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 100 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 101 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 102 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 103 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 104 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 105 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 106 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 107 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 108 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 109 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 110 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 111 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 112 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 113 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 114 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 115 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 116 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 117 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 118 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 119 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 120 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 121 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 122 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 123 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 124 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 125 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 126 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 127 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 128 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 129 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 130 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 131 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 132 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 133 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 134 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 135 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 136 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 137 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 138 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 139 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 140 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 141 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 142 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 143 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 144 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 145 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 146 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 147 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 148 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 149 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 150 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 151 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 152 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 153 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 154 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 155 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 156 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 157 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 158 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 159 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 160 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 161 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 162 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 163 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 164 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 165 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 166 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 167 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 168 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 169 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 170 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 171 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 172 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 173 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 174 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 175 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 176 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 177 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 178 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 179 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 180 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 181 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 182 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 183 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 184 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 185 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 186 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 187 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 188 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 189 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 190 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 191 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 192 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 193 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 194 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 195 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 196 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 197 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 198 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 199 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 200 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 201 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 202 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 203 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 204 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 205 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 206 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 207 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 208 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 209 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 210 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 211 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 212 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 213 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 214 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 215 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 216 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 217 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 218 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 219 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 220 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 221 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 222 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 223 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 224 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 225 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 226 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 227 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 228 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 229 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 230 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 231 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 232 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 233 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 234 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 235 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 236 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 237 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 238 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 239 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 240 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 241 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 242 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 243 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 244 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 245 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 246 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 247 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 248 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 249 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 250 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 251 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 252 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 253 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 254 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 255 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 256 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 257 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 258 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 259 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 260 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 261 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 262 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 263 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 264 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 265 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 266 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 267 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 268 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 269 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 270 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 271 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 272 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 273 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 274 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 275 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 276 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 277 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 278 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 279 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 280 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 281 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 282 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 283 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 284 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 285 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 286 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 287 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 288 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 289 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 290 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 291 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 292 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 293 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 294 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 295 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 296 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 297 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 298 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 299 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 300 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 301 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 302 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 303 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 304 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 305 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 306 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 307 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 308 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 309 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 310 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 311 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 312 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 313 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 314 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 315 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 316 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 317 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 318 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 319 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 320 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 321 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 322 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 323 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 324 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 325 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 326 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 327 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 328 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 329 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 330 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 331 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 332 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 333 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 334 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 335 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 336 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 337 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 338 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 339 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 340 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 341 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 342 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 343 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 344 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 345 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 346 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 347 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 348 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 349 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 350 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 351 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 352 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 353 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 354 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 355 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 356 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 357 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 358 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 359 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 360 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 361 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 362 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 363 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 364 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 365 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 366 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 367 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 368 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 369 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 370 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 371 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 372 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 373 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 374 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 375 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 376 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 377 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 378 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 379 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 380 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 381 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 382 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 383 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 384 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 385 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 386 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 387 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 388 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 389 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 390 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 391 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 392 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 393 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 394 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 395 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 396 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 397 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 398 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 399 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 400 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 401 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 402 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 403 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 404 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 405 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 406 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 407 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 408 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 409 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 410 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 411 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 412 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 413 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 414 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 415 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 416 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 417 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 418 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 419 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 420 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 421 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 422 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 423 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 424 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 425 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 426 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 427 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 428 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 429 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 430 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 431 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 432 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 433 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 434 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 435 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 436 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 437 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 438 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 439 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 440 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 441 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 442 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 443 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 444 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 445 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 446 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 447 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 448 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 449 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 450 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 451 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 452 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 453 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 454 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 455 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 456 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 457 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 458 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 459 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 460 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 461 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 462 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 463 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 464 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 465 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 466 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 467 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 468 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 469 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 470 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 471 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 472 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 473 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 474 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 475 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 476 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 477 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 478 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 479 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 480 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 481 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 482 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 483 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 484 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 485 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 486 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 487 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 488 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 489 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 490 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 491 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 492 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 493 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 494 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 495 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 496 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 497 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 498 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 499 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 500 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 501 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 502 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 503 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 504 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 505 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 506 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 507 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 508 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 509 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 510 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 511 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 512 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 513 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 514 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 515 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 516 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 517 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 518 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 519 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 520 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 521 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 522 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 523 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 524 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 525 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 526 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 527 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 528 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 529 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 530 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 531 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 532 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 533 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 534 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 535 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 536 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 537 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 538 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 539 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 540 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 541 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 542 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 543 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 544 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 545 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 546 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 547 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 548 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 549 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 550 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 551 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 552 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 553 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 554 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 555 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 556 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 557 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 558 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 559 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 560 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 561 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 562 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 563 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 564 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 565 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 566 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 567 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 568 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 569 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 570 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 571 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 572 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 573 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 574 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 575 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 576 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 577 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 578 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 579 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 580 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 581 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 582 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 583 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 584 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 585 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 586 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 587 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 588 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 589 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 590 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 591 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 592 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 593 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 594 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 595 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 596 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 597 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 598 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 599 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 600 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 601 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 602 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 603 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 604 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 605 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 606 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 607 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 608 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 609 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 610 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 611 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 612 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 613 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 614 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 615 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 616 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 617 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 618 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 619 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 620 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 621 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 622 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 623 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 624 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 625 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 626 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 627 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 628 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 629 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 630 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 631 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 632 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 633 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 634 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 635 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 636 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 637 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 638 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 639 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 640 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 641 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 642 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 643 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 644 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 645 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 646 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 647 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 648 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 649 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 650 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 651 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 652 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 653 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 654 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 655 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 656 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 657 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 658 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 659 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 660 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 661 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 662 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 663 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 664 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 665 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 666 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 667 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 668 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 669 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 670 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 671 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 672 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 673 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 674 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 675 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 676 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 677 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 678 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 679 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 680 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 681 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 682 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 683 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 684 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 685 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 686 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 687 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 688 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 689 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 690 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 691 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 692 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 693 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 694 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 695 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 696 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 697 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 698 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 699 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 700 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 701 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 702 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 703 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 704 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 705 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 706 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 707 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 708 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 709 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 710 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 711 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 712 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 713 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 714 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 715 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 716 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 717 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 718 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 719 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 720 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 721 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 722 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 723 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 724 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 725 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 726 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 727 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 728 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 729 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 730 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 731 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 732 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 733 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 734 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 735 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 736 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 737 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 738 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 739 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 740 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 741 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 742 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 743 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 744 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 745 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 746 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 747 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 748 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 749 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 750 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 751 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 752 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 753 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 754 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 755 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 756 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 757 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 758 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 759 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 760 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 761 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 762 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 763 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 764 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 765 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 766 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 767 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 768 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 769 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 770 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 771 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 772 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 773 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 774 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 775 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 776 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 777 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 778 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 779 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 780 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 781 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 782 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 783 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 784 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 785 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 786 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 787 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 788 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 789 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 790 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 791 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 792 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 793 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 794 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 795 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 796 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 797 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 798 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 799 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 800 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 801 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 802 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 803 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 804 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 805 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 806 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 807 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 808 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 809 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 810 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 811 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 812 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 813 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 814 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 815 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 816 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 817 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 818 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 819 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 820 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 821 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 822 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 823 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 824 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 825 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 826 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 827 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 828 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 829 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 830 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 831 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 832 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 833 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 834 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 835 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 836 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 837 1 . . . . . 1.8 1.8 5.3 parsed_1b4c 1 838 1 . . . . . 1.8 1.8 5.3 parsed_1b4c 1 839 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 840 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 841 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 842 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 843 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 844 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 845 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 846 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 847 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 848 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 849 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 850 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 851 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 852 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 853 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 854 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 855 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 856 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 857 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 858 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 859 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 860 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 861 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 862 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 863 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 864 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 865 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 866 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 867 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 868 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 869 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 870 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 871 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 872 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 873 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 874 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 875 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 876 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 877 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 878 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 879 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 880 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 881 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 882 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 883 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 884 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 885 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 886 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 887 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 888 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 889 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 890 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 891 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 892 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 893 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 894 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 895 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 896 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 897 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 898 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 899 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 900 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 901 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 902 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 903 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 904 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 905 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 906 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 907 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 908 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 909 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 910 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 911 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 912 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 913 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 914 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 915 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 916 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 917 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 918 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 919 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 920 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 921 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 922 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 923 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 924 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 925 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 926 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 927 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 928 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 929 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 930 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 931 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 932 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 933 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 934 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 935 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 936 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 937 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 938 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 939 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 940 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 941 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 942 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 943 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 944 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 945 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 946 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 947 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 948 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 949 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 950 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 951 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 952 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 953 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 954 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 955 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 956 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 957 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 958 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 959 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 960 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 961 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 962 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 963 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 964 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 965 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 966 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 967 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 968 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 969 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 970 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 971 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 972 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 973 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 974 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 975 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 976 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 977 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 978 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 979 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 980 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 981 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 982 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 983 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 984 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 985 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 986 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 987 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 988 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 989 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 990 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 991 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 992 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 993 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 994 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 995 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 996 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 997 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 998 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 999 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1000 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1001 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1002 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1003 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1004 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1005 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1006 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1007 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1008 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1009 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1010 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1011 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1012 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1013 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1014 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1015 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1016 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1017 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1018 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1019 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1020 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1021 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1022 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1023 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1024 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1025 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1026 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1027 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1028 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1029 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1030 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1031 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1032 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1033 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1034 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1035 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1036 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1037 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1038 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1039 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1040 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1041 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1042 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1043 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1044 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1045 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1046 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1047 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1048 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1049 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1050 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1051 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1052 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1053 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1054 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1055 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1056 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1057 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1058 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1059 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1060 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1061 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1062 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1063 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1064 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1065 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1066 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1067 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1068 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1069 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1070 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1071 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1072 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1073 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1074 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1075 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1076 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1077 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1078 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1079 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1080 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1081 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1082 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1083 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1084 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1085 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1086 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1087 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1088 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1089 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1090 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1091 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1092 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1093 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1094 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1095 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1096 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1097 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1098 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1099 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1100 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1101 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1102 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1103 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1104 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1105 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1106 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1107 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1108 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1109 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1110 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1111 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1112 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1113 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1114 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1115 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1116 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1117 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1118 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1119 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1120 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1121 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1122 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1123 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1124 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1125 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1126 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1127 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1128 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1129 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1130 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1131 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1132 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1133 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1134 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1135 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1136 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1137 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1138 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1139 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1140 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1141 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1142 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1143 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1144 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1145 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1146 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1147 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1148 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1149 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1150 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1151 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1152 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1153 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1154 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1155 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1156 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1157 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1158 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1159 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1160 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1161 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1162 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1163 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1164 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1165 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1166 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1167 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1168 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1169 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1170 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1171 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1172 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1173 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1174 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1175 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1176 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1177 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1178 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1179 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1180 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1181 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1182 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1183 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1184 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1185 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1186 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1187 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1188 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1189 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1190 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1191 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1192 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1193 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1194 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1195 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1196 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1197 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1198 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1199 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1200 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1201 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1202 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1203 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1204 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1205 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1206 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1207 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1208 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1209 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1210 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1211 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1212 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1213 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1214 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1215 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1216 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1217 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1218 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1219 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1220 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1221 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1222 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1223 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1224 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1225 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1226 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1227 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1228 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1229 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1230 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1231 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1232 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1233 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1234 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1235 1 . . . . . 1.8 1.8 4.6 parsed_1b4c 1 1236 1 . . . . . 1.8 1.8 4.6 parsed_1b4c 1 1237 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1238 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1239 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1240 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1241 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1242 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1243 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1244 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1245 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1246 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1247 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1248 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1249 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1250 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1251 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1252 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1253 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1254 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1255 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1256 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1257 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1258 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1259 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1260 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1261 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1262 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1263 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1264 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1265 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1266 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1267 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1268 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1269 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1270 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1271 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1272 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1273 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1274 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1275 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1276 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1277 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1278 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1279 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1280 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1281 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1282 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1283 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1284 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1285 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1286 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1287 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1288 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1289 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1290 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1291 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1292 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1293 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1294 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1295 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1296 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1297 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1298 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1299 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1300 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1301 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1302 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1303 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1304 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1305 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1306 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1307 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1308 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1309 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1310 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1311 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1312 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1313 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1314 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1315 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1316 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1317 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1318 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1319 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1320 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1321 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1322 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1323 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1324 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1325 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1326 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1327 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1328 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1329 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1330 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1331 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1332 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1333 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1334 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1335 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1336 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1337 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1338 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1339 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1340 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1341 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1342 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1343 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1344 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1345 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1346 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1347 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1348 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1349 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1350 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1351 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1352 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1353 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1354 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1355 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1356 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1357 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1358 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1359 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1360 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1361 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1362 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1363 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1364 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1365 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1366 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1367 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1368 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1369 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1370 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1371 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1372 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1373 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1374 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1375 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1376 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1377 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1378 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1379 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1380 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1381 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1382 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1383 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1384 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1385 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1386 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1387 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1388 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1389 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1390 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1391 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1392 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1393 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1394 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1395 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1396 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1397 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1398 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1399 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1400 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1401 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1402 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1403 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1404 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1405 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1406 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1407 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1408 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1409 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1410 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1411 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1412 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1413 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1414 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1415 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1416 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1417 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1418 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1419 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1420 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1421 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1422 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1423 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1424 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1425 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1426 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1427 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1428 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1429 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1430 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1431 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1432 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1433 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 1434 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 1435 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1436 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1437 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1438 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1439 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1440 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1441 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1442 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1443 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1444 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1445 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1446 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1447 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1448 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1449 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1450 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1451 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 1452 1 . . . . . 1.8 1.8 3.0 parsed_1b4c 1 1453 1 . . . . . 1.8 1.8 3.2 parsed_1b4c 1 1454 1 . . . . . 1.8 1.8 3.2 parsed_1b4c 1 1455 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1456 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1457 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1458 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1459 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1460 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1461 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1462 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1463 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1464 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1465 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1466 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1467 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1468 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1469 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1470 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1471 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1472 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1473 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1474 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1475 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1476 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1477 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1478 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1479 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1480 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1481 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1482 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1483 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1484 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1485 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1486 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1487 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1488 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1489 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1490 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1491 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1492 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1493 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1494 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1495 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1496 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1497 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1498 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1499 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1500 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1501 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1502 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1503 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1504 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1505 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1506 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1507 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1508 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1509 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1510 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1511 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1512 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1513 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1514 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1515 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1516 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1517 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1518 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1519 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1520 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1521 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1522 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1523 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1524 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1525 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1526 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1527 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1528 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1529 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1530 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1531 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1532 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1533 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1534 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1535 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1536 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1537 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1538 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1539 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1540 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1541 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1542 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1543 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1544 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1545 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1546 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1547 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1548 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1549 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1550 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1551 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1552 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1553 1 . . . . . 1.8 1.8 4.3 parsed_1b4c 1 1554 1 . . . . . 1.8 1.8 4.3 parsed_1b4c 1 1555 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1556 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1557 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1558 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1559 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1560 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1561 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1562 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1563 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1564 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1565 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1566 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1567 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1568 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1569 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1570 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1571 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1572 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1573 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1574 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1575 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1576 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1577 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1578 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1579 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1580 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1581 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1582 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1583 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1584 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1585 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1586 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1587 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1588 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1589 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1590 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1591 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1592 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1593 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1594 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1595 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1596 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1597 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1598 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1599 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1600 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1601 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1602 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1603 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1604 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1605 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1606 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1607 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1608 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1609 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1610 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1611 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1612 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1613 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1614 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1615 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1616 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1617 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1618 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1619 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1620 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1621 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1622 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1623 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1624 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1625 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1626 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1627 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1628 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1629 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1630 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1631 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1632 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1633 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1634 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1635 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1636 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1637 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1638 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1639 1 . . . . . 1.8 1.8 4.3 parsed_1b4c 1 1640 1 . . . . . 1.8 1.8 4.3 parsed_1b4c 1 1641 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1642 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1643 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1644 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1645 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1646 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1647 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1648 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1649 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1650 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1651 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1652 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1653 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1654 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1655 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1656 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1657 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1658 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1659 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1660 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1661 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1662 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1663 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1664 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1665 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1666 1 . . . . . 1.8 1.8 3.5 parsed_1b4c 1 1667 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1668 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1669 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1670 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1671 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1672 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1673 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1674 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1675 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1676 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1677 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1678 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1679 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1680 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1681 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1682 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1683 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1684 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1685 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1686 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1687 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1688 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1689 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1690 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1691 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1692 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1693 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1694 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1695 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1696 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1697 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1698 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1699 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1700 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1701 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1702 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1703 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1704 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1705 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1706 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1707 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1708 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1709 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1710 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1711 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1712 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1713 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1714 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1715 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1716 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1717 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1718 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1719 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1720 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1721 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1722 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1723 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1724 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1725 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1726 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1727 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1728 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1729 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1730 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1731 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1732 1 . . . . . 1.8 1.8 2.9 parsed_1b4c 1 1733 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1734 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1735 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1736 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1737 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1738 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1739 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1740 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1741 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1742 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1743 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1744 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1745 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1746 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1747 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1748 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1749 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1750 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1751 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1752 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1753 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1754 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1755 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1756 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1757 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1758 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1759 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1760 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1761 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1762 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1763 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1764 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1765 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1766 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1767 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1768 1 . . . . . 1.8 1.8 5.0 parsed_1b4c 1 1769 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1770 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1771 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1772 1 . . . . . 1.8 1.8 4.2 parsed_1b4c 1 1773 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1774 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1775 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1776 1 . . . . . 1.8 1.8 6.0 parsed_1b4c 1 1777 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1778 1 . . . . . 1.8 1.8 3.3 parsed_1b4c 1 1779 1 . . . . . 1.8 1.8 4.3 parsed_1b4c 1 1780 1 . . . . . 1.8 1.8 4.3 parsed_1b4c 1 stop_ loop_ _Dist_constraint_comment_org.ID _Dist_constraint_comment_org.Comment_text _Dist_constraint_comment_org.Comment_begin_line _Dist_constraint_comment_org.Comment_begin_column _Dist_constraint_comment_org.Comment_end_line _Dist_constraint_comment_org.Comment_end_column _Dist_constraint_comment_org.Entry_ID _Dist_constraint_comment_org.Distance_constraint_list_ID 1 ; Ser 1a (nh-10.23; n= 121.93 ppm) hn104 no sidechain peaks in 3D TOCSY INTRA I assign (segid="sbm1" and resid 1 and name ha) (segid="sbm1" and resid 1 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 1 and name ha) (segid="sbm2" and resid 1 and name hn) 1.8 0 4.2 {vw, 4.66d, , 0} amb assign (segid="sbm1" and resid 1 and name hb) (segid="sbm1" and resid 1 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid 1 and name hb) (segid="sbm2" and resid 1 and name hn) 1.8 0 ? {, , , } Ser 1b (nh-9.95ppm; n= 120.73) hn108 NOTES 3D NOESY: noesy100-115 61 30 no sidechain peaks in 3D TOCSY sc NOEs at 4.33, 2.27, 1.84, 1.73 NN, 98, could ovlp nn+2 N+2 (hn70/hn71) 98 N+3 (hn55) 128 N+4 (hn26) 112 NOTES 4D CN: signals stronger in 4D than 3D as exected in range of H2O Glu 2 INTRA ; 1 1 29 7 parsed_1b4c 1 2 "{m, 4.04, 8}" 32 1 32 21 parsed_1b4c 1 3 ; {s, 2.08, 10} assign (segid="sbm1" and resid 2 and name hg*) (segid="sbm1" and resid 2 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 2 and name hg*) (segid="sbm2" and resid 2 and name hn) 1.8 0 1.7 {m?, 2.46, 10} remove 1ha-2hn b/c dispersive and very weak in 3d NOTES 3D NOESY (nh- 8.93ppm; n= 120.7) hn62 noesy100- 202 98 30 NN (hn70), 8.94, could ovlp hn62 NN+2 (hn55) 129 NN+3 (hn24/hn26?), 113 NOTES 4D CN: Y= S1 or F43 Leu 3a INTRA ; 36 1 57 7 parsed_1b4c 1 4 ; {m, 4.04, 9, 0} S assign (segid="sbm1" and resid 3 and name ha) (segid="sbm1" and resid 3 and name hd*) 1.8 0 4.4 S assign (segid="sbm2" and resid 3 and name ha) (segid="sbm2" and resid 3 and name hd*) 1.8 0 4.4 {d', m, 4.04, 10?, 2.9, amb ovlp 10ha} shows in 3D and 4D ; 60 1 64 66 parsed_1b4c 1 5 ; {b<, s, 1.89, 11ov?, 0.6} S assign (segid="sbm1" and resid 3 and name hb*) (segid="sbm1" and resid 3 and name hn) 1.8 0 1.7 S assign (segid="sbm2" and resid 3 and name hb*) (segid="sbm2" and resid 3 and name hn) 1.8 0 1.7 {b>, m?, 1.75, 10, 0} ovlp? 39hb* at 1.73 amb assign (segid="sbm1" and resid 3 and name hg) (segid="sbm1" and resid 3 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hg) (segid="sbm2" and resid 3 and name hn) 1.8 0 4.2 {vw, 1.54, 1, 0, amb}, not sure if hg @ 1.21 or 1.54, think 1.54 based on 4Dcc for hd1&2 S assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm1" and resid 3 and name hn) 1.8 0 3.2 S assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm2" and resid 3 and name hn) 1.8 0 3.2 {d', w, 0.99, 3, 2.9} S assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm1" and resid 3 and name hn) 1.8 0 3.2 S assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm2" and resid 3 and name hn) 1.8 0 3.2 {d'', w, 0.75, 3, 2.9, amb} NOTES 3D NOESY: noesy100- 201 98 29 ovlps hn62(E2) in 1H and one 15N plane away NN (hn55) 129, ovlps hn62(E2) (nh- 8.94; n= 121.37) hn70 Leu 3b (nh- 9.01ppm) hn73 NOTES 3D NOESY: noesy100- 194 95 28 NN (hn35) 7.76ppm, vw(9), 142 NOTES 4D CN: could not find Leu 3c (nh- 8.92; n= 121.62) hn71 overlaps L3a in 1H and 15N in 3D Glu 4a INTRA I assign (segid="sbm1" and resid 4 and name ha) (segid="sbm1" and resid 4 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 4 and name ha) (segid="sbm2" and resid 4 and name hn) 1.8 0 3.2 {w, 3.27, 5, 0} ; 68 1 108 24 parsed_1b4c 1 6 ; {m, 2.24, 8ov, 1}, E4ahn at 2.24 seen by E4bhn also amb assign (segid="sbm1" and resid 4 and name hg*??) (segid="sbm1" and resid 4 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 4 and name hg*??) (segid="sbm2" and resid 4 and name hn) 1.8 0 3.2 {w, 2.43, 6, 1.0, amb} NOTES 3D NOESY: noesy100-273 129 31 NN-1 (hn70/71) 98, could ovlp nn-2 NN-2 (hn62), could ovlp nn-1 Glu 4b (nh- 7.73ppm; n= 118.47) hn35 NOTES 3D NOESY: noesy100- 305 142 33 K5 NN (hn30) 7.89ppm, (~3), ~137 ovlps E4b hn35 NOTES 4D CN: could not find ha=3.33 Lys 5a INTRA ; 112 1 133 7 parsed_1b4c 1 7 "{m, 3.90, 7, 0}" 136 1 136 24 parsed_1b4c 1 8 ; {s, 1.89, 11, 1} assign (segid="sbm1" and resid 5 and name hg*) (segid="sbm1" and resid 5 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 5 and name hg*) (segid="sbm2" and resid 5 and name hn) 1.8 0 3.2 {w, 1.43, 3, 1} ; 140 1 144 24 parsed_1b4c 1 9 ; {w?, 1.65 ovlp 6hb*?, 11, 1} I assign (segid="sbm1" and resid 5 and name he*) (segid="sbm1" and resid 5 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 5 and name he*) (segid="sbm2" and resid 5 and name hn) 1.8 0 4.2 {vw, 2.90, 5*, 1} NOTES 3D NOESY: noesy100- 233 112 35 (nh- 8.57ppm; n= 117.59) hn24; multiple with hn26 and hn30 A6a NN (hn83) 131, could ovlp nn-1 NN-2 (hn70/71) 97, could ovlp NN-3, not ovlpd in hn70/71 strip NN-3 (hn62) 97, could ovlp NN-2 Lys5c (nh- 8.51ppm; n= 117.59) hn26 3D NOESY: noesy100- 238 114 35 NN-1 (hn55), could ovlp nn NN (hn83) 131, could ovlp nn-1 NN-2 (hn70/71) 98, could ovlp NN-3 NN-3 (hn62) 98, could ovlp NN-2 4D CN: 1.65 may be hd and hg Lys 5b (nh- 7.88ppm; n= 118.15) hn30 NOTES 3D NOESY: noesy100- 292 137 34 Ala 6a INTRA I assign (segid="sbm1" and resid 6 and name ha) (segid="sbm1" and resid 6 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 6 and name ha) (segid="sbm2" and resid 6 and name hn) 1.8 0 3.2 {w, 4.28, 5, 0} ; 148 1 181 24 parsed_1b4c 1 10 ; {s, 1.67, 18, 1.1} could have inter contribution from A9hb* NOTES 3D NOESY: noesy100- 279 131 26 aN-2 (hn55) 3.3ppm,~304, ovlpd w/another peak Ala 6b (nh- 8.18ppm) hn82 NOTES 3D NOESY: noesy100- 267 126 26 M7 NN (hn8) 8.33ppm, (2), 121 could ovlp V8 nn+2 K5 aN-1 (hn30) 4.01ppm, (2), 280 could ovlp an-3,an-4 V8 NN+2 (hn42) 8.34ppm, (), could ovlp M7 nn L3b aN-3 (hn70/71) 4.01ppm, (2), 280 could ovlp an-1/-4 E2 aN-4 (hn62) 4.01ppm, (2), 280 could ovlp an-1/-3 NOTES 4D CN: could not find Met 7 INTRA I assign (segid="sbm1" and resid 7 and name ha) (segid="sbm1" and resid 7 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 7 and name ha) (segid="sbm2" and resid 7 and name hn) 1.8 0 3.2 {w, 4.80, 3, 0} ; 185 1 209 25 parsed_1b4c 1 11 "{mw, 4.75, 8, 1.5}" 213 1 213 27 parsed_1b4c 1 12 ; {b<, s?, 2.54, 12?, 0.6} RS assign (segid="sbm1" and resid 7 and name hb*) (segid="sbm1" and resid 7 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 7 and name hb*) (segid="sbm2" and resid 7 and name hn) 1.8 0 1.7 {b>, m, 2.11, 8, 0} I assign (segid="sbm1" and resid 7 and name hg*) (segid="sbm1" and resid 7 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 7 and name hg*) (segid="sbm2" and resid 7 and name hn) 1.8 0 3.2 {w, 2.85, 6, 1.0, cn} NOTES 3D NOESY noesy100- 254 121 39 (nh- 8.33ppm; n= 115.25) hn8 close to hn9[N38], L44d&e V8 NN (hn43) 114, could ovlp K5 nn-2, as well as L44,N38 K5 bN-1 (hn83) 365, ovlps L44hb and hg K5 NN-2 (hn24), could ovlp nn, as well as L44,N38 A9 NN+2 9 (hn81) 140, could ovlp hn[9]N38 nn-1[13] L3 aN-4 (hn70) (9/3), 279, could ovlp other peaks hn9[N38]an-4, ha12[L44a], ha10[L44] NOTES 4D CN same coordinates as N38 ha dispersive in 3D 5 ctrs in 4D go with 3 Val 8a INTRA I assign (segid="sbm1" and resid 8 and name ha) (segid="sbm1" and resid 8 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 8 and name ha) (segid="sbm2" and resid 8 and name hn) 1.8 0 3.2 {w, 3.52, 6, 0} ; 217 1 248 24 parsed_1b4c 1 13 ; {s, 2.24, 10, 0} assign (segid="sbm1" and resid 8 and name hg2*) (segid="sbm1" and resid 8 and name hn) 1.8 0 1.1 assign (segid="sbm2" and resid 8 and name hg2*) (segid="sbm2" and resid 8 and name hn) 1.8 0 1.1 {g<, s, 1.24, 10, 2.2} I assign (segid="sbm1" and resid 8 and name hg1*) (segid="sbm1" and resid 8 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 8 and name hg1*) (segid="sbm2" and resid 8 and name hn) 1.8 0 3.2 {g>, w, 0.97, 6, 2.2} NOTES 3D NOESY: noesy100- 239 113 33 (nh- 8.50ppm; n= 199.20) hn43 NN-1 (hn8) 8.33, 121, could ovlp NN+2 NN+2 (hn52) 8.29, could ovlp nn-1 aN-3 (hn24) 3.90ppm, ovlps hn40[E67] an-1/an-3, but it's real NOTES 4D CN: V8 is in same cube as E67 Val 8b (nh- 8.34ppm; n= 119.20) hn42, wkr than hn43 NOTES 3D NOESY: noesy100- 253 120 32 NN-1 (hn) 8.33ppm, (),could ovlp hn42 NN+2 (hn65) 8.4ppm, (), could ovlp hn42 Ala 9 INTRA I assign (segid="sbm1" and resid 9 and name ha) (segid="sbm1" and resid 9 and name hn) 1.8 0 1.5 I assign (segid="sbm2" and resid 9 and name ha) (segid="sbm2" and resid 9 and name hn) 1.8 0 1.5 {m?, 4.28, 7?, 0} ; 252 1 284 26 parsed_1b4c 1 14 ; {s, 1.65, 11, 1.1} NOTES 3D NOESY: noesy100- 307 143 27 (nh- 7.71ppm; n= 122.98) hn81 V8a or b NN-1 (hn43) 114, could ovlp nn+2 L10 or b NN (hn52) 8.31ppm,, 122, could ovlp nn-2 M7 NN-2 (hn8) 8.33ppm, could ovlp nn I11 NN+2 (hn65) 8.4ppm, could ovlp nn-1 Leu 10a INTRA I assign (segid="sbm1" and resid 10 and name ha) (segid="sbm1" and resid 10 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 10 and name ha) (segid="sbm2" and resid 10 and name hn) 1.8 0 1.7 {m, 4.12, 9, 0} I assign (segid="sbm1" and resid 10 and name ha) (segid="sbm1" and resid 10 and name hd*) 1.8 0 0.9 I assign (segid="sbm2" and resid 10 and name ha) (segid="sbm2" and resid 10 and name hd*) 1.8 0 0.9 {d'', s, 4.12, >10} ; 288 1 312 28 parsed_1b4c 1 15 ; {s, 2.52, 10, 0.6} I assign (segid="sbm1" and resid 10 and name hg?) (segid="sbm1" and resid 10 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 10 and name hg?) (segid="sbm2" and resid 10 and name hn) 1.8 0 1.7 {m, 2.00, 12, 0, amb}, not sure which is 10hg, above or below I assign (segid="sbm1" and resid 10 and name hg?) (segid="sbm1" and resid 10 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 10 and name hg?) (segid="sbm2" and resid 10 and name hn) 1.8 0 1.7 {m, 1.81, ?, 0} I assign (segid="sbm1" and resid 10 and name hd*) (segid="sbm1" and resid 10 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 10 and name hd*) (segid="sbm2" and resid 10 and name hn) 1.8 0 3.2 {d', w, 1.08, 6, 2.9} I assign (segid="sbm1" and resid 10 and name hd*) (segid="sbm1" and resid 10 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 10 and name hd*) (segid="sbm2" and resid 10 and name hn) 1.8 0 3.2 {d'', w, 1.02, 5, 2.9} NOTES 3D NOESY: noesy100- 257 122 32 Leu 10a (nh- 8.29ppm; n= 119.76) hn52; strgr of the pair in the HSQC Leu 10b (nh- 8.26ppm; n= 119.60) hn48 Ile 11a INTRA I assign (segid="sbm1" and resid 11 and name ha) (segid="sbm1" and resid 11 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 11 and name ha) (segid="sbm2" and resid 11 and name hn) 1.8 0 4.2 {vw, 3.39, 2, 0} ; 316 1 348 25 parsed_1b4c 1 16 ; {m, 1.67, 8, 0} amb assign (segid="sbm1" and resid 11 and name hg1*) (segid="sbm1" and resid 11 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid 11 and name hg1*) (segid="sbm2" and resid 11 and name hn) 1.8 0 ? {, 1.81, ?, ?} amb assign (segid="sbm1" and resid 11 and name hd*) (segid="sbm1" and resid 11 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 11 and name hd*) (segid="sbm2" and resid 11 and name hn) 1.8 0 4.2 {vw, 0.12, 2ov, 1.5, amb} amb assign (segid="sbm1" and resid 11 and name hg2*) (segid="sbm1" and resid 11 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 11 and name hg2*) (segid="sbm2" and resid 11 and name hn) 1.8 0 4.2 {vw, 0.15, 2ov, 1.5, amb} NOTES 3D NOESY: noesy100- 246 117 29 Ile 11a (nh- 8.44ppm; n= 121.21) hn65 close to hn67 (V13), but wkr than hn67 Ile 11b (nh- 8.39ppm; n= 121.21) hn65a, wkr than hn65 NN (hn) 8.1ppm, (), could be ovlpd NN-1 (hn) 8.2ppm, (), could be ovlpd NOTES 4D CN: too weak Asp 12 INTRA I assign (segid="sbm1" and resid 12 and name ha) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 12 and name ha) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 4.26, 6*, 0} ; 352 1 384 26 parsed_1b4c 1 17 ; {b<, s, 2.90, 9/~20, 0.6} RS assign (segid="sbm1" and resid 12 and name hb*) (segid="sbm1" and resid 12 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 12 and name hb*) (segid="sbm2" and resid 12 and name hn) 1.8 0 1.7 {b>, m, 2.81, 7/~20, 0.6} NOTES 3D NOESY: noesy100- 269 127 30 Illhb could also be K26hb* (nh- 8.15ppm; n= 120.73) hn64; in NOESY seems to have vw mult peak Val 13 INTRA ; 388 1 405 7 parsed_1b4c 1 18 "{s, 3.82, 10, 0}" 408 1 408 25 parsed_1b4c 1 19 ; {s, 2.30, 13, 0} assign (segid="sbm1" and resid 13 and name hg2*) (segid="sbm1" and resid 13 and name hn) 1.8 0 1.1 assign (segid="sbm2" and resid 13 and name hg2*) (segid="sbm2" and resid 13 and name hn) 1.8 0 1.1 {s, 1.21, 15, 2.7} NOTES 3D NOESY (nh- 8.41ppm) hn67 noesy100- 248 118 29 F14 NN (hn50) 8.4ppm, could ovlp w/hn[67]- assumed f14hn-acd I11 NN-2 (hn65) 8.4ppm, could ovlp w/hn[67] NOTES HNH (clvl=0.1): 119.68 (7) F14 and 120.73 D12 Phe 14a Phe 14b INTRA ; 412 1 433 7 parsed_1b4c 1 20 ; {m, 3.52, 9, 0} RS assign (segid="sbm1" and resid 14 and name hb*) (segid="sbm1" and resid 14 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 14 and name hb*) (segid="sbm2" and resid 14 and name hn) 1.8 0 1.7 {m, 3.14, 9, 1.0} ; 436 1 440 26 parsed_1b4c 1 21 "{s, 2.68, 10, 0.6}" 444 1 444 27 parsed_1b4c 1 22 ; {w, 6.24, 3, 2.4} amb assign (segid="sbm1" and resid 14 and name he*) (segid="sbm1" and resid 14 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 14 and name he*) (segid="sbm2" and resid 14 and name hn) 1.8 0 3.2 {w, 7.11, 5, 2.4}, could be to F73he* also NOTES 3D NOESY: noesy100- ~244 117 31 V13 NN-1 ovlps diag D12 NN-2 (hn64) 8.17ppm very weak but seems to be there NOTES 4D CN an-4 or G66 4.15 in 3D and 4.17 in 4D, 13C goes w/G66 not an-4 sofrom another cube ? Phe 14a (nh- 8.47ppm; n= 119.76) hn50 strgr of the pair Phe 14b (nh- 8.43ppm; n= 119.84) hn51 His 15 INTRA I assign (segid="sbm1" and resid 15 and name ha) (segid="sbm1" and resid 15 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 15 and name ha) (segid="sbm2" and resid 15 and name hn) 1.8 0 4.2 {vw, 5.15, 7*, 0} ; 448 1 471 26 parsed_1b4c 1 23 ; {m?, 3.20, 4, 0.6} med-stg relative to diagonal RS assign (segid="sbm1" and resid 15 and name hb*) (segid="sbm1" and resid 15 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 15 and name hb*) (segid="sbm2" and resid 15 and name hn) 1.8 0 1.7 {m?, 3.09, 4, 0.6} med-stg relative to diagonal NOTES 3D NOESY: noesy100- 219 106 35 bN-1 (hn50) 3.14ppm, (4/2), ovlps beta2 NN-2 (hn67) 8.4ppm, could ovlp NN-1 (nh- 8.74ppm; n= 117.42) hn109 - VERY WEAK SIGNAL FOR 3D AND 4D Gln 16 INTRA ; 475 1 492 7 parsed_1b4c 1 24 "{m, 3.82, 8, 0}" 495 1 495 25 parsed_1b4c 1 25 ; {b<, s?, 2.41, 15/>10, 0.6, cn} R assign (segid="sbm1" and resid 16 and name hb*) (segid="sbm1" and resid 16 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 16 and name hb*) (segid="sbm2" and resid 16 and name hn) 1.8 0 1.1 {b>, s?, 2.14, 16/>10, 0, cn} assign (segid="sbm1" and resid 16 and name hg*) (segid="sbm1" and resid 16 and name hn) 1.8 0 1.5 assign (segid="sbm2" and resid 16 and name hg*) (segid="sbm2" and resid 16 and name hn) 1.8 0 1.5 {g', m, 2.47, 10/9, 0, cn} R assign (segid="sbm1" and resid 16 and name hg*) (segid="sbm1" and resid 16 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 16 and name hg*) (segid="sbm2" and resid 16 and name hn) 1.8 0 3.2 {g'', w?, 2.22, 9/7, 0, cn} I assign (segid="sbm1" and resid 16 and name he2*) (segid="sbm1" and resid 16 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 16 and name he2*) (segid="sbm2" and resid 16 and name hn) 1.8 0 4.2 {e2', vw, 7.11, 5*, 1.0} I assign (segid="sbm1" and resid 16 and name he2*) (segid="sbm1" and resid 16 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 16 and name he2*) (segid="sbm2" and resid 16 and name hn) 1.8 0 4.2 {e2'', vw, 6.78, *, 1.0} NOTES 3D NOESY: noesy100- 255 120 27 F14 NN-2 (hn50) 8.4ppm, (),could ovlp diag (nh- 8.32ppm; n= 122.25) hn75; close in 15n/1H to hn74(E72) Tyr 17 INTRA ; 499 1 531 7 parsed_1b4c 1 26 "{s, 4.15, 10, 0}" 534 1 534 25 parsed_1b4c 1 27 ; {s, 2.65, >10, 1} I assign (segid="sbm1" and resid 17 and name hd*) (segid="sbm1" and resid 17 and name hb*) 1.8 0 3.2 I assign (segid="sbm2" and resid 17 and name hd*) (segid="sbm2" and resid 17 and name hb*) 1.8 0 3.2 {w, 7.30, 6, 3.4} amb assign (segid="sbm1" and resid 17 and name hd*) (segid="sbm1" and resid 17 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 17 and name hd*) (segid="sbm2" and resid 17 and name hn) 1.8 0 1.7 {m?, 7.30, ovlps 17hn, 2.4} SD? assign (segid="sbm1" and resid 17 and name he*) (segid="sbm1" and resid 17 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 17 and name he*) (segid="sbm2" and resid 17 and name hn) 1.8 0 4.2 {vw, 6.68, 2, 2.4} NOTES 3D NOESY (nh- 7.37ppm; n= 115.73) hn14 noesy100- 336 156 38 aN-2 (hn109) 5.15ppm, other signals are present in 4D CN at 5.1 that aren't H15 NOTES 4D CN aN-1 (hn75) 3.82ppm is only 1 contour not all Y17 peaks optimize at one 15N value Q16hg2 could alos be M79hb1 Ser 18 INTRA I assign (segid="sbm1" and resid 18 and name ha) (segid="sbm1" and resid 18 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 18 and name ha) (segid="sbm2" and resid 18 and name hn) 1.8 0 3.2 {w, 4.01, 5*, 0} I assign (segid="sbm1" and resid 18 and name hb*) (segid="sbm1" and resid 18 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 18 and name hb*) (segid="sbm2" and resid 18 and name hn) 1.8 0 3.2 {w, 3.49, 3*, 1} ? assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 18 and name hn) 1.8 0 ? ? assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 18 and name hn) 1.8 0 ? {vw, 2.38, 6*, ?}, Q16hb1 2.41, E31hg* 2.35 (E31hg* not see pk @ 9.64), or Y17hb2? NOTES 3D NOESY: noesy100- 140 72 29 (nh- 9.64ppm; n= 121.37) hn112 vwk peak, may be multiple seems to have mult peaks in NOESY 9.66, 9.63, 9.60 aN-4 (hn50) 3.49ppm, could ovlp beta NOTES 4D CN - too weak Gly 19 INTRA ; 538 1 592 7 parsed_1b4c 1 28 ; {s, 3.98, 8, 1.0} looks stg relative to diagonal ? RS assign (segid="sbm1" and resid 19 and name ha*) (segid="sbm1" and resid 19 and name hn) 1.8 0 1.1 RS assign (segid="sbm2" and resid 19 and name ha*) (segid="sbm2" and resid 19 and name hn) 1.8 0 1.1 {s, 3.71, 8, 1.0} looks stg relative to diagonal ? AMB amb/art assign (segid="sbm1" and resid 31 and name hg*) (segid="sbm1" and resid 19 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 31 and name hg*) (segid="sbm2" and resid 19 and name hn) 1.8 0 4.2 {vw, 2.38, 3*, 1.0, amb}, could be 16hb1 2.41 ?, 31hg* at 2.35 NOTES 3D NOESY: noesy100- 280 132 51 S18 aN-1 (hn112) 3.9ppm, could ovlp alpha1 (nh- 8.02ppm; n= 107.28) hn1, may be multiple Arg 20 INTRA ; 595 1 617 7 parsed_1b4c 1 29 "{s, 3.96, 10, stg in 4d}" 620 1 620 33 parsed_1b4c 1 30 ; {s, 1.86, >10, 1} assign (segid="sbm1" and resid 20 and name hg*) (segid="sbm1" and resid 20 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 20 and name hg*) (segid="sbm2" and resid 20 and name hn) 1.8 0 1.7 {g', m, 1.78, 10, cn} RS assign (segid="sbm1" and resid 20 and name hg*) (segid="sbm1" and resid 20 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 20 and name hg*) (segid="sbm2" and resid 20 and name hn) 1.8 0 3.2 {w, 1.59, 6} I assign (segid="sbm1" and resid 20 and name hd*) (segid="sbm1" and resid 20 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 20 and name hd*) (segid="sbm2" and resid 20 and name hn) 1.8 0 4.2 {vw, 3.17, 1} NOTES 3D NOESY: noesy100- 353 163 33 (nh- 7.17ppm; n= 118.63) hn38 Glu 21 INTRA I assign (segid="sbm1" and resid 21 and name ha) (segid="sbm1" and resid 21 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 21 and name ha) (segid="sbm2" and resid 21 and name hn) 1.8 0 3.2 {w, 4.20, 12&4, 0} ; 624 1 651 27 parsed_1b4c 1 31 ; {b<, m, 2.08, 9/7, 0.6} amb/RS assign (segid="sbm1" and resid 21 and name hb*) (segid="sbm1" and resid 21 and name hn) 1.8 0 1.7 amb/RS assign (segid="sbm2" and resid 21 and name hb*) (segid="sbm2" and resid 21 and name hn) 1.8 0 1.7 {b>, m?, 1.89, 12ov/6, 0.6} 20hb* at 1.86 assign (segid="sbm1" and resid 21 and name hg*) (segid="sbm1" and resid 21 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 21 and name hg*) (segid="sbm2" and resid 21 and name hn) 1.8 0 1.7 {m, 2.18, 10/~8, 1} NOTES 3D NOESY: noesy100- ~302 142/143 38 G22 NN (hn3) 8.3ppm, could ovlp N37 nn (nh- 7.77ppm; n= 115.81) (hn15) - close N37 (hn13) in 1H and 15N Gly 22 INTRA R assign (segid="sbm1" and resid 22 and name ha*) (segid="sbm1" and resid 22 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 22 and name ha*) (segid="sbm2" and resid 22 and name hn) 1.8 0 1.7 {a', m, 3.90, 10, 1.0} ; 655 1 678 31 parsed_1b4c 1 32 ; {a'', s, 3.68, >10, 0} NOTES 3D NOESY: noesy100- 252 120 48 NOTES 4D CN (nh- 8.35ppm; n= 109.13) hn3 E21hb1 could also be K55hb1,E91hb1,K5hb*,M57hb2 E21hb2 could also be K55hb2,E91hb2,V52hb,V53hb,V80hb E21hg* could also be E46hg*,E49hg2 Asp 23 INTRA ; 682 1 698 7 parsed_1b4c 1 33 "{m, 4.48, 8, 0, cn, amb}" 701 1 701 33 parsed_1b4c 1 34 ; {b<, m, 2.73, 10, 0.6} RS assign (segid="sbm1" and resid 23 and name hb*) (segid="sbm1" and resid 23 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 23 and name hb*) (segid="sbm2" and resid 23 and name hn) 1.8 0 1.7 {b>, m, 2.62, 10, 0.6 AMB amb/art assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 23 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 23 and name hn) 1.8 0 4.2 {vw, 4.69, 4*, 0, amb} NOTES 3D NOESY (nh- 8.61ppm; n= 125.47) hn86 noesy100- 229 110 23 NN (hn) 8.57ppm, could ovlp hn86 NOTES 4D CN: Close to O1 in D1, so signal not so good Lys 24 INTRA I assign (segid="sbm1" and resid 24 and name ha) (segid="sbm1" and resid 24 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 24 and name ha) (segid="sbm2" and resid 24 and name hn) 1.8 0 3.2 {vw, 4.26, 1, 0} ; 705 1 731 25 parsed_1b4c 1 35 ; {s, 1.67, 9, 1} I assign (segid="sbm1" and resid 24 and name hg*) (segid="sbm1" and resid 24 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 24 and name hg*) (segid="sbm2" and resid 24 and name hn) 1.8 0 3.2 {w, 1.13, 6, 1} ? assign (segid="sbm1" and resid 24 and name hd*) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 ? assign (segid="sbm2" and resid 24 and name hd*) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 1.51?, 8*, 1.0}, 26hd* at 1.51, not sure about 24hd* ? assign (segid="sbm1" and resid 24 and name he*) (segid="sbm1" and resid 24 and name hn) 1.8 0 ? ? assign (segid="sbm2" and resid 24 and name he*) (segid="sbm2" and resid 24 and name hn) 1.8 0 ? {, ?, , 1.0} AMB art? assign (segid="sbm1" and resid ? and name ?) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name ?) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 {vw, 0.72-5, 1, 1.5, amb}, 40hd2* 0.72, 3hd2* 0.75, 44hd** 0.75, 77hg1*, 0.77 art? assign (segid="sbm1" and resid ? and name ?) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name ?) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 7.08, 2*, 0} , could be 14hd* at 7.11 art? assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 2.22, ~5*, 0, amb} art? assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 2.43, 1*, 0, amb} NOTES 3D NOESY: noesy100- 232 111 22 NN-1 (hn86) 8.6ppm,could ovlp hn106 beta-N-1 (hn86) ovlps hn86 (D23) from 15N plane one up NOTES 4D CN: ha only sidechain atom of K24 present His 25 INTRA I assign (segid="sbm1" and resid 25 and name ha) (segid="sbm1" and resid 25 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 25 and name ha) (segid="sbm2" and resid 25 and name hn) 1.8 0 3.2 {w, 4.90, 0/4} R assign (segid="sbm1" and resid 25 and name hb*) (segid="sbm1" and resid 25 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 25 and name hb*) (segid="sbm2" and resid 25 and name hn) 1.8 0 3.2 {b<, w, 3.68, 4} ; 735 1 784 25 parsed_1b4c 1 36 ; {b>, s, 3.25, 8} stg relative to other pks AMB art? assign (segid="sbm1" and resid 14 and name ha) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 14 and name ha) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 3.52, 3*, 0, amb} amb assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 5.34, 7*, 0} , D69ha sees wk pk @ 9.10, K26ha sees vw pk @ 9.19 - ?? NOTES 3D NOESY: noesy100- 184 90 35 (nh- 9.14ppm; n= 117.50) hn25 close to hn21 (E51) in 1H and 15N K26 (NN) 7.71ppm, could ovlp E21(n-2) from next 15N plane, so use 6 ctrs vs. 9 8.57/7.11 are dispersive so intensity may be reduced 6.78/7.11 correspond to Q16 he22 and he21, both are present in 200 ms NOESY NOTES 4D CN: ha 7 ctrs in 4D 1 in 3D go with 4 ctrs Lys 26 INTRA ; 788 1 813 7 parsed_1b4c 1 37 "{s?, 5.37, 9}" 816 1 816 22 parsed_1b4c 1 38 ; {s, 1.73, >10} I assign (segid="sbm1" and resid 26 and name hg*) (segid="sbm1" and resid 26 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 26 and name hg*) (segid="sbm2" and resid 26 and name hn) 1.8 0 3.2 {g', w, 1.51, 6, cn} I assign (segid="sbm1" and resid 26 and name hg*) (segid="sbm1" and resid 26 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 26 and name hg*) (segid="sbm2" and resid 26 and name hn) 1.8 0 3.2 {g'', w, 1.26, 3, cn} I assign (segid="sbm1" and resid 26 and name hd*) (segid="sbm1" and resid 26 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 26 and name hd*) (segid="sbm2" and resid 26 and name hn) 1.8 0 3.2 {w, 1.51, 4, 1, cn} I assign (segid="sbm1" and resid 26 and name he*) (segid="sbm1" and resid 26 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 26 and name he*) (segid="sbm2" and resid 26 and name hn) 1.8 0 4.2 {e', vw, 3.03, 8*, 1.0} I assign (segid="sbm1" and resid 26 and name he*) (segid="sbm1" and resid 26 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 26 and name he*) (segid="sbm2" and resid 26 and name hn) 1.8 0 3.2 {e'', w, 2.73, 3, 1.0} I assign (segid="sbm1" and resid 26 and name he*) (segid="sbm1" and resid 26 and name hg*) 1.8 0 3.2 I assign (segid="sbm2" and resid 26 and name he*) (segid="sbm2" and resid 26 and name hg*) 1.8 0 3.2 {w, 3.00, 4, 2.0} assign (segid="sbm1" and resid 26 and name ha) (segid="sbm1" and resid 26 and name hg*) 1.8 0 3.2 assign (segid="sbm2" and resid 26 and name ha) (segid="sbm2" and resid 26 and name hg*) 1.8 0 3.2 {w, 5.37, 3, 0.6} NOTES 3D: noesy100- 309 144 35 H25 (NN-1) 9.17ppm, (9), 90, could also be F70; F70 has 7.11/7.30 NOTES 4D CN hb could also ovlp I11hb,Ihb hd 5 at H=596, 3 at H=595, split difference and use 4 contours hg1 could ovlp K5,K28,K55 hg2 could ovlp K33,K48 hd* could ovlp K48hd* NOTES 13C NOESY: 23hb1-26ha could also be 69hb2 (commented out above), but probably to 23hb1 33ha-26hb* could also be from s18b* or v8(ab)ha; viol!- now think above is 33ha-36hb, 36hb & K26hb* overlap 23hb1-26hg2 could also be intra to 26he2, which may be at 2.72(42.07) Leu 27 INTRA I assign (segid="sbm1" and resid 27 and name ha) (segid="sbm1" and resid 27 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 27 and name ha) (segid="sbm2" and resid 27 and name hn) 1.8 0 4.2 {vw, 4.80, *, 0} ; 820 1 872 25 parsed_1b4c 1 39 ; {m, 4.84, 9, 1.7} amb/R assign (segid="sbm1" and resid 27 and name hb*) (segid="sbm1" and resid 27 and name hn) 1.8 0 1.7 amb/R assign (segid="sbm2" and resid 27 and name hb*) (segid="sbm2" and resid 27 and name hn) 1.8 0 1.7 {m?, 1.51, 12ov, 0.6} 26hg1 and 26hd* at 1.51 ; 876 1 880 54 parsed_1b4c 1 40 ; {m, 1.26, 9 ov?, 0.6} I assign (segid="sbm1" and resid 27 and name hg) (segid="sbm1" and resid 27 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 27 and name hg) (segid="sbm2" and resid 27 and name hn) 1.8 0 1.7 {m?, 1.51, 12ov, 0} ; 884 1 888 28 parsed_1b4c 1 41 ; {mw, 0.61, 7, 3.4?} NOTES 3D NOESY: noesy100- 223 107 31 ha missing in 3D; very weak in 200ms NOTES 4D NOESY: too weak, in solvent ridge Lys 28 INTRA I assign (segid="sbm1" and resid 28 and name hn) (segid="sbm1" and resid 28 and name hg*) 1.8 0 4.2 I assign (segid="sbm2" and resid 28 and name hn) (segid="sbm2" and resid 28 and name hg*) 1.8 0 4.2 {vw, 9.19, 1, 1.0} I assign (segid="sbm1" and resid 28 and name ha) (segid="sbm1" and resid 28 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 28 and name ha) (segid="sbm2" and resid 28 and name hn) 1.8 0 3.2 {w, 4.93, 3, 0} I assign (segid="sbm1" and resid 28 and name ha) (segid="sbm1" and resid 28 and name hg*) 1.8 0 3.2 I assign (segid="sbm2" and resid 28 and name ha) (segid="sbm2" and resid 28 and name hg*) 1.8 0 3.2 {w, 4.89, 4, 1.0} I assign (segid="sbm1" and resid 28 and name ha) (segid="sbm1" and resid 28 and name hd*) 1.8 0 4.2 I assign (segid="sbm2" and resid 28 and name ha) (segid="sbm2" and resid 28 and name hd*) 1.8 0 4.2 {vw, 4.89, 2, 1.0} R assign (segid="sbm1" and resid 28 and name hb*) (segid="sbm1" and resid 28 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 28 and name hb*) (segid="sbm2" and resid 28 and name hn) 1.8 0 3.2 {b<, w?, 2.35, 9/4 ovlp 31hg*?, 0.6, cn} ; 892 1 924 49 parsed_1b4c 1 42 ; {b>, m, 1.73ov, 8, 0.6, cn} assign (segid="sbm1" and resid 28 and name hg*) (segid="sbm1" and resid 28 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 28 and name hg*) (segid="sbm2" and resid 28 and name hn) 1.8 0 1.7 {m, 1.54, 9, 1, cn} I assign (segid="sbm1" and resid 28 and name hd*) (segid="sbm1" and resid 28 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 28 and name hd*) (segid="sbm2" and resid 28 and name hn) 1.8 0 3.2 {w, 1.73 ov?, 5, 1, cn} I assign (segid="sbm1" and resid 28 and name he*) (segid="sbm1" and resid 28 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 28 and name he*) (segid="sbm2" and resid 28 and name hn) 1.8 0 4.2 {vw, 3.01, 6*, 1} AMB amb/art assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 28 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 28 and name hn) 1.8 0 4.2 {vw, 3.82, 1*, 0}, 13ha 3.82, 16ha 3.82, 60ha 3.85, 29ha 3.77 NOTES 3D NOESY: noesy100- 179 88 24 NN (hn89) 9.15ppm, vw(7), 91, nearly ovlps hn85 NOTES 4D CN: L27 an >10 in 4D vw in 3D go with 5 ctrs Lys 29 INTRA ; 928 1 956 7 parsed_1b4c 1 43 "{m, 3.77, 9/5}" 959 1 959 23 parsed_1b4c 1 44 ; {s, 2.30, >10} assign (segid="sbm1" and resid 29 and name hg*) (segid="sbm1" and resid 29 and name hn) 1.8 0 2.4 assign (segid="sbm2" and resid 29 and name hg*) (segid="sbm2" and resid 29 and name hn) 1.8 0 2.4 {mw?, 1.78, 10} some SD?? I/RS assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 29 and name hn) 1.8 0 1.7 I/RS assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 29 and name hn) 1.8 0 1.7 {d', m, 1.53, 10ov?} I assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 29 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 29 and name hn) 1.8 0 1.7 {d'', m, 1.07, 8, 1.0} I assign (segid="sbm1" and resid 29 and name he*) (segid="sbm1" and resid 29 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 29 and name he*) (segid="sbm2" and resid 29 and name hn) 1.8 0 4.2 {vw, 2.81, 3, 1} NOTES 3D NOESY: noesy100- 188 92 21 NN-1 (hn) ppm, (), ovlps hn89 NOTES 4D CN: ha NOEs fairly strong, the rest are weak NOTES 13C: K29ha close to S41(e)hb at 3.79(61.90) so could have some ambiguity Ser 30 INTRA ; 963 1 992 7 parsed_1b4c 1 45 "{s, 4.17, 10, 0}" 995 1 995 25 parsed_1b4c 1 46 ; {s, 3.88, >10, 1} NOTES 3D NOESY: noesy100- 166 83 40 NOTES 4D CN: none of the NOEs to K29 are in the 4D Glu 31 INTRA I assign (segid="sbm1" and resid 31 and name ha) (segid="sbm1" and resid 31 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 31 and name ha) (segid="sbm2" and resid 31 and name hn) 1.8 0 3.2 {w, 4.31, 4, 0} ; 999 1 1013 24 parsed_1b4c 1 47 ; {b<, s, 2.52, >10&9, 0.6} RS assign (segid="sbm1" and resid 31 and name hb*) (segid="sbm1" and resid 31 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 31 and name hb*) (segid="sbm2" and resid 31 and name hn) 1.8 0 1.7 {b>, m?, 2.05, 9&4, 0.6} assign (segid="sbm1" and resid 31 and name hg*) (segid="sbm1" and resid 31 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 31 and name hg*) (segid="sbm2" and resid 31 and name hn) 1.8 0 1.7 {m, 2.35, >10ov/~10, 1.0} 28hb1 ovlps NOTES 3D NOESY: noesy100- 368 170 25 Leu 32 INTRA ; 1017 1 1035 7 parsed_1b4c 1 48 "{s, 4.01, 10, 0}" 1038 1 1038 25 parsed_1b4c 1 49 ; {d', s, 3.97, 12, 2.2} amb/RS assign (segid="sbm1" and resid 32 and name hb*) (segid="sbm1" and resid 32 and name hn) 1.8 0 1.7 amb/RS assign (segid="sbm2" and resid 32 and name hb*) (segid="sbm2" and resid 32 and name hn) 1.8 0 1.7 {m?, 2.16, ~13/2, 0.6} ; 1042 1 1046 31 parsed_1b4c 1 50 ; {s, 1.35, ~16/~10, 0.6} amb assign (segid="sbm1" and resid 32 and name hg) (segid="sbm1" and resid 32 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 32 and name hg) (segid="sbm2" and resid 32 and name hn) 1.8 0 1.7 {m?, 1.51, 10, 0} 27hb1 also at 1.51 and could be as close I/RS assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 32 and name hn) 1.8 0 4.2 I/RS assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 32 and name hn) 1.8 0 4.2 {d', vw, 1.21, 2, 2.9, amb} ; 1050 1 1058 36 parsed_1b4c 1 51 ; {d'', w, 0.94, 6, 2.9, ncn} NOTES 3D NOESY: noesy100- 249 118 27 Lys 33 INTRA ; 1062 1 1073 7 parsed_1b4c 1 52 "{s, 3.49, >10, 0}" 1076 1 1076 26 parsed_1b4c 1 53 ; {b<, s, 1.94, 15, 0.6} R assign (segid="sbm1" and resid 33 and name hb*) (segid="sbm1" and resid 33 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 33 and name hb*) (segid="sbm2" and resid 33 and name hn) 1.8 0 3.2 {w, 1.65, 6, 0, ncn} amb assign (segid="sbm1" and resid 33 and name hg*) (segid="sbm1" and resid 33 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 33 and name hg*) (segid="sbm2" and resid 33 and name hn) 1.8 0 3.2 {g', w?, 1.37, 8ov/2, 1.0, ncn} ovlps 32hb2 at 1.35 amb assign (segid="sbm1" and resid 33 and name hg*) (segid="sbm1" and resid 33 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 33 and name hg*) (segid="sbm2" and resid 33 and name hn) 1.8 0 3.2 {g'', w?, 1.21, 10ov/0, 1.0, ncn} 32hd1*? at 1.21 and 60hb2 at 1.24 I assign (segid="sbm1" and resid 33 and name hd*) (segid="sbm1" and resid 33 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 33 and name hd*) (segid="sbm2" and resid 33 and name hn) 1.8 0 3.2 {w, 2.16, ~7ov/3, 1.0, ncn} I assign (segid="sbm1" and resid 33 and name hd*) (segid="sbm1" and resid 33 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 33 and name hd*) (segid="sbm2" and resid 33 and name hn) 1.8 0 4.2 {vw, 1.65, 6ov/2, 1.0, ncn} I assign (segid="sbm1" and resid 33 and name he*) (segid="sbm1" and resid 33 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 33 and name he*) (segid="sbm2" and resid 33 and name hn) 1.8 0 3.2 {w, 2.90, 3, 1, n} NOTES 3D NOESY: noesy100- 278 131 31 NN-2 (hn84) 7.0ppm, (), could ovlp NN Glu 34 INTRA ; 1080 1 1115 7 parsed_1b4c 1 54 "{s, 4.04, >10, 0}" 1118 1 1118 27 parsed_1b4c 1 55 ; {s, 2.33, ~15 ovlp, 0.6} I/RS assign (segid="sbm1" and resid 34 and name hb*) (segid="sbm1" and resid 34 and name hn) 1.8 0 1.1 I/RS assign (segid="sbm2" and resid 34 and name hb*) (segid="sbm2" and resid 34 and name hn) 1.8 0 1.1 {s, 2.19, ~15, 0.6} assign (segid="sbm1" and resid 34 and name hg*) (segid="sbm1" and resid 34 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 34 and name hg*) (segid="sbm2" and resid 34 and name hn) 1.8 0 1.7 {m, 2.46, 9/~10, 1.0, ncn} RS assign (segid="sbm1" and resid 34 and name hg*) (segid="sbm1" and resid 34 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 34 and name hg*) (segid="sbm2" and resid 34 and name hn) 1.8 0 1.7 {m, 2.28, 10/~10, 1.0, ncn} NOTES 3D NOESY: noesy100- 375 173 34 Leu 35 INTRA ; 1122 1 1144 7 parsed_1b4c 1 56 "{s, 3.58, >10, 0}" 1147 1 1147 26 parsed_1b4c 1 57 ; {d', m, 3.55, 8, 2.2} RS assign (segid="sbm1" and resid 35 and name hb*) (segid="sbm1" and resid 35 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 35 and name hb*) (segid="sbm2" and resid 35 and name hn) 1.8 0 1.7 {m?, 1.67, ~15ov?/8, 0.6} 35hg may ovlp but think it is at 0.78 ; 1151 1 1155 72 parsed_1b4c 1 58 ; {s, 0.94, ~15/~15, 0.6} amb assign (segid="sbm1" and resid 35 and name hg?) (segid="sbm1" and resid 35 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 35 and name hg?) (segid="sbm2" and resid 35 and name hn) 1.8 0 3.2 {w?, 0.77, 8, 0} other possibilities at 0.77 L3hd2* and V77hg1* - both look too far, 36hg12? amb assign (segid="sbm1" and resid 35 and name hg?) (segid="sbm1" and resid 35 and name hn) 1.8 0 1.1 amb assign (segid="sbm2" and resid 35 and name hg?) (segid="sbm2" and resid 35 and name hn) 1.8 0 1.1 {w?, 1.67, >10ov/3, 0} ovlp 35hb1?, previously assigned 1.72/36.2 - dont think so I assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 35 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 35 and name hn) 1.8 0 1.7 {d', m?, 0.61, 9, 2.9} I assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 35 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 35 and name hn) 1.8 0 1.7 {d'', m?, 0.39, 9/?, 2.9, n} NOTES 3D NOESY: noesy100- 268 127 28 NOTES 4D CN L32ha could also be L44, M57, E91 ha's L35ha could also overlap Q50ha, Q71ha L35bn-1 could overlap E49hb1, E72hb1 Ile 36 INTRA ; 1159 1 1190 7 parsed_1b4c 1 59 ; {s, 3.22, 10, 0} assign (segid="sbm1" and resid 36 and name ha) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 1.5 assign (segid="sbm2" and resid 36 and name ha) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 1.5 {m, 3.48, 12/ov, 1.5} ; 1193 1 1197 30 parsed_1b4c 1 60 "{w, 3.48, 8, 1.5}" 1201 1 1201 26 parsed_1b4c 1 61 ; {s, 1.75, 15/>20, 0} amb assign (segid="sbm1" and resid 36 and name hg1*) (segid="sbm1" and resid 36 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 36 and name hg1*) (segid="sbm2" and resid 36 and name hn) 1.8 0 3.2 {g1', w, ~1.75, 15/4, 1.0, cn} I assign (segid="sbm1" and resid 36 and name hg1*) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 3.2 I assign (segid="sbm2" and resid 36 and name hg1*) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 3.2 {g1', w, ~1.75, 7, 2.5} amb assign (segid="sbm1" and resid 36 and name hg1*) (segid="sbm1" and resid 36 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 36 and name hg1*) (segid="sbm2" and resid 36 and name hn) 1.8 0 3.2 {g1'', w?, ~0.78, >10/1ov, 1.0, cn} 36hg2* and 35hg also at ~0.78 assign (segid="sbm1" and resid 36 and name hg2*) (segid="sbm1" and resid 36 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 36 and name hg2*) (segid="sbm2" and resid 36 and name hn) 1.8 0 3.2 {w?, 0.78ov, >10/5, 1.5} 36hg12 and 35hg also at ~0.78 ; 1205 1 1221 63 parsed_1b4c 1 62 ; {w?, 0.59, 10ov/5, 1.5} 35hd1* at 0.61 close to 36hn, probably closer than 36hd* NOTES 3D NOESY: noesy100- 235 112 29 NOTES 4D CN: V56hg2 signal doesn't max at H=522 Asn 37 INTRA ; 1225 1 1236 7 parsed_1b4c 1 63 "{s, 4.20, 10, 0}" 1239 1 1239 25 parsed_1b4c 1 64 ; {s, 2.71, ~15/~15, 0.6} R assign (segid="sbm1" and resid 37 and name hb*) (segid="sbm1" and resid 37 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 37 and name hb*) (segid="sbm2" and resid 37 and name hn) 1.8 0 1.7 {m, 2.57, >10/8, 0.6} amb assign (segid="sbm1" and resid 37 and name hd2*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 37 and name hd2*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 7.18, 9*, 1.0??} ovlps 38hn at 7.19 amb assign (segid="sbm1" and resid 37 and name hd2*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 37 and name hd2*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 6.31, 2, 1.0} NOTES 3D NOESY: noesy100- 300 141 38 Asn 38 INTRA ; 1243 1 1266 7 parsed_1b4c 1 65 "{s, 4.66, >10, 0, cn}" 1269 1 1269 30 parsed_1b4c 1 66 ; {s, 3.03, ~15/7, 0.6} RS assign (segid="sbm1" and resid 38 and name hb*) (segid="sbm1" and resid 38 and name hn) 1.8 0 1.1 RS assign (segid="sbm2" and resid 38 and name hb*) (segid="sbm2" and resid 38 and name hn) 1.8 0 1.1 {s, 2.81, ~15/7, 0.6} I assign (segid="sbm1" and resid 38 and name hd2*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 38 and name hd2*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 7.56, 2, 1.0} I assign (segid="sbm1" and resid 38 and name hd2*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 38 and name hd2*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 7.06, 1, 1.0} NOTES 3D NOESY: noesy100- 255 121 39 NOTES 4D CN: N37ha could also be E21ha no good evidence for 35ha-38hb1/2 NOE, but assigned 38hb2-35ha dont see 41hb*-38ha or vice versa, could be b/c 38ha at carrier frequencey Glu 39 INTRA I assign (segid="sbm1" and resid 39 and name ha) (segid="sbm1" and resid 39 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 39 and name ha) (segid="sbm2" and resid 39 and name hn) 1.8 0 4.2 {vw, 4.83, 3*, 0} ; 1273 1 1301 26 parsed_1b4c 1 67 ; {m, 1.73, 8, 1} amb assign (segid="sbm1" and resid 39 and name hg*) (segid="sbm1" and resid 39 and name hn) 1.8 0 1.5 amb assign (segid="sbm2" and resid 39 and name hg*) (segid="sbm2" and resid 39 and name hn) 1.8 0 1.5 {m, 2.79, 10 ovlp, 1.0} 38hb2 also at 2.79 I assign (segid="sbm1" and resid 39 and name hg*) (segid="sbm1" and resid 39 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 39 and name hg*) (segid="sbm2" and resid 39 and name hn) 1.8 0 3.2 {w, 2.35, 4, 1.0, ncn} 3D NOESY: noesy100- 184 90 39 4D CN: hb1? Wk signal at 2.41, 30.32 which could ovlp hg2 in 3D 13C: 39hb*-36ha assigned, dont see 36ha-39hb* Leu 40 INTRA I assign (segid="sbm1" and resid 40 and name ha) (segid="sbm1" and resid 40 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 40 and name ha) (segid="sbm2" and resid 40 and name hn) 1.8 0 3.2 {w, 5.04, 4, 0, ncn} ; 1305 1 1329 29 parsed_1b4c 1 68 "{m, 5.04, 11, 2.2}" 1333 1 1333 27 parsed_1b4c 1 69 ; {m, 2.05, 10/5, 0.6, ncn} amb assign (segid="sbm1" and resid 40 and name hb*) (segid="sbm1" and resid 40 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 40 and name hb*) (segid="sbm2" and resid 40 and name hn) 1.8 0 3.2 {w, 1.83, 8/2, 0.6, ncn} ovlps 39hb* at 1.73 I assign (segid="sbm1" and resid 40 and name hg) (segid="sbm1" and resid 40 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 40 and name hg) (segid="sbm2" and resid 40 and name hn) 1.8 0 3.2 {w, 1.47, 6, 0, ncn} ; 1337 1 1345 29 parsed_1b4c 1 70 ; {d', w, 0.91, 5, 2.9, ncn} V80hg2* at 0.94 amb assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 40 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 40 and name hn) 1.8 0 3.2 {d'', w, 0.75, 9ovlp, 2.9, amb} 44hd*, 3hd2* and V77hg1* also near 0.75 NOTES 3D NOESY: noesy100- 298 139 33 Dont see 40hb*-37ha or 37ha-40hb* Ser 41d INTRA ; 1349 1 1364 7 parsed_1b4c 1 71 "{m, 4.01, 9}" 1367 1 1367 21 parsed_1b4c 1 72 ; {s, 3.85, 11} AMB amb assign (segid="sbm1" and resid ? and name hn) (segid="sbm1" and resid 41 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name hn) (segid="sbm2" and resid 41 and name hn) 1.8 0 4.2 {vw, 8.33, 5*, 0}, 7hn, 38hn, F43hn, or L44hn ?? ?!assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 41 and name hn) 1.8 0 4.2 ?!assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 41 and name hn) 1.8 0 4.2 {vw, 1.73-5, 8*, 0}, too many choices - all 41 multiples see it NOTES 3D NOESY: noesy100- 394 181 44 (nh- 6.70ppm; n= 111.79) hn97 mult peak with 98/99 Ser 41e (nh- 6.71ppm; n= 112.27) hn98 NOTES 3D NOESY: noesy100- 393 ~181 43 7.41 is dispersive NOTES 4D CN: overlaps Ser 41d Ser 41f (nh- 6.78ppm; n= 112.75) hn99 NOTES 3D NOESY: noesy100- 387 ~178 43 7.41 is dipsersive NOTES 4D CN: Ser41f missing or too weak His 42d INTRA I assign (segid="sbm1" and resid 42 and name ha) (segid="sbm1" and resid 42 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 42 and name ha) (segid="sbm2" and resid 42 and name hn) 1.8 0 4.2 {?, 4.64, ?, 0} I assign (segid="sbm1" and resid 42 and name hb*) (segid="sbm1" and resid 42 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 42 and name hb*) (segid="sbm2" and resid 42 and name hn) 1.8 0 4.2 {b<, vw, 3.60, 2, 0.6} I assign (segid="sbm1" and resid 42 and name hb*) (segid="sbm1" and resid 42 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 42 and name hb*) (segid="sbm2" and resid 42 and name hn) 1.8 0 3.2 {b>, w, 3.33, 3, 0.6} AMB M assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 42 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 42 and name hn) 1.8 0 4.2 {vw, 0.74, 4*, ?} , too many choices NOTES 3D NOESY: noesy100- 135 70 27 His 42e (nh- 9.57ppm; n= 122.25) hn105 NOTES 3D NOESY: noesy100- 148 75 28 His 42f (nh- 9.46ppm; n= 121.37) hn100 NOTES 3D NOESY: noesy100- 157 79 29 Phe 43d INTRA I assign (segid="sbm1" and resid 43 and name ha) (segid="sbm1" and resid 43 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 43 and name ha) (segid="sbm2" and resid 43 and name hn) 1.8 0 4.2 {vw, 4.64, 4*, 0} ; 1371 1 1438 27 parsed_1b4c 1 73 "{m?, 3.39, 5, 1.0}" 1442 1 1442 28 parsed_1b4c 1 74 ; {w, 7.17, 3, 2.4, amb} I assign (segid="sbm1" and resid 43 and name he*) (segid="sbm1" and resid 43 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 43 and name he*) (segid="sbm2" and resid 43 and name hn) 1.8 0 4.2 {vw, 7.36, 4*, 2.4, amb} AMB NOTES 3D NOESY: noesy100- 242 116 25 ha dispersive Phe 43e (nh- 8.33ppm; n= 123.78) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Phe 43f (nh- 8.06ppm; n= 123.22) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Leu 44d INTRA ; 1446 1 1469 7 parsed_1b4c 1 75 ; {m, 4.04, 8, 0} amb assign (segid="sbm1" and resid 44 and name hb*) (segid="sbm1" and resid 44 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 44 and name hb*) (segid="sbm2" and resid 44 and name hn) 1.8 0 3.2 {b<, w?, 1.75, 10ov, 0.6} ; 1472 1 1476 34 parsed_1b4c 1 76 ; {b>, s, 1.62, 10, 0.6} amb assign (segid="sbm1" and resid 44 and name hg) (segid="sbm1" and resid 44 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 44 and name hg) (segid="sbm2" and resid 44 and name hn) 1.8 0 3.2 {w?, 1.75, 10ov, 0} I assign (segid="sbm1" and resid 44 and name hd*) (segid="sbm1" and resid 44 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 44 and name hd*) (segid="sbm2" and resid 44 and name hn) 1.8 0 1.7 {m, 0.78, 10, 2.3} NOTES 3D NOESY: noesy100- ~254 ~120 39 alpha- 4.04 ppm (8) ~279 ovlps N38 an-4[9/31] & M7 an-4[8/70] beta- 1.75 ppm (10) 363 ovlps M7 bn-1[8/83] NN-1 (hn102) 8.50ppm, (9/2), 115 ovlps nn[43] Leu 44e (nh- 8.28ppm; n= 115.41) hn12 NOTES 3D NOESY: noesy100- ~257 ~122 39 NN-1 (hn103) 8.33ppm, (), could ovlp hn12 Leu 44f (nh- 8.15ppm; n= 115.33) hn11 NOTES 3D NOESY: noesy100- 268 ~128 39 NN-1 (hn123)8.06ppm, (5), 131 nearly ovlps hn11 NOTES 4D CN: too weak and overlapped Glu 45 INTRA ; 1480 1 1510 7 parsed_1b4c 1 77 "{s, 4.23, 10}" 1513 1 1513 23 parsed_1b4c 1 78 ; {s, 2.24, 10} assign (segid="sbm1" and resid 45 and name hg*) (segid="sbm1" and resid 45 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 45 and name hg*) (segid="sbm2" and resid 45 and name hn) 1.8 0 1.7 {g', m, 2.79, 10} RS assign (segid="sbm1" and resid 45 and name hg*) (segid="sbm1" and resid 45 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 45 and name hg*) (segid="sbm2" and resid 45 and name hn) 1.8 0 1.7 {g'', m, 2.35, 8, 1.0} AMB amb/art? assign (segid="sbm1" and resid 84 and name ha) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 84 and name ha) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 4.68, 5, 0, cn}, chem shift 84ha not in 3D; could be 42ha as assigned NOTES 3D NOESY: noesy100- 338 157 33 Glu 45e (nh- 7.35ppm; n= 118.63) hn36 NOTES 3D NOESY: noesy100- 338 157 33 NOE to 8.15 verifies that d/f overlap Glu 45f (nh- 7.32ppm; n= 118.63) hn37 NOTES 3D NOESY: noesy100- 340 159 33 NN-2 (hn103) 8.3ppm, (), could ovlp nn-1! Glu 46d Glu 46e Glu 46f INTRA I assign (segid="sbm1" and resid 46 and name ha) (segid="sbm1" and resid 46 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 46 and name ha) (segid="sbm2" and resid 46 and name hn) 1.8 0 4.2 {vw, 4.64, 4*&6, 0} ; 1517 1 1554 29 parsed_1b4c 1 79 ; {m, 1.97, 8, 1} assign (segid="sbm1" and resid 46 and name hg*) (segid="sbm1" and resid 46 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 46 and name hg*) (segid="sbm2" and resid 46 and name hn) 1.8 0 1.7 {m, 2.22, 10, 1} ovlps 46hb< AMB amb assign (segid="sbm1" and resid C and name hb?) (segid="sbm1" and resid 46 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid C and name hb?) (segid="sbm2" and resid 46 and name hn) 1.8 0 1.7 {m, 1.97, 9, 0, cn} , E91hb1, 5hb*, 55hb*, 31hb2 amb/art? assign (segid="sbm1" and resid 47 and name hg1*) (segid="sbm1" and resid 46 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 47 and name hg1*) (segid="sbm2" and resid 46 and name hn) 1.8 0 4.2 {vw, 1.10, 6*, 1.0}, could be 80hg1* at 1.10; 47hg12 at 1.07 amb assign (segid="sbm1" and resid and name h?) (segid="sbm1" and resid 46 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid and name h?) (segid="sbm2" and resid 46 and name hn) 1.8 0 ? {w, 1.78, 5, , }, 44hg, 47hb, or 47hg11 NOTES 3D NOESY: noesy100- 313 ~146 32 NN (hn116) 7.82ppm, (8/2), ~140 nearly ovlps hn45 beta-N-1 (hn36) 2.22ppm, (10/2), could ovlp beta Ile 47 INTRA assign (segid="sbm1" and resid 47 and name ha) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 1.1 assign (segid="sbm2" and resid 47 and name ha) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 1.1 {s, 3.90, 10, 1.5} AMB art? assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 4.2 {vw, 3.83, 2, 1.5} NOTES 3D NOESY: noesy100-302 141 28 (values from HOHAHA-HSQC) hn too weak to observe in 3D or 4D Ile 47e? (nh- 7.81ppm) N= 122.25 hn116 very weak peak NOTES 4D CN: too weak Lys 48 nitrogen data too weak INTRA SEQ MED LONG INTER AMB NOTES 3D NOESY: noesy100- 217 105 20 an-1 and he could overlap NOTES 4D CN: too weak Glu 49 INTRA I assign (segid="sbm1" and resid 49 and name ha) (segid="sbm1" and resid 49 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 49 and name ha) (segid="sbm2" and resid 49 and name hn) 1.8 0 3.2 {w, 4.80 5, cn} ; 1558 1 1636 25 parsed_1b4c 1 80 ; {b<, s, 2.09, >10ovlp/~10, 0.6, cn} RS assign (segid="sbm1" and resid 49 and name hb*) (segid="sbm1" and resid 49 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 49 and name hb*) (segid="sbm2" and resid 49 and name hn) 1.8 0 1.7 {m, 2.03, >10ovlp/~10, 0.6} amb assign (segid="sbm1" and resid 49 and name hg*) (segid="sbm1" and resid 49 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 49 and name hg*) (segid="sbm2" and resid 49 and name hn) 1.8 0 1.7 {g', m, 2.28, 8ovlp/8, 1.0, cn} amb assign (segid="sbm1" and resid 49 and name hg*) (segid="sbm1" and resid 49 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 49 and name hg*) (segid="sbm2" and resid 49 and name hn) 1.8 0 1.7 {m, 2.13, >10ovlp/7, 1.0, cn} 50hb1 at 2.16 NOTES 3D NOESY: noesy100- 304 ~141 31 NN (hn88) 8.5ppm, , ~113 ovlps nn-1 NN-2 (hn116) 7.8ppm, (), could ovlp hn59 NOTES 4D CN: plane overlaps K55, so any NOEs from the CN could be to K55hn Gln 50 - INTRA ; 1640 1 1663 16 parsed_1b4c 1 81 "{s, 3.66, 12}{DJW lowered this to 1.7}" 1666 1 1666 48 parsed_1b4c 1 82 ; {b<, s, 2.16, 18/6} 49hg2 at 2.13 ? RS assign (segid="sbm1" and resid 50 and name hb*) (segid="sbm1" and resid 50 and name hn) 1.8 0 1.1 RS assign (segid="sbm2" and resid 50 and name hb*) (segid="sbm2" and resid 50 and name hn) 1.8 0 1.1 {b>, s, 1.94, 15/8} amb assign (segid="sbm1" and resid 50 and name hg*) (segid="sbm1" and resid 50 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 50 and name hg*) (segid="sbm2" and resid 50 and name hn) 1.8 0 3.2 {w, 2.35, 9ov/4} 51hg* also at 2.35 NOTES 3D NOESY: noesy100- 237 113 22 NOTES 4D CN: close to D23 in H and N, baseline troulbes at N=11, h=515-525 Glu 51 INTRA ; 1670 1 1689 7 parsed_1b4c 1 83 "{s, 4.09, >10, 0}" 1692 1 1692 27 parsed_1b4c 1 84 ; {s, 2.05, >10ov?/>10, 0} amb assign (segid="sbm1" and resid 51 and name hg*) (segid="sbm1" and resid 51 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 51 and name hg*) (segid="sbm2" and resid 51 and name hn) 1.8 0 1.7 {m?, 2.35, >10/~10, 0} 50hg* also at 2.35 AMB art? assign (segid="sbm1" and resid X and name hb?) (segid="sbm1" and resid 51 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid X and name hb?) (segid="sbm2" and resid 51 and name hn) 1.8 0 4.2 {vw, 2.79, 2, 0, ncn}, X= N37hb1, N38hb2, F76hb2 - dont like any NOTES 3D NOESY: noesy100- 184 90 36 NN-2 (hn59) 7.71ppm, (6), 144 ovlps hn[25]H25 nn[27] beta-N-1 (hn88) 1.9ppm, (), could ovlp beta, beta and beta-1 carbons also overlap Val 52 INTRA ; 1696 1 1717 7 parsed_1b4c 1 85 "{m, 3.63, 8, 0}" 1720 1 1720 25 parsed_1b4c 1 86 ; {s, 2.11, 13, 0} assign (segid="sbm1" and resid 52 and name hg2*) (segid="sbm1" and resid 52 and name hn) 1.8 0 1.1 assign (segid="sbm2" and resid 52 and name hg2*) (segid="sbm2" and resid 52 and name hn) 1.8 0 1.1 {s, 1.02, 11, 1.5, g<} assign (segid="sbm1" and resid 52 and name hg1*) (segid="sbm1" and resid 52 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 52 and name hg1*) (segid="sbm2" and resid 52 and name hn) 1.8 0 1.7 {w?, 0.83, 9/4, 1.5, g>} AMB NOTES 3D NOESY: noesy100- 365 168 34 Val 53 INTRA ; 1724 1 1744 7 parsed_1b4c 1 87 "{m, 3.36, 9, 0}" 1747 1 1747 24 parsed_1b4c 1 88 ; {s, 2.08, >10/ovlp, 0} I assign (segid="sbm1" and resid 53 and name hg1*) (segid="sbm1" and resid 53 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 53 and name hg1*) (segid="sbm2" and resid 53 and name hn) 1.8 0 3.2 {w, 0.96, 5/ovlp, 1.5, cn} assign (segid="sbm1" and resid 53 and name hg2*) (segid="sbm1" and resid 53 and name hn) 1.8 0 1.1 assign (segid="sbm2" and resid 53 and name hg2*) (segid="sbm2" and resid 53 and name hn) 1.8 0 1.1 {s, 0.90, >10, 1.5, cn} AMB NOTES 3D NOESY: noesy100- 387 178 32 beta-N-1 (hn2.0) 2.0ppm, (10/2),could ovlp beta, ovlps in Carbon as well Asp 54 INTRA ; 1751 1 1772 7 parsed_1b4c 1 89 "{m, 4.28, 9, 0}" 1775 1 1775 25 parsed_1b4c 1 90 ; {s, 2.65, >10, 1} AMB art? assign (segid="sbm1" and resid 76 and name he*) (segid="sbm1" and resid 54 and name hn) 1.8 0 6.6 art? assign (segid="sbm2" and resid 76 and name he*) (segid="sbm2" and resid 54 and name hn) 1.8 0 6.6 {vw, 7.30, 7*, 2.4}, shoulder of bigger peak NOTES 3D NOESY: noesy100- 227 108 31 V52 alpha-N-2 (hn34) 3.66ppm, (9/2), 293 could ovlp an-4 Q50 alpha-N-4 (hn88) 3.66ppm, (9/2), 293 could ovlp an-2 NOTES 4D CN: close to O1 in D1 Lys 55 hn nearly ovlps E49 INTRA ; 1779 1 1799 7 parsed_1b4c 1 91 "{s, 4.15, 10, 0}" 1802 1 1802 26 parsed_1b4c 1 92 ; {s, 1.97, ~10, 1, cn} assign (segid="sbm1" and resid 55 and name hg*) (segid="sbm1" and resid 55 and name hn) 1.8 0 2.4 assign (segid="sbm2" and resid 55 and name hg*) (segid="sbm2" and resid 55 and name hn) 1.8 0 2.4 {mw, 1.51, 7, 1, cn} amb assign (segid="sbm1" and resid 55 and name hd*) (segid="sbm1" and resid 55 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 55 and name hd*) (segid="sbm2" and resid 55 and name hn) 1.8 0 1.7 {m, 1.65?, 7, 1, cn} I assign (segid="sbm1" and resid 55 and name he*) (segid="sbm1" and resid 55 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 55 and name he*) (segid="sbm2" and resid 55 and name hn) 1.8 0 4.2 {vw, 2.92, 9*, 1, cn} NOTES 3D NOESY: noesy100- 302 141 31 NOTES 4D CN: plane overlaps E49, so NOEs from 4D CN could be to E49 instead Val 56 INTRA ; 1806 1 1830 7 parsed_1b4c 1 93 "{s, 3.60, >10, 0}" 1833 1 1833 27 parsed_1b4c 1 94 ; {s, 2.35, >10ov bn+1, 0} assign (segid="sbm1" and resid 56 and name hg2*) (segid="sbm1" and resid 56 and name hn) 1.8 0 1.1 assign (segid="sbm2" and resid 56 and name hg2*) (segid="sbm2" and resid 56 and name hn) 1.8 0 1.1 {s, 1.21, >>10, 1.5} assign (segid="sbm1" and resid 56 and name hg1*) (segid="sbm1" and resid 56 and name hn) 1.8 0 2.4 assign (segid="sbm2" and resid 56 and name hg1*) (segid="sbm2" and resid 56 and name hn) 1.8 0 2.4 {mw?, 0.83, 10, 1.5} NOTES 3D NOESY: noesy100- 278 131 27 E58 NN+2 (hn39) 8.27ppm, (), could ovlp nn V52 alpha-N-4 (hn34) 3.66ppm, (10/2), ~293, could ovlp ha Met 57 INTRA ; 1837 1 1857 7 parsed_1b4c 1 95 "{s, 4.03, 10, 0}" 1860 1 1860 25 parsed_1b4c 1 96 ; {b<, s, 2.33, >10ov, 0.6, cn/amb} R assign (segid="sbm1" and resid 57 and name hb*) (segid="sbm1" and resid 57 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 57 and name hb*) (segid="sbm2" and resid 57 and name hn) 1.8 0 1.7 {b>, m, 1.89, 10, 0.6} assign (segid="sbm1" and resid 57 and name hg*) (segid="sbm1" and resid 57 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 57 and name hg*) (segid="sbm2" and resid 57 and name hn) 1.8 0 1.7 {m?, 2.84, >10, 1.0, cn} viol with stg asbd8 ? assign (segid="sbm1" and resid 57 and name he*) (segid="sbm1" and resid 57 and name hn) 1.8 0 ? ? assign (segid="sbm2" and resid 57 and name he*) (segid="sbm2" and resid 57 and name hn) 1.8 0 ? {?, 1.99, ?, 1.5} NOTES 3D NOESY: noesy100- 256 ~121 37 E58 NN (hn39) 8.27ppm, (>10/2), ~123 ovlps hn19 V56 beta-N-1 (hn80) 2.33ppm, (10/2), ovlps hb2 in H and C Glu 58 INTRA ; 1864 1 1887 7 parsed_1b4c 1 97 "{s, 4.04, 15, 0}" 1890 1 1890 26 parsed_1b4c 1 98 ; {s, 2.13, 15, 1} assign (segid="sbm1" and resid 58 and name hg*) (segid="sbm1" and resid 58 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 58 and name hg*) (segid="sbm2" and resid 58 and name hn) 1.8 0 1.7 {m, 2.38, 11&10, 1.0} I assign (segid="sbm1" and resid 58 and name hg*) (segid="sbm1" and resid 58 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 58 and name hg*) (segid="sbm2" and resid 58 and name hn) 1.8 0 1.7 {m?, 2.27, 12&4, 1.0} NOTES 3D NOESY: noesy100- 260 123 33 NOTES 4D CN M57 NN-1 (hn19) 8.30ppm, (), could ovlp hn39 T59 NN (hn18) 8.04ppm, (12), 132 could ovlp nn-2[80] Thr 59 INTRA ; 1894 1 1915 7 parsed_1b4c 1 99 "{s, 3.98, 15}" 1918 1 1918 23 parsed_1b4c 1 100 ; {m, 4.42, 9} assign (segid="sbm1" and resid 59 and name hg2*) (segid="sbm1" and resid 59 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 59 and name hg2*) (segid="sbm2" and resid 59 and name hn) 1.8 0 1.7 {m?, 1.37, 11} NOTES 3D NOESY: noesy100- 298 140 29 D61 NN (hn20) 7.7ppm, (11), ovlps L60 hn[68] Asp 61 INTRA ; 1922 1 1937 7 parsed_1b4c 1 101 "{s, 4.39, >10}" 1940 1 1940 23 parsed_1b4c 1 102 ; {s, 2.65, 16} NOTES 3D NOESY: noesy100- 304 142 36 NN-1 (hn68) 7.81ppm, (25/3), could ovlp D61 hn20 NN (hn53) 7.78ppm, (25/3), could ovlp D61 hn20 Glu 62 INTRA ; 1944 1 1956 7 parsed_1b4c 1 103 "{s, 4.12, 16, 0}" 1959 1 1959 26 parsed_1b4c 1 104 "{s, 2.11, 18, 1}" 1963 1 1963 26 parsed_1b4c 1 105 ; {m?, 2.38, 11} NOTES 3D NOESY: noesy100- 301 141 32 NN-1 (hn20) 7.74ppm, (), ovlps E62 hn53 NN-2 (hn68) 7.81ppm, (), ovlps E62 hn53 Asp 63 INTRA ; 1967 1 1979 7 parsed_1b4c 1 106 "{m, 5.02, 9, 0}" 1982 1 1982 25 parsed_1b4c 1 107 ; {s, 2.57, 12, 1} NOTES 3D NOESY: noesy100- 350 162 34 E62 NN-1 (hn53) 7.79ppm, (14/2), 141 could ovlp nn-2[20] D61 NN-2 (hn20) 7.74ppm, (14/2), 141 could ovlp nn-1[53] Gly 64 INTRA ; 1986 1 1996 7 parsed_1b4c 1 108 ; {s, 3.93, 14, 0} NOTES 3D NOESY: noesy100- 290 136 49 G66 NN+2 (hn4) 8.09ppm, (), could ovlp nn Asp 65 INTRA ; 1999 1 2008 7 parsed_1b4c 1 109 ; {m/s, 4.88, 8} R assign (segid="sbm1" and resid 65 and name hb*) (segid="sbm1" and resid 65 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 65 and name hb*) (segid="sbm2" and resid 65 and name hn) 1.8 0 1.1 {b<, s, 2.81, 11} ; 2011 1 2015 27 parsed_1b4c 1 110 ; {b>, s, 2.60, 15} NOTES 3D NOESY: noesy100- 274 129 38 NN (hn4) 8.09ppm, (24/2), could ovlp hn16 Gly 66 INTRA ; 2019 1 2030 7 parsed_1b4c 1 111 ; {a>, s, 3.88, 14} RS assign (segid="sbm1" and resid 66 and name ha*) (segid="sbm1" and resid 66 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 66 and name ha*) (segid="sbm2" and resid 66 and name hn) 1.8 0 1.7 {a<, s, 4.15, 11} NOTES 3D NOESY: noesy100- 274 129 47 D65 NN-1 (hn16) 8.09ppm, (), ovlps hn4 Glu 67 INTRA ; 2033 1 2046 7 parsed_1b4c 1 112 "{m-s, 5.07, 8, 0}" 2049 1 2049 27 parsed_1b4c 1 113 "{s, 1.97, 14ov, 1}" 2053 1 2053 28 parsed_1b4c 1 114 ; I assign (segid="sbm1" and resid 67 and name hg*) (segid="sbm1" and resid 67 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 67 and name hg*) (segid="sbm2" and resid 67 and name hn) 1.8 0 1.7 {g', m, 2.38, 8, 1.0, cn} I assign (segid="sbm1" and resid 67 and name hg*) (segid="sbm1" and resid 67 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 67 and name hg*) (segid="sbm2" and resid 67 and name hn) 1.8 0 4.2 {g'', vw, 2.03, ?/1, 0, cn} NOTES 3D NOESY: noesy100- 241 115 33 D65 NN-2 (hn16) 8.09ppm, (), could ovlp nn-1 Cys 68 INTRA ; 2061 1 2076 7 parsed_1b4c 1 115 ; {ms, 5.18, 9} R assign (segid="sbm1" and resid 68 and name hb*) (segid="sbm1" and resid 68 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 68 and name hb*) (segid="sbm2" and resid 68 and name hn) 1.8 0 1.7 {b<, m, 3.11, 8} ; 2079 1 2083 26 parsed_1b4c 1 116 "{b>, s, 2.84, 11}" 2087 1 2087 27 parsed_1b4c 1 117 ; NOTES 3D NOESY: noesy100- 164 82 31 X/Y= R20hg1,hg2 not in 4D NOESY, also observed for G66 NOTES 4D CN K26ha 4 ctrs in 4D 9* in 3D go with 2 K28ha 6ctrs in 4D 3 in 3D go with 4 Asp 69 INTRA ; 2093 1 2105 7 parsed_1b4c 1 118 ; {m, 5.34, 8} R assign (segid="sbm1" and resid 69 and name hb*) (segid="sbm1" and resid 69 and name hn) 1.8 0 2.4 R assign (segid="sbm2" and resid 69 and name hb*) (segid="sbm2" and resid 69 and name hn) 1.8 0 2.4 {b<, w, 3.55, 6} ; 2108 1 2112 26 parsed_1b4c 1 119 "{b>, m?, 2.79, 10?}" 2116 1 2116 29 parsed_1b4c 1 120 ; NOTES 3D NOESY: noesy100- 233 111 27 Phe 70 INTRA ; 2121 1 2126 7 parsed_1b4c 1 121 "{w, 3.39, 3; but med rel to others}" 2129 1 2129 45 parsed_1b4c 1 122 "{s, 2.60, 6} strong relative to others" 2133 1 2133 50 parsed_1b4c 1 123 "{w, 6.32, 1}" 2137 1 2137 22 parsed_1b4c 1 124 ; I assign (segid="sbm1" and resid 70 and name he*) (segid="sbm1" and resid 70 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 70 and name he*) (segid="sbm2" and resid 70 and name hn) 1.8 0 4.2 {vw, 6.95, 4*} amb assign (segid="sbm1" and resid 70 and name hz) (segid="sbm1" and resid 70 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 70 and name hz) (segid="sbm2" and resid 70 and name hn) 1.8 0 4.2 {vw, 7.11, 8*} 14he* and 73he* at 7.11 and close in space NOTES 3D NOESY: noesy100- 181 89 32 Gln 71 INTRA ; 2145 1 2159 7 parsed_1b4c 1 125 "{s, 3.55, 15, 0}" 2162 1 2162 26 parsed_1b4c 1 126 ; {s, 2.13, 17ovlp/>10, 1.0} 71hg2 at 2.16?, 72hb2 at 2.09 should be wk assign (segid="sbm1" and resid 71 and name hg*) (segid="sbm1" and resid 71 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 71 and name hg*) (segid="sbm2" and resid 71 and name hn) 1.8 0 1.7 {g', m, 2.30, 14ovlp/10, 1.0} 72hg2 at 2.33? RS assign (segid="sbm1" and resid 71 and name hg*) (segid="sbm1" and resid 71 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 71 and name hg*) (segid="sbm2" and resid 71 and name hn) 1.8 0 1.7 {g'', m, 2.16, 17ovlp/10, 1.0} 71b* at 2.13 I assign (segid="sbm1" and resid 71 and name he2*) (segid="sbm1" and resid 71 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 71 and name he2*) (segid="sbm2" and resid 71 and name hn) 1.8 0 4.2 {e2', vw, 7.32, 1ov?, 1.0} assign (segid="sbm1" and resid 71 and name he2*) (segid="sbm1" and resid 71 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 71 and name he2*) (segid="sbm2" and resid 71 and name hn) 1.8 0 4.2 {e2'', vw, 6.73, 3*, 1.0} ; 2166 1 2182 34 parsed_1b4c 1 127 ; NOTES 3D NOESY: noesy100- 288 135 35 D69 NN-2 (hn78) 8.58ppm, (4/2), 110 could ovlp nn+2 F73 NN+2 (hn72) 8.62ppm, (4/2), 110 could ovlp nn-2 Glu 72 close to Q16 in 1H and 15N INTRA ; 2193 1 2202 7 parsed_1b4c 1 128 "{s, 4.01, 12, 0}" 2205 1 2205 26 parsed_1b4c 1 129 ; {b<, s, 2.35, 17, 0.6} RS assign (segid="sbm1" and resid 72 and name hb*) (segid="sbm1" and resid 72 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 72 and name hb*) (segid="sbm2" and resid 72 and name hn) 1.8 0 1.7 {b>, m, 2.09, 8, 0.6} ; 2209 1 2213 31 parsed_1b4c 1 130 "{g', m, 2.46, 9, 1.0}" 2217 1 2217 31 parsed_1b4c 1 131 ; RS assign (segid="sbm1" and resid 72 and name hg*) (segid="sbm1" and resid 72 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 72 and name hg*) (segid="sbm2" and resid 72 and name hn) 1.8 0 1.7 {g'', m, 2.33, 8, 1.0} NOTES 3D NOESY: noesy100- 254 121 28 M74 NN+2 (hn32) 8.00ppm, () could ovlp nn-1 Phe 73 INTRA I assign (segid="sbm1" and resid 73 and name ha) (segid="sbm1" and resid 73 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 73 and name ha) (segid="sbm2" and resid 73 and name hn) 1.8 0 3.2 {w, 4.39, 4, 0} ; 2225 1 2241 25 parsed_1b4c 1 132 ; {s, 3.33, 12, 0.6} RS assign (segid="sbm1" and resid 73 and name hb*) (segid="sbm1" and resid 73 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 73 and name hb*) (segid="sbm2" and resid 73 and name hn) 1.8 0 1.7 {m?, 3.22, 10, 0.6} amb assign (segid="sbm1" and resid 73 and name hd*) (segid="sbm1" and resid 73 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 73 and name hd*) (segid="sbm2" and resid 73 and name hn) 1.8 0 1.7 {m, 6.92, 7, 2.4, amb} NOTES 3D NOESY: noesy100- 229 110 29 Q71 NN-2 (hn28) 7.93ppm, (), could ovlp nn NOTES 4D CN: close to O1 in D1 so intensity greatly attenuated Met 74 INTRA ; 2245 1 2265 7 parsed_1b4c 1 133 ; {s, 3.68, 10, 0} amb assign (segid="sbm1" and resid 74 and name ha) (segid="sbm1" and resid 74 and name he*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 74 and name ha) (segid="sbm2" and resid 74 and name he*) 1.8 0 1.5 {m, 3.69, 10, 1.5, vvw cfilt} R assign (segid="sbm1" and resid 74 and name hb*) (segid="sbm1" and resid 74 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 74 and name hb*) (segid="sbm2" and resid 74 and name hn) 1.8 0 1.7 {b<, m, 1.67, 13ov, 0.6, amb} 74he* at ~1.64 ; 2268 1 2276 53 parsed_1b4c 1 134 ; {b>, s, 1.48, 13&10, 0.6, cn} assign (segid="sbm1" and resid 74 and name hg*) (segid="sbm1" and resid 74 and name hn) 1.8 0 2.4 assign (segid="sbm2" and resid 74 and name hg*) (segid="sbm2" and resid 74 and name hn) 1.8 0 2.4 {mw?, 1.94, 7, 1, ncn} amb assign (segid="sbm1" and resid 74 and name he*) (segid="sbm1" and resid 74 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 74 and name he*) (segid="sbm2" and resid 74 and name hn) 1.8 0 3.2 {w, 1.64, 13ov, 1.5, amb} NOTES 3D NOESY: noesy100- 282 133 34 F76 NN+2 (hn23) 7.99ppm, (), could ovlp M74 hn32 Ala 75 INTRA ; 2280 1 2298 7 parsed_1b4c 1 135 "{s, 4.01, 12, 0, cn}" 2301 1 2301 30 parsed_1b4c 1 136 ; {s, 1.24, 19, 1.1} NOTES 3D NOESY: noesy100- 294 138 22 M74 NN-1 (hn32) 8.00ppm, (14/2), 133 ovlps nn F76 NN (hn23) 7.99ppm, (14/2), 133 ovlps nn-1 Phe 76 INTRA I assign (segid="sbm1" and resid 76 and name ha) (segid="sbm1" and resid 76 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 76 and name ha) (segid="sbm2" and resid 76 and name hn) 1.8 0 3.2 {w, 4.31, 5, 0, cn} ; 2305 1 2320 29 parsed_1b4c 1 137 ; {b<, s, 3.06, 13/11, 0.6} RS assign (segid="sbm1" and resid 76 and name hb*) (segid="sbm1" and resid 76 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 76 and name hb*) (segid="sbm2" and resid 76 and name hn) 1.8 0 1.7 {b>, m, 2.81, 10/5, 0.6} amb assign (segid="sbm1" and resid 76 and name hd*) (segid="sbm1" and resid 76 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 76 and name hd*) (segid="sbm2" and resid 76 and name hn) 1.8 0 1.7 {m, 7.30, 9, 2.4, amb} NOTES 3D NOESY: noesy100- 283 133 35 ha vw in 3D NOESY and 10 ctrs in 4D go with 5 ctrs Val 77 INTRA ; 2324 1 2343 7 parsed_1b4c 1 138 "{s, 3.44, 11, 0}" 2346 1 2346 26 parsed_1b4c 1 139 ; {s, 1.73, 15, 0} amb assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm1" and resid 77 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm2" and resid 77 and name hn) 1.8 0 1.7 {m?, 0.77, 11, 1.5} 3hd2* may contribute as inter assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm1" and resid 77 and name hn) 1.8 0 1.1 assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm2" and resid 77 and name hn) 1.8 0 1.1 {s, 0.48, 15, 1.5} NOTES 3D NOESY: noesy100- 244 116 35 A75 NN-2 (hn87) 7.8ppm, (5/2), 139 could ovlp nn+2 M79 NN+2 (hn79) 7.8ppm, (5/2), 139 could ovlp nn-2 Ser 78 INTRA ; 2350 1 2371 7 parsed_1b4c 1 140 "{s?, 3.66, 10ov, 0}" 2374 1 2374 29 parsed_1b4c 1 141 ; {s, 3.96, 13ov, 0} NOTES 3D NOESY: noesy100- 228 109 32 M79 NN (hn79) 7.85ppm, (12), 139 could ovlp nn+2 Met 79 INTRA ; 2378 1 2389 7 parsed_1b4c 1 142 "{s, 3.93, 11}" 2392 1 2392 23 parsed_1b4c 1 143 ; {b<, s, 2.22, 15} I assign (segid="sbm1" and resid 79 and name hb*) (segid="sbm1" and resid 79 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 79 and name hb*) (segid="sbm2" and resid 79 and name hn) 1.8 0 1.7 {b>, m?, 1.92, 13ov?/~9} 79he* at 1.92 also I assign (segid="sbm1" and resid 79 and name hg*) (segid="sbm1" and resid 79 and name hn) 1.8 0 1.1 I assign (segid="sbm2" and resid 79 and name hg*) (segid="sbm2" and resid 79 and name hn) 1.8 0 1.1 {g', s, 2.52, 12/~12} I assign (segid="sbm1" and resid 79 and name hg*) (segid="sbm1" and resid 79 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 79 and name hg*) (segid="sbm2" and resid 79 and name hn) 1.8 0 3.2 {g'', w?, 2.35, 9/5} I assign (segid="sbm1" and resid 79 and name he*) (segid="sbm1" and resid 79 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 79 and name he*) (segid="sbm2" and resid 79 and name hn) 1.8 0 3.2 {w?, 1.92ov, 13} NOTES 3D NOESY: noesy100- 297 139 27 V80 NN (hn22) 7.80ppm, (25/2), ~139 could ovlp M79 hn79 Val 80 - INTRA ; 2396 1 2421 16 parsed_1b4c 1 144 "{s, 3.39, 11}" 2424 1 2424 22 parsed_1b4c 1 145 ; {s, 2.05, 9} assign (segid="sbm1" and resid 80 and name hg2*) (segid="sbm1" and resid 80 and name hn) 1.8 0 1.1 assign (segid="sbm2" and resid 80 and name hg2*) (segid="sbm2" and resid 80 and name hn) 1.8 0 1.1 {s, 1.10, 14} amb assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 80 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 80 and name hn) 1.8 0 1.7 {m?, 0.94, 9ov} assign (segid="sbm1" and resid 80 and name ha) (segid="sbm1" and resid 80 and name hg2*) 1.8 0 1.1 assign (segid="sbm2" and resid 80 and name ha) (segid="sbm2" and resid 80 and name hg2*) 1.8 0 1.1 {s, 3.37, >12, 1.5} NOTES 3D NOESY: noesy100- 298 139 36 M79 NN-1 (hn79) ppm, (22/2), ~139 ovlps V80 hn22 T81 NN+2 (hn) ppm, (), could ovlp hn22 NOTES 4D CN: M79 an-1 could also be R20, F88 Thr 81 INTRA I assign (segid="sbm1" and resid 81 and name ha) (segid="sbm1" and resid 81 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 81 and name ha) (segid="sbm2" and resid 81 and name hn) 1.8 0 3.2 {w?, 3.68, 6ov} ; 2428 1 2457 25 parsed_1b4c 1 146 ; {m?, 4.26, 8} assign (segid="sbm1" and resid 81 and name hg2*) (segid="sbm1" and resid 81 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 81 and name hg2*) (segid="sbm2" and resid 81 and name hn) 1.8 0 1.7 {m?, 1.05, 8} NOTES 3D NOESY: noesy100- ~270 ~127 38 V80 NN-1 (hn22) 7.80ppm, (10/3), ~139 could ovlp nn and nn-2 T82 NN (hn111) 7.87ppm, (10/3), ~139 could ovlp nn-1/-2 M79 NN-2 (hn79) 7.83ppm, (10/3), ~139 could ovlp nn and nn-1 NOTES 4D CN V80 aN-1 (hn22) and V77 aN-4 (hn29) 3.4ppm, ovlp @ C=67.23; could also be I11 or V53 S78an-3 could also be S41ha,hb or I47hb Thr 82 INTRA I assign (segid="sbm1" and resid 82 and name ha) (segid="sbm1" and resid 82 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 82 and name ha) (segid="sbm2" and resid 82 and name hn) 1.8 0 4.2 {vw, 3.28, 2} I assign (segid="sbm1" and resid 82 and name hb) (segid="sbm1" and resid 82 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 82 and name hb) (segid="sbm2" and resid 82 and name hn) 1.8 0 4.2 {vw, 3.74, 8*} assign (segid="sbm1" and resid 82 and name hg2*) (segid="sbm1" and resid 82 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 82 and name hg2*) (segid="sbm2" and resid 82 and name hn) 1.8 0 3.2 {w?, 0.59, 6} NOTES 3D NOESY: noesy100- 293 137 45 there was some uncertainty about the assignment of ha and hb however a unique noe was observed for A83 to 3.79,68.38 consistent with the current assignment of the ha and hb for T82 M79 aN-3 (hn79) 3.96ppm, vw(9), ~282 could ovlp an-4; strgr at 8.6ppm S78 aN-4 (hn49) 3.96ppm, vw(9), ~282 could ovlp an-3; strgr at 8.6ppm vw pk 100ms NOESY looks like two peaks 7.88/7.86 Ala 83 INTRA ; 2461 1 2507 7 parsed_1b4c 1 147 "{m, 4.48, 9, cn}" 2510 1 2510 26 parsed_1b4c 1 148 ; {s, 1.61, 17} NOTES 3D NOESY: noesy100- 347 160 29 ha dispersive in 3D NOESY; hb 17 ctrs in both expts so 9 ctrs used for ha Cys 84 INTRA I assign (segid="sbm1" and resid 84 and name ha) (segid="sbm1" and resid 84 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 84 and name ha) (segid="sbm2" and resid 84 and name hn) 1.8 0 4.2 {vw, 4.75, 5*} I assign (segid="sbm1" and resid 84 and name hb*) (segid="sbm1" and resid 84 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 84 and name hb*) (segid="sbm2" and resid 84 and name hn) 1.8 0 4.2 {b<, vw, 2.98, 7*} I assign (segid="sbm1" and resid 84 and name hb*) (segid="sbm1" and resid 84 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 84 and name hb*) (segid="sbm2" and resid 84 and name hn) 1.8 0 4.2 {b>, vw, 2.73, 1, 0.6} NOTES 3D NOESY: noesy100- 325 151 37 His 85? INTRA (nh- 8.35ppm) hn119 seems to be multiple 8.35, 8.34, 8.33 nn region differs a little between 100 and 200 ms noesy100- ~254 ~121 48 alpha?- 3.68 ppm () ~292 ovlps has[3], could be 3.8 instead beta1- 2.16 ppm () 348 ovlps peak from G22(hn3) beta2- 1.89 ppm () 358 ovlps peak from G22 Glu 86? INTRA (nh- 8.01ppm) hn107 dispersive amide in 100ms close to E91 in 1H and 15N noesy100- 281 ~132 20 alpha- 4.36 ppm () missing in NOESY, present in TOCSY beta1- 2.22 ppm vw(8) 346 close to negative peak beta2- 1.86 ppm (4) 359 gamma1- 2.57 ppm vw(9) 340 gamma2- 2.38 ppm vw(6) 333 close to negative peak Phe 87 INTRA (nh- 8.61ppm) hn122 noesy100- 229 ~109 25 alpha- 3.96 ppm (4) 282 beta1- 2.00 ppm (5) 354 beta2- 1.86 ppm (5) 359 could ovpl b2n-1 ??in tocsy- 1.56 ppm (3) Phe 88 INTRA ; 2514 1 2593 8 parsed_1b4c 1 149 ; {s, 3.98, 10} I assign (segid="sbm1" and resid 88 and name hb*) (segid="sbm1" and resid 88 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 88 and name hb*) (segid="sbm2" and resid 88 and name hn) 1.8 0 1.7 {b<, m, 3.30, 8/4} ; 2596 1 2600 28 parsed_1b4c 1 150 ; {b>, m, 2.95, 10/~10} amb assign (segid="sbm1" and resid 88 and name hd*) (segid="sbm1" and resid 88 and name hn) 1.8 0 1.1 amb assign (segid="sbm2" and resid 88 and name hd*) (segid="sbm2" and resid 88 and name hn) 1.8 0 1.1 {s, 7.33, 11, amb} amb assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 88 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 88 and name hn) 1.8 0 4.2 {vw, 7.14, 8*, 2.4} probably 88he* NOTES 3D NOESY: noesy100- 329 ~153 40 E89 NN (hn60) 7.57ppm, (~6), ~149 ovlps F88 hn5 Glu 89 INTRA ; 2604 1 2623 7 parsed_1b4c 1 151 ; {s, 4.17, 11} R assign (segid="sbm1" and resid 89 and name hb*) (segid="sbm1" and resid 89 and name hn) 1.8 0 2.3 R assign (segid="sbm2" and resid 89 and name hb*) (segid="sbm2" and resid 89 and name hn) 1.8 0 2.3 {b<, m?, 1.97, 12/ov?} ; 2626 1 2630 32 parsed_1b4c 1 152 ; {b>, s, 1.81, 14} I assign (segid="sbm1" and resid 89 and name hg*) (segid="sbm1" and resid 89 and name hn) 1.8 0 1.7 I assign (segid="sbm2" and resid 89 and name hg*) (segid="sbm2" and resid 89 and name hn) 1.8 0 1.7 {m?, 2.16, 12ov} NOTES 3D NOESY: noesy100-320 149 31 His 90 INTRA ; 2634 1 2647 7 parsed_1b4c 1 153 ; {m, 4.66, 7, cn} I assign (segid="sbm1" and resid 90 and name hb*) (segid="sbm1" and resid 90 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 90 and name hb*) (segid="sbm2" and resid 90 and name hn) 1.8 0 4.2 {b<, vw, 3.14, *} I assign (segid="sbm1" and resid 90 and name hb*) (segid="sbm1" and resid 90 and name hn) 1.8 0 4.2 I assign (segid="sbm2" and resid 90 and name hb*) (segid="sbm2" and resid 90 and name hn) 1.8 0 4.2 {b>, vw, 3.06, *} NOTES 3D NOESY: noesy100- 274 129 32 ha dispersive in 3D, stronger in 4D E91 NN (hn90) ppm, (17/2), ~129 could ovlp H90 hn114 Glu 91 INTRA I assign (segid="sbm1" and resid 91 and name ha) (segid="sbm1" and resid 91 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 91 and name ha) (segid="sbm2" and resid 91 and name hn) 1.8 0 3.2 {w, 4.04, 5} I assign (segid="sbm1" and resid 91 and name hb*) (segid="sbm1" and resid 91 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 91 and name hb*) (segid="sbm2" and resid 91 and name hn) 1.8 0 3.2 {b<, w, 2.00, 3} ; 2650 1 2673 26 parsed_1b4c 1 154 ; {b>, m, 1.86, 8} I assign (segid="sbm1" and resid 91 and name hg*) (segid="sbm1" and resid 91 and name hn) 1.8 0 3.2 I assign (segid="sbm2" and resid 91 and name hg*) (segid="sbm2" and resid 91 and name hn) 1.8 0 3.2 {w, 2.16, 4} NOTES 3D NOESY noesy100- 273 129 20 H90 NN-1 (hn114) 8.0ppm, (), could ovlp E91 hn90 NOTES 4D CN H90ha 13 ctrs in 4D close to H2O in 3D go with 6 ctrs Note 1: number in parentheses are number of contours seen at lvl=0.02 of NOESY-HMQC for weak peaks and at lvl=0.1 for others Nilges et al. Biopolymers 29, 813-822, (1990). note 2: Naming- upfield = > , downfield = < previous naming was downfield "1" and upfield "2" Two beta protons are named downfield beta proton, hb1, and upfield beta proton, hb2; if degenerate, then hb*. For CH3 protons the protons hb11,hb12,hb13 and hb21,hb22,hb23. If degenerate, use hb1* for the downfield and hb2* for the upfield. Gamma, delta, epsilon, and eta, protons were treated in a similar manner. note 3a: Pseudo-corrections - NOT USED as of noe10.tbl, swith to sum averaging - ACD 971126 (a) CH3 groups add 1.0 A to the upper limit (b) CH2 group with degenerate protons add 1.0 A to the upper limit (c) degenerate CH3 groups for V, L add 1.7 A to the upper limit (d) aromatics add 2.3 A to the upper limit Conditions for 3D 100 ms NOESY-HSQC contour level = 0.1 # of levels= 20 level mult= 1.2 strong noe (>10 contour) = 1.8 0 0.9 (0 to 2.7 angstroms) strong noe (>10 contour) = 1.8 0 1.1 (0 to 2.9 angstroms for hn) medium noe (7-10 contours) = 1.8 0 1.5 (0 to 3.3 angstroms) medium noe (7-10 contours) = 1.8 0 1.7 (0 to 3.5 angstroms for hns) weak noe (3-6 countours) = 1.8 0 3.2 (0 to 5.0 angstroms) very weak noe (<3 countours) = 1.8 0 4.2 (0 to 6.0 angstroms) very weak(not seen at lvl=0.1) = 1.8 0 4.2 (0 to 6.0 angstroms) residue (nh- ppm) arbitrary assignment (destination residue) (origin residue) assign (segid="sbm1" and resid and name hn) (segid="sbm1" and resid and name hn) {s-m-w, dest'n ppm, # contours,correction} order: intraresidue sequentials medium range long range ordered by dest'n ppm value notes about questions Definitions of codes for commenting out NOEs !I!: all intraresidue NOEs commented out !viol!: comment out b/c violation in xplor run(s) !R!: redundant; weaker of two removed, if equal # levels first appearing removed !amb!: ambiguous and may not necessarily be resolved from any NOESY spectra ******************************************************************************************* **** DATA FROM 3D 13C-EDITED AND 4D 13C,13C-EDITED NOESY SPECTRA ************************** ******************************************************************************************* All parameters not mentioned here are same for the 13C-edited NOESY Conditions for 3D 13C-edited NOESY-HSQC contour level = 0.2 # of levels= 20 level mult= 1.2 strong noe (>10 contours) = 1.8 0 0.9 (0 to 2.7 angstroms) medium noe (7-10 contours) = 1.8 0 1.5 (0 to 3.3 angstroms) weak noe (3-6 countours) = 1.8 0 3.2 (0 to 5.0 angstroms) very weak noe (<3 countours) = 1.8 0 4.2 (0 to 6.0 angstroms) very weak(not seen at lvl=0.1) = 1.8 0 4.2 (0 to 6.0 angstroms) ******************************************************************************************* Ser 1a (nh-10.23; n= 121.93 ppm) hn104 no sidechain peaks in 3D TOCSY SEQ M assign (segid="sbm1" and resid 0 and name ha) (segid="sbm1" and resid 1 and name hn) 1.8 0 3.2 M assign (segid="sbm2" and resid 0 and name ha) (segid="sbm2" and resid 1 and name hn) 1.8 0 3.2 {w, 3.82, 5, 0} ; 2677 1 2767 24 parsed_1b4c 1 155 ; {vw, 8.93, 4*, 0} AMB amb assign (segid="sbm1" and resid and name h) (segid="sbm1" and resid 1 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid and name h) (segid="sbm2" and resid 1 and name hn) 1.8 0 ? {, 0.61, 2*, } amb assign (segid="sbm1" and resid ? and name h) (segid="sbm1" and resid 1 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid ? and name h) (segid="sbm2" and resid 1 and name hn) 1.8 0 ? {, 1.70, ?*, } amb assign (segid="sbm1" and resid ? and name h) (segid="sbm1" and resid 1 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid ? and name h) (segid="sbm2" and resid 1 and name hn) 1.8 0 ? {, 2.60, 4*, } amb assign (segid="sbm1" and resid ? and name h) (segid="sbm1" and resid 1 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid ? and name h) (segid="sbm2" and resid 1 and name hn) 1.8 0 ? {, 8.39, 3*, } NOTES 3D NOESY: noesy100-92 51 28 NOE, hn[], D2(pt), ovlp NN,98, could ovlp nn+2 N+2 (hn70/hn71), 98, could ovlp nn N+3 (hn55), 129 N+4 (hn26), 112 Ser 1b (nh-9.95ppm; n= 120.73) hn108 NOTES 3D NOESY: noesy100-115 61 30 no sidechain peaks in 3D TOCSY sc NOEs at 4.33, 2.27, 1.84, 1.73 NN, 98, could ovlp nn+2 N+2 (hn70/hn71) 98 N+3 (hn55) 128 N+4 (hn26) 112 NOTES 4D CN: signals stronger in 4D than 3D as exected in range of H2O Glu 2 SEQ ; 2771 1 2813 5 parsed_1b4c 1 156 ; {s, 4.66, 11?, 0, cn, amb} R assign (segid="sbm1" and resid 3 and name hn) (segid="sbm1" and resid 2 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 3 and name hn) (segid="sbm2" and resid 2 and name hn) 1.8 0 1.1 {s?, 8.94, ovlps 2hn, 0} remove 1ha-2hn b/c dispersive and very weak in 3d NOTES 3D NOESY (nh- 8.93ppm; n= 120.7) hn62 noesy100- 202 98 30 NN (hn70), 8.94, could ovlp hn62 NN+2 (hn55) 129 NN+3 (hn24/hn26?), 113 NOTES 4D CN: Y= S1 or F43 Leu 3a SEQ ; 2816 1 2837 5 parsed_1b4c 1 157 "{s?, 8.94, ovlps 3hn, 0}" 2840 1 2840 33 parsed_1b4c 1 158 "{mw, 4.04, 8, 0, cn, amb}" 2844 1 2844 35 parsed_1b4c 1 159 ; {m, 2.08, 7, 1} amb assign (segid="sbm1" and resid 2 and name hg*) (segid="sbm1" and resid 3 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 2 and name hg*) (segid="sbm2" and resid 3 and name hn) 1.8 0 3.2 {w?, 2.47, 13/*, 1}, s in 4D but vw in 3D? R assign (segid="sbm1" and resid 4 and name hn) (segid="sbm1" and resid 3 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 4 and name hn) (segid="sbm2" and resid 3 and name hn) 1.8 0 1.1 {s, 8.11, 14?, 0}, 3a/c see 4ahn at 8.11, 3bhn sees 4bhn at 7.73 M assign (segid="sbm1" and resid 4 and name hb*) (segid="sbm1" and resid 3 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 4 and name hb*) (segid="sbm2" and resid 3 and name hn) 1.8 0 4.2 {vw, 2.27, 6*, 1.0, amb}, or inter to 34hg2, 13hb ?? NOTES 3D NOESY: noesy100- 201 98 29 ovlps hn62(E2) in 1H and one 15N plane away NN (hn55) 129, ovlps hn62(E2) (nh- 8.94; n= 121.37) hn70 Leu 3b (nh- 9.01ppm) hn73 NOTES 3D NOESY: noesy100- 194 95 28 NN (hn35) 7.76ppm, vw(9), 142 NOTES 4D CN: could not find Leu 3c (nh- 8.92; n= 121.62) hn71 overlaps L3a in 1H and 15N in 3D Glu 4a SEQ ; 2848 1 2880 5 parsed_1b4c 1 160 "{s?, 8.96, 7ov, 0}, 4ahn sees above, 4bhn see 9.04 but is vw, relatively stg for strip" 2883 1 2883 95 parsed_1b4c 1 161 ; {mw, 4.04, 5?, 0} amb/R assign (segid="sbm1" and resid 3 and name hb*) (segid="sbm1" and resid 4 and name hn) 1.8 0 3.2 amb/R assign (segid="sbm2" and resid 3 and name hb*) (segid="sbm2" and resid 4 and name hn) 1.8 0 3.2 {w, 1.89, 6ov, 1.0}, not seen by E4bhn ; 2887 1 2891 47 parsed_1b4c 1 162 ; {s?, 1.75, 10 ov?, 1.0} 39hb* may contribute as inter amb assign (segid="sbm1" and resid 3 and name hg) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hg) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 {vw, 1.54?, 1, 0, amb} SD? assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 {vw, 0.99d', 2, 2.9, amb} ; 2895 1 2903 34 parsed_1b4c 1 163 "{w, 0.75, 3, 2.9, amb}" 2907 1 2907 31 parsed_1b4c 1 164 ; {s?, 8.53-8, 7, 0}, this is 5a/chn; vw pk to 5bhn at 7.88 also seen; vice versa for E4bhn amb/DL assign (segid="sbm1" and resid 5 and name hd*) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 amb/DL assign (segid="sbm2" and resid 5 and name hd*) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 {w, 1.73, 10 ov, 1} could be 39hb*?? NOTES 3D NOESY: noesy100-273 129 31 NN-1 (hn70/71) 98, could ovlp nn-2 NN-2 (hn62), could ovlp nn-1 Glu 4b (nh- 7.73ppm; n= 118.47) hn35 NOTES 3D NOESY: noesy100- 305 142 33 K5 NN (hn30) 7.89ppm, (~3), ~137 ovlps E4b hn35 NOTES 4D CN: could not find ha=3.33 Lys 5a SEQ R assign (segid="sbm1" and resid 4 and name hn) (segid="sbm1" and resid 5 and name hn) 1.8 0 1.5 R assign (segid="sbm2" and resid 4 and name hn) (segid="sbm2" and resid 5 and name hn) 1.8 0 1.5 {m, 8.09, 7?, 0}, 4bhn vw at 7.79 seen by 5ahn, vw 7.74 by 5chn, w at 7.76 by 5bhn ; 2911 1 2934 91 parsed_1b4c 1 165 "{w, 3.28, 7*, 0}, 4.28 is 4ahn, 5bhn sees 4bhn at 4.33" 2938 1 2938 63 parsed_1b4c 1 166 ; {w, 2.24, 4, 1.0, amb} vw or not there for 5bhn M assign (segid="sbm1" and resid 6 and name hn) (segid="sbm1" and resid 5 and name hn) 1.8 0 3.2 M assign (segid="sbm2" and resid 6 and name hn) (segid="sbm2" and resid 5 and name hn) 1.8 0 3.2 {w, 8.20, 4, 0}, this peak only shows for 5b-hn NOTES 3D NOESY: noesy100- 233 112 35 (nh- 8.57ppm; n= 117.59) hn24; multiple with hn26 and hn30 A6a NN (hn83) 131, could ovlp nn-1 NN-2 (hn70/71) 97, could ovlp NN-3, not ovlpd in hn70/71 strip NN-3 (hn62) 97, could ovlp NN-2 Lys5c (nh- 8.51ppm; n= 117.59) hn26 3D NOESY: noesy100- 238 114 35 NN-1 (hn55), could ovlp nn NN (hn83) 131, could ovlp nn-1 NN-2 (hn70/71) 98, could ovlp NN-3 NN-3 (hn62) 98, could ovlp NN-2 4D CN: 1.65 may be hd and hg Lys 5b (nh- 7.88ppm; n= 118.15) hn30 NOTES 3D NOESY: noesy100- 292 137 34 Ala 6a SEQ ; 2942 1 2971 5 parsed_1b4c 1 167 "{s?, 8.55, 10, 0}, above is 5a/c-hn, 6b-hn sees 5b-hn at 7.90 (so does 6a-hn vw)" 2974 1 2974 89 parsed_1b4c 1 168 "{mw, 3.90-3, 6, 0}, above is 5a/c-ha, 6b-hn sees 5b-hn at 4.01" 2978 1 2978 71 parsed_1b4c 1 169 ; {s, 1.89, 13?, 1}, above is 5a/c-hb*, 6b-hn sees 5b-hb* at 1.94 9 lvls amb assign (segid="sbm1" and resid 5 and name hg*) (segid="sbm1" and resid 6 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 5 and name hg*) (segid="sbm2" and resid 6 and name hn) 1.8 0 4.2 {vw, 1.43, 8*, 1.0, amb}, above is 5a-hg*, 6b-hn sees 5b/c-hg* at 1.48 R assign (segid="sbm1" and resid 7 and name hn) (segid="sbm1" and resid 6 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 7 and name hn) (segid="sbm2" and resid 6 and name hn) 1.8 0 1.1 {s, 8.33, 10, 0} M assign (segid="sbm1" and resid 7 and name hg*) (segid="sbm1" and resid 6 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 7 and name hg*) (segid="sbm2" and resid 6 and name hn) 1.8 0 4.2 {vw, 2.84, 2, 1.0, amb}, notsen by 6b-hn NOTES 3D NOESY: noesy100- 279 131 26 aN-2 (hn55) 3.3ppm,~304, ovlpd w/another peak Ala 6b (nh- 8.18ppm) hn82 NOTES 3D NOESY: noesy100- 267 126 26 M7 NN (hn8) 8.33ppm, (2), 121 could ovlp V8 nn+2 K5 aN-1 (hn30) 4.01ppm, (2), 280 could ovlp an-3,an-4 V8 NN+2 (hn42) 8.34ppm, (), could ovlp M7 nn L3b aN-3 (hn70/71) 4.01ppm, (2), 280 could ovlp an-1/-4 E2 aN-4 (hn62) 4.01ppm, (2), 280 could ovlp an-1/-3 NOTES 4D CN: could not find Met 7 SEQ ; 2982 1 3013 5 parsed_1b4c 1 170 "{s, 8.06, 10, 0}" 3016 1 3016 25 parsed_1b4c 1 171 ; {w, 4.28, 2?, 0, amb} R assign (segid="sbm1" and resid 8 and name hn) (segid="sbm1" and resid 7 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 8 and name hn) (segid="sbm2" and resid 7 and name hn) 1.8 0 1.1 {s?, 8.5, 9?, 0} assign (segid="sbm1" and resid 8 and name hg2*) (segid="sbm1" and resid 7 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 8 and name hg2*) (segid="sbm2" and resid 7 and name hn) 1.8 0 4.2 {vw?, 1.21, 4, 1.5, ncn} viol as wk asbd8 amb assign (segid="sbm1" and resid 8 and name hg1*) (segid="sbm1" and resid 7 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 8 and name hg1*) (segid="sbm2" and resid 7 and name hn) 1.8 0 3.2 {vw, 0.99, 7, 2.9, ncn} NOTES 3D NOESY noesy100- 254 121 39 (nh- 8.33ppm; n= 115.25) hn8 close to hn9[N38], L44d&e V8 NN (hn43) 114, could ovlp K5 nn-2, as well as L44,N38 K5 bN-1 (hn83) 365, ovlps L44hb and hg K5 NN-2 (hn24), could ovlp nn, as well as L44,N38 A9 NN+2 9 (hn81) 140, could ovlp hn[9]N38 nn-1[13] L3 aN-4 (hn70) (9/3), 279, could ovlp other peaks hn9[N38]an-4, ha12[L44a], ha10[L44] NOTES 4D CN same coordinates as N38 ha dispersive in 3D 5 ctrs in 4D go with 3 Val 8a SEQ ; 3020 1 3051 5 parsed_1b4c 1 172 "{s?, 8.3, 7, 0} strong b/c signal split by 2 resonances" 3054 1 3054 64 parsed_1b4c 1 173 ; {w, 2.54, 2, 1.0} R assign (segid="sbm1" and resid 9 and name hn) (segid="sbm1" and resid 8 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 9 and name hn) (segid="sbm2" and resid 8 and name hn) 1.8 0 1.1 {s?, 7.74, 6, 0} strong b/c signal split by 2 resonances NOTES 3D NOESY: noesy100- 239 113 33 (nh- 8.50ppm; n= 199.20) hn43 NN-1 (hn8) 8.33, 121, could ovlp NN+2 NN+2 (hn52) 8.29, could ovlp nn-1 aN-3 (hn24) 3.90ppm, ovlps hn40[E67] an-1/an-3, but it's real NOTES 4D CN: V8 is in same cube as E67 Val 8b (nh- 8.34ppm; n= 119.20) hn42, wkr than hn43 NOTES 3D NOESY: noesy100- 253 120 32 NN-1 (hn) 8.33ppm, (),could ovlp hn42 NN+2 (hn65) 8.4ppm, (), could ovlp hn42 Ala 9 SEQ ; 3058 1 3081 5 parsed_1b4c 1 174 "{s?, 8.53, 8, 0}" 3084 1 3084 25 parsed_1b4c 1 175 "{w, 3.52, 4, 0}" 3088 1 3088 24 parsed_1b4c 1 176 "{s, 2.24, 10, 0}" 3092 1 3092 25 parsed_1b4c 1 177 "{w, 1.21, 5, 2.9}" 3096 1 3096 26 parsed_1b4c 1 178 ; {m/w, 0.96, 7, 2.9} R assign (segid="sbm1" and resid 10 and name hn) (segid="sbm1" and resid 9 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 10 and name hn) (segid="sbm2" and resid 9 and name hn) 1.8 0 1.1 {s, 8.31, 11, 0} SD? assign (segid="sbm1" and resid 10 and name ha) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 10 and name ha) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 4.12, 5*, 0, amb} amb assign (segid="sbm1" and resid 10 and name hb*) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 10 and name hb*) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 2.49, 2, 0, amb} NOTES 3D NOESY: noesy100- 307 143 27 (nh- 7.71ppm; n= 122.98) hn81 V8a or b NN-1 (hn43) 114, could ovlp nn+2 L10 or b NN (hn52) 8.31ppm,, 122, could ovlp nn-2 M7 NN-2 (hn8) 8.33ppm, could ovlp nn I11 NN+2 (hn65) 8.4ppm, could ovlp nn-1 Leu 10a SEQ ; 3100 1 3127 5 parsed_1b4c 1 179 "{s?, 7.74, 9, 0}" 3130 1 3130 25 parsed_1b4c 1 180 "{w, 4.28, 9*, 0, amb}" 3134 1 3134 30 parsed_1b4c 1 181 "{s, 1.65, 13, 1.5} some contribution may be from A6hb* as intermolecular" 3138 1 3138 81 parsed_1b4c 1 182 ; {s, 8.47, 10, 0, amb} SD? assign (segid="sbm1" and resid 11 and name ha) (segid="sbm1" and resid 10 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 11 and name ha) (segid="sbm2" and resid 10 and name hn) 1.8 0 4.2 {vw, 3.39, 3*, 0, amb} amb assign (segid="sbm1" and resid 11 and name hg2/d*) (segid="sbm1" and resid 10 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 11 and name hg2/d*) (segid="sbm2" and resid 10 and name hn) 1.8 0 4.2 {vw, 0.10-2, 4*, 1.5} NOTES 3D NOESY: noesy100- 257 122 32 Leu 10a (nh- 8.29ppm; n= 119.76) hn52; strgr of the pair in the HSQC Leu 10b (nh- 8.26ppm; n= 119.60) hn48 Ile 11a SEQ R assign (segid="sbm1" and resid 10 and name hn) (segid="sbm1" and resid 11 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 10 and name hn) (segid="sbm2" and resid 11 and name hn) 1.8 0 3.2 {w, 8.2, 3, ?} ; 3142 1 3164 23 parsed_1b4c 1 183 ; {mw, 4.12, 6?, 0, amb} amb assign (segid="sbm1" and resid 10 and name hb*) (segid="sbm1" and resid 11 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 10 and name hb*) (segid="sbm2" and resid 11 and name hn) 1.8 0 3.2 {w, 2.46, 3, 1} off in CS R assign (segid="sbm1" and resid 12 and name hn) (segid="sbm1" and resid 11 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 12 and name hn) (segid="sbm2" and resid 11 and name hn) 1.8 0 3.2 {w, 8.1, 3, ?} NOTES 3D NOESY: noesy100- 246 117 29 Ile 11a (nh- 8.44ppm; n= 121.21) hn65 close to hn67 (V13), but wkr than hn67 Ile 11b (nh- 8.39ppm; n= 121.21) hn65a, wkr than hn65 NN (hn) 8.1ppm, (), could be ovlpd NN-1 (hn) 8.2ppm, (), could be ovlpd NOTES 4D CN: too weak Asp 12 SEQ ; 3168 1 3191 5 parsed_1b4c 1 184 "{s?, 8.42, 9?, 0, amb}" 3194 1 3194 31 parsed_1b4c 1 185 "{w, 3.39, 5*, 0, amb}" 3198 1 3198 30 parsed_1b4c 1 186 ; {s, 1.67, 10, 0} assign (segid="sbm1" and resid 11 and name hg2*) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 11 and name hg2*) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 0.15, 8*, 1.5, amb} R assign (segid="sbm1" and resid 13 and name hn) (segid="sbm1" and resid 12 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 13 and name hn) (segid="sbm2" and resid 12 and name hn) 1.8 0 1.1 {s?, 8.42, 9?, 0} SD? assign (segid="sbm1" and resid 13 and name ha) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 13 and name ha) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 3.39, 5*, 0, amb 16ha} assign (segid="sbm1" and resid 13 and name hg*) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 13 and name hg*) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 1.21, 2, 2.9} NOTES 3D NOESY: noesy100- 269 127 30 Illhb could also be K26hb* (nh- 8.15ppm; n= 120.73) hn64; in NOESY seems to have vw mult peak Val 13 SEQ ; 3202 1 3229 5 parsed_1b4c 1 187 "{s?, 8.17, 8, 0}" 3232 1 3232 25 parsed_1b4c 1 188 "{w, 4.28, 6*, 0, amb}" 3236 1 3236 30 parsed_1b4c 1 189 ; {m, 2.90, 8, 1.0} RS assign (segid="sbm1" and resid 12 and name hb*) (segid="sbm1" and resid 13 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 12 and name hb*) (segid="sbm2" and resid 13 and name hn) 1.8 0 1.7 {m, 2.81, 8, 1.0} assign (segid="sbm1" and resid 12 and name hb*) (segid="sbm1" and resid 13 and name hg2*) 1.8 0 2.4 assign (segid="sbm2" and resid 12 and name hb*) (segid="sbm2" and resid 13 and name hg2*) 1.8 0 2.4 {mw, 2.81-90, 6, 2.5} {DJW removed} ; 3240 1 3248 44 parsed_1b4c 1 190 ; {s?, 8.4, ?, 0} SD? assign (segid="sbm1" and resid 14 and name ha) (segid="sbm1" and resid 13 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 14 and name ha) (segid="sbm2" and resid 13 and name hn) 1.8 0 4.2 {vw, 3.52, 1, 0, amb} assign (segid="sbm1" and resid 14 and name ha) (segid="sbm1" and resid 13 and name hg1*) 1.8 0 3.2 assign (segid="sbm2" and resid 14 and name ha) (segid="sbm2" and resid 13 and name hg1*) 1.8 0 3.2 {w, 3.52, 3, 1.5} {DJW removed} NOTES 3D NOESY (nh- 8.41ppm) hn67 noesy100- 248 118 29 F14 NN (hn50) 8.4ppm, could ovlp w/hn[67]- assumed f14hn-acd I11 NN-2 (hn65) 8.4ppm, could ovlp w/hn[67] NOTES HNH (clvl=0.1): 119.68 (7) F14 and 120.73 D12 Phe 14a Phe 14b SEQ R assign (segid="sbm1" and resid 13 and name hn) (segid="sbm1" and resid 14 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 13 and name hn) (segid="sbm2" and resid 14 and name hn) 1.8 0 1.1 {s, 8.4, ? ovlps 14hn, 0} ; 3252 1 3278 34 parsed_1b4c 1 191 "{mw, 3.86, 5, 0, ncn}" 3282 1 3282 30 parsed_1b4c 1 192 "{s, 2.30, 10, 0}" 3286 1 3286 25 parsed_1b4c 1 193 "{m, 1.21, 9, 1.5, ncn}" 3290 1 3290 31 parsed_1b4c 1 194 ; {w, 8.72, 4, 0} NOTES 3D NOESY: noesy100- ~244 117 31 V13 NN-1 ovlps diag D12 NN-2 (hn64) 8.17ppm very weak but seems to be there NOTES 4D CN an-4 or G66 4.15 in 3D and 4.17 in 4D, 13C goes w/G66 not an-4 sofrom another cube ? Phe 14a (nh- 8.47ppm; n= 119.76) hn50 strgr of the pair Phe 14b (nh- 8.43ppm; n= 119.84) hn51 His 15 SEQ R assign (segid="sbm1" and resid 14 and name hn) (segid="sbm1" and resid 15 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 14 and name hn) (segid="sbm2" and resid 15 and name hn) 1.8 0 4.2 {vw, 8.44, 7*, 0} ; 3294 1 3312 26 parsed_1b4c 1 195 "{vw, 3.49, 5*, 0}" 3316 1 3316 27 parsed_1b4c 1 196 ; {vw, 2.68, 7*, 1.0} assign (segid="sbm1" and resid 14 and name hd*) (segid="sbm1" and resid 15 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 14 and name hd*) (segid="sbm2" and resid 15 and name hn) 1.8 0 4.2 {vw, 6.24, 7*, 2.4} DJW removed} amb assign (segid="sbm1" and resid 14 and name he*) (segid="sbm1" and resid 15 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 14 and name he*) (segid="sbm2" and resid 15 and name hn) 1.8 0 4.2 {vw, 7.11, 3*, 2.4}, could be F73he*, 16he21, 73hz, 70hz R assign (segid="sbm1" and resid 16 and name hn) (segid="sbm1" and resid 15 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 16 and name hn) (segid="sbm2" and resid 15 and name hn) 1.8 0 1.7 {m?, 8.33, 3, 0} med-stg relative to diagonal NOTES 3D NOESY: noesy100- 219 106 35 bN-1 (hn50) 3.14ppm, (4/2), ovlps beta2 NN-2 (hn67) 8.4ppm, could ovlp NN-1 (nh- 8.74ppm; n= 117.42) hn109 - VERY WEAK SIGNAL FOR 3D AND 4D Gln 16 SEQ ; 3320 1 3344 5 parsed_1b4c 1 197 "{m?, 8.74, 5, 0}" 3347 1 3347 26 parsed_1b4c 1 198 "{w, 5.15, 3, 0}" 3351 1 3351 24 parsed_1b4c 1 199 ; {vw, 3.22, 9*, 1.0} RS assign (segid="sbm1" and resid 15 and name hb*) (segid="sbm1" and resid 16 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 15 and name hb*) (segid="sbm2" and resid 16 and name hn) 1.8 0 4.2 {vw, 3.09, 9*, 1.0} R assign (segid="sbm1" and resid 17 and name hn) (segid="sbm1" and resid 16 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 17 and name hn) (segid="sbm2" and resid 16 and name hn) 1.8 0 1.1 {s, 7.38, 10, 0} assign (segid="sbm1" and resid 17 and name hb*) (segid="sbm1" and resid 16 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 17 and name hb*) (segid="sbm2" and resid 16 and name hn) 1.8 0 3.2 {w, 2.65, 4, 1.0, amb} {DJW removed} NOTES 3D NOESY: noesy100- 255 120 27 F14 NN-2 (hn50) 8.4ppm, (),could ovlp diag (nh- 8.32ppm; n= 122.25) hn75; close in 15n/1H to hn74(E72) Tyr 17 SEQ ; 3355 1 3378 5 parsed_1b4c 1 200 "{s, 8.33, 11, 0}" 3381 1 3381 25 parsed_1b4c 1 201 "{mw?, 3.82, 7&1 ovlp w/13ha?, 0, ncn}" 3385 1 3385 47 parsed_1b4c 1 202 ; {m, 2.38, 10&1, 1.0} RS assign (segid="sbm1" and resid 16 and name hb*) (segid="sbm1" and resid 17 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 16 and name hb*) (segid="sbm2" and resid 17 and name hn) 1.8 0 1.7 {m?, 2.19, 10ovlp/4, 1.0} ; 3389 1 3393 34 parsed_1b4c 1 203 "{w, 2.20, 4, 3.4}" 3397 1 3397 26 parsed_1b4c 1 204 ; {w, 2.19, 10ovlp/5, 1.0} R assign (segid="sbm1" and resid 18 and name hn) (segid="sbm1" and resid 17 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 18 and name hn) (segid="sbm2" and resid 17 and name hn) 1.8 0 1.7 {m, 9.67, 8, 0} ; 3401 1 3405 24 parsed_1b4c 1 205 ; {vw, 4.01, 7*, 0, amb} assign (segid="sbm1" and resid 18 and name hb*) (segid="sbm1" and resid 17 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 18 and name hb*) (segid="sbm2" and resid 17 and name hn) 1.8 0 4.2 {vw, 3.49, 2ov?, 1.0, amb} {DJW removed} NOTES 3D NOESY (nh- 7.37ppm; n= 115.73) hn14 noesy100- 336 156 38 aN-2 (hn109) 5.15ppm, other signals are present in 4D CN at 5.1 that aren't H15 NOTES 4D CN aN-1 (hn75) 3.82ppm is only 1 contour not all Y17 peaks optimize at one 15N value Q16hg2 could alos be M79hb1 Ser 18 SEQ ; 3409 1 3428 5 parsed_1b4c 1 206 "{s, 7.38, 1, 0} strong relative to other peaks" 3431 1 3431 55 parsed_1b4c 1 207 "{w, 4.15, 2*, 0}" 3435 1 3435 25 parsed_1b4c 1 208 ; {w, 2.65, 8*, 1} R assign (segid="sbm1" and resid 19 and name hn) (segid="sbm1" and resid 18 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 19 and name hn) (segid="sbm2" and resid 18 and name hn) 1.8 0 3.2 {w, 8.06, 3*, 0} NOTES 3D NOESY: noesy100- 140 72 29 (nh- 9.64ppm; n= 121.37) hn112 vwk peak, may be multiple seems to have mult peaks in NOESY 9.66, 9.63, 9.60 aN-4 (hn50) 3.49ppm, could ovlp beta NOTES 4D CN - too weak Gly 19 SEQ assign (segid="sbm1" and resid 18 and name hn) (segid="sbm1" and resid 19 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 18 and name hn) (segid="sbm2" and resid 19 and name hn) 1.8 0 3.2 {w, 9.67, 1}{DJW removed for now} amb assign (segid="sbm1" and resid 18 and name ha) (segid="sbm1" and resid 19 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid 18 and name ha) (segid="sbm2" and resid 19 and name hn) 1.8 0 ? {?, 3.9, ? ovlp 19ha1} assign (segid="sbm1" and resid 18 and name hb*) (segid="sbm1" and resid 19 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 18 and name hb*) (segid="sbm2" and resid 19 and name hn) 1.8 0 3.2 {w, 3.47, 4*}{DJW removed for now} R assign (segid="sbm1" and resid 20 and name hn) (segid="sbm1" and resid 19 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 20 and name hn) (segid="sbm2" and resid 19 and name hn) 1.8 0 3.2 {w, 7.17, 3, 0} assign (segid="sbm1" and resid 20 and name hb*) (segid="sbm1" and resid 19 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 20 and name hb*) (segid="sbm2" and resid 19 and name hn) 1.8 0 4.2 {vw, 1.84, 5*, 1.0, amb} NOTES 3D NOESY: noesy100- 280 132 51 S18 aN-1 (hn112) 3.9ppm, could ovlp alpha1 (nh- 8.02ppm; n= 107.28) hn1, may be multiple Arg 20 SEQ ; 3439 1 3487 5 parsed_1b4c 1 209 ; {w, 8.04, 3} amb/R assign (segid="sbm1" and resid 19 and name ha*) (segid="sbm1" and resid 20 and name hn) 1.8 0 3.2 amb/R assign (segid="sbm2" and resid 19 and name ha*) (segid="sbm2" and resid 20 and name hn) 1.8 0 3.2 {w?, 3.96, 10ovlp? 20ha?, amb} assign (segid="sbm1" and resid 19 and name ha*) (segid="sbm1" and resid 20 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 19 and name ha*) (segid="sbm2" and resid 20 and name hn) 1.8 0 3.2 {w, 3.71, 3, amb}{DJW removed for now} R assign (segid="sbm1" and resid 21 and name hn) (segid="sbm1" and resid 20 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 21 and name hn) (segid="sbm2" and resid 20 and name hn) 1.8 0 3.2 {w, 7.79, 6} NOTES 3D NOESY: noesy100- 353 163 33 (nh- 7.17ppm; n= 118.63) hn38 Glu 21 SEQ ; 3490 1 3512 5 parsed_1b4c 1 210 "{s?, 7.19, 9} 37hd21 7.18-37hn contributing ?" 3515 1 3515 54 parsed_1b4c 1 211 "{m, 3.96, 8/6, cn 4.04/58.9}, L3,L10,E34,E51,E58,E72,F88 also listed for 4D CS" 3519 1 3519 87 parsed_1b4c 1 212 ; {w, 1.86, 12ov&6, ncn} amb assign (segid="sbm1" and resid 22 and name hn) (segid="sbm1" and resid 21 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid 22 and name hn) (segid="sbm2" and resid 21 and name hn) 1.8 0 ? {?, 8.33, 11, amb} could be 38hn 8.32 to 37hn NOTES 3D NOESY: noesy100- ~302 142/143 38 G22 NN (hn3) 8.3ppm, could ovlp N37 nn (nh- 7.77ppm; n= 115.81) (hn15) - close N37 (hn13) in 1H and 15N Gly 22 SEQ ; 3523 1 3538 5 parsed_1b4c 1 213 "{vw, 7.79, 9*}" 3541 1 3541 23 parsed_1b4c 1 214 "{s, 1.91, 10/9}, {m, 2.08, 8/7}{DJW moved down to weak for test}" 3545 1 3545 73 parsed_1b4c 1 215 ; {m, 2.19, 9/~9, cn}{moveed to wak for test} DJW} R assign (segid="sbm1" and resid 23 and name hn) (segid="sbm1" and resid 22 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 23 and name hn) (segid="sbm2" and resid 22 and name hn) 1.8 0 4.2 {vw, 8.63, 8*, 0} amb/art assign (segid="sbm1" and resid 23 and name ha) (segid="sbm1" and resid 22 and name hn) 1.8 0 1.1 amb/art assign (segid="sbm2" and resid 23 and name ha) (segid="sbm2" and resid 22 and name hn) 1.8 0 1.1 {s, 4.48, 3*/>15, 0, cn}, no clear peak in 3d, only 4d NOTES 3D NOESY: noesy100- 252 120 48 NOTES 4D CN (nh- 8.35ppm; n= 109.13) hn3 E21hb1 could also be K55hb1,E91hb1,K5hb*,M57hb2 E21hb2 could also be K55hb2,E91hb2,V52hb,V53hb,V80hb E21hg* could also be E46hg*,E49hg2 Asp 23 SEQ ; 3549 1 3571 5 parsed_1b4c 1 216 "{vw, 8.39, 4*}" 3574 1 3574 23 parsed_1b4c 1 217 ; {s?, 3.88, 11&4} RS assign (segid="sbm1" and resid 22 and name ha*) (segid="sbm1" and resid 23 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 22 and name ha*) (segid="sbm2" and resid 23 and name hn) 1.8 0 1.7 {m, 3.68, 9/0?, amb}, G22ha2 makes sense in 3d; 4D sees wk G19ha2 but looks too far amb assign (segid="sbm1" and resid 24 and name hn) (segid="sbm1" and resid 23 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid 24 and name hn) (segid="sbm2" and resid 23 and name hn) 1.8 0 ? {w?, 8.57, 10, ovlp 23hn} NOTES 3D NOESY (nh- 8.61ppm; n= 125.47) hn86 noesy100- 229 110 23 NN (hn) 8.57ppm, could ovlp hn86 NOTES 4D CN: Close to O1 in D1, so signal not so good Lys 24 SEQ amb assign (segid="sbm1" and resid 23 and name hn) (segid="sbm1" and resid 24 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 23 and name hn) (segid="sbm2" and resid 24 and name hn) 1.8 0 1.7 {m, 8.6, ?} ; 3578 1 3602 20 parsed_1b4c 1 218 "{w, 4.48, 5*}" 3606 1 3606 22 parsed_1b4c 1 219 ; {w, 2.7, 3} RS assign (segid="sbm1" and resid 23 and name hb*) (segid="sbm1" and resid 24 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 23 and name hb*) (segid="sbm2" and resid 24 and name hn) 1.8 0 3.2 {w, 2.6, 4} R assign (segid="sbm1" and resid 25 and name hn) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 25 and name hn) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 9.17, 1} amb assign (segid="sbm1" and resid 25 and name ha) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 25 and name ha) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 4.91, 4*, amb} NOTES 3D NOESY: noesy100- 232 111 22 NN-1 (hn86) 8.6ppm,could ovlp hn106 beta-N-1 (hn86) ovlps hn86 (D23) from 15N plane one up NOTES 4D CN: ha only sidechain atom of K24 present His 25 SEQ ; 3610 1 3634 5 parsed_1b4c 1 220 "{vw, 8.57, 7*}" 3637 1 3637 23 parsed_1b4c 1 221 "{vw, 4.26, 2}, could also be D12 ,E45,D54; 4ctrs in 4D 1 in 3D go with 24" 3641 1 3641 82 parsed_1b4c 1 222 ; {w, 1.70, 3, 1} SD assign (segid="sbm1" and resid 24 and name hg*) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 SD assign (segid="sbm2" and resid 24 and name hg*) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 1.13, 1, 1} ; 3645 1 3649 25 parsed_1b4c 1 223 ; {s, 7.71, 9} stg relative to other peaks and diagonal amb assign (segid="sbm1" and resid 26 and name hg*) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 26 and name hg*) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 1.26, ~12*, 1.0, amb} amb assign (segid="sbm1" and resid 26 and name hg*/d*) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 26 and name hg*/d*) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 1.51, 1, 1/0, amb} AMB art? assign (segid="sbm1" and resid 14 and name ha) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 14 and name ha) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 3.52, 3*, 0, amb} amb assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 5.34, 7*, 0} , D69ha sees wk pk @ 9.10, K26ha sees vw pk @ 9.19 - ?? NOTES 3D NOESY: noesy100- 184 90 35 (nh- 9.14ppm; n= 117.50) hn25 close to hn21 (E51) in 1H and 15N K26 (NN) 7.71ppm, could ovlp E21(n-2) from next 15N plane, so use 6 ctrs vs. 9 8.57/7.11 are dispersive so intensity may be reduced 6.78/7.11 correspond to Q16 he22 and he21, both are present in 200 ms NOESY NOTES 4D CN: ha 7 ctrs in 4D 1 in 3D go with 4 ctrs Lys 26 SEQ R assign (segid="sbm1" and resid 25 and name hn) (segid="sbm1" and resid 26 and name hn) 1.8 0 1.5 R assign (segid="sbm2" and resid 25 and name hn) (segid="sbm2" and resid 26 and name hn) 1.8 0 1.5 {m, 9.17, 9, 0} ; 3653 1 3688 24 parsed_1b4c 1 224 ; {vw, 4.91, 2, 0} RS assign (segid="sbm1" and resid 25 and name hb*) (segid="sbm1" and resid 26 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 25 and name hb*) (segid="sbm2" and resid 26 and name hn) 1.8 0 4.2 {vw, 3.66, 8*, 1.0} ; 3692 1 3696 28 parsed_1b4c 1 225 ; {w, 3.25, 3, 1.0} R assign (segid="sbm1" and resid 27 and name hn) (segid="sbm1" and resid 26 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 27 and name hn) (segid="sbm2" and resid 26 and name hn) 1.8 0 4.2 {vw, 8.69, 8*, 0} assign (segid="sbm1" and resid 27 and name hd*) (segid="sbm1" and resid 26 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 27 and name hd*) (segid="sbm2" and resid 26 and name hn) 1.8 0 4.2 {vw, 0.61-4, 5*, 2.9} {DJW removed} NOTES 3D: noesy100- 309 144 35 H25 (NN-1) 9.17ppm, (9), 90, could also be F70; F70 has 7.11/7.30 NOTES 4D CN hb could also ovlp I11hb,Ihb hd 5 at H=596, 3 at H=595, split difference and use 4 contours hg1 could ovlp K5,K28,K55 hg2 could ovlp K33,K48 hd* could ovlp K48hd* NOTES 13C NOESY: 23hb1-26ha could also be 69hb2 (commented out above), but probably to 23hb1 33ha-26hb* could also be from s18b* or v8(ab)ha; viol!- now think above is 33ha-36hb, 36hb & K26hb* overlap 23hb1-26hg2 could also be intra to 26he2, which may be at 2.72(42.07) Leu 27 SEQ ; 3700 1 3728 5 parsed_1b4c 1 226 "{vw, 7.71, 7*, 0}" 3731 1 3731 26 parsed_1b4c 1 227 ; {s?, 5.37, ~17 ovlp?, 0, amb} D69ha@5.34/51.6, K26ha@5.37/54.3, 26ha sees w @8.62, 69ha sees vw @8.77 ; 3735 1 3736 81 parsed_1b4c 1 228 ; {s?, 1.73, ~13, 1.0}, maybe 28hb2 or 28hd*, 28hd* sees wk pk @8.67 so assign 28hd* below amb assign (segid="sbm1" and resid 26 and name hg*) (segid="sbm1" and resid 27 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 26 and name hg*) (segid="sbm2" and resid 27 and name hn) 1.8 0 3.2 {w?, 1.26, 9 ov 27hb2?, 1.0, amb} amb assign (segid="sbm1" and resid 26 and name hg*) (segid="sbm1" and resid 27 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 26 and name hg*) (segid="sbm2" and resid 27 and name hn) 1.8 0 3.2 {w?, 1.51, 12 ovlp 27hb1/g ?, 1.0, amb} amb assign (segid="sbm1" and resid 26 and name hd*) (segid="sbm1" and resid 27 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 26 and name hd*) (segid="sbm2" and resid 27 and name hn) 1.8 0 3.2 {w?, 1.51, 12 ovlp 27hb1/g ? , 1.0, amb} R assign (segid="sbm1" and resid 28 and name hn) (segid="sbm1" and resid 27 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 28 and name hn) (segid="sbm2" and resid 27 and name hn) 1.8 0 4.2 {vw, 9.23, 9*, 0} amb assign (segid="sbm1" and resid 28 and name hb*) (segid="sbm1" and resid 27 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 28 and name hb*) (segid="sbm2" and resid 27 and name hn) 1.8 0 4.2 {vw, 2.33, 7*ov, 1.0} amb assign (segid="sbm1" and resid 28 and name hd*) (segid="sbm1" and resid 27 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 28 and name hd*) (segid="sbm2" and resid 27 and name hn) 1.8 0 3.2 {w?, 1.73, ~13 ovlp 26hb* ?, 1} NOTES 3D NOESY: noesy100- 223 107 31 ha missing in 3D; very weak in 200ms NOTES 4D NOESY: too weak, in solvent ridge Lys 28 SEQ ; 3740 1 3775 5 parsed_1b4c 1 229 ; {vw, 8.71, 7*, 0} amb assign (segid="sbm1" and resid 27 and name hn) (segid="sbm1" and resid 28 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 27 and name hn) (segid="sbm2" and resid 28 and name hd*) 1.8 0 4.2 {vw, 8.67, 2, 1.0} ; 3778 1 3782 27 parsed_1b4c 1 230 ; {s?, 4.80, >10, 0, 4d15n} assign (segid="sbm1" and resid 27 and name hb*) (segid="sbm1" and resid 28 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 27 and name hb*) (segid="sbm2" and resid 28 and name hn) 1.8 0 4.2 {vw, 1.26, 4ov, 1.0, amb} ; 3786 1 3790 34 parsed_1b4c 1 231 "{m, 0.64, 8, 3.4}" 3794 1 3794 26 parsed_1b4c 1 232 ; {vw, 9.15, 7*, 0} amb assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 28 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 28 and name hn) 1.8 0 3.2 {w?, 1.54, 9 ov 28hg*?, 1.0} dont think so NOTES 3D NOESY: noesy100- 179 88 24 NN (hn89) 9.15ppm, vw(7), 91, nearly ovlps hn85 NOTES 4D CN: L27 an >10 in 4D vw in 3D go with 5 ctrs Lys 29 SEQ R assign (segid="sbm1" and resid 28 and name hn) (segid="sbm1" and resid 29 and name hn) 1.8 0 ? R assign (segid="sbm2" and resid 28 and name hn) (segid="sbm2" and resid 29 and name hn) 1.8 0 ? {w?, 9.1, ? ovlps own hn, 0} ; 3798 1 3815 41 parsed_1b4c 1 233 ; {s, 4.85, 10/>>10, 0, ncn} SD? assign (segid="sbm1" and resid 28 and name he*) (segid="sbm1" and resid 29 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 28 and name he*) (segid="sbm2" and resid 29 and name hn) 1.8 0 4.2 {vw, 3.03, 3*, 1.0, amb} R assign (segid="sbm1" and resid 30 and name hn) (segid="sbm1" and resid 29 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 30 and name hn) (segid="sbm2" and resid 29 and name hn) 1.8 0 1.7 {m, 9.37, 7, 0} SD? assign (segid="sbm1" and resid 30 and name ha) (segid="sbm1" and resid 29 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 30 and name ha) (segid="sbm2" and resid 29 and name hn) 1.8 0 4.2 {vw, 4.17, 5*ov, 0, amb} NOTES 3D NOESY: noesy100- 188 92 21 NN-1 (hn) ppm, (), ovlps hn89 NOTES 4D CN: ha NOEs fairly strong, the rest are weak NOTES 13C: K29ha close to S41(e)hb at 3.79(61.90) so could have some ambiguity Ser 30 SEQ ; 3819 1 3843 5 parsed_1b4c 1 234 "{m, 9.10, 8, 0}" 3846 1 3846 24 parsed_1b4c 1 235 ; {m?, 2.33, >10/0, 1} 29hb1 at 2.33 amb assign (segid="sbm1" and resid 29 and name hg*) (segid="sbm1" and resid 30 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 29 and name hg*) (segid="sbm2" and resid 30 and name hn) 1.8 0 1.7 {m?, 1.75, ~10, 1, amb} assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 30 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 30 and name hn) 1.8 0 3.2 {w, 1.53, 5, 1.0} {DJW removed} RS assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 30 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 30 and name hn) 1.8 0 4.2 {vw, 1.08, 7*, 1.0} SD? assign (segid="sbm1" and resid 29 and name he*) (segid="sbm1" and resid 30 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 29 and name he*) (segid="sbm2" and resid 30 and name hn) 1.8 0 4.2 {vw, 2.81, 4*, 1} ; 3850 1 3866 26 parsed_1b4c 1 236 "{s, 7.00, 10, 0}" 3870 1 3870 25 parsed_1b4c 1 237 ; {vw, 2.52, 6*, 1.0, amb} NOTES 3D NOESY: noesy100- 166 83 40 NOTES 4D CN: none of the NOEs to K29 are in the 4D Glu 31 SEQ R assign (segid="sbm1" and resid 30 and name hn) (segid="sbm1" and resid 31 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 30 and name hn) (segid="sbm2" and resid 31 and name hn) 1.8 0 1.1 {s?, 9.36, 9, 0} ; 3874 1 3887 25 parsed_1b4c 1 238 "{mw, 4.17, 5, 0}" 3891 1 3891 25 parsed_1b4c 1 239 ; {mw, 3.88, 6, 1} R assign (segid="sbm1" and resid 32 and name hn) (segid="sbm1" and resid 31 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 32 and name hn) (segid="sbm2" and resid 31 and name hn) 1.8 0 1.1 {s, 8.42, >10, 0} amb/SD? assign (segid="sbm1" and resid 32 and name ha) (segid="sbm1" and resid 31 and name hn) 1.8 0 4.2 amb/SD? assign (segid="sbm2" and resid 32 and name ha) (segid="sbm2" and resid 31 and name hn) 1.8 0 4.2 {vw, 4.01, 2, 0, amb}, S18ha and L32ha at 4.01 - 18ha looks too far G19ha1 at 3.98 but it sees 7.01 and only 31hn makes sense to 19ha1 amb assign (segid="sbm1" and resid 32 and name hb*) (segid="sbm1" and resid 31 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 32 and name hb*) (segid="sbm2" and resid 31 and name hn) 1.8 0 3.2 {w, 1.35, 3, 1.0, amb} NOTES 3D NOESY: noesy100- 368 170 25 Leu 32 SEQ ; 3895 1 3917 5 parsed_1b4c 1 240 "{s, 7.00, >10, 0}" 3920 1 3920 26 parsed_1b4c 1 241 ; {m, 2.52, 8/5, 1.0} RS assign (segid="sbm1" and resid 31 and name hb*) (segid="sbm1" and resid 32 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 31 and name hb*) (segid="sbm2" and resid 32 and name hn) 1.8 0 3.2 {w?, 2.05, 6&0, 1.0} ; 3924 1 3928 29 parsed_1b4c 1 242 ; {w, 2.35, 5, 1.0, ncn} art? assign (segid="sbm1" and resid 31 and name hb*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 31 and name hb*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 4.2 {vw, 2.5, 3, 3.9} R assign (segid="sbm1" and resid 33 and name hn) (segid="sbm1" and resid 32 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 33 and name hn) (segid="sbm2" and resid 32 and name hn) 1.8 0 1.1 {s, 8.06, 10, 0} SD? assign (segid="sbm1" and resid 33 and name ha) (segid="sbm1" and resid 32 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 33 and name ha) (segid="sbm2" and resid 32 and name hn) 1.8 0 4.2 {vw, 3.49, 7*, 0, amb} SD? assign (segid="sbm1" and resid 33 and name hb*) (segid="sbm1" and resid 32 and name hn) 1.8 0 3.2 SD? assign (segid="sbm2" and resid 33 and name hb*) (segid="sbm2" and resid 32 and name hn) 1.8 0 3.2 {w, 1.65, 3, 1.0, ncn} amb/art? assign (segid="sbm1" and resid 33 and name hg*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 33 and name hg*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 4.2 {vw, 1.42, 3, 3.9} amb/art? assign (segid="sbm1" and resid 33 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 amb/art? assign (segid="sbm2" and resid 33 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {w, 2.20, 4, 3.9} NOTES 3D NOESY: noesy100- 249 118 27 Lys 33 SEQ ; 3932 1 3965 5 parsed_1b4c 1 243 "{s?, 8.42, 10, 0}" 3968 1 3968 27 parsed_1b4c 1 244 "{mw, 4.01, 6ov, 0}" 3972 1 3972 28 parsed_1b4c 1 245 ; {s, 2.19, 11/5, 1.0, ncn} amb/RS assign (segid="sbm1" and resid 32 and name hb*) (segid="sbm1" and resid 33 and name hn) 1.8 0 3.2 amb/RS assign (segid="sbm2" and resid 32 and name hb*) (segid="sbm2" and resid 33 and name hn) 1.8 0 3.2 {w?, 1.35 ov, 6, 1.0, n} amb assign (segid="sbm1" and resid 32 and name hg) (segid="sbm1" and resid 33 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 32 and name hg) (segid="sbm2" and resid 33 and name hn) 1.8 0 1.7 {m?, 1.51, 8/?, 0, n, amb} nothing else looks close enough ; 3976 1 3984 67 parsed_1b4c 1 246 ; {w, 0.94, 5, 2.9, ncn} R assign (segid="sbm1" and resid 34 and name hn) (segid="sbm1" and resid 33 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 34 and name hn) (segid="sbm2" and resid 33 and name hn) 1.8 0 1.1 {s, 6.92, 11, 0} amb assign (segid="sbm1" and resid 34 and name ha) (segid="sbm1" and resid 33 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 34 and name ha) (segid="sbm2" and resid 33 and name hn) 1.8 0 4.2 {vw, 4.04, 6ov, 0, amb} NOTES 3D NOESY: noesy100- 278 131 31 NN-2 (hn84) 7.0ppm, (), could ovlp NN Glu 34 SEQ ; 3988 1 4006 5 parsed_1b4c 1 247 "{s, 8.06, >10, 0}" 4009 1 4009 29 parsed_1b4c 1 248 "{mw, 3.49, 6, 0}" 4013 1 4013 25 parsed_1b4c 1 249 ; {s, 1.97, >10&8, 1.0} RS assign (segid="sbm1" and resid 33 and name hb*) (segid="sbm1" and resid 34 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 33 and name hb*) (segid="sbm2" and resid 34 and name hn) 1.8 0 1.7 {m, 1.65, ~10&5, 1.0} assign (segid="sbm1" and resid 33 and name hg*) (segid="sbm1" and resid 34 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 33 and name hg*) (segid="sbm2" and resid 34 and name hn) 1.8 0 3.2 {w, 1.24, 5, 1.0, n, amb} could be 13hg1*/hg2* or 32hd1* but both look too far {DJW removed} SD? assign (segid="sbm1" and resid 33 and name hg*) (segid="sbm1" and resid 34 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 33 and name hg*) (segid="sbm2" and resid 34 and name hn) 1.8 0 4.2 {vw, 1.46, 1, 1.0, n, amb} SD? assign (segid="sbm1" and resid 33 and name he*) (segid="sbm1" and resid 34 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 33 and name he*) (segid="sbm2" and resid 34 and name hn) 1.8 0 4.2 {vw, 2.87, 6*, 1.0, amb} R assign (segid="sbm1" and resid 35 and name hn) (segid="sbm1" and resid 34 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 35 and name hn) (segid="sbm2" and resid 34 and name hn) 1.8 0 1.1 {s, 8.17, 10, 0} assign (segid="sbm1" and resid 35 and name hb*) (segid="sbm1" and resid 34 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 35 and name hb*) (segid="sbm2" and resid 34 and name hn) 1.8 0 4.2 {vw, 0.94, 2, 1.0, n, amb} 32hd2* also at 0.94 but looks too far NOTES 3D NOESY: noesy100- 375 173 34 Leu 35 SEQ ; 4017 1 4050 5 parsed_1b4c 1 250 "{s, 6.92, >10, 0}" 4053 1 4053 26 parsed_1b4c 1 251 "{mw?, 4.04, 12ov, 0, amb}" 4057 1 4057 34 parsed_1b4c 1 252 ; {m?, 2.33, 13ovlp/~12, 1.0} viol at stg in asbd8 RS assign (segid="sbm1" and resid 34 and name hb*) (segid="sbm1" and resid 35 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 34 and name hb*) (segid="sbm2" and resid 35 and name hn) 1.8 0 1.7 {m?, 2.19, 11/~12, 1.0} viol as stg in asbd8, and as med in asbd9 ; 4061 1 4065 74 parsed_1b4c 1 253 ; {w, 2.46, 3, 1.0, ncn} RS assign (segid="sbm1" and resid 34 and name hg*) (segid="sbm1" and resid 35 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 34 and name hg*) (segid="sbm2" and resid 35 and name hn) 1.8 0 3.2 {w, 2.28, 5, 1.0, ncn} ; 4069 1 4073 31 parsed_1b4c 1 254 ; {s, 8.58, 10, 0} SD? assign (segid="sbm1" and resid 36 and name ha) (segid="sbm1" and resid 35 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 36 and name ha) (segid="sbm2" and resid 35 and name hn) 1.8 0 4.2 {vw, 3.22, 5*, 0, amb} ; 4077 1 4081 31 parsed_1b4c 1 255 ; {d', m, 3.19, 10, 2.9} amb assign (segid="sbm1" and resid 36 and name hb) (segid="sbm1" and resid 35 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 36 and name hb) (segid="sbm2" and resid 35 and name hn) 1.8 0 4.2 {vw, 1.67, >10ov/4, 0, cn} may be in shoulder of 1.67 amb assign (segid="sbm1" and resid 36 and name hg1*) (segid="sbm1" and resid 35 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 36 and name hg1*) (segid="sbm2" and resid 35 and name hn) 1.8 0 3.2 {w?, 0.77, 8, 1.0} other possibilities at 0.77 L3hd2* and V77hg1* - both look too far assign (segid="sbm1" and resid 36 and name hg2*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 3.2 assign (segid="sbm2" and resid 36 and name hg2*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 3.2 {d', w, 0.78, 4, 4.4} {DJW removed} assign (segid="sbm1" and resid 36 and name hd*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 3.2 assign (segid="sbm2" and resid 36 and name hd*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 3.2 {d', w, 0.57, 5, 4.4} {DJW removed} NOTES 3D NOESY: noesy100- 268 127 28 NOTES 4D CN L32ha could also be L44, M57, E91 ha's L35ha could also overlap Q50ha, Q71ha L35bn-1 could overlap E49hb1, E72hb1 Ile 36 SEQ R assign (segid="sbm1" and resid 35 and name hn) (segid="sbm1" and resid 36 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 35 and name hn) (segid="sbm2" and resid 36 and name hn) 1.8 0 1.7 {m, 8.17, 7, 0} ; 4085 1 4118 24 parsed_1b4c 1 256 ; {mw, 3.52, 5?, 0, amb} ovlp pk at 3.52? amb/RS assign (segid="sbm1" and resid 35 and name hb*) (segid="sbm1" and resid 36 and name hn) 1.8 0 1.1 amb/RS assign (segid="sbm2" and resid 35 and name hb*) (segid="sbm2" and resid 36 and name hn) 1.8 0 1.1 {s?, 1.65, >10ov/7?, 1.0, cn} strong shoulder on pk at 1.75 ; 4122 1 4126 68 parsed_1b4c 1 257 ; {m, 0.94, 7/2, 1.0, cn} amb assign (segid="sbm1" and resid 35 and name hg) (segid="sbm1" and resid 36 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid 35 and name hg) (segid="sbm2" and resid 36 and name hn) 1.8 0 ? {?, ~0.78, 1, 0, cn} 36hg12 and 36hg2* also at ~0.78 ; 4130 1 4134 61 parsed_1b4c 1 258 ; {w?, 0.59, 10ov/?, 2.9} 36hd* at 0.59 also R assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 36 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 36 and name hd*) 1.8 0 3.2 {w, 0.57, 6, 4.4} RS assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 36 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 36 and name hn) 1.8 0 3.2 {w, 0.39, 3, 2.9, amb} L60hd1* also at 0.39 R assign (segid="sbm1" and resid 37 and name hn) (segid="sbm1" and resid 36 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 37 and name hn) (segid="sbm2" and resid 36 and name hn) 1.8 0 1.7 {m, 7.82, 7, 0} SD? assign (segid="sbm1" and resid 37 and name ha) (segid="sbm1" and resid 36 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 37 and name ha) (segid="sbm2" and resid 36 and name hn) 1.8 0 4.2 {vw, 4.20, 6*, 0, amb} assign (segid="sbm1" and resid 37 and name ha) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 1.5 assign (segid="sbm2" and resid 37 and name ha) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 1.5 {m, 4.19, 8, 1.5} {DJW removed} NOTES 3D NOESY: noesy100- 235 112 29 NOTES 4D CN: V56hg2 signal doesn't max at H=522 Asn 37 SEQ ; 4138 1 4168 5 parsed_1b4c 1 259 "{s, 8.58, 11, 0}" 4171 1 4171 26 parsed_1b4c 1 260 "{mw, 3.22, 6, 0}" 4175 1 4175 25 parsed_1b4c 1 261 ; {s, 1.78, 13/7, 0} 36hg11 also at ~1.78 amb assign (segid="sbm1" and resid 36 and name hg1*) (segid="sbm1" and resid 37 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 36 and name hg1*) (segid="sbm2" and resid 37 and name hn) 1.8 0 1.7 {m, 1.78, 13/?, 1.0, amb} 36hb also at ~1.78 RS assign (segid="sbm1" and resid 36 and name hg1*) (segid="sbm1" and resid 37 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 36 and name hg1*) (segid="sbm2" and resid 37 and name hn) 1.8 0 3.2 {w?, 0.80, 12/?, 1.0, amb} 36hg12 also at 0.78, viol as med for asbd8 ; 4179 1 4187 78 parsed_1b4c 1 262 "{m, 0.80, 12/7, 1.5, cn} 36hg12 also at 0.78" 4191 1 4191 53 parsed_1b4c 1 263 "{w, 0.58, 5, 1.5, ncn}" 4195 1 4195 31 parsed_1b4c 1 264 ; {s, 8.33, 10, 0} SD? assign (segid="sbm1" and resid 38 and name ha) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 38 and name ha) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 4.69, ~7*, 0, amb} assign (segid="sbm1" and resid 38 and name hb*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 38 and name hb*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 3.03, ~9*, 1.0, ncn} art/SD? assign (segid="sbm1" and resid 38 and name hd2*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 art/SD? assign (segid="sbm2" and resid 38 and name hd2*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 7.57, 6*, 1.0, amb} E89hn also at 7.56 NOTES 3D NOESY: noesy100- 300 141 38 Asn 38 SEQ amb/R assign (segid="sbm1" and resid 37 and name hn) (segid="sbm1" and resid 38 and name hn) 1.8 0 1.1 amb/R assign (segid="sbm2" and resid 37 and name hn) (segid="sbm2" and resid 38 and name hn) 1.8 0 1.1 {s, 7.81, ~11, 0} ; 4199 1 4225 26 parsed_1b4c 1 265 "{mw, 4.20, 5, 0}" 4229 1 4229 26 parsed_1b4c 1 266 ; {s, 2.71, ~14/7?, 1.0, cn} amb assign (segid="sbm1" and resid 37 and name hb*) (segid="sbm1" and resid 38 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 37 and name hb*) (segid="sbm2" and resid 38 and name hn) 1.8 0 1.7 {w?, 2.57, ~12/6?, 1.0, cn} ovlps M7hb (M7hn close to 38hn in CS) R assign (segid="sbm1" and resid 39 and name hn) (segid="sbm1" and resid 38 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 39 and name hn) (segid="sbm2" and resid 38 and name hn) 1.8 0 1.7 {m, 9.18, 9, 0} NOTES 3D NOESY: noesy100- 255 121 39 NOTES 4D CN: N37ha could also be E21ha no good evidence for 35ha-38hb1/2 NOE, but assigned 38hb2-35ha dont see 41hb*-38ha or vice versa, could be b/c 38ha at carrier frequencey Glu 39 SEQ ; 4233 1 4253 5 parsed_1b4c 1 267 ; {s, 8.33, 9} stg relative to other pks amb assign (segid="sbm1" and resid 38 and name ha) (segid="sbm1" and resid 39 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 38 and name ha) (segid="sbm2" and resid 39 and name hn) 1.8 0 4.2 {vw, 3.66, 0*} ; 4256 1 4260 23 parsed_1b4c 1 268 ; {m, 3.03, 6/6, cn} amb assign (segid="sbm1" and resid 38 and name hb*) (segid="sbm1" and resid 39 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 38 and name hb*) (segid="sbm2" and resid 39 and name hn) 1.8 0 3.2 {w, 2.79, 10/5, 1.0, cn} ovlps 39hg1 SD? assign (segid="sbm1" and resid 38 and name hd2*) (segid="sbm1" and resid 39 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 38 and name hd2*) (segid="sbm2" and resid 39 and name hn) 1.8 0 4.2 {vw, 7.57, 2*, 1.0} assign (segid="sbm1" and resid 38 and name hd2*) (segid="sbm1" and resid 39 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 38 and name hd2*) (segid="sbm2" and resid 39 and name hn) 1.8 0 4.2 {vw, 7.06, 9*, 1.0} {DJW removed} R assign (segid="sbm1" and resid 40 and name hn) (segid="sbm1" and resid 39 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 40 and name hn) (segid="sbm2" and resid 39 and name hn) 1.8 0 1.1 {s, 7.82, 10, 0} amb assign (segid="sbm1" and resid 40 and name hg) (segid="sbm1" and resid 39 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 40 and name hg) (segid="sbm2" and resid 39 and name hn) 1.8 0 4.2 {vw, 1.46-8, 3*, 1.0} 3D NOESY: noesy100- 184 90 39 4D CN: hb1? Wk signal at 2.41, 30.32 which could ovlp hg2 in 3D 13C: 39hb*-36ha assigned, dont see 36ha-39hb* Leu 40 SEQ ; 4264 1 4295 5 parsed_1b4c 1 269 "{s, 9.18, 10}" 4298 1 4298 22 parsed_1b4c 1 270 "{vw, 4.86, 3*, ncn}" 4302 1 4302 28 parsed_1b4c 1 271 ; {m, 1.73, 8&3} amb/SD? assign (segid="sbm1" and resid 39 and name hg*) (segid="sbm1" and resid 40 and name hn) 1.8 0 3.2 amb/SD? assign (segid="sbm2" and resid 39 and name hg*) (segid="sbm2" and resid 40 and name hn) 1.8 0 3.2 {w, 2.35, 3, ncn} R assign (segid="sbm1" and resid 41 and name hn) (segid="sbm1" and resid 40 and name hn) 1.8 0 1.5 R assign (segid="sbm2" and resid 41 and name hn) (segid="sbm2" and resid 40 and name hn) 1.8 0 1.5 {m, 6.73, 8} assign (segid="sbm1" and resid 41 and name hb*) (segid="sbm1" and resid 40 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 41 and name hb*) (segid="sbm2" and resid 40 and name hn) 1.8 0 4.2 {vw, 3.85, 1, amb} amb assign (segid="sbm1" and resid 41 and name ha) (segid="sbm1" and resid 40 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 41 and name ha) (segid="sbm2" and resid 40 and name hn) 1.8 0 4.2 {vw, 4.04, 9*, amb}, could be 2ha or 3ha at 4.04 also, but no cfilt for these NOTES 3D NOESY: noesy100- 298 139 33 Dont see 40hb*-37ha or 37ha-40hb* Ser 41d - SEQ ; 4306 1 4331 15 parsed_1b4c 1 272 "{m?, 7.82, 9/7/5} strong relative to other peaks" 4334 1 4334 63 parsed_1b4c 1 273 ; {w, 5.04, 4} M assign (segid="sbm1" and resid 40 and name hb*) (segid="sbm1" and resid 41 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 40 and name hb*) (segid="sbm2" and resid 41 and name hn) 1.8 0 4.2 {vw, 2.08, 9*} assign (segid="sbm1" and resid 40 and name hg) (segid="sbm1" and resid 41 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 40 and name hg) (segid="sbm2" and resid 41 and name hn) 1.8 0 4.2 {vw, 1.48, 5*} amb assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 41 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 41 and name hn) 1.8 0 4.2 {vw, 0.94, 5*, amb} 80hg2* ; 4338 1 4350 35 parsed_1b4c 1 274 ; {vw, 0.71, ~8*, amb} ovlps 3hd2* at 0.75 ? M assign (segid="sbm1" and resid 42 and name hn) (segid="sbm1" and resid 41 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 42 and name hn) (segid="sbm2" and resid 41 and name hn) 1.8 0 4.2 {vw, 9.72, 1} NOTES 3D NOESY: noesy100- 394 181 44 (nh- 6.70ppm; n= 111.79) hn97 mult peak with 98/99 Ser 41e (nh- 6.71ppm; n= 112.27) hn98 NOTES 3D NOESY: noesy100- 393 ~181 43 7.41 is dispersive NOTES 4D CN: overlaps Ser 41d Ser 41f (nh- 6.78ppm; n= 112.75) hn99 NOTES 3D NOESY: noesy100- 387 ~178 43 7.41 is dipsersive NOTES 4D CN: Ser41f missing or too weak His 42d - SEQ R assign (segid="sbm1" and resid 41 and name hn) (segid="sbm1" and resid 42 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 41 and name hn) (segid="sbm2" and resid 42 and name hn) 1.8 0 4.2 {vw, 6.70, 9*} ; 4354 1 4380 24 parsed_1b4c 1 275 "{vw, 4.04, 5*}" 4384 1 4384 23 parsed_1b4c 1 276 "{w, 3.88, 1}" 4388 1 4388 21 parsed_1b4c 1 277 ; {s?, 8.47, 6} strong relative to other peaks NOTES 3D NOESY: noesy100- 135 70 27 His 42e (nh- 9.57ppm; n= 122.25) hn105 NOTES 3D NOESY: noesy100- 148 75 28 His 42f (nh- 9.46ppm; n= 121.37) hn100 NOTES 3D NOESY: noesy100- 157 79 29 Phe 43d SEQ R assign (segid="sbm1" and resid 42 and name hn) (segid="sbm1" and resid 43 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 42 and name hn) (segid="sbm2" and resid 43 and name hn) 1.8 0 3.2 {w, 9.72, 5} amb assign (segid="sbm1" and resid 44 and name hn) (segid="sbm1" and resid 43 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 44 and name hn) (segid="sbm2" and resid 43 and name hn) 1.8 0 3.2 {w, 8.33, 3} NOTES 3D NOESY: noesy100- 242 116 25 ha dispersive Phe 43e (nh- 8.33ppm; n= 123.78) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Phe 43f (nh- 8.06ppm; n= 123.22) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Leu 44d SEQ amb assign (segid="sbm1" and resid 43 and name hn) (segid="sbm1" and resid 44 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 43 and name hn) (segid="sbm2" and resid 44 and name hn) 1.8 0 3.2 {?, 8.5, 9ovlp?} amb assign (segid="sbm1" and resid 45 and name hn) (segid="sbm1" and resid 44 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 45 and name hn) (segid="sbm2" and resid 44 and name hn) 1.8 0 3.2 {w, 7.38, 6, 0} 43he* at 7.40 43hn - 44hn assign weak b/c may overlap w/hn[115] NOTES 3D NOESY: noesy100- ~254 ~120 39 alpha- 4.04 ppm (8) ~279 ovlps N38 an-4[9/31] & M7 an-4[8/70] beta- 1.75 ppm (10) 363 ovlps M7 bn-1[8/83] NN-1 (hn102) 8.50ppm, (9/2), 115 ovlps nn[43] Leu 44e (nh- 8.28ppm; n= 115.41) hn12 NOTES 3D NOESY: noesy100- ~257 ~122 39 NN-1 (hn103) 8.33ppm, (), could ovlp hn12 Leu 44f (nh- 8.15ppm; n= 115.33) hn11 NOTES 3D NOESY: noesy100- 268 ~128 39 NN-1 (hn123)8.06ppm, (5), 131 nearly ovlps hn11 NOTES 4D CN: too weak and overlapped Glu 45 - SEQ R assign (segid="sbm1" and resid 44 and name hn) (segid="sbm1" and resid 45 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 44 and name hn) (segid="sbm2" and resid 45 and name hn) 1.8 0 3.2 {w, 8.33, 4} ; 4392 1 4460 22 parsed_1b4c 1 278 "{w, 4.07, 4}" 4464 1 4464 21 parsed_1b4c 1 279 ; {vw, 1.75, 6ov&1} RS assign (segid="sbm1" and resid 44 and name hb*) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 44 and name hb*) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 1.59, 1, amb} assign (segid="sbm1" and resid 44 and name hd*) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 44 and name hd*) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 0.75, 2} {DJW removed} R assign (segid="sbm1" and resid 46 and name hn) (segid="sbm1" and resid 45 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 46 and name hn) (segid="sbm2" and resid 45 and name hn) 1.8 0 1.1 {s, 7.65, 10} SD/art? assign (segid="sbm1" and resid 46 and name hb*) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 SD/art? assign (segid="sbm2" and resid 46 and name hb*) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 1.97, 8*, amb} NOTES 3D NOESY: noesy100- 338 157 33 Glu 45e (nh- 7.35ppm; n= 118.63) hn36 NOTES 3D NOESY: noesy100- 338 157 33 NOE to 8.15 verifies that d/f overlap Glu 45f (nh- 7.32ppm; n= 118.63) hn37 NOTES 3D NOESY: noesy100- 340 159 33 NN-2 (hn103) 8.3ppm, (), could ovlp nn-1! Glu 46d Glu 46e Glu 46f SEQ ; 4468 1 4503 5 parsed_1b4c 1 280 "{s, 7.36, 11}" 4506 1 4506 25 parsed_1b4c 1 281 "{m, 4.20, 7, cn, amb}" 4510 1 4510 31 parsed_1b4c 1 282 ; {w, 2.22, 4, cn} SD? assign (segid="sbm1" and resid 45 and name hg*) (segid="sbm1" and resid 46 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 45 and name hg*) (segid="sbm2" and resid 46 and name hn) 1.8 0 4.2 {vw, 2.79, ~10*, amb} ; 4514 1 4518 30 parsed_1b4c 1 283 ; {w, 7.82, 8ovlp} amb assign (segid="sbm1" and resid 47 and name hg2*) (segid="sbm1" and resid 46 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 47 and name hg2*) (segid="sbm2" and resid 46 and name hn) 1.8 0 3.2 {w, 0.75, 2} think it is 44hd* amb assign (segid="sbm1" and resid 47 and name hd*) (segid="sbm1" and resid 46 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 47 and name hd*) (segid="sbm2" and resid 46 and name hn) 1.8 0 4.2 {vw, 0.94, 1}, V80hg2* and V53hg1* also near 0.94 AMB amb assign (segid="sbm1" and resid C and name hb?) (segid="sbm1" and resid 46 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid C and name hb?) (segid="sbm2" and resid 46 and name hn) 1.8 0 1.7 {m, 1.97, 9, 0, cn} , E91hb1, 5hb*, 55hb*, 31hb2 amb/art? assign (segid="sbm1" and resid 47 and name hg1*) (segid="sbm1" and resid 46 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 47 and name hg1*) (segid="sbm2" and resid 46 and name hn) 1.8 0 4.2 {vw, 1.10, 6*, 1.0}, could be 80hg1* at 1.10; 47hg12 at 1.07 amb assign (segid="sbm1" and resid and name h?) (segid="sbm1" and resid 46 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid and name h?) (segid="sbm2" and resid 46 and name hn) 1.8 0 ? {w, 1.78, 5, , }, 44hg, 47hb, or 47hg11 NOTES 3D NOESY: noesy100- 313 ~146 32 NN (hn116) 7.82ppm, (8/2), ~140 nearly ovlps hn45 beta-N-1 (hn36) 2.22ppm, (10/2), could ovlp beta Ile 47 SEQ amb assign (segid="sbm1" and resid 48 and name hg*) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 48 and name hg*) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 4.2 {vw, 1.28, 3, 2.5} AMB art? assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 4.2 {vw, 3.83, 2, 1.5} NOTES 3D NOESY: noesy100-302 141 28 (values from HOHAHA-HSQC) hn too weak to observe in 3D or 4D Ile 47e? (nh- 7.81ppm) N= 122.25 hn116 very weak peak NOTES 4D CN: too weak Lys 48 nitrogen data too weak INTRA SEQ MED LONG INTER AMB NOTES 3D NOESY: noesy100- 217 105 20 an-1 and he could overlap NOTES 4D CN: too weak Glu 49 SEQ ; 4522 1 4599 5 parsed_1b4c 1 284 "{s?, 8.77, 10}" 4602 1 4602 23 parsed_1b4c 1 285 "{w, 4.42, 6&1, cn}" 4606 1 4606 27 parsed_1b4c 1 286 "{w, 1.73, 9ovlp/5}" 4610 1 4610 27 parsed_1b4c 1 287 ; {w, 1.35, 4} R assign (segid="sbm1" and resid 50 and name hn) (segid="sbm1" and resid 49 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 50 and name hn) (segid="sbm2" and resid 49 and name hn) 1.8 0 3.2 {?, 8.5, ?} NOTES 3D NOESY: noesy100- 304 ~141 31 NN (hn88) 8.5ppm, , ~113 ovlps nn-1 NN-2 (hn116) 7.8ppm, (), could ovlp hn59 NOTES 4D CN: plane overlaps K55, so any NOEs from the CN could be to K55hn Gln 50 SEQ assign (segid="sbm1" and resid 49 and name hn) (segid="sbm1" and resid 50 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 49 and name hn) (segid="sbm2" and resid 50 and name hn) 1.8 0 4.2 {vw, 7.76, 2} ; 4614 1 4633 22 parsed_1b4c 1 288 "{vw, 4.80, 8*, amb}" 4637 1 4637 29 parsed_1b4c 1 289 ; {s, 9.18, 10} SD? assign (segid="sbm1" and resid 51 and name ha) (segid="sbm1" and resid 50 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 51 and name ha) (segid="sbm2" and resid 50 and name hn) 1.8 0 4.2 {vw, 4.09, 8*, amb} NOTES 3D NOESY: noesy100- 237 113 22 NOTES 4D CN: close to D23 in H and N, baseline troulbes at N=11, h=515-525 Glu 51 SEQ R assign (segid="sbm1" and resid 50 and name hn) (segid="sbm1" and resid 51 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 50 and name hn) (segid="sbm2" and resid 51 and name hn) 1.8 0 1.1 {s, 8.55, 9, 0} ; 4641 1 4658 25 parsed_1b4c 1 290 ; {mw?, 3.66, 10ov/2, 0} amb assign (segid="sbm1" and resid 50 and name hb*) (segid="sbm1" and resid 51 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 50 and name hb*) (segid="sbm2" and resid 51 and name hn) 1.8 0 1.7 {m, 1.94, >10 ov51hb1/0, 1.0, amb} amb assign (segid="sbm1" and resid 50 and name hb*) (segid="sbm1" and resid 51 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 50 and name hb*) (segid="sbm2" and resid 51 and name hn) 1.8 0 1.7 {m, 2.16, >10 ov51hb1/0, 1.0, amb} ; 4662 1 4670 44 parsed_1b4c 1 291 ; {s, 7.06, >10, 0}{ made med for test, DJW} assign (segid="sbm1" and resid 52 and name hg2*) (segid="sbm1" and resid 51 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 52 and name hg2*) (segid="sbm2" and resid 51 and name hn) 1.8 0 3.2 {w?, 1.02, 5/1, 1.5, ncn} viol for w asbd9 {DJW removed} NOTES 3D NOESY: noesy100- 184 90 36 NN-2 (hn59) 7.71ppm, (6), 144 ovlps hn[25]H25 nn[27] beta-N-1 (hn88) 1.9ppm, (), could ovlp beta, beta and beta-1 carbons also overlap Val 52 SEQ R assign (segid="sbm1" and resid 51 and name hn) (segid="sbm1" and resid 52 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 51 and name hn) (segid="sbm2" and resid 52 and name hn) 1.8 0 1.1 {s, 9.18, 10, 0} ; 4674 1 4693 26 parsed_1b4c 1 292 ; {mw, 4.09, 5, 0, cn} assign (segid="sbm1" and resid 51 and name hb*) (segid="sbm1" and resid 52 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 51 and name hb*) (segid="sbm2" and resid 52 and name hn) 1.8 0 1.7 {m?, 2.10, >10ov/8ov, 0, cn} assign (segid="sbm1" and resid 51 and name hb*) (segid="sbm1" and resid 52 and name hg2*) 1.8 0 3.2 assign (segid="sbm2" and resid 51 and name hb*) (segid="sbm2" and resid 52 and name hg2*) 1.8 0 3.2 {g', w, 2.05, 11, 3.9} mostly to 49hb1 ? {DJW removed} assign (segid="sbm1" and resid 51 and name hg*) (segid="sbm1" and resid 52 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 51 and name hg*) (segid="sbm2" and resid 52 and name hn) 1.8 0 4.2 {w, 2.34, 6, 1.0, ncn} R assign (segid="sbm1" and resid 53 and name hn) (segid="sbm1" and resid 52 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 53 and name hn) (segid="sbm2" and resid 52 and name hn) 1.8 0 1.1 {s, 6.78, 10, 0} SD? assign (segid="sbm1" and resid 53 and name ha) (segid="sbm1" and resid 52 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 53 and name ha) (segid="sbm2" and resid 52 and name hn) 1.8 0 4.2 {vw, 3.36, 7*, 0, amb} assign (segid="sbm1" and resid 53 and name hg2*) (segid="sbm1" and resid 52 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 53 and name hg2*) (segid="sbm2" and resid 52 and name hn) 1.8 0 4.2 {vw, 0.90, ?/3, 1.5, cn} {DJW removed} NOTES 3D NOESY: noesy100- 365 168 34 Val 53 SEQ ; 4697 1 4730 5 parsed_1b4c 1 293 "{s, 7.06, 11, 0}" 4733 1 4733 25 parsed_1b4c 1 294 "{mw, 3.63, 8ovlp, 0, amb}" 4737 1 4737 34 parsed_1b4c 1 295 "{s, 2.11, >10/ovlp, 0, amb}" 4741 1 4741 36 parsed_1b4c 1 296 ; {m, 0.83, 7&2, 1.5, cn} R assign (segid="sbm1" and resid 54 and name hn) (segid="sbm1" and resid 53 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 54 and name hn) (segid="sbm2" and resid 53 and name hn) 1.8 0 1.1 {s, 8.66, 10, 0} assign (segid="sbm1" and resid 54 and name ha) (segid="sbm1" and resid 53 and name hg1*) 1.8 0 3.2 assign (segid="sbm2" and resid 54 and name ha) (segid="sbm2" and resid 53 and name hg1*) 1.8 0 3.2 {w, 4.26, 5, 1.5, amb} {DJW removed} SD? assign (segid="sbm1" and resid 54 and name hb*) (segid="sbm1" and resid 53 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 54 and name hb*) (segid="sbm2" and resid 53 and name hn) 1.8 0 4.2 {vw, 2.68, 9*, 1.0, amb} NOTES 3D NOESY: noesy100- 387 178 32 beta-N-1 (hn2.0) 2.0ppm, (10/2),could ovlp beta, ovlps in Carbon as well Asp 54 SEQ ; 4745 1 4766 5 parsed_1b4c 1 297 "{s?, 6.78, 10, 0}" 4769 1 4769 26 parsed_1b4c 1 298 "{mw?, 3.36, 8ovlp?, 0}, V80ha @ 3.39 also ?" 4773 1 4773 52 parsed_1b4c 1 299 ; {s, 2.08, 10, 0} R assign (segid="sbm1" and resid 55 and name hn) (segid="sbm1" and resid 54 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 55 and name hn) (segid="sbm2" and resid 54 and name hn) 1.8 0 1.1 {s, 7.79, 12, 0} amb assign (segid="sbm1" and resid 55 and name hg*) (segid="sbm1" and resid 54 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 55 and name hg*) (segid="sbm2" and resid 54 and name hn) 1.8 0 3.2 {w, 1.51, 5, 1.0, amb} NOTES 3D NOESY: noesy100- 227 108 31 V52 alpha-N-2 (hn34) 3.66ppm, (9/2), 293 could ovlp an-4 Q50 alpha-N-4 (hn88) 3.66ppm, (9/2), 293 could ovlp an-2 NOTES 4D CN: close to O1 in D1 Lys 55 hn nearly ovlps E49 SEQ ; 4777 1 4798 5 parsed_1b4c 1 300 "{s, 8.66, 10, 0}" 4801 1 4801 25 parsed_1b4c 1 301 "{w, 4.28, 3, 0, amb}" 4805 1 4805 29 parsed_1b4c 1 302 ; {s, 2.65, 10&9, 1, cn} R assign (segid="sbm1" and resid 56 and name hn) (segid="sbm1" and resid 55 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 56 and name hn) (segid="sbm2" and resid 55 and name hn) 1.8 0 1.1 {s, 8.06, 10, 0} SD? assign (segid="sbm1" and resid 56 and name ha) (segid="sbm1" and resid 55 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 56 and name ha) (segid="sbm2" and resid 55 and name hn) 1.8 0 4.2 {vw, 3.36, 1, 0, amb} amb assign (segid="sbm1" and resid 56 and name hg2*) (segid="sbm1" and resid 55 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 56 and name hg2*) (segid="sbm2" and resid 55 and name hn) 1.8 0 3.2 {w, 1.21, 5, 1.5, amb} NOTES 3D NOESY: noesy100- 302 141 31 NOTES 4D CN: plane overlaps E49, so NOEs from 4D CN could be to E49 instead Val 56 SEQ ; 4809 1 4831 5 parsed_1b4c 1 303 "{s, 7.79, >10, 0}" 4834 1 4834 28 parsed_1b4c 1 304 "{mw, 4.15, 6, 0, ncn, amb}" 4838 1 4838 35 parsed_1b4c 1 305 ; {s, 2.00, >10, 1.0} assign (segid="sbm1" and resid 55 and name hb*) (segid="sbm1" and resid 56 and name hg2*) 1.8 0 1.5 assign (segid="sbm2" and resid 55 and name hb*) (segid="sbm2" and resid 56 and name hg2*) 1.8 0 1.5 {m, 1.92, 8, 2.5} {DJW removed} assign (segid="sbm1" and resid 55 and name hg*) (segid="sbm1" and resid 56 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 55 and name hg*) (segid="sbm2" and resid 56 and name hn) 1.8 0 3.2 {w, 1.51, 6, 1.0, amb} {DJW removed} amb/sani assign (segid="sbm1" and resid 55 and name he*) (segid="sbm1" and resid 56 and name hg2*) 1.8 0 4.2 amb/sani assign (segid="sbm2" and resid 55 and name he*) (segid="sbm2" and resid 56 and name hg2*) 1.8 0 4.2 {vw, 2.91, 2, 2.5} R assign (segid="sbm1" and resid 57 and name hn) (segid="sbm1" and resid 56 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 57 and name hn) (segid="sbm2" and resid 56 and name hn) 1.8 0 1.1 {s, 8.33, >10, 0} assign (segid="sbm1" and resid 57 and name hg*) (segid="sbm1" and resid 56 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 57 and name hg*) (segid="sbm2" and resid 56 and name hn) 1.8 0 4.2 {vw?, 2.84, 4, 1.0, amb} viol for wk asbd8 {DJW removed} amb/art? assign (segid="sbm1" and resid 57 and name he*) (segid="sbm1" and resid 56 and name hg2*) 1.8 0 3.2 amb/art? assign (segid="sbm2" and resid 57 and name he*) (segid="sbm2" and resid 56 and name hg2*) 1.8 0 3.2 {w, 2.06, 6 shoulder, 2.5, amb} 80hb at 2.05? NOTES 3D NOESY: noesy100- 278 131 27 E58 NN+2 (hn39) 8.27ppm, (), could ovlp nn V52 alpha-N-4 (hn34) 3.66ppm, (10/2), ~293, could ovlp ha Met 57 SEQ ; 4842 1 4877 5 parsed_1b4c 1 306 "{s?, 8.06, 10, 0}" 4880 1 4880 27 parsed_1b4c 1 307 "{mw, 3.60, 6, 0}" 4884 1 4884 26 parsed_1b4c 1 308 "{m?, 2.3, >10ov, 0, cn/amb}" 4888 1 4888 36 parsed_1b4c 1 309 "{mw?, 1.21, 8, 1.5, cn}" 4892 1 4892 32 parsed_1b4c 1 310 ; {m, 0.83, 10, 1, cn} assign (segid="sbm1" and resid 56 and name hg1*) (segid="sbm1" and resid 57 and name he*) 1.8 0 1.5 assign (segid="sbm2" and resid 56 and name hg1*) (segid="sbm2" and resid 57 and name he*) 1.8 0 1.5 {m, 0.78, 9, 3.0} {DJW removed} R assign (segid="sbm1" and resid 58 and name hn) (segid="sbm1" and resid 57 and name hn) 1.8 0 ? R assign (segid="sbm2" and resid 58 and name hn) (segid="sbm2" and resid 57 and name hn) 1.8 0 ? {s, 8.2, ?, 0} assign (segid="sbm1" and resid 58 and name hb*) (segid="sbm1" and resid 57 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 58 and name hb*) (segid="sbm2" and resid 57 and name hn) 1.8 0 4.2 {vw, 2.13, 2, 1.0, amb} NOTES 3D NOESY: noesy100- 256 ~121 37 E58 NN (hn39) 8.27ppm, (>10/2), ~123 ovlps hn19 V56 beta-N-1 (hn80) 2.33ppm, (10/2), ovlps hb2 in H and C Glu 58 SEQ ; 4896 1 4918 5 parsed_1b4c 1 311 "{s?, 8.3, >10?, 0, amb}" 4921 1 4921 32 parsed_1b4c 1 312 "{mw, 4.03, 15?, 0, amb}" 4925 1 4925 32 parsed_1b4c 1 313 ; {s, 2.33, 10 ovlps 58hg1/2, 1.0, amb} amb assign (segid="sbm1" and resid 57 and name hb*) (segid="sbm1" and resid 58 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 57 and name hb*) (segid="sbm2" and resid 58 and name hn) 1.8 0 3.2 {w?, 1.89, 8&1, 1.0} viol for med asbd9 ; 4929 1 4933 48 parsed_1b4c 1 314 ; {w, 2.87, 5, 1.0, amb} R assign (segid="sbm1" and resid 59 and name hn) (segid="sbm1" and resid 58 and name hn) 1.8 0 ? R assign (segid="sbm2" and resid 59 and name hn) (segid="sbm2" and resid 58 and name hn) 1.8 0 ? {?, 8.04, 12?, 0} NOTES 3D NOESY: noesy100- 260 123 33 NOTES 4D CN M57 NN-1 (hn19) 8.30ppm, (), could ovlp hn39 T59 NN (hn18) 8.04ppm, (12), 132 could ovlp nn-2[80] Thr 59 SEQ ; 4937 1 4953 5 parsed_1b4c 1 315 "{s, 8.27, ~16, 0, amb}" 4956 1 4956 32 parsed_1b4c 1 316 "{mw?, 4.04, 15ovlp59hb/9, 0, ncn}" 4960 1 4960 42 parsed_1b4c 1 317 "{s, 4.42, 10, 1}" 4964 1 4964 25 parsed_1b4c 1 318 ; {s, 7.82, 13, 0} SD? assign (segid="sbm1" and resid 60 and name ha) (segid="sbm1" and resid 59 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 60 and name ha) (segid="sbm2" and resid 59 and name hn) 1.8 0 4.2 {vw, 3.85, 9*, 0, amb} assign (segid="sbm1" and resid 60 and name hb*) (segid="sbm1" and resid 59 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 60 and name hb*) (segid="sbm2" and resid 59 and name hn) 1.8 0 4.2 {vw?, 1.70, 9 ovlp?, 1.0} 60hg also @ 1.70, and 55hd* and 33hb2 @ 1.65 ?? amb assign (segid="sbm1" and resid 60 and name hg) (segid="sbm1" and resid 59 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 60 and name hg) (segid="sbm2" and resid 59 and name hn) 1.8 0 3.2 {w?, 1.70, 9 ovlp?, 0} 60hb1 also @ 1.70, and 55hd* and 33hb2 @ 1.65 ?? assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 59 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 59 and name hn) 1.8 0 4.2 {vw, 0.39, 6*, 2.9, amb} RS assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 59 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 59 and name hn) 1.8 0 4.2 {vw, 0.07, 8*, 2.9, amb} NOTES 3D NOESY: noesy100- 281 132 37 NN-1 (hn39) 8.2ppm, (14), 123 could ovlp nn-2[19] NN-2 (hn19) 8.3ppm, (14/2), could ovlp nn-1[39] Leu 60 SEQ R assign (segid="sbm1" and resid 59 and name hn) (segid="sbm1" and resid 60 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 59 and name hn) (segid="sbm2" and resid 60 and name hn) 1.8 0 1.1 {s?, 8.04, 8, 0} ; 4968 1 5003 25 parsed_1b4c 1 319 "{w, 4.42, 3, 0, cn}" 5007 1 5007 28 parsed_1b4c 1 320 "{m, 3.98, 8 ovlp 57ha/~7, 0, ncn}" 5011 1 5011 42 parsed_1b4c 1 321 ; {m, 1.37, 7, 1.5, ncn} R assign (segid="sbm1" and resid 61 and name hn) (segid="sbm1" and resid 60 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 61 and name hn) (segid="sbm2" and resid 60 and name hn) 1.8 0 1.1 {s, 7.7, 11, 0} assign (segid="sbm1" and resid 61 and name hb*) (segid="sbm1" and resid 60 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 61 and name hb*) (segid="sbm2" and resid 60 and name hn) 1.8 0 4.2 {vw, 2.65, 8*, 1.0, amb} NOTES 3D NOESY: noesy100- 298 140 29 D61 NN (hn20) 7.7ppm, (11), ovlps L60 hn[68] Asp 61 SEQ ; 5015 1 5033 5 parsed_1b4c 1 322 "{s, 7.8, 25?, 0, amb}" 5036 1 5036 30 parsed_1b4c 1 323 "{w, 3.85, 3, 0, ncn}" 5040 1 5040 29 parsed_1b4c 1 324 ; {s, 1.67, 12ovlp, 1.0} 33hb2 at 1.65, 60hg at 1.70 RS assign (segid="sbm1" and resid 60 and name hb*) (segid="sbm1" and resid 61 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 60 and name hb*) (segid="sbm2" and resid 61 and name hn) 1.8 0 1.7 {m, 1.24, 8, 1.0, n} assign (segid="sbm1" and resid 60 and name hg) (segid="sbm1" and resid 61 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 60 and name hg) (segid="sbm2" and resid 61 and name hn) 1.8 0 3.2 {w, 1.67, 12ovlp, 0, amb} 33hb2 at 1.65, 60hb1 at 1.70 assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 61 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 61 and name hn) 1.8 0 4.2 {w, 0.39, 4, 2.9, n} {DJW removed} RS assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 61 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 61 and name hn) 1.8 0 3.2 {vw, 0.07, 2, 2.9, n} R assign (segid="sbm1" and resid 62 and name hn) (segid="sbm1" and resid 61 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 62 and name hn) (segid="sbm2" and resid 61 and name hn) 1.8 0 1.1 {s, 7.8, 25?, 0} NOTES 3D NOESY: noesy100- 304 142 36 NN-1 (hn68) 7.81ppm, (25/3), could ovlp D61 hn20 NN (hn53) 7.78ppm, (25/3), could ovlp D61 hn20 Glu 62 SEQ ; 5044 1 5075 5 parsed_1b4c 1 325 "{s?, 7.7, ?ovlps own}" 5078 1 5078 30 parsed_1b4c 1 326 "{w, 4.39, 4}" 5082 1 5082 21 parsed_1b4c 1 327 "{s, 2.66, >10/8?, ncn, amb}" 5086 1 5086 36 parsed_1b4c 1 328 ; {s, 7.22, 11} NOTES 3D NOESY: noesy100- 301 141 32 NN-1 (hn20) 7.74ppm, (), ovlps E62 hn53 NN-2 (hn68) 7.81ppm, (), ovlps E62 hn53 Asp 63 SEQ R assign (segid="sbm1" and resid 62 and name hn) (segid="sbm1" and resid 63 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 62 and name hn) (segid="sbm2" and resid 63 and name hn) 1.8 0 1.1 {s, 7.78, 14?, 0} ; 5090 1 5104 27 parsed_1b4c 1 329 "{m?, 4.12, 12/8, 0} G66ha1 at 4.12 also" 5108 1 5108 48 parsed_1b4c 1 330 "{m?, 2.11, 12/8, 0}" 5112 1 5112 28 parsed_1b4c 1 331 ; {w, 2.35, 4, 1.0, ncn} R assign (segid="sbm1" and resid 64 and name hn) (segid="sbm1" and resid 63 and name hn) 1.8 0 1.5 R assign (segid="sbm2" and resid 64 and name hn) (segid="sbm2" and resid 63 and name hn) 1.8 0 1.5 {m, 7.93, 7, 0} NOTES 3D NOESY: noesy100- 350 162 34 E62 NN-1 (hn53) 7.79ppm, (14/2), 141 could ovlp nn-2[20] D61 NN-2 (hn20) 7.74ppm, (14/2), 141 could ovlp nn-1[53] Gly 64 SEQ ; 5116 1 5131 5 parsed_1b4c 1 332 "{m, 7.21, 8}{made weak for test DJW}" 5134 1 5134 45 parsed_1b4c 1 333 "{m, 5.02, 10} viol as s 971205 {Made weak for test; DJW}" 5138 1 5138 65 parsed_1b4c 1 334 ; {w, 2.57, 3, ncn} R assign (segid="sbm1" and resid 65 and name hn) (segid="sbm1" and resid 64 and name hn) 1.8 0 1.7 R assign (segid="sbm2" and resid 65 and name hn) (segid="sbm2" and resid 64 and name hn) 1.8 0 1.7 {m, 8.12, 7} NOTES 3D NOESY: noesy100- 290 136 49 G66 NN+2 (hn4) 8.09ppm, (), could ovlp nn Asp 65 SEQ ; 5142 1 5154 5 parsed_1b4c 1 335 "{m, 7.93, 8}{made weak for test DJW}" 5157 1 5157 45 parsed_1b4c 1 336 ; {s, 3.93, 10{made med for test DJW} amb assign (segid="sbm1" and resid 66 and name hn) (segid="sbm1" and resid 65 and name hn) 1.8 0 1.1 amb assign (segid="sbm2" and resid 66 and name hn) (segid="sbm2" and resid 65 and name hn) 1.8 0 1.1 {?, 8.0, 24?, 0} ovlps own at 8.09 NOTES 3D NOESY: noesy100- 274 129 38 NN (hn4) 8.09ppm, (24/2), could ovlp hn16 Gly 66 SEQ ; 5161 1 5175 5 parsed_1b4c 1 337 "{w?, 8.09, ?, amb} ovlp at 8.09" 5178 1 5178 40 parsed_1b4c 1 338 "{w, 4.88, 4}" 5182 1 5182 21 parsed_1b4c 1 339 ; {w, 2.81, 6} RS assign (segid="sbm1" and resid 65 and name hb*) (segid="sbm1" and resid 66 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 65 and name hb*) (segid="sbm2" and resid 66 and name hn) 1.8 0 3.2 {w, 2.60, 6} R assign (segid="sbm1" and resid 67 and name hn) (segid="sbm1" and resid 66 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 67 and name hn) (segid="sbm2" and resid 66 and name hn) 1.8 0 3.2 {w, 8.50, 4} NOTES 3D NOESY: noesy100- 274 129 47 D65 NN-1 (hn16) 8.09ppm, (), ovlps hn4 Glu 67 SEQ ; 5186 1 5202 5 parsed_1b4c 1 340 "{w, 8.11, 6} amb b/c 65hn also at 8.09 but it looks too far {made weak for test DJW}" 5205 1 5205 93 parsed_1b4c 1 341 ; {s, 4.15, 14}{made med for test DJW} RS assign (segid="sbm1" and resid 66 and name ha*) (segid="sbm1" and resid 67 and name hn) 1.8 0 1.1 RS assign (segid="sbm2" and resid 66 and name ha*) (segid="sbm2" and resid 67 and name hn) 1.8 0 1.1 {s, 3.88, 13} ; 5209 1 5213 22 parsed_1b4c 1 342 ; {vw, 9.40, 1} assign (segid="sbm1" and resid 68 and name hg*) (segid="sbm1" and resid 67 and name ha) 1.8 0 3.2 assign (segid="sbm2" and resid 68 and name hg*) (segid="sbm2" and resid 67 and name ha) 1.8 0 3.2 assign (segid="sbm1" and resid 68 and name ha) (segid="sbm1" and resid 67 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 68 and name ha) (segid="sbm2" and resid 67 and name hn) 1.8 0 4.2 {vw, 5.18, 4*, amb} NOTES 3D NOESY: noesy100- 241 115 33 D65 NN-2 (hn16) 8.09ppm, (), could ovlp nn-1 Cys 68 SEQ ; 5217 1 5232 5 parsed_1b4c 1 343 "{s, 5.07, 15}" 5235 1 5235 22 parsed_1b4c 1 344 "{m, 1.99, 9}" 5239 1 5239 21 parsed_1b4c 1 345 ; {w, 2.35, 5/3, cn} R assign (segid="sbm1" and resid 67 and name hg*) (segid="sbm1" and resid 68 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 67 and name hg*) (segid="sbm2" and resid 68 and name hn) 1.8 0 3.2 {w, 1.96, 9ovlp/2, cn} R assign (segid="sbm1" and resid 69 and name hn) (segid="sbm1" and resid 68 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 69 and name hn) (segid="sbm2" and resid 68 and name hn) 1.8 0 4.2 {vw, 8.60, *} NOTES 3D NOESY: noesy100- 164 82 31 X/Y= R20hg1,hg2 not in 4D NOESY, also observed for G66 NOTES 4D CN K26ha 4 ctrs in 4D 9* in 3D go with 2 K28ha 6ctrs in 4D 3 in 3D go with 4 Asp 69 SEQ ; 5246 1 5265 5 parsed_1b4c 1 346 "{vw, 9.39, 5*, 0}" 5268 1 5268 26 parsed_1b4c 1 347 "{s, 5.18, 18}" 5272 1 5272 23 parsed_1b4c 1 348 ; {m/w sd?, 3.11, 8} amb/R assign (segid="sbm1" and resid 68 and name hb*) (segid="sbm1" and resid 69 and name hn) 1.8 0 3.2 amb/R assign (segid="sbm2" and resid 68 and name hb*) (segid="sbm2" and resid 69 and name hn) 1.8 0 3.2 {w, 2.79, 10ov?} 68hb2 at 2.84 R assign (segid="sbm1" and resid 70 and name hn) (segid="sbm1" and resid 69 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 70 and name hn) (segid="sbm2" and resid 69 and name hn) 1.8 0 4.2 {vw, 9.18, 5*, 0} NOTES 3D NOESY: noesy100- 233 111 27 Phe 70 SEQ ; 5276 1 5291 5 parsed_1b4c 1 349 "{vw, 8.61, 4*}" 5294 1 5294 23 parsed_1b4c 1 350 "{s, 5.34, 7} strong relative to others" 5298 1 5298 50 parsed_1b4c 1 351 ; {m/s, 3.55, 9} strong relative to others RS assign (segid="sbm1" and resid 69 and name hb*) (segid="sbm1" and resid 70 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 69 and name hb*) (segid="sbm2" and resid 70 and name hn) 1.8 0 1.7 {m, 2.73, 8} R assign (segid="sbm1" and resid 71 and name hn) (segid="sbm1" and resid 70 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 71 and name hn) (segid="sbm2" and resid 70 and name hn) 1.8 0 3.2 {w, 7.95, 4} NOTES 3D NOESY: noesy100- 181 89 32 Gln 71 SEQ ; 5302 1 5319 5 parsed_1b4c 1 352 "{s?, 9.20, 7, 0}" 5322 1 5322 25 parsed_1b4c 1 353 "{mw, 3.39, 4, 0, amb}" 5326 1 5326 30 parsed_1b4c 1 354 "{s, 2.57, 10, 1}" 5333 1 5333 25 parsed_1b4c 1 355 ; {w, 6.32, 5, 2.4, amb} R assign (segid="sbm1" and resid 72 and name hn) (segid="sbm1" and resid 71 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 72 and name hn) (segid="sbm2" and resid 71 and name hn) 1.8 0 1.1 {s, 8.36, 14, 0} amb/SD? assign (segid="sbm1" and resid 72 and name ha) (segid="sbm1" and resid 71 and name hn) 1.8 0 3.2 amb/SD? assign (segid="sbm2" and resid 72 and name ha) (segid="sbm2" and resid 71 and name hn) 1.8 0 3.2 {w, 3.98, 5/5, 0, ncn} 3.98/59.3 fm 3D/4D: 20ha, 88ha, 5ha, 72ha NOTES 3D NOESY: noesy100- 288 135 35 D69 NN-2 (hn78) 8.58ppm, (4/2), 110 could ovlp nn+2 F73 NN+2 (hn72) 8.62ppm, (4/2), 110 could ovlp nn-2 Glu 72 close to Q16 in 1H and 15N SEQ ; 5337 1 5358 5 parsed_1b4c 1 356 "{s, 7.94, 12, 0}" 5361 1 5361 26 parsed_1b4c 1 357 "{mw, 3.55, 6, 0}" 5365 1 5365 25 parsed_1b4c 1 358 ; {s, 2.13, 17, 1} R assign (segid="sbm1" and resid 73 and name hn) (segid="sbm1" and resid 72 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 73 and name hn) (segid="sbm2" and resid 72 and name hn) 1.8 0 1.1 {s, 8.63, 11, 0} assign (segid="sbm1" and resid 73 and name hb*) (segid="sbm1" and resid 72 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 73 and name hb*) (segid="sbm2" and resid 72 and name hn) 1.8 0 4.2 {vw, 3.33, ~10*, 1.0, amb} NOTES 3D NOESY: noesy100- 254 121 28 M74 NN+2 (hn32) 8.00ppm, () could ovlp nn-1 Phe 73 SEQ ; 5369 1 5387 5 parsed_1b4c 1 359 "{s, 8.36, 11, 0}" 5390 1 5390 27 parsed_1b4c 1 360 "{mw, 4.01, 5, 0}" 5394 1 5394 26 parsed_1b4c 1 361 ; {m?, 2.34, 9ov, 1.0} RS assign (segid="sbm1" and resid 72 and name hb*) (segid="sbm1" and resid 73 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 72 and name hb*) (segid="sbm2" and resid 73 and name hn) 1.8 0 3.2 {w, 2.11, 6ov, 1.0} assign (segid="sbm1" and resid 72 and name hg*) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 72 and name hg*) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 2.49, 1, 1.0, amb} amb assign (segid="sbm1" and resid 72 and name hg*) (segid="sbm1" and resid 73 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 72 and name hg*) (segid="sbm2" and resid 73 and name hn) 1.8 0 3.2 {w, 2.34, 9ov, 1.0, amb} R assign (segid="sbm1" and resid 74 and name hn) (segid="sbm1" and resid 73 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 74 and name hn) (segid="sbm2" and resid 73 and name hn) 1.8 0 1.1 {s?, 8.01, 8, 0} NOTES 3D NOESY: noesy100- 229 110 29 Q71 NN-2 (hn28) 7.93ppm, (), could ovlp nn NOTES 4D CN: close to O1 in D1 so intensity greatly attenuated Met 74 SEQ ; 5398 1 5425 5 parsed_1b4c 1 362 "{s?, 8.63, 9, 0}" 5428 1 5428 26 parsed_1b4c 1 363 "{vw, 4.39, 6*, 0}" 5432 1 5432 27 parsed_1b4c 1 364 ; {m, 3.33, 8, 1.0} RS assign (segid="sbm1" and resid 73 and name hb*) (segid="sbm1" and resid 74 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 73 and name hb*) (segid="sbm2" and resid 74 and name hn) 1.8 0 3.2 {w, 3.22, 6, 1.0} ; 5436 1 5440 26 parsed_1b4c 1 365 ; {m, 6.92, 9, 2.4, amb} amb/art? assign (segid="sbm1" and resid 73 and name hd*) (segid="sbm1" and resid 74 and name he*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 73 and name hd*) (segid="sbm2" and resid 74 and name he*) 1.8 0 4.2 {vw, 6.88, 1*, 4.4} amb assign (segid="sbm1" and resid 73/14 and name he*) (segid="sbm1" and resid 74 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 73/14 and name he*) (segid="sbm2" and resid 74 and name hn) 1.8 0 3.2 {w, 7.11, 3, 2.4, amb} ; 5444 1 5452 31 parsed_1b4c 1 366 ; {s?, 7.87, 10, 0} assign (segid="sbm1" and resid 75 and name ha) (segid="sbm1" and resid 74 and name he*) 1.8 0 4.2 assign (segid="sbm2" and resid 75 and name ha) (segid="sbm2" and resid 74 and name he*) 1.8 0 4.2 {vw, 3.90, 2, 1.5, wk cfilt 3.99} think cfilt for S78hb* b/c 75ha looks closer as intra amb assign (segid="sbm1" and resid 75 and name hb*) (segid="sbm1" and resid 74 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 75 and name hb*) (segid="sbm2" and resid 74 and name hn) 1.8 0 4.2 {vw, 1.24, 10*, 1.5, amb} 27hb2 1.26 and 32hd1* 1.21 possible NOTES 3D NOESY: noesy100- 282 133 34 F76 NN+2 (hn23) 7.99ppm, (), could ovlp M74 hn32 Ala 75 SEQ R assign (segid="sbm1" and resid 74 and name hn) (segid="sbm1" and resid 75 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 74 and name hn) (segid="sbm2" and resid 75 and name hn) 1.8 0 1.1 {s?, 8.0, 14ov, 0} ; 5456 1 5477 28 parsed_1b4c 1 367 "{mw, 3.68, 6, 0}" 5481 1 5481 25 parsed_1b4c 1 368 ; {s?, 1.67, 9, 1.0} RS assign (segid="sbm1" and resid 74 and name hb*) (segid="sbm1" and resid 75 and name hn) 1.8 0 1.1 RS assign (segid="sbm2" and resid 74 and name hb*) (segid="sbm2" and resid 75 and name hn) 1.8 0 1.1 {s?, 1.48, 8, 1.0} assign (segid="sbm1" and resid 74 and name hg*) (segid="sbm1" and resid 75 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 74 and name hg*) (segid="sbm2" and resid 75 and name hn) 1.8 0 3.2 {w, 1.94, 1, 1.0, amb} R assign (segid="sbm1" and resid 76 and name hn) (segid="sbm1" and resid 75 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 76 and name hn) (segid="sbm2" and resid 75 and name hn) 1.8 0 1.1 {s?, 7.9, 14ov, 0} assign (segid="sbm1" and resid 76 and name hb*) (segid="sbm1" and resid 75 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 76 and name hb*) (segid="sbm2" and resid 75 and name hn) 1.8 0 4.2 {vw, 3.06, 8*, 1.0, amb} SD? assign (segid="sbm1" and resid 76 and name hb*) (segid="sbm1" and resid 75 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 76 and name hb*) (segid="sbm2" and resid 75 and name hn) 1.8 0 4.2 {vw, 2.81, 6*, 1.0, amb} NOTES 3D NOESY: noesy100- 294 138 22 M74 NN-1 (hn32) 8.00ppm, (14/2), 133 ovlps nn F76 NN (hn23) 7.99ppm, (14/2), 133 ovlps nn-1 Phe 76 SEQ ; 5485 1 5516 5 parsed_1b4c 1 369 "{s, 7.87, 13, 0}" 5519 1 5519 25 parsed_1b4c 1 370 "{mw, 4.01, 8ov, 0, amb}" 5523 1 5523 33 parsed_1b4c 1 371 ; {s, 1.24, 15, 1} R assign (segid="sbm1" and resid 77 and name hn) (segid="sbm1" and resid 76 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 77 and name hn) (segid="sbm2" and resid 76 and name hn) 1.8 0 1.1 {s, 8.47, 11, 0} SD? assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm1" and resid 76 and name hn) 1.8 0 3.2 SD? assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm2" and resid 76 and name hn) 1.8 0 3.2 {w, 0.48, 3, 1.5, ncn} amb assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm1" and resid 76 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm2" and resid 76 and name hn) 1.8 0 4.2 {vw, 0.80, 2ov, 1.5, ncn} 77hg1 at 0.78, 56hg2* at 0.83, could be both?, 77hg1* looks too far NOTES 3D NOESY: noesy100- 283 133 35 ha vw in 3D NOESY and 10 ctrs in 4D go with 5 ctrs Val 77 SEQ ; 5527 1 5549 5 parsed_1b4c 1 372 "{s, 8.01, 11, 0}" 5552 1 5552 26 parsed_1b4c 1 373 "{vw, 4.34, 6*, 0}" 5556 1 5556 27 parsed_1b4c 1 374 ; {m, 3.06, 9, 1.0} RS assign (segid="sbm1" and resid 76 and name hb*) (segid="sbm1" and resid 77 and name hn) 1.8 0 1.7 RS assign (segid="sbm2" and resid 76 and name hb*) (segid="sbm2" and resid 77 and name hn) 1.8 0 1.7 {m, 2.81, 7ov?, 1.0} ; 5560 1 5564 29 parsed_1b4c 1 375 ; {w, 7.30, 2, 2.4, amb} R assign (segid="sbm1" and resid 78 and name hn) (segid="sbm1" and resid 77 and name hn) 1.8 0 1.1 R assign (segid="sbm2" and resid 78 and name hn) (segid="sbm2" and resid 77 and name hn) 1.8 0 1.1 {s, 8.63, 10, 0} NOTES 3D NOESY: noesy100- 244 116 35 A75 NN-2 (hn87) 7.8ppm, (5/2), 139 could ovlp nn+2 M79 NN+2 (hn79) 7.8ppm, (5/2), 139 could ovlp nn-2 Ser 78 SEQ ; 5568 1 5583 5 parsed_1b4c 1 376 "{s?, 8.47, 10, 0}" 5586 1 5586 26 parsed_1b4c 1 377 "{mw, 3.41, 6, 0}" 5590 1 5590 25 parsed_1b4c 1 378 "{s, 1.73, 10ov?, 0}" 5594 1 5594 28 parsed_1b4c 1 379 "{m, 0.77, 8, 1.5, amb}" 5598 1 5598 31 parsed_1b4c 1 380 "{w, 0.48, 7, 1.5, ncn}" 5602 1 5602 31 parsed_1b4c 1 381 ; {s, 7.83, 12ov, 0} amb assign (segid="sbm1" and resid 79 and name hg*) (segid="sbm1" and resid 78 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 79 and name hg*) (segid="sbm2" and resid 78 and name hn) 1.8 0 3.2 {w, 2.35, 4, 1.0, amb} NOTES 3D NOESY: noesy100- 228 109 32 M79 NN (hn79) 7.85ppm, (12), 139 could ovlp nn+2 Met 79 SEQ ; 5606 1 5620 5 parsed_1b4c 1 382 "{s, 8.6, 10, 0}" 5623 1 5623 24 parsed_1b4c 1 383 "{mw, 3.63, 6, 0}" 5627 1 5627 25 parsed_1b4c 1 384 "{w, 3.93, 4, 1, cn}" 5631 1 5631 28 parsed_1b4c 1 385 ; {s?, 7.8, ?, 0} assign (segid="sbm1" and resid 80 and name hg2*) (segid="sbm1" and resid 79 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 80 and name hg2*) (segid="sbm2" and resid 79 and name hn) 1.8 0 4.2 {vw, 1.10, 3, 1.5, amb} vw b/c some SD? NOTES 3D NOESY: noesy100- 297 139 27 V80 NN (hn22) 7.80ppm, (25/2), ~139 could ovlp M79 hn79 Val 80 SEQ ; 5635 1 5649 5 parsed_1b4c 1 386 "{s?, 7.8, 22?, 0, amb}" 5652 1 5652 32 parsed_1b4c 1 387 "{mw, 3.93, 6, 0}" 5656 1 5656 26 parsed_1b4c 1 388 "{w?, 2.22, 9&6, 1.0} viol for med asbd9" 5660 1 5660 48 parsed_1b4c 1 389 "{m, 1.92ov, 9&7, 1.0}" 5664 1 5664 30 parsed_1b4c 1 390 "{w, 2, 1.85, 2.5}" 5668 1 5668 26 parsed_1b4c 1 391 ; {w, 2.53, 2/4, 1.0, cn} assign (segid="sbm1" and resid 79 and name hg*) (segid="sbm1" and resid 80 and name hg2*) 1.8 0 4.2 assign (segid="sbm2" and resid 79 and name hg*) (segid="sbm2" and resid 80 and name hg2*) 1.8 0 4.2 {vw, 2, 2.49, 3.5} ; 5672 1 5676 27 parsed_1b4c 1 392 ; {w, 2.28, 4/4, 1.0, cn} assign (segid="sbm1" and resid 79 and name he*) (segid="sbm1" and resid 80 and name hg2*) 1.8 0 4.2 assign (segid="sbm2" and resid 79 and name he*) (segid="sbm2" and resid 80 and name hg2*) 1.8 0 4.2 {vw, 1.85, 2, 3.0} ; 5680 1 5684 27 parsed_1b4c 1 393 ; {m?, 8.17, 6, 0} assign (segid="sbm1" and resid 81 and name hb) (segid="sbm1" and resid 80 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 81 and name hb) (segid="sbm2" and resid 80 and name hn) 1.8 0 4.2 {vw, 4.28, 5*ov, 0, amb} NOTES 3D NOESY: noesy100- 298 139 36 M79 NN-1 (hn79) ppm, (22/2), ~139 ovlps V80 hn22 T81 NN+2 (hn) ppm, (), could ovlp hn22 NOTES 4D CN: M79 an-1 could also be R20, F88 Thr 81 SEQ ; 5688 1 5704 5 parsed_1b4c 1 394 "{s?, 7.8, ~18, 0}" 5707 1 5707 26 parsed_1b4c 1 395 "{mw, 3.39, 6ov, 0, amb}" 5711 1 5711 32 parsed_1b4c 1 396 "{m, 2.05, 10, 0}" 5715 1 5715 25 parsed_1b4c 1 397 "{m?, 0.94, 8ov, 1.5, amb}" 5719 1 5719 42 parsed_1b4c 1 398 ; {s?, 7.8?, ~18, 0} NOTES 3D NOESY: noesy100- ~270 ~127 38 V80 NN-1 (hn22) 7.80ppm, (10/3), ~139 could ovlp nn and nn-2 T82 NN (hn111) 7.87ppm, (10/3), ~139 could ovlp nn-1/-2 M79 NN-2 (hn79) 7.83ppm, (10/3), ~139 could ovlp nn and nn-1 NOTES 4D CN V80 aN-1 (hn22) and V77 aN-4 (hn29) 3.4ppm, ovlp @ C=67.23; could also be I11 or V53 S78an-3 could also be S41ha,hb or I47hb Thr 82 SEQ ; 5723 1 5738 5 parsed_1b4c 1 399 "{vw, 8.13, 8*, 0}" 5741 1 5741 27 parsed_1b4c 1 400 "{w, 4.28, 4*, 0}" 5745 1 5745 26 parsed_1b4c 1 401 ; {w, 3.66, 4*, 0} assign (segid="sbm1" and resid 81 and name hg2*) (segid="sbm1" and resid 82 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 81 and name hg2*) (segid="sbm2" and resid 82 and name hn) 1.8 0 3.2 {w, 1.02, 8*, 1.5, amb} ; 5749 1 5753 32 parsed_1b4c 1 402 ; {w, 7.27, 3, 0} NOTES 3D NOESY: noesy100- 293 137 45 there was some uncertainty about the assignment of ha and hb however a unique noe was observed for A83 to 3.79,68.38 consistent with the current assignment of the ha and hb for T82 M79 aN-3 (hn79) 3.96ppm, vw(9), ~282 could ovlp an-4; strgr at 8.6ppm S78 aN-4 (hn49) 3.96ppm, vw(9), ~282 could ovlp an-3; strgr at 8.6ppm vw pk 100ms NOESY looks like two peaks 7.88/7.86 Ala 83 SEQ ; 5757 1 5771 5 parsed_1b4c 1 403 "{s?, 7.90, 8}" 5774 1 5774 23 parsed_1b4c 1 404 "{w, 3.30, 4}" 5778 1 5778 22 parsed_1b4c 1 405 "{w, 3.77, 4}" 5782 1 5782 21 parsed_1b4c 1 406 ; {w, 0.59, 3} R assign (segid="sbm1" and resid 84 and name hn) (segid="sbm1" and resid 83 and name hn) 1.8 0 1.5 R assign (segid="sbm2" and resid 84 and name hn) (segid="sbm2" and resid 83 and name hn) 1.8 0 1.5 {m, 7.52, 9} assign (segid="sbm1" and resid 84 and name hb*) (segid="sbm1" and resid 83 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 84 and name hb*) (segid="sbm2" and resid 83 and name hn) 1.8 0 4.2 {vw, 2.73, 4*, amb} NOTES 3D NOESY: noesy100- 347 160 29 ha dispersive in 3D NOESY; hb 17 ctrs in both expts so 9 ctrs used for ha Cys 84 SEQ ; 5786 1 5804 5 parsed_1b4c 1 407 "{s, 7.25, 7} strong relative to others" 5807 1 5807 50 parsed_1b4c 1 408 "{w, 4.48, 1, amb}" 5811 1 5811 26 parsed_1b4c 1 409 ; {w, 1.62, 4} NOTES 3D NOESY: noesy100- 325 151 37 His 85? SEQ assign (segid="sbm1" and resid 86 and name hn) (segid="sbm1" and resid 85 and name hn) assign (segid="sbm2" and resid 86 and name hn) (segid="sbm2" and resid 85 and name hn) ??NN (hn107) 8.0ppm, vw(), braod peak assign (segid="sbm1" and resid 84 and name ha) (segid="sbm1" and resid 85 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 84 and name ha) (segid="sbm2" and resid 85 and name hn) 1.8 0 4.2 alpha-N-1 (hn110) 4.7ppm, (), ~255, dispersive in 100ms and 200ms strgr, assign (segid="sbm1" and resid 84 and name hb*) (segid="sbm1" and resid 85 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 84 and name hb*) (segid="sbm2" and resid 85 and name hn) 1.8 0 4.2 beta1-N-1 (hn110) 3.00ppm, vw(), 317, centered more at 254 assign (segid="sbm1" and resid 84and name hb*) (segid="sbm1" and resid 85 and name hn) assign (segid="sbm2" and resid 84and name hb*) (segid="sbm2" and resid 85 and name hn) beta2-N-1 (hn110) 2.7ppm, (), could ovlp another peak (nh- 8.35ppm) hn119 seems to be multiple 8.35, 8.34, 8.33 nn region differs a little between 100 and 200 ms noesy100- ~254 ~121 48 alpha?- 3.68 ppm () ~292 ovlps has[3], could be 3.8 instead beta1- 2.16 ppm () 348 ovlps peak from G22(hn3) beta2- 1.89 ppm () 358 ovlps peak from G22 Glu 86? INTRA SEQ assign (segid="sbm1" and resid 85 and name hb) (segid="sbm1" and resid 86 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 85 and name hb) (segid="sbm2" and resid 86 and name hn) 1.8 0 4.2 beta1-N-1 (hn119) 2.2ppm, (), could ovlp beta1 assign (segid="sbm1" and resid 85 and name hb) (segid="sbm1" and resid 86 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 85 and name hb) (segid="sbm2" and resid 86 and name hn) 1.8 0 3.2 beta2-N-1 (hn119) ppm, (4/2), could ovlp beta2 (nh- 8.01ppm) hn107 dispersive amide in 100ms close to E91 in 1H and 15N noesy100- 281 ~132 20 alpha- 4.36 ppm () missing in NOESY, present in TOCSY beta1- 2.22 ppm vw(8) 346 close to negative peak beta2- 1.86 ppm (4) 359 gamma1- 2.57 ppm vw(9) 340 gamma2- 2.38 ppm vw(6) 333 close to negative peak Phe 87 SEQ assign (segid="sbm1" and resid 86 and name hn) (segid="sbm1" and resid 87 and name hn) assign (segid="sbm2" and resid 86 and name hn) (segid="sbm2" and resid 87 and name hn) ?? NN-1 (hn) 8.01ppm, (), negative peak at 8.01 assign (segid="sbm1" and resid 86 and name hb) (segid="sbm1" and resid 87 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 86 and name hb) (segid="sbm2" and resid 87 and name hn) 1.8 0 4.2 beta-N-1 (hn107) 2.19ppm, vw(3), ~347, close to negative peak assign (segid="sbm1" and resid 86 and name hb) (segid="sbm1" and resid 87 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 86 and name hb) (segid="sbm2" and resid 87 and name hn) 1.8 0 4.2 beta-N-1 (hn107) 1.84ppm, (), could ovlp beta2 assign (segid="sbm1" and resid 88 and name hn) (segid="sbm1" and resid 87 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 88 and name hn) (segid="sbm2" and resid 87 and name hn) 1.8 0 4.2 NN (hn5) 7.49ppm, vw(3), ~152 (nh- 8.61ppm) hn122 noesy100- 229 ~109 25 alpha- 3.96 ppm (4) 282 beta1- 2.00 ppm (5) 354 beta2- 1.86 ppm (5) 359 could ovpl b2n-1 ??in tocsy- 1.56 ppm (3) Phe 88 SEQ amb assign (segid="sbm1" and resid 87 and name hn) (segid="sbm1" and resid 88 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 87 and name hn) (segid="sbm2" and resid 88 and name hn) 1.8 0 3.2 {w?, 7.5, 6?} ; 5815 1 5912 22 parsed_1b4c 1 410 "{w, 3.98, 3, cn}" 5916 1 5916 25 parsed_1b4c 1 411 "{w, 2.43, 3, ncn}" 5920 1 5920 26 parsed_1b4c 1 412 "{vw, 6.10, 9*}" 5924 1 5924 23 parsed_1b4c 1 413 ; {m, 6.50, ~10, 2Droe, amb} amb assign (segid="sbm1" and resid 87 and name hz) (segid="sbm1" and resid 88 and name he*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 87 and name hz) (segid="sbm2" and resid 88 and name he*) 1.8 0 1.5 {m, 6.97, >10, 2Droe, amb} amb assign (segid="sbm1" and resid 89 and name hn) (segid="sbm1" and resid 88 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 89 and name hn) (segid="sbm2" and resid 88 and name hn) 1.8 0 1.7 {m?, ~7.6, 9ov, amb} assign (segid="sbm1" and resid 89 and name ha) (segid="sbm1" and resid 88 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 89 and name ha) (segid="sbm2" and resid 88 and name hn) 1.8 0 4.2 {vw, 4.20, ~12*, 0, amb} amb assign (segid="sbm1" and resid 89 and name hb*) (segid="sbm1" and resid 88 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 89 and name hb*) (segid="sbm2" and resid 88 and name hn) 1.8 0 4.2 {vw, 1.81, 6*, 1.0, amb} assign (segid="sbm1" and resid 89 and name hb*) (segid="sbm1" and resid 88 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 89 and name hb*) (segid="sbm2" and resid 88 and name hn) 1.8 0 4.2 {vw, 1.97, 9*, 1.0, amb} amb/SD assign (segid="sbm1" and resid 89 and name hg*) (segid="sbm1" and resid 88 and name hn) 1.8 0 4.2 amb/SD assign (segid="sbm2" and resid 89 and name hg*) (segid="sbm2" and resid 88 and name hn) 1.8 0 4.2 {vw, 2.16, 10*, 0, amb} NOTES 3D NOESY: noesy100- 329 ~153 40 E89 NN (hn60) 7.57ppm, (~6), ~149 ovlps F88 hn5 Glu 89 SEQ ; 5928 1 5962 5 parsed_1b4c 1 414 "{w, 7.46, 6}" 5965 1 5965 22 parsed_1b4c 1 415 "{m, 3.98, 10ov, amb}" 5969 1 5969 30 parsed_1b4c 1 416 ; {w, 3.30, 4} RS assign (segid="sbm1" and resid 88 and name hb*) (segid="sbm1" and resid 89 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 88 and name hb*) (segid="sbm2" and resid 89 and name hn) 1.8 0 3.2 {w, 2.95, 4} ; 5973 1 5977 21 parsed_1b4c 1 417 "{w, 7.33, 6, amb}" 5981 1 5981 26 parsed_1b4c 1 418 ; {vw, 8.12, 2} amb assign (segid="sbm1" and resid 90 and name ha) (segid="sbm1" and resid 89 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 90 and name ha) (segid="sbm2" and resid 89 and name hn) 1.8 0 4.2 {vw?, 3.98, 10ov} assign (segid="sbm1" and resid 90 and name hb*) (segid="sbm1" and resid 89 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 90 and name hb*) (segid="sbm2" and resid 89 and name hn) 1.8 0 4.2 {vw, 3.14, 7*, amb} NOTES 3D NOESY: noesy100-320 149 31 His 90 SEQ R assign (segid="sbm1" and resid 89 and name hn) (segid="sbm1" and resid 90 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 89 and name hn) (segid="sbm2" and resid 90 and name hn) 1.8 0 4.2 {vw, 7.57, 5*, 0} ; 5985 1 6005 27 parsed_1b4c 1 419 ; {s, 4.17, 7, 0, ncn, amb} R assign (segid="sbm1" and resid 91 and name hn) (segid="sbm1" and resid 90 and name hn) 1.8 0 ? R assign (segid="sbm2" and resid 91 and name hn) (segid="sbm2" and resid 90 and name hn) 1.8 0 ? {?, 8.0, ?, 0} NOTES 3D NOESY: noesy100- 274 129 32 ha dispersive in 3D, stronger in 4D E91 NN (hn90) ppm, (17/2), ~129 could ovlp H90 hn114 Glu 91 SEQ amb assign (segid="sbm1" and resid 90 and name hn) (segid="sbm1" and resid 91 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 90 and name hn) (segid="sbm2" and resid 91 and name hn) 1.8 0 3.2 {w?, 8.09, ?, amb} ; 6009 1 6026 28 parsed_1b4c 1 420 "{s, 4.66, 6, cn} strong relative to other pks" 6030 1 6030 54 parsed_1b4c 1 421 ; {vw, 3.14, 6*} RS assign (segid="sbm1" and resid 90 and name hb*) (segid="sbm1" and resid 91 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 90 and name hb*) (segid="sbm2" and resid 91 and name hn) 1.8 0 4.2 {vw, 3.06, 6*} NOTES 3D NOESY noesy100- 273 129 20 H90 NN-1 (hn114) 8.0ppm, (), could ovlp E91 hn90 NOTES 4D CN H90ha 13 ctrs in 4D close to H2O in 3D go with 6 ctrs Note 1: number in parentheses are number of contours seen at lvl=0.02 of NOESY-HMQC for weak peaks and at lvl=0.1 for others Nilges et al. Biopolymers 29, 813-822, (1990). note 2: Naming- upfield = > , downfield = < previous naming was downfield "1" and upfield "2" Two beta protons are named downfield beta proton, hb1, and upfield beta proton, hb2; if degenerate, then hb*. For CH3 protons the protons hb11,hb12,hb13 and hb21,hb22,hb23. If degenerate, use hb1* for the downfield and hb2* for the upfield. Gamma, delta, epsilon, and eta, protons were treated in a similar manner. note 3a: Pseudo-corrections - NOT USED as of noe10.tbl, swith to sum averaging - ACD 971126 (a) CH3 groups add 1.0 A to the upper limit (b) CH2 group with degenerate protons add 1.0 A to the upper limit (c) degenerate CH3 groups for V, L add 1.7 A to the upper limit (d) aromatics add 2.3 A to the upper limit Conditions for 3D 100 ms NOESY-HSQC contour level = 0.1 # of levels= 20 level mult= 1.2 strong noe (>10 contour) = 1.8 0 0.9 (0 to 2.7 angstroms) strong noe (>10 contour) = 1.8 0 1.1 (0 to 2.9 angstroms for hn) medium noe (7-10 contours) = 1.8 0 1.5 (0 to 3.3 angstroms) medium noe (7-10 contours) = 1.8 0 1.7 (0 to 3.5 angstroms for hns) weak noe (3-6 countours) = 1.8 0 3.2 (0 to 5.0 angstroms) very weak noe (<3 countours) = 1.8 0 4.2 (0 to 6.0 angstroms) very weak(not seen at lvl=0.1) = 1.8 0 4.2 (0 to 6.0 angstroms) residue (nh- ppm) arbitrary assignment (destination residue) (origin residue) assign (segid="sbm1" and resid and name hn) (segid="sbm1" and resid and name hn) {s-m-w, dest'n ppm, # contours,correction} order: intraresidue sequentials medium range long range ordered by dest'n ppm value notes about questions Definitions of codes for commenting out NOEs !I!: all intraresidue NOEs commented out !viol!: comment out b/c violation in xplor run(s) !R!: redundant; weaker of two removed, if equal # levels first appearing removed !amb!: ambiguous and may not necessarily be resolved from any NOESY spectra ******************************************************************************************* **** DATA FROM 3D 13C-EDITED AND 4D 13C,13C-EDITED NOESY SPECTRA ************************** ******************************************************************************************* All parameters not mentioned here are same for the 13C-edited NOESY Conditions for 3D 13C-edited NOESY-HSQC contour level = 0.2 # of levels= 20 level mult= 1.2 strong noe (>10 contours) = 1.8 0 0.9 (0 to 2.7 angstroms) medium noe (7-10 contours) = 1.8 0 1.5 (0 to 3.3 angstroms) weak noe (3-6 countours) = 1.8 0 3.2 (0 to 5.0 angstroms) very weak noe (<3 countours) = 1.8 0 4.2 (0 to 6.0 angstroms) very weak(not seen at lvl=0.1) = 1.8 0 4.2 (0 to 6.0 angstroms) ******************************************************************************************* M = restraint not used b/c pk does not show for all of mulpiples (ie 3a,3b,3c not all show the peak) Ser 1a (nh-10.23; n= 121.93 ppm) hn104 no sidechain peaks in 3D TOCSY MED ; 6034 1 6122 5 parsed_1b4c 1 422 ; {vw, 8.96/9, 4*, 0}, 3ahn 8.94, 3bhn 9.01, 3chhn 8.92 R assign (segid="sbm1" and resid 4 and name hn) (segid="sbm1" and resid 1 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 4 and name hn) (segid="sbm2" and resid 1 and name hn) 1.8 0 4.2 {vw, 8.09, 5*, 0} assign (segid="sbm1" and resid 4 and name hb*) (segid="sbm1" and resid 1 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 4 and name hb*) (segid="sbm2" and resid 1 and name hn) 1.8 0 4.2 {vw?, 2.00, 7*, 1.0, amb}, 4b-hb* 2.00, helix 1 cap ? {DJW removed}? R assign (segid="sbm1" and resid 4 and name hb*) (segid="sbm1" and resid 1 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 4 and name hb*) (segid="sbm2" and resid 1 and name hn) 1.8 0 3.2 {w?, 2.22, 5*, 1.0, amb}, TO OTHER 4hb*:4a_hb* at 2.24, helix 1 cap assign (segid="sbm1" and resid 4 and name hg*) (segid="sbm1" and resid 1 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 4 and name hg*) (segid="sbm2" and resid 1 and name hn) 1.8 0 4.2 {vw?, 2.43, 7*, 1.0, amb}, 2hg* 2.46 ? {DJW removed}? amb assign (segid="sbm1" and resid 5 and name hn) (segid="sbm1" and resid 1 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 5 and name hn) (segid="sbm2" and resid 1 and name hn) 1.8 0 4.2 {vw, 8.55/8, 4*, 0}, K5chn 8.51, K5ahn 8.57; K5bhn 7.88 vvw cl=0.01 in 3D NOTES 3D NOESY: noesy100-92 51 28 NOE, hn[], D2(pt), ovlp NN,98, could ovlp nn+2 N+2 (hn70/hn71), 98, could ovlp nn N+3 (hn55), 129 N+4 (hn26), 112 Ser 1b (nh-9.95ppm; n= 120.73) hn108 NOTES 3D NOESY: noesy100-115 61 30 no sidechain peaks in 3D TOCSY sc NOEs at 4.33, 2.27, 1.84, 1.73 NN, 98, could ovlp nn+2 N+2 (hn70/hn71) 98 N+3 (hn55) 128 N+4 (hn26) 112 NOTES 4D CN: signals stronger in 4D than 3D as exected in range of H2O Glu 2 MED ; 6125 1 6169 5 parsed_1b4c 1 423 ; {vw, 8.09, *, 0} assign (segid="sbm1" and resid 5 and name hn) (segid="sbm1" and resid 2 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 5 and name hn) (segid="sbm2" and resid 2 and name hn) 1.8 0 4.2 {vw, 8.53, *, 0} {DJW removed} ; 6172 1 6176 39 parsed_1b4c 1 424 ; {m?, 1.89, 8?, 1.0} NOTES 3D NOESY (nh- 8.93ppm; n= 120.7) hn62 noesy100- 202 98 30 NN (hn70), 8.94, could ovlp hn62 NN+2 (hn55) 129 NN+3 (hn24/hn26?), 113 NOTES 4D CN: Y= S1 or F43 Leu 3a MED M assign (segid="sbm1" and resid 5 and name hn) (segid="sbm1" and resid 3 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 5 and name hn) (segid="sbm2" and resid 3 and name hn) 1.8 0 4.2 {vw, 8.55, *, 0} ; 6180 1 6198 27 parsed_1b4c 1 425 ; {m?, 1.68, 10?, 1.5} assign (segid="sbm1" and resid 7 and name he*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 4.2 assign (segid="sbm2" and resid 7 and name he*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 4.2 {vw, 2.09, 2, 4.4, d'} {DJW removed} Leu 3b (nh- 9.01ppm) hn73 NOTES 3D NOESY: noesy100- 194 95 28 NN (hn35) 7.76ppm, vw(9), 142 NOTES 4D CN: could not find Leu 3c (nh- 8.92; n= 121.62) hn71 overlaps L3a in 1H and 15N in 3D Glu 4a MED M assign (segid="sbm1" and resid 0 and name ha) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 0 and name ha) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 {vw, 3.90, 5*, 0, amb} M assign (segid="sbm1" and resid 1 and name hn) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 1 and name hn) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 {vw, 10.24, *3, 0}, this is S1ahn, S1bhn at 9.95 also here R/M assign (segid="sbm1" and resid 2 and name hn) (segid="sbm1" and resid 4 and name hn) 1.8 0 3.2 R/M assign (segid="sbm2" and resid 2 and name hn) (segid="sbm2" and resid 4 and name hn) 1.8 0 3.2 {w, 8.96, 7ov, 0} ; 6202 1 6232 33 parsed_1b4c 1 426 "{w, 4.04, 5ov, 0, amb}" 6236 1 6236 31 parsed_1b4c 1 427 ; {mw?, 2.54, 4?, 1.0} NOTES 3D NOESY: noesy100-273 129 31 NN-1 (hn70/71) 98, could ovlp nn-2 NN-2 (hn62), could ovlp nn-1 Glu 4b (nh- 7.73ppm; n= 118.47) hn35 NOTES 3D NOESY: noesy100- 305 142 33 K5 NN (hn30) 7.89ppm, (~3), ~137 ovlps E4b hn35 NOTES 4D CN: could not find ha=3.33 Lys 5a MED M assign (segid="sbm1" and resid 2 and name hn) (segid="sbm1" and resid 5 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 2 and name hn) (segid="sbm2" and resid 5 and name hn) 1.8 0 4.2 {vw, 8.98, 2*, 0} ; 6240 1 6258 26 parsed_1b4c 1 428 ; {w, 4.04, 3, 0} R assign (segid="sbm1" and resid 3 and name hn) (segid="sbm1" and resid 5 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 3 and name hn) (segid="sbm2" and resid 5 and name hn) 1.8 0 4.2 {vw, 8.98, 3*, 0} ; 6262 1 6266 26 parsed_1b4c 1 429 ; {w, 4.04, 3?, 0} M assign (segid="sbm1" and resid 7 and name hn) (segid="sbm1" and resid 5 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 7 and name hn) (segid="sbm2" and resid 5 and name hn) 1.8 0 4.2 {vw, 8.33, 9*, 0} ; 6270 1 6274 26 parsed_1b4c 1 430 ; {mw?, 2.24, 4, 0} assign (segid="sbm1" and resid 8 and name hg2*) (segid="sbm1" and resid 5 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 8 and name hg2*) (segid="sbm2" and resid 5 and name hn) 1.8 0 4.2 {vw, 1.24, 9*, 2.9, amb} could be v13hg* but seems too far {DJW removed} M assign (segid="sbm1" and resid 8 and name hg1*) (segid="sbm1" and resid 5 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 8 and name hg1*) (segid="sbm2" and resid 5 and name hn) 1.8 0 4.2 {vw, 0.97, 3*, 2.9} NOTES 3D NOESY: noesy100- 233 112 35 (nh- 8.57ppm; n= 117.59) hn24; multiple with hn26 and hn30 A6a NN (hn83) 131, could ovlp nn-1 NN-2 (hn70/71) 97, could ovlp NN-3, not ovlpd in hn70/71 strip NN-3 (hn62) 97, could ovlp NN-2 Lys5c (nh- 8.51ppm; n= 117.59) hn26 3D NOESY: noesy100- 238 114 35 NN-1 (hn55), could ovlp nn NN (hn83) 131, could ovlp nn-1 NN-2 (hn70/71) 98, could ovlp NN-3 NN-3 (hn62) 98, could ovlp NN-2 4D CN: 1.65 may be hd and hg Lys 5b (nh- 7.88ppm; n= 118.15) hn30 NOTES 3D NOESY: noesy100- 292 137 34 Ala 6a MED ; 6278 1 6311 5 parsed_1b4c 1 431 "{w, 4.07, 2ov, 0, ncn}" 6314 1 6314 31 parsed_1b4c 1 432 "{w, 4.07, 2ov, 0, amb}" 6318 1 6318 31 parsed_1b4c 1 433 "{w, 8.06, ?, 0, amb}, above is 4a-hn, 6b-hn sees 4b-hn at 7.74" 6322 1 6322 71 parsed_1b4c 1 434 ; {m?, 1.65, >10?, 1.5, amb}, A6hb* and A9hb* ovlp in both 13c and 1h NOTES 3D NOESY: noesy100- 279 131 26 aN-2 (hn55) 3.3ppm,~304, ovlpd w/another peak Ala 6b (nh- 8.18ppm) hn82 NOTES 3D NOESY: noesy100- 267 126 26 M7 NN (hn8) 8.33ppm, (2), 121 could ovlp V8 nn+2 K5 aN-1 (hn30) 4.01ppm, (2), 280 could ovlp an-3,an-4 V8 NN+2 (hn42) 8.34ppm, (), could ovlp M7 nn L3b aN-3 (hn70/71) 4.01ppm, (2), 280 could ovlp an-1/-4 E2 aN-4 (hn62) 4.01ppm, (2), 280 could ovlp an-1/-3 NOTES 4D CN: could not find Met 7 MED ; 6326 1 6344 5 parsed_1b4c 1 435 "{w?, 4.04, 9?, 0, amb}" 6347 1 6347 31 parsed_1b4c 1 436 "{mw, 3.30, 5, 0}" 6351 1 6351 25 parsed_1b4c 1 437 "{w?, 8.5, 9?, 0, amb}" 6355 1 6355 30 parsed_1b4c 1 438 ; {w, 3.88, 2, 0} R assign (segid="sbm1" and resid 9 and name hn) (segid="sbm1" and resid 7 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 9 and name hn) (segid="sbm2" and resid 7 and name hn) 1.8 0 3.2 {w?, 7.7, 11 ovlp?, 0} dont see 10hb*-7ha b/c 7ha in along carrier, but assigned 7ha-10hb* assign (segid="sbm1" and resid 10 and name hb*) (segid="sbm1" and resid 7 and name he*) 1.8 0 3.2 assign (segid="sbm2" and resid 10 and name hb*) (segid="sbm2" and resid 7 and name he*) 1.8 0 3.2 {w, 2.52, 4, wk cfilt??} for test14d strucs: intramolecular: Average=4.653 Angtroms, stand. dev.=0.4284, min= 4.014, max= 5.361 intermolecular: Average=8.302 Angtroms, stand. dev.=0.5395, min= 7.24, max= 9.299 {DJW removed} NOTES 3D NOESY noesy100- 254 121 39 (nh- 8.33ppm; n= 115.25) hn8 close to hn9[N38], L44d&e V8 NN (hn43) 114, could ovlp K5 nn-2, as well as L44,N38 K5 bN-1 (hn83) 365, ovlps L44hb and hg K5 NN-2 (hn24), could ovlp nn, as well as L44,N38 A9 NN+2 9 (hn81) 140, could ovlp hn[9]N38 nn-1[13] L3 aN-4 (hn70) (9/3), 279, could ovlp other peaks hn9[N38]an-4, ha12[L44a], ha10[L44] NOTES 4D CN same coordinates as N38 ha dispersive in 3D 5 ctrs in 4D go with 3 Val 8a MED M assign (segid="sbm1" and resid 4 and name ha) (segid="sbm1" and resid 8 and name hn) 1.8 0 3.2 M assign (segid="sbm2" and resid 4 and name ha) (segid="sbm2" and resid 8 and name hn) 1.8 0 3.2 {w, 3.28, 2*, 0, amb} ; 6359 1 6393 30 parsed_1b4c 1 439 ; {w, 3.90, 3, 0, amb}, above is for 5a/c-hn, 8b-hn sees 5b-hn at 3.98 R assign (segid="sbm1" and resid 10 and name hn) (segid="sbm1" and resid 8 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 10 and name hn) (segid="sbm2" and resid 8 and name hn) 1.8 0 3.2 {w, 8.33, 7ovlp?, 0} ; 6397 1 6401 30 parsed_1b4c 1 440 ; {m?, 1.67, 8?, 0}, 8 lvls in 3d along 8ha in d1 but only 1 lvl @ d2=ha NOTES 3D NOESY: noesy100- 239 113 33 (nh- 8.50ppm; n= 199.20) hn43 NN-1 (hn8) 8.33, 121, could ovlp NN+2 NN+2 (hn52) 8.29, could ovlp nn-1 aN-3 (hn24) 3.90ppm, ovlps hn40[E67] an-1/an-3, but it's real NOTES 4D CN: V8 is in same cube as E67 Val 8b (nh- 8.34ppm; n= 119.20) hn42, wkr than hn43 NOTES 3D NOESY: noesy100- 253 120 32 NN-1 (hn) 8.33ppm, (),could ovlp hn42 NN+2 (hn65) 8.4ppm, (), could ovlp hn42 Ala 9 MED ; 6405 1 6424 5 parsed_1b4c 1 441 ; {w, 3.93, 1, 0, amb} assign (segid="sbm1" and resid 5 and name hb*) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 5 and name hb*) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 1.97, 9*, 1.0, amb} {DJW removed} assign (segid="sbm1" and resid 6 and name hn) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 6 and name hn) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 8.06, 9*, 0, amb} ; 6427 1 6435 31 parsed_1b4c 1 442 "{mw?, 4.28, 7?, 0, amb}" 6439 1 6439 32 parsed_1b4c 1 443 ; {w, 8.31, 11ovlp?, 0, acd11} assign (segid="sbm1" and resid 7 and name hb*) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 7 and name hb*) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 2.52, 2, 1.0, amb} {DJW removed} ; 6443 1 6447 46 parsed_1b4c 1 444 ; {w, 8.39-44, 8ovlp?, 0, amb} assign (segid="sbm1" and resid 12 and name hb*) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 12 and name hb*) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 2.81, 3*, 1.0, amb} {DJW removed} ; 6451 1 6455 47 parsed_1b4c 1 445 ; {m, 2.81, 11?, 1.0} RS assign (segid="sbm1" and resid 12 and name hb*) (segid="sbm1" and resid 9 and name ha) 1.8 0 1.5 RS assign (segid="sbm2" and resid 12 and name hb*) (segid="sbm2" and resid 9 and name ha) 1.8 0 1.5 {m, 2.90, 11?, 1.0} NOTES 3D NOESY: noesy100- 307 143 27 (nh- 7.71ppm; n= 122.98) hn81 V8a or b NN-1 (hn43) 114, could ovlp nn+2 L10 or b NN (hn52) 8.31ppm,, 122, could ovlp nn-2 M7 NN-2 (hn8) 8.33ppm, could ovlp nn I11 NN+2 (hn65) 8.4ppm, could ovlp nn-1 Leu 10a MED ; 6459 1 6478 5 parsed_1b4c 1 446 "{w, 4.28, 9*, 0, amb}" 6481 1 6481 30 parsed_1b4c 1 447 "{w, 4.80, 6*, 0}" 6485 1 6485 25 parsed_1b4c 1 448 ; {w?, 4.75, 1*, 1.0}, only shows at cl=0.06, but at carrier in D1 and D2 so may be stronger, shows @ D2=2.53 ; 6489 1 6490 44 parsed_1b4c 1 449 ; {m, 4.75, 9, 2.9, no cfilt} amb assign (segid="sbm1" and resid 7 and name he*) (segid="sbm1" and resid 10 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 7 and name he*) (segid="sbm2" and resid 10 and name hd*) 1.8 0 3.2 {w, 2.06, 11, 4.4} mostly due to intermolecular contribution ; 6494 1 6498 69 parsed_1b4c 1 450 "{w, 3.52, 1, 0}" 6502 1 6502 24 parsed_1b4c 1 451 ; {w, 8.50, 10ovlp?, 0, acd11} amb assign (segid="sbm1" and resid 8 and name hg1*) (segid="sbm1" and resid 10 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 8 and name hg1*) (segid="sbm2" and resid 10 and name hn) 1.8 0 3.2 {w, 0.90, 3, 2.9, cn} not in 3D ; 6506 1 6510 40 parsed_1b4c 1 452 "{w, 8.17, 4, 0}" 6514 1 6514 24 parsed_1b4c 1 453 "{m, 2.30, 11?, 0}" 6518 1 6518 26 parsed_1b4c 1 454 ; {d'', w, 2.27, 4, 2.9} assign (segid="sbm1" and resid 13 and name hg*) (segid="sbm1" and resid 10 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 13 and name hg*) (segid="sbm2" and resid 10 and name hn) 1.8 0 4.2 {vw, 1.21, 2, 2.9} RS assign (segid="sbm1" and resid 13 and name hg*) (segid="sbm1" and resid 10 and name hd*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 13 and name hg*) (segid="sbm2" and resid 10 and name hd*) 1.8 0 3.2 {d', w, 1.21, 5, 5.8} ; 6522 1 6530 30 parsed_1b4c 1 455 ; {d'', w, 1.21, 6, 5.8} NOTES 3D NOESY: noesy100- 257 122 32 Leu 10a (nh- 8.29ppm; n= 119.76) hn52; strgr of the pair in the HSQC Leu 10b (nh- 8.26ppm; n= 119.60) hn48 Ile 11a MED ; 6534 1 6545 5 parsed_1b4c 1 456 ; {w, 3.52, 1, 0} assigned 8ha-11hb amb assign (segid="sbm1" and resid 9 and name hn) (segid="sbm1" and resid 11 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid 9 and name hn) (segid="sbm2" and resid 11 and name hn) 1.8 0 ? {w, 7.74, 3, 0} ; 6548 1 6554 24 parsed_1b4c 1 457 ; {w, 4.28, 4*, 0} assigned 11ha-14hb1&2 NOTES 3D NOESY: noesy100- 246 117 29 Ile 11a (nh- 8.44ppm; n= 121.21) hn65 close to hn67 (V13), but wkr than hn67 Ile 11b (nh- 8.39ppm; n= 121.21) hn65a, wkr than hn65 NN (hn) 8.1ppm, (), could be ovlpd NN-1 (hn) 8.2ppm, (), could be ovlpd NOTES 4D CN: too weak Asp 12 MED ; 6558 1 6574 5 parsed_1b4c 1 458 "{w, 3.52, 1, 0, amb}" 6577 1 6577 29 parsed_1b4c 1 459 "{w, 4.28, 2, 0}" 6581 1 6581 24 parsed_1b4c 1 460 "{w, 4.12, 6*, 0, amb}" 6585 1 6585 30 parsed_1b4c 1 461 ; {w, 3.09, 2*, 1.0, amb} NOTES 3D NOESY: noesy100- 269 127 30 Illhb could also be K26hb* (nh- 8.15ppm; n= 120.73) hn64; in NOESY seems to have vw mult peak Val 13 MED ; 6589 1 6600 5 parsed_1b4c 1 462 "{w, 4.28, 6*, 0, amb}" 6603 1 6603 30 parsed_1b4c 1 463 "{m?, 4.12, 6, 0}" 6607 1 6607 25 parsed_1b4c 1 464 "{w, 8.4, ?, 0, note}" 6611 1 6611 29 parsed_1b4c 1 465 ; {w, 3.39, 2, 0, amb} amb/art assign (segid="sbm1" and resid 15 and name hb*) (segid="sbm1" and resid 13 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 15 and name hb*) (segid="sbm2" and resid 13 and name hn) 1.8 0 4.2 {vw, 3.20, 5*, 1.0} ; 6615 1 6619 28 parsed_1b4c 1 466 ; {m?, 2.14, 7?, 1.0} RS assign (segid="sbm1" and resid 16 and name hb*) (segid="sbm1" and resid 13 and name ha) 1.8 0 3.2 RS assign (segid="sbm2" and resid 16 and name hb*) (segid="sbm2" and resid 13 and name ha) 1.8 0 3.2 {w, 2.41, 6?, 1.0} assign (segid="sbm1" and resid 16 and name hb*) (segid="sbm1" and resid 13 and name hg1*) 1.8 0 4.2 assign (segid="sbm2" and resid 16 and name hb*) (segid="sbm2" and resid 13 and name hg1*) 1.8 0 4.2 {vw, 2.34, 3, 2.5}{DJW removed} ; 6623 1 6631 40 parsed_1b4c 1 467 "{w, 2.22, 4, 2.5}" 6635 1 6635 26 parsed_1b4c 1 468 ; {mw, 7.30, 7, 3.9} R assign (segid="sbm1" and resid 17 and name hd*) (segid="sbm1" and resid 13 and name hg*) 1.8 0 3.2 R assign (segid="sbm2" and resid 17 and name hd*) (segid="sbm2" and resid 13 and name hg*) 1.8 0 3.2 {w, 7.30, 4, 3.9} NOTES 3D NOESY (nh- 8.41ppm) hn67 noesy100- 248 118 29 F14 NN (hn50) 8.4ppm, could ovlp w/hn[67]- assumed f14hn-acd I11 NN-2 (hn65) 8.4ppm, could ovlp w/hn[67] NOTES HNH (clvl=0.1): 119.68 (7) F14 and 120.73 D12 Phe 14a Phe 14b MED ; 6639 1 6658 5 parsed_1b4c 1 469 "{w, 4.12, 8?, 0, amb}" 6661 1 6661 30 parsed_1b4c 1 470 "{w, 3.39, 3, 0, ncn}" 6665 1 6665 29 parsed_1b4c 1 471 ; {w?, 3.39, 3?, 1.0, ovlps 14ha} amb assign (segid="sbm1" and resid 11 and name ha) (segid="sbm1" and resid 14 and name hb*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 11 and name ha) (segid="sbm2" and resid 14 and name hb*) 1.8 0 3.2 {w, 3.33, 1, 1.0, ovlps 14ha} amb assign (segid="sbm1" and resid 11 and name hd*) (segid="sbm1" and resid 14 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 11 and name hd*) (segid="sbm2" and resid 14 and name hn) 1.8 0 4.2 {vw, 0.15, 6*, 1.5, amb} amb assign (segid="sbm1" and resid 11 and name hg2*) (segid="sbm1" and resid 14 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 11 and name hg2*) (segid="sbm2" and resid 14 and name hn) 1.8 0 4.2 {vw, 0.18, 6*, 1.5, amb} ; 6669 1 6681 33 parsed_1b4c 1 472 "{w, 8.17, 5*, 0}" 6685 1 6685 26 parsed_1b4c 1 473 ; {w, 8.32, 6, 0} amb/art assign (segid="sbm1" and resid 17 and name hn) (segid="sbm1" and resid 14 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 17 and name hn) (segid="sbm2" and resid 14 and name hn) 1.8 0 4.2 {vw, 7.38, 1*, 0, amb} ; 6689 1 6693 32 parsed_1b4c 1 474 ; {w?, 2.67, ?, 0}, vw pk in 4D NOTES 3D NOESY: noesy100- ~244 117 31 V13 NN-1 ovlps diag D12 NN-2 (hn64) 8.17ppm very weak but seems to be there NOTES 4D CN an-4 or G66 4.15 in 3D and 4.17 in 4D, 13C goes w/G66 not an-4 sofrom another cube ? Phe 14a (nh- 8.47ppm; n= 119.76) hn50 strgr of the pair Phe 14b (nh- 8.43ppm; n= 119.84) hn51 His 15 MED ; 6697 1 6712 5 parsed_1b4c 1 475 "{w, 3.38, 2*, 0}" 6715 1 6715 25 parsed_1b4c 1 476 "{w, 8.4, 7*, 0}" 6719 1 6719 24 parsed_1b4c 1 477 ; {w, 3.82, 2*, 0} 16ha also at 3.82 but looks too far dont see 18hb*-15ha or 15ha-18hb* NOTES 3D NOESY: noesy100- 219 106 35 bN-1 (hn50) 3.14ppm, (4/2), ovlps beta2 NN-2 (hn67) 8.4ppm, could ovlp NN-1 (nh- 8.74ppm; n= 117.42) hn109 - VERY WEAK SIGNAL FOR 3D AND 4D Gln 16 MED ; 6723 1 6737 5 parsed_1b4c 1 478 "{w, 3.82, 3, 0}" 6740 1 6740 24 parsed_1b4c 1 479 ; {w, 1.21, 3, 3.4, ncn} R/amb assign (segid="sbm1" and resid 14 and name hn) (segid="sbm1" and resid 16 and name hn) 1.8 0 ? R/amb assign (segid="sbm2" and resid 14 and name hn) (segid="sbm2" and resid 16 and name hn) 1.8 0 ? {?, 8.4, ?, 0} NOTES 3D NOESY: noesy100- 255 120 27 F14 NN-2 (hn50) 8.4ppm, (),could ovlp diag (nh- 8.32ppm; n= 122.25) hn75; close in 15n/1H to hn74(E72) Tyr 17 MED ; 6744 1 6758 5 parsed_1b4c 1 480 ; {w?, 3.82, 7 ovlp 16ha?, 0, amb} assign (segid="sbm1" and resid 13 and name hg1*) (segid="sbm1" and resid 17 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 13 and name hg1*) (segid="sbm2" and resid 17 and name hn) 1.8 0 4.2 {vw, 1.21, 1, 2.9, amb}{DJW removed} R assign (segid="sbm1" and resid 13 and name hg*) (segid="sbm1" and resid 17 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 13 and name hg*) (segid="sbm2" and resid 17 and name hd*) 1.8 0 3.2 {w, 1.21, 4, 5.1} amb assign (segid="sbm1" and resid 13 and name hg*) (segid="sbm1" and resid 17 and name he*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 13 and name hg*) (segid="sbm2" and resid 17 and name he*) 1.8 0 1.5 {m, 1.21, 10, 5.1} neither 13hg1/2 see 17he* R assign (segid="sbm1" and resid 14 and name ha) (segid="sbm1" and resid 17 and name hb*) 1.8 0 4.2 R assign (segid="sbm2" and resid 14 and name ha) (segid="sbm2" and resid 17 and name hb*) 1.8 0 4.2 {vw, 3.52, 2*, 0} ; 6761 1 6777 26 parsed_1b4c 1 481 ; {w, 5.15, 6*, 0} amb assign (segid="sbm1" and resid 15 and name hb*) (segid="sbm1" and resid 17 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 15 and name hb*) (segid="sbm2" and resid 17 and name hn) 1.8 0 4.2 {vw, 3.20, 4*ov, 1.0, amb} R assign (segid="sbm1" and resid 19 and name hn) (segid="sbm1" and resid 17 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 19 and name hn) (segid="sbm2" and resid 17 and name hn) 1.8 0 4.2 {vw, 8.04, 4*, 0} amb assign (segid="sbm1" and resid 20 and name hn) (segid="sbm1" and resid 17 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 20 and name hn) (segid="sbm2" and resid 17 and name hn) 1.8 0 4.2 {vw, 7.17, 9*ov, amb} 20hn not see 17hn amb assign (segid="sbm1" and resid 20 and name hd*) (segid="sbm1" and resid 17 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 20 and name hd*) (segid="sbm2" and resid 17 and name hn) 1.8 0 4.2 {vw, 3.17, 4* ov?, 1.0}, could be 14hb1 at 3.14, and 15hb1 at 3.20 amb/art assign (segid="sbm1" and resid 20 and name hd*) (segid="sbm1" and resid 17 and name ha) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 20 and name hd*) (segid="sbm2" and resid 17 and name ha) 1.8 0 4.2 {w, 3.14, 3, 1} NOTES 3D NOESY (nh- 7.37ppm; n= 115.73) hn14 noesy100- 336 156 38 aN-2 (hn109) 5.15ppm, other signals are present in 4D CN at 5.1 that aren't H15 NOTES 4D CN aN-1 (hn75) 3.82ppm is only 1 contour not all Y17 peaks optimize at one 15N value Q16hg2 could alos be M79hb1 Ser 18 MED ; 6781 1 6816 5 parsed_1b4c 1 482 "{w, 5.15, 5*, 0}" 6819 1 6819 25 parsed_1b4c 1 483 ; {w, 8.33, 8*, 0} 16hn not see it NOTES 3D NOESY: noesy100- 140 72 29 (nh- 9.64ppm; n= 121.37) hn112 vwk peak, may be multiple seems to have mult peaks in NOESY 9.66, 9.63, 9.60 aN-4 (hn50) 3.49ppm, could ovlp beta NOTES 4D CN - too weak Gly 19 MED assign (segid="sbm1" and resid 15 and name ha) (segid="sbm1" and resid 19 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 15 and name ha) (segid="sbm2" and resid 19 and name hn) 1.8 0 4.2 {vw, 5.15, 5*, 0}{DJW removed for now} assign (segid="sbm1" and resid 17 and name hn) (segid="sbm1" and resid 19 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 17 and name hn) (segid="sbm2" and resid 19 and name hn) 1.8 0 4.2 {vw, 7.38, 4*, 0}{DJW Removed for now} assign (segid="sbm1" and resid 17 and name hb*) (segid="sbm1" and resid 19 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 17 and name hb*) (segid="sbm2" and resid 19 and name hn) 1.8 0 4.2 {w, 2.65, 2*, 1.0, amb} {DJW removed} NOTES 3D NOESY: noesy100- 280 132 51 S18 aN-1 (hn112) 3.9ppm, could ovlp alpha1 (nh- 8.02ppm; n= 107.28) hn1, may be multiple Arg 20 MED assign (segid="sbm1" and resid 17 and name ha) (segid="sbm1" and resid 20 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 17 and name ha) (segid="sbm2" and resid 20 and name hn) 1.8 0 4.2 {vw, 4.15, 6*, 0}, could be 30ha at 4.17, or 21ha at 4.20?? vios w/ sani {DJW removed for now)i amb assign (segid="sbm1" and resid 17 and name ha) (segid="sbm1" and resid 20 and name hb*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 17 and name ha) (segid="sbm2" and resid 20 and name hb*) 1.8 0 3.2 {w, 4.14, 4?, 1.0, amb} amb assign (segid="sbm1" and resid 17 and name ha) (segid="sbm1" and resid 20 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 17 and name ha) (segid="sbm2" and resid 20 and name hd*) 1.8 0 3.2 {w, 4.14, 5, 1.0, amb} NOTES 3D NOESY: noesy100- 353 163 33 (nh- 7.17ppm; n= 118.63) hn38 Glu 21 MED amb assign (segid="sbm1" and resid 17 and name hn) (segid="sbm1" and resid 21 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid 17 and name hn) (segid="sbm2" and resid 21 and name hn) 1.8 0 ? {?, 7.38, 2*, 0} 17hn not see 21hn NOTES 3D NOESY: noesy100- ~302 142/143 38 G22 NN (hn3) 8.3ppm, could ovlp N37 nn (nh- 7.77ppm; n= 115.81) (hn15) - close N37 (hn13) in 1H and 15N Gly 22 MED NOTES 3D NOESY: noesy100- 252 120 48 NOTES 4D CN (nh- 8.35ppm; n= 109.13) hn3 E21hb1 could also be K55hb1,E91hb1,K5hb*,M57hb2 E21hb2 could also be K55hb2,E91hb2,V52hb,V53hb,V80hb E21hg* could also be E46hg*,E49hg2 Asp 23 MED amb assign (segid="sbm1" and resid 26 and name hg*) (segid="sbm1" and resid 23 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 26 and name hg*) (segid="sbm2" and resid 23 and name hn) 1.8 0 4.2 {vw, 1.51, ~6*, 1.0, amb} 26g1 sees it RS assign (segid="sbm1" and resid 26 and name hg*) (segid="sbm1" and resid 23 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 26 and name hg*) (segid="sbm2" and resid 23 and name hn) 1.8 0 4.2 {vw, 1.26, 3*, 1.0,} amb/art? assign (segid="sbm1" and resid 21 and name hb*) (segid="sbm1" and resid 23 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 21 and name hb*) (segid="sbm2" and resid 23 and name hn) 1.8 0 4.2 {vw, ~1.9, 5*, 1.0, amb}, could be to R20hb* also but do not think so NOTES 3D NOESY (nh- 8.61ppm; n= 125.47) hn86 noesy100- 229 110 23 NN (hn) 8.57ppm, could ovlp hn86 NOTES 4D CN: Close to O1 in D1, so signal not so good Lys 24 MED assign (segid="sbm1" and resid 26 and name hn) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 26 and name hn) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 7.71, 4*, 0, amb}{DJW removed} NOTES 3D NOESY: noesy100- 232 111 22 NN-1 (hn86) 8.6ppm,could ovlp hn106 beta-N-1 (hn86) ovlps hn86 (D23) from 15N plane one up NOTES 4D CN: ha only sidechain atom of K24 present His 25 MED amb assign (segid="sbm1" and resid 23 and name hb*) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 23 and name hb*) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 2.71, 8*, 1.0, amb} amb assign (segid="sbm1" and resid 23 and name hb*) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 23 and name hb*) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 2.62, 8*, 1.0, amb} NOTES 3D NOESY: noesy100- 184 90 35 (nh- 9.14ppm; n= 117.50) hn25 close to hn21 (E51) in 1H and 15N K26 (NN) 7.71ppm, could ovlp E21(n-2) from next 15N plane, so use 6 ctrs vs. 9 8.57/7.11 are dispersive so intensity may be reduced 6.78/7.11 correspond to Q16 he22 and he21, both are present in 200 ms NOESY NOTES 4D CN: ha 7 ctrs in 4D 1 in 3D go with 4 ctrs Lys 26 MED amb assign (segid="sbm1" and resid 21 and name hb*) (segid="sbm1" and resid 26 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 21 and name hb*) (segid="sbm2" and resid 26 and name hn) 1.8 0 4.2 {vw, 1.89, 2, 1.0, amb} not sure peak is real amb assign (segid="sbm1" and resid 23 and name hb*) (segid="sbm1" and resid 26 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 23 and name hb*) (segid="sbm2" and resid 26 and name hn) 1.8 0 4.2 {vw, 2.73, 3, 1.0, amb} 23hb1 does not see pk at 7.7, but only assignment makes sense amb/art assign (segid="sbm1" and resid 23 and name hb*) (segid="sbm1" and resid 26 and name ha) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 23 and name hb*) (segid="sbm2" and resid 26 and name ha) 1.8 0 4.2 {w, 2.72, 3, 1.0}, 23hb1 not see 26ha amb assign (segid="sbm1" and resid 23 and name hb*) (segid="sbm1" and resid 26 and name hg*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 23 and name hb*) (segid="sbm2" and resid 26 and name hg*) 1.8 0 4.2 {vw, 2.72, 1, 2.0} amb/RS assign (segid="sbm1" and resid 23 and name hb*) (segid="sbm1" and resid 26 and name hn) 1.8 0 4.2 amb/RS assign (segid="sbm2" and resid 23 and name hb*) (segid="sbm2" and resid 26 and name hn) 1.8 0 4.2 {vw, 2.6, ~8*, 1.0, amb} amb assign (segid="sbm1" and resid 23 and name hb*) (segid="sbm1" and resid 26 and name hb*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 23 and name hb*) (segid="sbm2" and resid 26 and name hb*) 1.8 0 3.2 {w, 2.63, 4, 2.0, amb rcp} ; 6823 1 6993 35 parsed_1b4c 1 484 ; {vw, 4.26, 1, 0, amb} NOTES 3D: noesy100- 309 144 35 H25 (NN-1) 9.17ppm, (9), 90, could also be F70; F70 has 7.11/7.30 NOTES 4D CN hb could also ovlp I11hb,Ihb hd 5 at H=596, 3 at H=595, split difference and use 4 contours hg1 could ovlp K5,K28,K55 hg2 could ovlp K33,K48 hd* could ovlp K48hd* NOTES 13C NOESY: 23hb1-26ha could also be 69hb2 (commented out above), but probably to 23hb1 33ha-26hb* could also be from s18b* or v8(ab)ha; viol!- now think above is 33ha-36hb, 36hb & K26hb* overlap 23hb1-26hg2 could also be intra to 26he2, which may be at 2.72(42.07) Leu 27 MED amb/SD assign (segid="sbm1" and resid 29 and name ha) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 amb/SD assign (segid="sbm2" and resid 29 and name ha) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 3.76, 1, 2.9} assign (segid="sbm1" and resid 31 and name ha) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 assign (segid="sbm2" and resid 31 and name ha) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 4.37, 2, 2.9}{DJW removed} ; 6997 1 7024 40 parsed_1b4c 1 485 ; {w, 2.49, 5, 3.9} RS assign (segid="sbm1" and resid 31 and name hb*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 31 and name hb*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 3.2 {w, 2.06, 5, 3.9} amb assign (segid="sbm1" and resid 31 and name hg*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 31 and name hg*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 3.2 {w, 2.27, 3, 3.9} ; 7028 1 7036 26 parsed_1b4c 1 486 ; {m, 4.00, 8, 2.9} assign (segid="sbm1" and resid 32 and name hb*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 3.2 assign (segid="sbm2" and resid 32 and name hb*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 3.2 {w, 1.28, 6, 3.9} {DJW removed} R assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 1.5 {m, 0.36, 10, 5.8} NOTES 3D NOESY: noesy100- 223 107 31 ha missing in 3D; very weak in 200ms NOTES 4D NOESY: too weak, in solvent ridge Lys 28 MED assign (segid="sbm1" and resid 31 and name hb*) (segid="sbm1" and resid 28 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 31 and name hb*) (segid="sbm2" and resid 28 and name hn) 1.8 0 3.2 {w, 2.52, 6&3, 1.0, cn} {DJW removed} RS assign (segid="sbm1" and resid 31 and name hb*) (segid="sbm1" and resid 28 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 31 and name hb*) (segid="sbm2" and resid 28 and name hn) 1.8 0 4.2 {vw?, 2.05, 4ov?/2, 1.0, cn} assign (segid="sbm1" and resid 31 and name hg*) (segid="sbm1" and resid 28 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 31 and name hg*) (segid="sbm2" and resid 28 and name hn) 1.8 0 3.2 {w?, 2.35, 9ov/4, 0, cn} {DJW removed} assign (segid="sbm1" and resid 31 and name hn) (segid="sbm1" and resid 28 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 31 and name hn) (segid="sbm2" and resid 28 and name hn) 1.8 0 4.2 {vw, 7.00, 7*, 0, amb}{DJW removed} assign (segid="sbm1" and resid 32 and name hn) (segid="sbm1" and resid 28 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 32 and name hn) (segid="sbm2" and resid 28 and name hn) 1.8 0 4.2 {vw, 8.42, 4*, 0, amb}, might be G22hn or E67hn but dont think so {DJW removed} assign (segid="sbm1" and resid 32 and name ha) (segid="sbm1" and resid 28 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 32 and name ha) (segid="sbm2" and resid 28 and name hn) 1.8 0 4.2 {vw, 4.01, 5*ov, 0, amb}{DJW removed} NOTES 3D NOESY: noesy100- 179 88 24 NN (hn89) 9.15ppm, vw(7), 91, nearly ovlps hn85 NOTES 4D CN: L27 an >10 in 4D vw in 3D go with 5 ctrs Lys 29 MED art? assign (segid="sbm1" and resid 27 and name hn) (segid="sbm1" and resid 29 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 27 and name hn) (segid="sbm2" and resid 29 and name hn) 1.8 0 4.2 {vw, 8.66, 2*, 0} ; 7040 1 7095 26 parsed_1b4c 1 487 ; {vw, 7.00, 1*, 0, amb} assign (segid="sbm1" and resid 31 and name hb*) (segid="sbm1" and resid 29 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 31 and name hb*) (segid="sbm2" and resid 29 and name hn) 1.8 0 4.2 {vw, 2.54, 7*, 1.0, amb}{DJW removed} assign (segid="sbm1" and resid 32 and name hn) (segid="sbm1" and resid 29 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 32 and name hn) (segid="sbm2" and resid 29 and name hn) 1.8 0 4.2 {vw, 8.42, 4*, 0, amb}{DJW removed} assign (segid="sbm1" and resid 32 and name hb*) (segid="sbm1" and resid 29 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 32 and name hb*) (segid="sbm2" and resid 29 and name hn) 1.8 0 3.2 {w, 2.13, 4, 1.0, amb}{DJW removed} assign (segid="sbm1" and resid 32 and name hb*) (segid="sbm1" and resid 29 and name ha) 1.8 0 1.5 assign (segid="sbm2" and resid 32 and name hb*) (segid="sbm2" and resid 29 and name ha) 1.8 0 1.5 {m, 2.15, 8, 1.0}{DJW removed} RS assign (segid="sbm1" and resid 32 and name hb*) (segid="sbm1" and resid 29 and name ha) 1.8 0 3.2 RS assign (segid="sbm2" and resid 32 and name hb*) (segid="sbm2" and resid 29 and name ha) 1.8 0 3.2 {w, 1.35, 5, 1.0} assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 29 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 29 and name hn) 1.8 0 4.2 {vw, 0.94, 5*, 2.9, amb}{DJW removed} NOTES 3D NOESY: noesy100- 188 92 21 NN-1 (hn) ppm, (), ovlps hn89 NOTES 4D CN: ha NOEs fairly strong, the rest are weak NOTES 13C: K29ha close to S41(e)hb at 3.79(61.90) so could have some ambiguity Ser 30 MED art? assign (segid="sbm1" and resid 28 and name hn) (segid="sbm1" and resid 30 and name hn) 1.8 0 3.2 art? assign (segid="sbm2" and resid 28 and name hn) (segid="sbm2" and resid 30 and name hn) 1.8 0 3.2 {w, 9.23, 3, 0} ; 7099 1 7138 24 parsed_1b4c 1 488 "{vw, 4.88, 1, 0, amb}" 7142 1 7142 30 parsed_1b4c 1 489 ; {w?, 2.33, <10/~9, 0, amb} 29hb 2.33 amb assign (segid="sbm1" and resid 28 and name he*) (segid="sbm1" and resid 30 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 28 and name he*) (segid="sbm2" and resid 30 and name hn) 1.8 0 3.2 {w, 3.04, 5/??, 1, amb} R assign (segid="sbm1" and resid 32 and name hn) (segid="sbm1" and resid 30 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 32 and name hn) (segid="sbm2" and resid 30 and name hn) 1.8 0 4.2 {vw, 8.42, 2, 0} assign (segid="sbm1" and resid 33 and name hb*) (segid="sbm1" and resid 30 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 33 and name hb*) (segid="sbm2" and resid 30 and name hn) 1.8 0 4.2 {vw, 1.94, 6*, 1.0, amb} 30ha-33hb1/2 assigned NOTES 3D NOESY: noesy100- 166 83 40 NOTES 4D CN: none of the NOEs to K29 are in the 4D Glu 31 MED assign (segid="sbm1" and resid 27 and name hd*) (segid="sbm1" and resid 31 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 27 and name hd*) (segid="sbm2" and resid 31 and name hn) 1.8 0 3.2 {w, 0.64, 5, 2.4, ncn} ; 7146 1 7173 31 parsed_1b4c 1 490 ; {vw, 9.22, 1, 0} amb assign (segid="sbm1" and resid 28 and name ha) (segid="sbm1" and resid 31 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 28 and name ha) (segid="sbm2" and resid 31 and name hn) 1.8 0 4.2 {vw, 4.93, 2*, 0, amb} RS assign (segid="sbm1" and resid 28 and name hb*) (segid="sbm1" and resid 31 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 28 and name hb*) (segid="sbm2" and resid 31 and name hn) 1.8 0 3.2 {w, 2.35, 3, 1.0, cn} amb assign (segid="sbm1" and resid 28 and name hb*) (segid="sbm1" and resid 31 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid 28 and name hb*) (segid="sbm2" and resid 31 and name hn) 1.8 0 1.7 {m?, 1.73, 11/0, 1.0, amb} K28hb2 or hd* at 1.73, K29hg* at 1.78 - none see pk at 7.00 amb assign (segid="sbm1" and resid 28 and name hg*) (segid="sbm1" and resid 31 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 28 and name hg*) (segid="sbm2" and resid 31 and name hn) 1.8 0 3.2 {w, 1.54, 5, amb} could be 29hd1 1.53 amb assign (segid="sbm1" and resid 28 and name hd*) (segid="sbm1" and resid 31 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 28 and name hd*) (segid="sbm2" and resid 31 and name hn) 1.8 0 3.2 {w?, 1.73, 11/0, amb} K28hb2 or hd* at 1.73, K29hg* at 1.78 - none see pk at 7.00 SD? assign (segid="sbm1" and resid 28 and name he*) (segid="sbm1" and resid 31 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 28 and name he*) (segid="sbm2" and resid 31 and name hn) 1.8 0 4.2 {vw, 3.01, 5*, 1, amb} ; 7177 1 7201 32 parsed_1b4c 1 491 ; {vw, 9.12, 4*, 0} R assign (segid="sbm1" and resid 33 and name hn) (segid="sbm1" and resid 31 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 33 and name hn) (segid="sbm2" and resid 31 and name hn) 1.8 0 4.2 {vw, 8.06, 2, 0, amb}, might be to 65hn or 66hn but dont think so assign (segid="sbm1" and resid 33 and name hb*) (segid="sbm1" and resid 31 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 33 and name hb*) (segid="sbm2" and resid 31 and name hn) 1.8 0 4.2 {vw, 1.92, 6*, 1.0, amb} assign (segid="sbm1" and resid 34 and name hn) (segid="sbm1" and resid 31 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 34 and name hn) (segid="sbm2" and resid 31 and name hn) 1.8 0 4.2 {vw, 6.89, 6*, 0, amb}{DJW removed} ; 7205 1 7217 44 parsed_1b4c 1 492 ; {mw?, 2.29, 13?ovlp, 1.0} amb assign (segid="sbm1" and resid 35 and name hb*) (segid="sbm1" and resid 31 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 35 and name hb*) (segid="sbm2" and resid 31 and name hn) 1.8 0 4.2 {vw, 0.94, 5*, 1.0, n} 32hd2* also at 0.94 but looks too far NOTES 3D NOESY: noesy100- 368 170 25 Leu 32 MED assign (segid="sbm1" and resid 27 and name hb*) (segid="sbm1" and resid 32 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 27 and name hb*) (segid="sbm2" and resid 32 and name hn) 1.8 0 3.2 {w, 1.51, 10 ovlp 32hg?, 1.0, amb} pk too stg for 32hg and 27hb1 close in model {DJW removed} assign (segid="sbm1" and resid 27 and name hd*) (segid="sbm1" and resid 32 and name hn) 1.8 0 1.7 assign (segid="sbm2" and resid 27 and name hd*) (segid="sbm2" and resid 32 and name hn) 1.8 0 1.7 {m, 0.64, 9, 3.4, ncn}{could be 35 or 27; DJW removed} assign (segid="sbm1" and resid 27 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 1.5 assign (segid="sbm2" and resid 27 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 1.5 {d', m, 0.57, 8, 5.8}{DJW removed} art? assign (segid="sbm1" and resid 28 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 28 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {w, 1.78, 6, 3.9} ; 7221 1 7249 26 parsed_1b4c 1 493 ; {m?, 3.77, 9&1, 0} R assign (segid="sbm1" and resid 29 and name ha) (segid="sbm1" and resid 32 and name hb*) 1.8 0 3.2 R assign (segid="sbm2" and resid 29 and name ha) (segid="sbm2" and resid 32 and name hb*) 1.8 0 3.2 {w, 3.76, 3, 1.0} ; 7253 1 7257 26 parsed_1b4c 1 494 ; {d'', w, 3.76, 4, 2.9} art? assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 1.49, 6, 3.9} ; 7261 1 7265 31 parsed_1b4c 1 495 "{w, 9.37, 7*, 0}" 7269 1 7269 26 parsed_1b4c 1 496 ; {w, 4.17, 7*, 0, amb} assign (segid="sbm1" and resid 35 and name hn) (segid="sbm1" and resid 32 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 35 and name hn) (segid="sbm2" and resid 32 and name hn) 1.8 0 4.2 {vw, 8.20, 8*, 0, amb}{DJW removed} 35hb1/2-32ha weak @ d2=4.01, 32ha - 35hb1&2 assigned as w assign (segid="sbm1" and resid 35 and name hb*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 assign (segid="sbm2" and resid 35 and name hb*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d', w, 0.93, 6, 3.9}{DJW removed} amb/R assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 amb/R assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d', w, 0.57, 7, 5.8} art? assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 0.57, 8, 5.8} off in 13C cs and does not look real amb assign (segid="sbm1" and resid 36 and name ha) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 36 and name ha) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 3.19, 4, 2.9} looks far, but peak looks real, probably 36hg2* to 40hd1* ; 7273 1 7295 90 parsed_1b4c 1 497 ; {d', m, 0.50, 8, 4.4} R assign (segid="sbm1" and resid 36 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 36 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w?, 0.59, 8, 4.4} could be some contribution as 36hd* to 40hd1* amb assign (segid="sbm1" and resid 36 and name hg2*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 36 and name hg2*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w?, 0.78, 6, 4.4} 2 lvls with LP, probably 36ha to 40hd1* NOTES 3D NOESY: noesy100- 249 118 27 Lys 33 MED ; 7299 1 7316 5 parsed_1b4c 1 498 ; {w, 3.79, 3ov, 0} amb assign (segid="sbm1" and resid 29 and name hb*) (segid="sbm1" and resid 33 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 29 and name hb*) (segid="sbm2" and resid 33 and name hn) 1.8 0 3.2 {w, 2.35, 8, 1, ncn} could be 56hb also SD assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 33 and name hn) 1.8 0 4.2 SD assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 33 and name hn) 1.8 0 4.2 {vw, 1.07, 2*, 1.0, amb} ; 7319 1 7327 33 parsed_1b4c 1 499 "{mw?, 4.17, 6, 0}" 7331 1 7331 26 parsed_1b4c 1 500 ; {mw, 4.17, 5, 1.0} RS assign (segid="sbm1" and resid 30 and name ha) (segid="sbm1" and resid 33 and name hb*) 1.8 0 4.2 RS assign (segid="sbm2" and resid 30 and name ha) (segid="sbm2" and resid 33 and name hb*) 1.8 0 4.2 {vw, 4.17, 2, 1.0} ; 7335 1 7339 27 parsed_1b4c 1 501 ; {w?, 7.0, ?, 0, amb} assign (segid="sbm1" and resid 31 and name hb*) (segid="sbm1" and resid 33 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 31 and name hb*) (segid="sbm2" and resid 33 and name hn) 1.8 0 4.2 {vw, 2.52, 1, 1.0, amb}{DJW removed} 33ha-36hb assigned, and 36hb-33ha also seen as weak amb assign (segid="sbm1" and resid 36 and name hg2*) (segid="sbm1" and resid 33 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 36 and name hg2*) (segid="sbm2" and resid 33 and name hn) 1.8 0 4.2 {vw, 0.80, 1, 1.5, n, amb} NOTES 3D NOESY: noesy100- 278 131 31 NN-2 (hn84) 7.0ppm, (), could ovlp NN Glu 34 MED ; 7343 1 7363 5 parsed_1b4c 1 502 "{w, 4.17, 4*, 0, amb}" 7366 1 7366 30 parsed_1b4c 1 503 "{w, 4.31, 3, 0}" 7370 1 7370 25 parsed_1b4c 1 504 "{b'', w, 4.33, ?, 1.0}" 7374 1 7374 31 parsed_1b4c 1 505 "{w, 8.42, 8*, 0}" 7378 1 7378 26 parsed_1b4c 1 506 ; {w, 3.98, 2, 0, cn} R assign (segid="sbm1" and resid 36 and name hn) (segid="sbm1" and resid 34 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 36 and name hn) (segid="sbm2" and resid 34 and name hn) 1.8 0 4.2 {vw, 8.58, 9*, 0, amb} assign (segid="sbm1" and resid 36 and name hg1*) (segid="sbm1" and resid 34 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 36 and name hg1*) (segid="sbm2" and resid 34 and name hn) 1.8 0 4.2 {vw, 0.78, 6*, 2.5, amb} 3hd2* at 0.78 looks too far {DJW removed} amb assign (segid="sbm1" and resid 36 and name hb/g11) (segid="sbm1" and resid 34 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 36 and name hb/g11) (segid="sbm2" and resid 34 and name hn) 1.8 0 4.2 {vw, ~1.75, 9*, 1.5, amb} assign (segid="sbm1" and resid 36 and name hd*) (segid="sbm1" and resid 34 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 36 and name hd*) (segid="sbm2" and resid 34 and name hn) 1.8 0 4.2 {vw, 0.61, 8*, 1.5, amb} 35hd1* at 0.61 looks too far SD? {DJW removed} assign (segid="sbm1" and resid 37 and name hb*) (segid="sbm1" and resid 34 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 37 and name hb*) (segid="sbm2" and resid 34 and name hn) 1.8 0 4.2 {vw, 2.71, 6*, 1.0, amb}{DJW removed} 34ha-37hb1/2 assigned NOTES 3D NOESY: noesy100- 375 173 34 Leu 35 MED ; 7382 1 7413 5 parsed_1b4c 1 507 "{mw?, 4.01, >10&5, 0, cn}" 7416 1 7416 34 parsed_1b4c 1 508 "{b', mw, 4.04, 4, 1.0}" 7420 1 7420 31 parsed_1b4c 1 509 ; {b'', w, 4.04, 3, 0} SD? assign (segid="sbm1" and resid 32 and name ha) (segid="sbm1" and resid 35 and name hd*) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 32 and name ha) (segid="sbm2" and resid 35 and name hd*) 1.8 0 4.2 {d', vw, 3.97, 1, 2.9} assign (segid="sbm1" and resid 32 and name ha) (segid="sbm1" and resid 35 and name hd*) 1.8 0 3.2 assign (segid="sbm2" and resid 32 and name ha) (segid="sbm2" and resid 35 and name hd*) 1.8 0 3.2 {d'', w, 3.97, 5, 2.9}{DJW removed} SD assign (segid="sbm1" and resid 32 and name hb*) (segid="sbm1" and resid 35 and name hn) 1.8 0 4.2 SD assign (segid="sbm2" and resid 32 and name hb*) (segid="sbm2" and resid 35 and name hn) 1.8 0 4.2 {vw, 1.37, 6*, 1.0, amb} ; 7424 1 7436 33 parsed_1b4c 1 510 ; {d', m, 1.14, 9, 5.8} RS assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 1.5 RS assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 1.5 {d'', m, 1.14, 9, 5.8} ; 7440 1 7444 31 parsed_1b4c 1 511 ; {w, 8.06, 5, 0} assign (segid="sbm1" and resid 33 and name hb*) (segid="sbm1" and resid 35 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 33 and name hb*) (segid="sbm2" and resid 35 and name hn) 1.8 0 4.2 {vw, 1.94, 2, 1.0, n, amb}{DJW removed} assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 35 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 35 and name hn) 1.8 0 3.2 {w, 1.21, 6/?*, 2.9, ncn}, V13hg** could contribute {DJW removed} ; 7448 1 7456 74 parsed_1b4c 1 512 ; {vw, 7.81, 8*, 0, amb} amb assign (segid="sbm1" and resid 37 and name hb*) (segid="sbm1" and resid 35 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 37 and name hb*) (segid="sbm2" and resid 35 and name hn) 1.8 0 4.2 {vw, 2.71, 9*, 1.0, amb} ; 7460 1 7464 33 parsed_1b4c 1 513 ; {w, 2.81, 3, 1.0}, 2.81/40.0 vw @ D2=3.57 amb assign (segid="sbm1" and resid 39 and name hb*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 39 and name hb*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 3.2 {d', w, 1.71, 6, 3.9, amb} SD/art? assign (segid="sbm1" and resid 39 and name hg*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 4.2 SD/art? assign (segid="sbm2" and resid 39 and name hg*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 4.2 {d', vw, 2.70, 1, 3.9} assign (segid="sbm1" and resid 39 and name hg*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 3.2 assign (segid="sbm2" and resid 39 and name hg*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 3.2 {d', w, 2.27, 4}{DJW removed} NOTES 3D NOESY: noesy100- 268 127 28 NOTES 4D CN L32ha could also be L44, M57, E91 ha's L35ha could also overlap Q50ha, Q71ha L35bn-1 could overlap E49hb1, E72hb1 Ile 36 MED ; 7468 1 7494 5 parsed_1b4c 1 514 ; {w, 4.01, 5?, 0, amb} assign (segid="sbm1" and resid 32 and name hg) (segid="sbm1" and resid 36 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 32 and name hg) (segid="sbm2" and resid 36 and name hn) 1.8 0 4.2 {vw, 1.51, 8*, 0, amb} 27hb1 also at 1.51 but looks too far assign (segid="sbm1" and resid 32 and name hg) (segid="sbm1" and resid 36 and name hd*) 1.8 0 3.2 assign (segid="sbm2" and resid 32 and name hg) (segid="sbm2" and resid 36 and name hd*) 1.8 0 3.2 {w, 1.42, 6, 1.5}{DJW removed} assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 36 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 36 and name hn) 1.8 0 3.2 {w, 1.21, 4, 2.9}, could be V13hg** but looks too far {DJW removed} ; 7497 1 7509 77 parsed_1b4c 1 515 "{m, 1.21, 9, 4.4}" 7513 1 7513 26 parsed_1b4c 1 516 "{mw, 3.49, 5?, 0, amb}" 7517 1 7517 31 parsed_1b4c 1 517 ; {w, 3.52, 3, 1.0} amb assign (segid="sbm1" and resid 33 and name ha) (segid="sbm1" and resid 36 and name hd*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 33 and name ha) (segid="sbm2" and resid 36 and name hd*) 1.8 0 1.5 {m?, 3.48, 10?ridge, 1.5} art? assign (segid="sbm1" and resid 33 and name he*) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 33 and name he*) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 3.2 {w, 2.91, 5, 2.5} ; 7521 1 7529 26 parsed_1b4c 1 518 ; {w, 6.89, 2, 0} amb assign (segid="sbm1" and resid 34 and name ha) (segid="sbm1" and resid 36 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 34 and name ha) (segid="sbm2" and resid 36 and name hn) 1.8 0 3.2 {w, 4.04, 5?, 0, amb} ; 7533 1 7537 30 parsed_1b4c 1 519 ; {w, 8.33, 4, 0, amb} amb assign (segid="sbm1" and resid 39 and name hb*) (segid="sbm1" and resid 36 and name ha) 1.8 0 3.2 amb assign (segid="sbm2" and resid 39 and name hb*) (segid="sbm2" and resid 36 and name ha) 1.8 0 3.2 {w?, 1.78, 8?, 1.0}, lots possibilities for 1.78 assign (segid="sbm1" and resid 40 and name hg) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 4.2 assign (segid="sbm2" and resid 40 and name hg) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 4.2 {vw, 1.42, 2, 1.5}{DJW removed} amb/R assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 1.5 amb/R assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 1.5 {m, 0.85, 12, 4.4, med cfilt} NOTES 3D NOESY: noesy100- 235 112 29 NOTES 4D CN: V56hg2 signal doesn't max at H=522 Asn 37 MED ; 7541 1 7563 5 parsed_1b4c 1 520 ; {w, 3.49, 2?, 0, amb} art? assign (segid="sbm1" and resid 33 and name hg*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 33 and name hg*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 1.43, 2*, 1.0, amb} assign (segid="sbm1" and resid 33 and name hg*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 33 and name hg*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 1.21, 2, 1.0, amb}{DJW Removed} assign (segid="sbm1" and resid 34 and name hn) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 34 and name hn) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 6.95, 4*, 0, amb}{DJW removed} ; 7566 1 7578 44 parsed_1b4c 1 521 "{m, 4.01, 8, 0, amb}" 7582 1 7582 29 parsed_1b4c 1 522 ; {mw, 4.04, 5, 1.0} RS assign (segid="sbm1" and resid 34 and name ha) (segid="sbm1" and resid 37 and name hb*) 1.8 0 4.2 RS assign (segid="sbm2" and resid 34 and name ha) (segid="sbm2" and resid 37 and name hb*) 1.8 0 4.2 {vw, 4.04, 1, 1.0} ; 7586 1 7590 27 parsed_1b4c 1 523 "{w, 8.17, 2, 0}" 7594 1 7594 24 parsed_1b4c 1 524 ; {vw, 9.15, 8*, 0} amb assign (segid="sbm1" and resid 39 and name hg*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 39 and name hg*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 2.33, 9*, 1.0}, could be 34hb1 at 2.33, M57hb1 2.33, V56hb 2.35 see no evidence for 40hb*-37ha or vice versa assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 0.90, 2, 2.9, cn}, could be other(?) L3hd1* at 0.93/26.8 {DJW removed} NOTES 3D NOESY: noesy100- 300 141 38 Asn 38 MED ; 7598 1 7618 5 parsed_1b4c 1 525 "{w, 4.04, 8?, 0, amb}" 7621 1 7621 30 parsed_1b4c 1 526 ; {mw, 3.57, 5, 0} 38hb2 to 35ha assigned amb assign (segid="sbm1" and resid 36 and name ha) (segid="sbm1" and resid 38 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 36 and name ha) (segid="sbm2" and resid 38 and name hn) 1.8 0 4.2 {vw, 3.22, ?, 0, amb} ; 7625 1 7631 30 parsed_1b4c 1 527 ; {w, 8.53, 6, 0, amb} NOTES 3D NOESY: noesy100- 255 121 39 NOTES 4D CN: N37ha could also be E21ha no good evidence for 35ha-38hb1/2 NOE, but assigned 38hb2-35ha dont see 41hb*-38ha or vice versa, could be b/c 38ha at carrier frequencey Glu 39 MED ; 7635 1 7647 5 parsed_1b4c 1 528 ; {w, 3.58, 2, 0, ncn} assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 39 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 39 and name hn) 1.8 0 3.2 {w, 0.61, 3, 2.9, n, amb}{DJW removed} ; 7650 1 7654 47 parsed_1b4c 1 529 ; {vw, 3.22, 1, 0} amb/sani assign (segid="sbm1" and resid 36 and name hn) (segid="sbm1" and resid 39 and name hn) 1.8 0 4.2 amb/sani assign (segid="sbm2" and resid 36 and name hn) (segid="sbm2" and resid 39 and name hn) 1.8 0 4.2 {vw, 8.58, 6*, 0} not sure 36hn sees 39hn R assign (segid="sbm1" and resid 37 and name hn) (segid="sbm1" and resid 39 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 37 and name hn) (segid="sbm2" and resid 39 and name hn) 1.8 0 3.2 {w, 7.78, 9ovlp/2?, 0} R assign (segid="sbm1" and resid 41 and name hn) (segid="sbm1" and resid 39 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 41 and name hn) (segid="sbm2" and resid 39 and name hn) 1.8 0 4.2 {vw, 6.70, 8*, 0} 3D NOESY: noesy100- 184 90 39 4D CN: hb1? Wk signal at 2.41, 30.32 which could ovlp hg2 in 3D 13C: 39hb*-36ha assigned, dont see 36ha-39hb* Leu 40 - MED amb/SD? assign (segid="sbm1" and resid 35 and name ha) (segid="sbm1" and resid 40 and name hn) 1.8 0 4.2 amb/SD? assign (segid="sbm2" and resid 35 and name ha) (segid="sbm2" and resid 40 and name hn) 1.8 0 4.2 {vw, 3.58, 3*, amb}, could be 42d-hb1 assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 40 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 40 and name hn) 1.8 0 3.2 {w, 0.64, 5}{DJW removed} SD? assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 40 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 40 and name hn) 1.8 0 4.2 {vw, 0.39, 5*} ; 7658 1 7691 23 parsed_1b4c 1 530 "{w, 0.57, 8}" 7695 1 7695 21 parsed_1b4c 1 531 "{w, 3.22, 5&2, ncn}" 7699 1 7699 28 parsed_1b4c 1 532 ; {d', m, 3.19, 9} assign (segid="sbm1" and resid 36 and name hg2*) (segid="sbm1" and resid 40 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 36 and name hg2*) (segid="sbm2" and resid 40 and name hn) 1.8 0 4.2 {vw, 0.77, 9ov/2, ncn}{DJW removed} assign (segid="sbm1" and resid 36 and name hg2*) (segid="sbm1" and resid 40 and name hd*) 1.8 0 1.5 assign (segid="sbm2" and resid 36 and name hg2*) (segid="sbm2" and resid 40 and name hd*) 1.8 0 1.5 {d<, m, 0.71, 6/11 w/o LP}{DJW removed} ; 7703 1 7711 48 parsed_1b4c 1 533 ; {vw, 4.20, 9*ov, 0, ncn} amb? assign (segid="sbm1" and resid 38 and name hn) (segid="sbm1" and resid 40 and name hn) 1.8 0 4.2 amb? assign (segid="sbm2" and resid 38 and name hn) (segid="sbm2" and resid 40 and name hn) 1.8 0 4.2 {vw, 8.33, 2, 0}, too many choices close by SD? assign (segid="sbm1" and resid 38 and name hb*) (segid="sbm1" and resid 40 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 38 and name hb*) (segid="sbm2" and resid 40 and name hn) 1.8 0 4.2 {vw, 3.06, 6*, 1.0, amb} R assign (segid="sbm1" and resid 43 and name hd*) (segid="sbm1" and resid 40 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 43 and name hd*) (segid="sbm2" and resid 40 and name hd*) 1.8 0 3.2 {d'', w, 7.16, 6, 5.4} ; 7715 1 7727 31 parsed_1b4c 1 534 ; {d'', w, 7.38, 3, 5.4} NOTES 3D NOESY: noesy100- 298 139 33 Dont see 40hb*-37ha or 37ha-40hb* Ser 41d MED ; 7731 1 7741 5 parsed_1b4c 1 535 "{vw, 4.20, 6*, 0}, not in 4D, but only assignment that makes sense" 7744 1 7744 75 parsed_1b4c 1 536 ; {vw, 9.18, 5*, 0} dont see 38ha-41hb* NOTES 3D NOESY: noesy100- 394 181 44 (nh- 6.70ppm; n= 111.79) hn97 mult peak with 98/99 Ser 41e (nh- 6.71ppm; n= 112.27) hn98 NOTES 3D NOESY: noesy100- 393 ~181 43 7.41 is dispersive NOTES 4D CN: overlaps Ser 41d Ser 41f (nh- 6.78ppm; n= 112.75) hn99 NOTES 3D NOESY: noesy100- 387 ~178 43 7.41 is dipsersive NOTES 4D CN: Ser41f missing or too weak His 42d MED ; 7748 1 7770 5 parsed_1b4c 1 537 ; {vw, 5.04, 6*, 0} NOTES 3D NOESY: noesy100- 135 70 27 His 42e (nh- 9.57ppm; n= 122.25) hn105 NOTES 3D NOESY: noesy100- 148 75 28 His 42f (nh- 9.46ppm; n= 121.37) hn100 NOTES 3D NOESY: noesy100- 157 79 29 Phe 43d MED ; 7773 1 7788 5 parsed_1b4c 1 538 ; {vw, 5.04, 6*, 0} R assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 43 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 43 and name hd*) 1.8 0 3.2 {w, 0.92, 4} ; 7791 1 7795 21 parsed_1b4c 1 539 "{vw, 0.72, 6*, 2.9}" 7799 1 7799 28 parsed_1b4c 1 540 ; {w, 0.64, 7, 5.4} NOTES 3D NOESY: noesy100- 242 116 25 ha dispersive Phe 43e (nh- 8.33ppm; n= 123.78) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Phe 43f (nh- 8.06ppm; n= 123.22) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Leu 44d MED ; 7803 1 7819 5 parsed_1b4c 1 541 "{m, 0.92, 11, 4.9}" 7822 1 7822 27 parsed_1b4c 1 542 ; {w, 1.00, 4, 3.9} RS assign (segid="sbm1" and resid 47 and name hg1*) (segid="sbm1" and resid 44 and name hd*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 47 and name hg1*) (segid="sbm2" and resid 44 and name hd*) 1.8 0 3.2 {w, 1.77, 4, 3.9} 43hn - 44hn assign weak b/c may overlap w/hn[115] NOTES 3D NOESY: noesy100- ~254 ~120 39 alpha- 4.04 ppm (8) ~279 ovlps N38 an-4[9/31] & M7 an-4[8/70] beta- 1.75 ppm (10) 363 ovlps M7 bn-1[8/83] NN-1 (hn102) 8.50ppm, (9/2), 115 ovlps nn[43] Leu 44e (nh- 8.28ppm; n= 115.41) hn12 NOTES 3D NOESY: noesy100- ~257 ~122 39 NN-1 (hn103) 8.33ppm, (), could ovlp hn12 Leu 44f (nh- 8.15ppm; n= 115.33) hn11 NOTES 3D NOESY: noesy100- 268 ~128 39 NN-1 (hn123)8.06ppm, (5), 131 nearly ovlps hn11 NOTES 4D CN: too weak and overlapped Glu 45 MED amb assign (segid="sbm1" and resid 40 and name hb*) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 40 and name hb*) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 2.05, 1, 1.0, amb}, V80hb at 2.05 also amb assign (segid="sbm1" and resid 42 and name ha) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 42 and name ha) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw?, 4.68/59.6, 5/3*, ncn} M assign (segid="sbm1" and resid 43 and name hn) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid 43 and name hn) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 8.47, 2*, 0} amb/SD? assign (segid="sbm1" and resid 43 and name hd*) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 amb/SD? assign (segid="sbm2" and resid 43 and name hd*) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 7.22, 1, 2.4, amb} amb assign (segid="sbm1" and resid 47 and name hb) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 47 and name hb) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 1.78, 6ov&3, 0, cn} NOTES 3D NOESY: noesy100- 338 157 33 Glu 45e (nh- 7.35ppm; n= 118.63) hn36 NOTES 3D NOESY: noesy100- 338 157 33 NOE to 8.15 verifies that d/f overlap Glu 45f (nh- 7.32ppm; n= 118.63) hn37 NOTES 3D NOESY: noesy100- 340 159 33 NN-2 (hn103) 8.3ppm, (), could ovlp nn-1! Glu 46d Glu 46e Glu 46f MED ; 7826 1 7891 5 parsed_1b4c 1 543 ; {w, 4.07, 5, 0, cn, amb} art/SD? assign (segid="sbm1" and resid 44 and name hn) (segid="sbm1" and resid 46 and name hn) 1.8 0 3.2 art/SD? assign (segid="sbm2" and resid 44 and name hn) (segid="sbm2" and resid 46 and name hn) 1.8 0 3.2 {w, 8.17, 5*, 0, amb}, sees 44f-hn at 8.17 and 44de-hn at 8.28/31 ; 7894 1 7898 74 parsed_1b4c 1 544 ; {w, 0.75, 2, 3.4} could be 47hg2* also NOTES 3D NOESY: noesy100- 313 ~146 32 NN (hn116) 7.82ppm, (8/2), ~140 nearly ovlps hn45 beta-N-1 (hn36) 2.22ppm, (10/2), could ovlp beta Ile 47 MED ; 7902 1 7914 5 parsed_1b4c 1 545 ; {w, 4.04, 7} R assign (segid="sbm1" and resid 44 and name hd*) (segid="sbm1" and resid 47 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 44 and name hd*) (segid="sbm2" and resid 47 and name hd*) 1.8 0 1.5 {m, 0.71, 11} ; 7917 1 7921 22 parsed_1b4c 1 546 ; {w, 0.71, ~5} R assign (segid="sbm1" and resid 49 and name hn) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 1.5 R assign (segid="sbm2" and resid 49 and name hn) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 1.5 {m, 7.68, 6} art/SD? assign (segid="sbm1" and resid 49 and name ha) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 4.2 art/SD? assign (segid="sbm2" and resid 49 and name ha) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 4.2 {vw, 4.75, 1} amb assign (segid="sbm1" and resid 49 and name hg*) (segid="sbm1" and resid 47 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 49 and name hg*) (segid="sbm2" and resid 47 and name hd*) 1.8 0 4.2 {vw, 2.06, 2} looks too far ; 7925 1 7937 36 parsed_1b4c 1 547 "{m?, 3.62, >>10}" 7941 1 7941 25 parsed_1b4c 1 548 ; {w, 2.13, 7} RS assign (segid="sbm1" and resid 50 and name hb*) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 50 and name hb*) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 3.2 {w, 1.92, 5} assign (segid="sbm1" and resid 50 and name hg*) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 4.2 assign (segid="sbm2" and resid 50 and name hg*) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 4.2 {vw, 2.34/33.1, 2}{DJW removed} NOTES 3D NOESY: noesy100-302 141 28 (values from HOHAHA-HSQC) hn too weak to observe in 3D or 4D Ile 47e? (nh- 7.81ppm) N= 122.25 hn116 very weak peak NOTES 4D CN: too weak Lys 48 nitrogen data too weak INTRA SEQ MED LONG INTER AMB NOTES 3D NOESY: noesy100- 217 105 20 an-1 and he could overlap NOTES 4D CN: too weak Glu 49 MED ; 7945 1 7990 5 parsed_1b4c 1 549 "{w, 3.96, 5}" 7993 1 7993 21 parsed_1b4c 1 550 ; {s, 0.75, 12} amb assign (segid="sbm1" and resid 47/53 and name hd/g2*) (segid="sbm1" and resid 49 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 47/53 and name hd/g2*) (segid="sbm2" and resid 49 and name hn) 1.8 0 3.2 {w, ~0.97?, 3, 1.5} amb assign (segid="sbm1" and resid 52 and name hn) (segid="sbm1" and resid 49 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 52 and name hn) (segid="sbm2" and resid 49 and name hn) 1.8 0 4.2 {vw, 7.05, 5*, 0, amb - side peak} amb assign (segid="sbm1" and resid 53 and name hg2*) (segid="sbm1" and resid 49 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 53 and name hg2*) (segid="sbm2" and resid 49 and name hn) 1.8 0 3.2 {w, 0.90-7?, 3, 1.5} NOTES 3D NOESY: noesy100- 304 ~141 31 NN (hn88) 8.5ppm, , ~113 ovlps nn-1 NN-2 (hn116) 7.8ppm, (), could ovlp hn59 NOTES 4D CN: plane overlaps K55, so any NOEs from the CN could be to K55hn Gln 50 MED SD? assign (segid="sbm1" and resid 47 and name ha) (segid="sbm1" and resid 50 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 47 and name ha) (segid="sbm2" and resid 50 and name hn) 1.8 0 4.2 {vw, 3.93, 4*} amb assign (segid="sbm1" and resid 47 and name hg2*) (segid="sbm1" and resid 50 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 47 and name hg2*) (segid="sbm2" and resid 50 and name hn) 1.8 0 4.2 {vw, 0.75, 9*, amb} ; 7997 1 8028 28 parsed_1b4c 1 551 ; {m, 2.11, 9ov?} amb assign (segid="sbm1" and resid 53 and name hg1*) (segid="sbm1" and resid 50 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 53 and name hg1*) (segid="sbm2" and resid 50 and name hn) 1.8 0 4.2 {vw, 0.94, 1, 1.5, amb} 53hg1*(0.96) further but closer in CS than 53hg2*(0.90) art? assign (segid="sbm1" and resid 48 and name hd*) (segid="sbm1" and resid 50 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 48 and name hd*) (segid="sbm2" and resid 50 and name hn) 1.8 0 4.2 {vw, 1.48, 3*, 1.0, amb} ; 8032 1 8040 33 parsed_1b4c 1 552 ; {vw, 7.06, 9*, 0} NOTES 3D NOESY: noesy100- 237 113 22 NOTES 4D CN: close to D23 in H and N, baseline troulbes at N=11, h=515-525 Glu 51 MED assign (segid="sbm1" and resid 47 and name hg2*) (segid="sbm1" and resid 51 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 47 and name hg2*) (segid="sbm2" and resid 51 and name hn) 1.8 0 4.2 {vw, 0.75, 1, 1.5, amb}{DJW removed} amb assign (segid="sbm1" and resid 49 and name hn) (segid="sbm1" and resid 51 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 49 and name hn) (segid="sbm2" and resid 51 and name hn) 1.8 0 3.2 {w, 7.71, 6, 0}, 49hn not see 9.15 and off in CS (49hn at 7.74) ; 8044 1 8061 72 parsed_1b4c 1 553 ; {w, 6.78, 9*, 0} assign (segid="sbm1" and resid 54 and name hn) (segid="sbm1" and resid 51 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 54 and name hn) (segid="sbm2" and resid 51 and name hn) 1.8 0 4.2 {vw, 8.64, 1, 0, amb}{DJW removed} ; 8065 1 8069 43 parsed_1b4c 1 554 ; {w?, 2.65, 14, 1.0} NOTES 3D NOESY: noesy100- 184 90 36 NN-2 (hn59) 7.71ppm, (6), 144 ovlps hn[25]H25 nn[27] beta-N-1 (hn88) 1.9ppm, (), could ovlp beta, beta and beta-1 carbons also overlap Val 52 MED amb assign (segid="sbm1" and resid 49 and name hb*) (segid="sbm1" and resid 52 and name hg2*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 49 and name hb*) (segid="sbm2" and resid 52 and name hg2*) 1.8 0 1.5 {g<, m, 2.06, 13, 3.9} 51hb* probably ovlps and 50hb1 may also RS assign (segid="sbm1" and resid 49 and name hb*) (segid="sbm1" and resid 52 and name hg*) 1.8 0 1.5 RS assign (segid="sbm2" and resid 49 and name hb*) (segid="sbm2" and resid 52 and name hg*) 1.8 0 1.5 {g<, m, 1.92, 11, 3.9} 50hb2 may ovlp assign (segid="sbm1" and resid 49 and name hg*) (segid="sbm1" and resid 52 and name hg2*) 1.8 0 2.4 assign (segid="sbm2" and resid 49 and name hg*) (segid="sbm2" and resid 52 and name hg2*) 1.8 0 2.4 {g<, mw, 2.20, 8ovlp, 3.9}{DJW removed based on ambiguities} ; 8073 1 8095 69 parsed_1b4c 1 555 ; {vw, 8.55, ~5*, 0, amb} assign (segid="sbm1" and resid 50 and name hb*) (segid="sbm1" and resid 52 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 50 and name hb*) (segid="sbm2" and resid 52 and name hn) 1.8 0 4.2 {vw?, 2.16, 6, 1.0, cn} viol for wk asbd9 amb/SD? assign (segid="sbm1" and resid 50 and name hb*) (segid="sbm1" and resid 52 and name hn) 1.8 0 3.2 amb/SD? assign (segid="sbm2" and resid 50 and name hb*) (segid="sbm2" and resid 52 and name hn) 1.8 0 3.2 {w?, 2.03, 8ov, 1.0, cn} R assign (segid="sbm1" and resid 54 and name hn) (segid="sbm1" and resid 52 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 54 and name hn) (segid="sbm2" and resid 52 and name hn) 1.8 0 4.2 {vw, 8.66, 2, 0} assign (segid="sbm1" and resid 54 and name hb*) (segid="sbm1" and resid 52 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 54 and name hb*) (segid="sbm2" and resid 52 and name hn) 1.8 0 4.2 {vw, 2.65, 7*, 1.0, amb}{DJW removed} assign (segid="sbm1" and resid 55 and name hn) (segid="sbm1" and resid 52 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 55 and name hn) (segid="sbm2" and resid 52 and name hn) 1.8 0 4.2 {vw, 7.76, 8*, 0, amb} ; 8099 1 8119 31 parsed_1b4c 1 556 ; {m, 1.96, 9?, 0} amb assign (segid="sbm1" and resid 55 and name hd*) (segid="sbm1" and resid 52 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 55 and name hd*) (segid="sbm2" and resid 52 and name hn) 1.8 0 4.2 {vw, 1.65, 6ov?, 1.0} A83hb* at ~1.65 and it looks much closer amb assign (segid="sbm1" and resid 55 and name hd*) (segid="sbm1" and resid 52 and name hg*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 55 and name hd*) (segid="sbm2" and resid 52 and name hg*) 1.8 0 3.2 {g', w, 1.63, 5, 4.4} could be inter? NOTES 3D NOESY: noesy100- 365 168 34 Val 53 MED art? assign (segid="sbm1" and resid 48 and name hb*) (segid="sbm1" and resid 53 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 48 and name hb*) (segid="sbm2" and resid 53 and name hg2*) 1.8 0 4.2 {vw#, 1.71, 1, 2.5} art? assign (segid="sbm1" and resid 48 and name hd*) (segid="sbm1" and resid 53 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 48 and name hd*) (segid="sbm2" and resid 53 and name hg2*) 1.8 0 4.2 {vw, 1.49, 2, 2.5} ; 8123 1 8147 27 parsed_1b4c 1 557 "{mw, 3.63, 8ov/2, 0, cn} 52ha at 3.63, 50ha at 3.60" 8151 1 8151 60 parsed_1b4c 1 558 ; {w, 3.62, 7, 1.5} art? assign (segid="sbm1" and resid 50 and name hb*) (segid="sbm1" and resid 53 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 50 and name hb*) (segid="sbm2" and resid 53 and name hg2*) 1.8 0 4.2 {vw, 1.92, 2, 2.5} art? assign (segid="sbm1" and resid 50 and name hg*) (segid="sbm1" and resid 53 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 50 and name hg*) (segid="sbm2" and resid 53 and name hg2*) 1.8 0 4.2 {vw, 2.34, 1, 2.5} ; 8155 1 8163 27 parsed_1b4c 1 559 "{w, 9.18, 7*, 0}" 8167 1 8167 25 parsed_1b4c 1 560 ; {w, 4.09, 5*, 0, amb} R assign (segid="sbm1" and resid 55 and name hn) (segid="sbm1" and resid 53 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 55 and name hn) (segid="sbm2" and resid 53 and name hn) 1.8 0 4.2 {vw, 7.79, 7*, 0} amb assign (segid="sbm1" and resid 56 and name hb) (segid="sbm1" and resid 53 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 56 and name hb) (segid="sbm2" and resid 53 and name hn) 1.8 0 4.2 {vw, 2.35, 1, 1.0, cn} 50hg*. 51hg*, 56hb all at 2.35 - 56hb close enough for vw ; 8171 1 8179 89 parsed_1b4c 1 561 "{m?, 2.34, 4, 0} med relative to others" 8183 1 8183 48 parsed_1b4c 1 562 ; {vw, 1.21, 5*, 1.5, amb} assign (segid="sbm1" and resid 57 and name hg*) (segid="sbm1" and resid 53 and name hg1*) 1.8 0 2.4 assign (segid="sbm2" and resid 57 and name hg*) (segid="sbm2" and resid 53 and name hg1*) 1.8 0 2.4 {mw, 2.77/32.9, 7, 2.5}{DJW removed} SD? assign (segid="sbm1" and resid 57 and name he*) (segid="sbm1" and resid 53 and name hg2*) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 57 and name he*) (segid="sbm2" and resid 53 and name hg2*) 1.8 0 4.2 {vw, 2, 1.92, 3.0} NOTES 3D NOESY: noesy100- 387 178 32 beta-N-1 (hn2.0) 2.0ppm, (10/2),could ovlp beta, ovlps in Carbon as well Asp 54 MED ; 8187 1 8204 5 parsed_1b4c 1 563 ; {w, 3.66, 9ov?, 0, amb} 52ha at 3.63 assign (segid="sbm1" and resid 51 and name hn) (segid="sbm1" and resid 54 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 51 and name hn) (segid="sbm2" and resid 54 and name hn) 1.8 0 4.2 {vw, 9.18, 6*, 0, amb}{DJW removed} ; 8207 1 8211 45 parsed_1b4c 1 564 "{m?, 4.09, 10ovlp?, 0}" 8215 1 8215 31 parsed_1b4c 1 565 "{w, 7.06, 4, 0}" 8219 1 8219 24 parsed_1b4c 1 566 ; {w, 3.63, 9ov?, 0, amb} SD? assign (segid="sbm1" and resid 56 and name hg2*) (segid="sbm1" and resid 54 and name hn) 1.8 0 3.2 SD? assign (segid="sbm2" and resid 56 and name hg2*) (segid="sbm2" and resid 54 and name hn) 1.8 0 3.2 {w, 1.24, 4, 0, amb} off in CS shaould be 1.21 for 56hg1* R assign (segid="sbm1" and resid 56 and name hn) (segid="sbm1" and resid 54 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 56 and name hn) (segid="sbm2" and resid 54 and name hn) 1.8 0 4.2 {vw, 8.06, 9*, 0} amb assign (segid="sbm1" and resid 56 and name hb) (segid="sbm1" and resid 54 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 56 and name hb) (segid="sbm2" and resid 54 and name hn) 1.8 0 4.2 {vw?, 2.35, 6ov?, 0, amb} 57hb1 at 2.33 assign (segid="sbm1" and resid 57 and name hn) (segid="sbm1" and resid 54 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 57 and name hn) (segid="sbm2" and resid 54 and name hn) 1.8 0 4.2 {vw, 8.33, 2, 0, amb}{DJW removed} amb assign (segid="sbm1" and resid 57 and name hb*) (segid="sbm1" and resid 54 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 57 and name hb*) (segid="sbm2" and resid 54 and name hn) 1.8 0 4.2 {w?, 2.35, 6ov?, 1.0, amb} 56hb at 2.35 ; 8223 1 8243 48 parsed_1b4c 1 567 ; {m, 2.29, 9, 1.0} RS assign (segid="sbm1" and resid 57 and name hb*) (segid="sbm1" and resid 54 and name ha) 1.8 0 4.2 RS assign (segid="sbm2" and resid 57 and name hb*) (segid="sbm2" and resid 54 and name ha) 1.8 0 4.2 {w, 1.87, 3, 1.0} amb assign (segid="sbm1" and resid 57 and name hg*) (segid="sbm1" and resid 54 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 57 and name hg*) (segid="sbm2" and resid 54 and name hn) 1.8 0 4.2 {vw, 2.87, 2, 1.0, amb} NOTES 3D NOESY: noesy100- 227 108 31 V52 alpha-N-2 (hn34) 3.66ppm, (9/2), 293 could ovlp an-4 Q50 alpha-N-4 (hn88) 3.66ppm, (9/2), 293 could ovlp an-2 NOTES 4D CN: close to O1 in D1 Lys 55 hn nearly ovlps E49 MED ; 8247 1 8268 5 parsed_1b4c 1 568 "{w, 4.09, ?, 0, amb}" 8271 1 8271 29 parsed_1b4c 1 569 ; {m, 3.66, 9ov, 0} assign (segid="sbm1" and resid 52 and name hn) (segid="sbm1" and resid 55 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 52 and name hn) (segid="sbm2" and resid 55 and name hn) 1.8 0 4.2 {vw, 7.06, 8*, 0, amb}{DWJ removed} ; 8275 1 8279 44 parsed_1b4c 1 570 "{w, 6.81, 9*, 0}" 8283 1 8283 26 parsed_1b4c 1 571 "{w, 3.36, 1, 0}" 8287 1 8287 24 parsed_1b4c 1 572 ; {w, 8.31, 2, 0} amb assign (segid="sbm1" and resid 57 and name hb*) (segid="sbm1" and resid 55 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 57 and name hb*) (segid="sbm2" and resid 55 and name hn) 1.8 0 4.2 {vw, 2.35, >10/4, 1.0, cn} ; 8291 1 8295 35 parsed_1b4c 1 573 ; {s?, 2.11, 15?, 0} NOTES 3D NOESY: noesy100- 302 141 31 NOTES 4D CN: plane overlaps E49, so NOEs from 4D CN could be to E49 instead Val 56 MED ; 8299 1 8309 5 parsed_1b4c 1 574 ; {w, 3.6, 4, 0, ncn} assign (segid="sbm1" and resid 53 and name hn) (segid="sbm1" and resid 56 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 53 and name hn) (segid="sbm2" and resid 56 and name hn) 1.8 0 4.2 {vw, 3.36, 7*, 0, amb}{DJW removed} ; 8312 1 8316 44 parsed_1b4c 1 575 "{m?, 3.36, 6, 0, ncn, amb}" 8320 1 8320 35 parsed_1b4c 1 576 "{m?, 3.34, 11, 1.5}" 8324 1 8324 28 parsed_1b4c 1 577 ; {w, 8.66, 2, 0} assign (segid="sbm1" and resid 54 and name hb*) (segid="sbm1" and resid 56 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 54 and name hb*) (segid="sbm2" and resid 56 and name hn) 1.8 0 4.2 {vw, 2.65, 2, 0, amb}{DJW removed} amb assign (segid="sbm1" and resid 58 and name hn) (segid="sbm1" and resid 56 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 58 and name hn) (segid="sbm2" and resid 56 and name hn) 1.8 0 3.2 {w?, 8.27, >10ov, 0, amb} ; 8328 1 8336 35 parsed_1b4c 1 578 ; {w, 4.42, 1, 0} NOTES 3D NOESY: noesy100- 278 131 27 E58 NN+2 (hn39) 8.27ppm, (), could ovlp nn V52 alpha-N-4 (hn34) 3.66ppm, (10/2), ~293, could ovlp ha Met 57 MED ; 8340 1 8351 5 parsed_1b4c 1 579 ; {w, 3.36, 3, 0} assign (segid="sbm1" and resid 53 and name hg1*) (segid="sbm1" and resid 57 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 53 and name hg1*) (segid="sbm2" and resid 57 and name hn) 1.8 0 3.2 {w, 0.96, 6, 1.5, amb} assign (segid="sbm1" and resid 53 and name hg1*) (segid="sbm1" and resid 57 and name he*) 1.8 0 1.5 assign (segid="sbm2" and resid 53 and name hg1*) (segid="sbm2" and resid 57 and name he*) 1.8 0 1.5 {m, 0.85, 12, 3.0}{DJW removed} ; 8354 1 8362 40 parsed_1b4c 1 580 ; {w, 4.28, 3, 0, ncn, amb} R assign (segid="sbm1" and resid 55 and name hn) (segid="sbm1" and resid 57 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 55 and name hn) (segid="sbm2" and resid 57 and name hn) 1.8 0 4.2 {vw, 7.79, 7*, 0} ; 8366 1 8370 26 parsed_1b4c 1 581 ; {mw?, 1.70, 7?, 1.0} RS assign (segid="sbm1" and resid 60 and name hb*) (segid="sbm1" and resid 57 and name ha) 1.8 0 4.2 RS assign (segid="sbm2" and resid 60 and name hb*) (segid="sbm2" and resid 57 and name ha) 1.8 0 4.2 {vw, 1.26, *, 1.0} assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 57 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 57 and name hn) 1.8 0 4.2 {vw, 0.39, 6*, 2.9, amb} ; 8374 1 8382 34 parsed_1b4c 1 582 ; {vw, 0.36, 6, 4.4} 60hd1* sees only vw 57he* 60hb1-57ha very weak at d2=4.04 NOTES 3D NOESY: noesy100- 256 ~121 37 E58 NN (hn39) 8.27ppm, (>10/2), ~123 ovlps hn19 V56 beta-N-1 (hn80) 2.33ppm, (10/2), ovlps hb2 in H and C Glu 58 MED ; 8386 1 8398 5 parsed_1b4c 1 583 ; {w, 4.28, 2, 0, ncn, amb} amb assign (segid="sbm1" and resid 54 and name hb*) (segid="sbm1" and resid 58 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 54 and name hb*) (segid="sbm2" and resid 58 and name hn) 1.8 0 3.2 {w, 2.65, 3, 1.0, amb} ; 8401 1 8405 31 parsed_1b4c 1 584 "{m, 4.15, 9, 0, ncn, amb}" 8409 1 8409 34 parsed_1b4c 1 585 ; {w, 3.60, 9*, 0} amb assign (segid="sbm1" and resid 60 and name hn) (segid="sbm1" and resid 58 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 60 and name hn) (segid="sbm2" and resid 58 and name hn) 1.8 0 3.2 {w, 7.76, 6, 0} ; 8413 1 8417 24 parsed_1b4c 1 586 ; {s, 2.65, 10, 1.0} NOTES 3D NOESY: noesy100- 260 123 33 NOTES 4D CN M57 NN-1 (hn19) 8.30ppm, (), could ovlp hn39 T59 NN (hn18) 8.04ppm, (12), 132 could ovlp nn-2[80] Thr 59 MED ; 8421 1 8433 5 parsed_1b4c 1 587 ; {w, 4.15, 5, 0, amb} amb assign (segid="sbm1" and resid 55 and name hg*) (segid="sbm1" and resid 59 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 55 and name hg*) (segid="sbm2" and resid 59 and name hn) 1.8 0 3.2 {w, 1.51, 3, 1.0, amb} ; 8436 1 8440 34 parsed_1b4c 1 588 ; {m, 3.60, 8, 0, amb} assign (segid="sbm1" and resid 56 and name hg1*) (segid="sbm1" and resid 59 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 56 and name hg1*) (segid="sbm2" and resid 59 and name hn) 1.8 0 4.2 {vw?, 0.83, 3, 1.5, amb} assign (segid="sbm1" and resid 56 and name ha) (segid="sbm1" and resid 59 and name hg2*) 1.8 0 3.2 assign (segid="sbm2" and resid 56 and name ha) (segid="sbm2" and resid 59 and name hg2*) 1.8 0 3.2 {w, 3.55, 5, 1.5} amb assign (segid="sbm1" and resid 57 and name hn) (segid="sbm1" and resid 59 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 57 and name hn) (segid="sbm2" and resid 59 and name hn) 1.8 0 3.2 {w, 8.28, 14? ovlp 58hn, 0, amb} art? assign (segid="sbm1" and resid 62 and name hg*) (segid="sbm1" and resid 59 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 62 and name hg*) (segid="sbm2" and resid 59 and name hg2*) 1.8 0 4.2 {vw, 2.34, 2, 2.5} assign (segid="sbm1" and resid 61 and name hb*) (segid="sbm1" and resid 59 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 61 and name hb*) (segid="sbm2" and resid 59 and name hn) 1.8 0 4.2 {vw, 2.67, 1, 1.0, amb} ; 8444 1 8464 32 parsed_1b4c 1 589 ; {mw?, 2.11, 7, 1.0e assign (segid="sbm1" and resid 62 and name hb*) (segid="sbm1" and resid 59 and name hg2*) 1.8 0 3.2 assign (segid="sbm2" and resid 62 and name hb*) (segid="sbm2" and resid 59 and name hg2*) 1.8 0 3.2 {w, 2.27, 5, 2.5} NOTES 3D NOESY: noesy100- 281 132 37 NN-1 (hn39) 8.2ppm, (14), 123 could ovlp nn-2[19] NN-2 (hn19) 8.3ppm, (14/2), could ovlp nn-1[39] Leu 60 MED ; 8468 1 8481 5 parsed_1b4c 1 590 ; {vw, 3.60, 9*, 0} SD? assign (segid="sbm1" and resid 56 and name hb) (segid="sbm1" and resid 60 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 56 and name hb) (segid="sbm2" and resid 60 and name hn) 1.8 0 4.2 {vw, 2.35, 1, 0, amb} assign (segid="sbm1" and resid 56 and name hg1*) (segid="sbm1" and resid 60 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 56 and name hg1*) (segid="sbm2" and resid 60 and name hn) 1.8 0 4.2 {vw, 0.83, ~10*/6, 1.5} assign (segid="sbm1" and resid 56 and name hg1*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 1.5 assign (segid="sbm2" and resid 56 and name hg1*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 1.5 {d', m, 0.78, 10, 4.4}{DJW removed} R assign (segid="sbm1" and resid 56 and name hg1*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 56 and name hg1*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 3.2 {d'', w, 0.78, 5, 4.4} ; 8484 1 8500 31 parsed_1b4c 1 591 ; {mw, 4.04, 5, 0, cn, amb} SD? assign (segid="sbm1" and resid 57 and name hb*) (segid="sbm1" and resid 60 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 57 and name hb*) (segid="sbm2" and resid 60 and name hn) 1.8 0 4.2 {vw, 1.89, 3, 1.0, amb} ; 8504 1 8508 32 parsed_1b4c 1 592 ; {d', w, 4.05, 5, 2.9} R assign (segid="sbm1" and resid 58 and name hn) (segid="sbm1" and resid 60 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 58 and name hn) (segid="sbm2" and resid 60 and name hn) 1.8 0 4.2 {vw, 8.31, 1, 0} ; 8512 1 8516 26 parsed_1b4c 1 593 ; {w, 4.04, 4, 0, cn, amb} art? assign (segid="sbm1" and resid 63 and name ha) (segid="sbm1" and resid 60 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 63 and name ha) (segid="sbm2" and resid 60 and name hd*) 1.8 0 4.2 {d'', vw, 4.97, 3, 2.9} NOTES 3D NOESY: noesy100- 298 140 29 D61 NN (hn20) 7.7ppm, (11), ovlps L60 hn[68] Asp 61 MED ; 8520 1 8534 5 parsed_1b4c 1 594 ; {w, 4.03, 10ovlp?, amb} 58ha at 4.03, 59hb at 3.98 amb assign (segid="sbm1" and resid 57 and name hg*) (segid="sbm1" and resid 61 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 57 and name hg*) (segid="sbm2" and resid 61 and name hn) 1.8 0 4.2 {vw, 2.84, 1, amb} assign (segid="sbm1" and resid 58 and name hn) (segid="sbm1" and resid 61 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 58 and name hn) (segid="sbm2" and resid 61 and name hn) 1.8 0 4.2 {vw, 8.28, 7*, amb} ; 8537 1 8545 28 parsed_1b4c 1 595 ; {m?, 4.01, 10?, 0, ncn, amb} 57ha at 4.03, 59hb at 3.98 assign (segid="sbm1" and resid 58 and name hg*) (segid="sbm1" and resid 61 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 58 and name hg*) (segid="sbm2" and resid 61 and name hn) 1.8 0 4.2 {vw, 2.27, 1, 1.0, amb} ; 8549 1 8553 32 parsed_1b4c 1 596 ; {vw, 8.04, 9*, 0} amb/SD? assign (segid="sbm1" and resid 59 and name hg2*) (segid="sbm1" and resid 61 and name hn) 1.8 0 4.2 amb/SD? assign (segid="sbm2" and resid 59 and name hg2*) (segid="sbm2" and resid 61 and name hn) 1.8 0 4.2 {vw, 1.37, 1, 1.5, amb}, 33hg1 may be at 1.37 assign (segid="sbm1" and resid 62 and name hb*) (segid="sbm1" and resid 61 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 62 and name hb*) (segid="sbm2" and resid 61 and name hn) 1.8 0 3.2 {w, 2.11, 7, 1.0, amb} amb assign (segid="sbm1" and resid 63/76 and name hn/ring) (segid="sbm1" and resid 61 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 63/77 and name hn/ring) (segid="sbm2" and resid 61 and name hn) 1.8 0 4.2 {vw, 7.25, 9*, 0} off in CS for 63 at 7.21 NOTES 3D NOESY: noesy100- 304 142 36 NN-1 (hn68) 7.81ppm, (25/3), could ovlp D61 hn20 NN (hn53) 7.78ppm, (25/3), could ovlp D61 hn20 Glu 62 ; 8557 1 8579 8 parsed_1b4c 1 597 "{w?, 4.04, ?, 0, amb} ovlps other peak at 3.98" 8582 1 8582 55 parsed_1b4c 1 598 ; {mw, 3.98, 11&5, 0} assign (segid="sbm1" and resid 59 and name hg2*) (segid="sbm1" and resid 62 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 59 and name hg2*) (segid="sbm2" and resid 62 and name hn) 1.8 0 4.2 {vw, 1.38, 1, 1.5, amb} ; 8586 1 8590 32 parsed_1b4c 1 599 "{w?, 7.8, ?, 0}" 8594 1 8594 24 parsed_1b4c 1 600 "{w, 3.85, 4*, 0, amb}" 8598 1 8598 32 parsed_1b4c 1 601 ; {vw, 1.21, 3ovlp?, 1.0, amb} 33hg2 1.21 SD? assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 62 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 62 and name hn) 1.8 0 4.2 {vw, 0.39, 4*, 2.9, amb} NOTES 3D NOESY: noesy100- 301 141 32 NN-1 (hn20) 7.74ppm, (), ovlps E62 hn53 NN-2 (hn68) 7.81ppm, (), ovlps E62 hn53 Asp 63 MED ; 8602 1 8619 5 parsed_1b4c 1 602 ; {w, 3.86, 5, 0, amb} S30hb* and G66ha2 at 3.88 assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 63 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 63 and name hn) 1.8 0 4.2 {vw, 0.07, 3*, 2.9, amb}{DJW removed} amb assign (segid="sbm1" and resid 61 and name hn) (segid="sbm1" and resid 63 and name hn) 1.8 0 1.1 amb assign (segid="sbm2" and resid 61 and name hn) (segid="sbm2" and resid 63 and name hn) 1.8 0 1.1 {s?, 7.74, ?, 0} amb assign (segid="sbm1" and resid 66 and name ha*) (segid="sbm1" and resid 63 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 66 and name ha*) (segid="sbm2" and resid 63 and name hn) 1.8 0 3.2 {w?, 4.12, 12ovlp, amb} G62ha at 4.12 also amb assign (segid="sbm1" and resid 66 and name ha*) (segid="sbm1" and resid 63 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 66 and name ha*) (segid="sbm2" and resid 63 and name hn) 1.8 0 4.2 {vw?, 3.86-8?, 5, 1.0, amb} S30hb* also at 3.88, 60ha at 3.85 NOTES 3D NOESY: noesy100- 350 162 34 E62 NN-1 (hn53) 7.79ppm, (14/2), 141 could ovlp nn-2[20] D61 NN-2 (hn20) 7.74ppm, (14/2), 141 could ovlp nn-1[53] Gly 64 MED assign (segid="sbm1" and resid 61 and name ha) (segid="sbm1" and resid 64 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 61 and name ha) (segid="sbm2" and resid 64 and name hn) 1.8 0 4.2 {vw, 4.39, 5*} 59ha at 4.32 but peak seems to be right on 4.39 assign (segid="sbm1" and resid 62 and name hn) (segid="sbm1" and resid 64 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 62 and name hn) (segid="sbm2" and resid 64 and name hn) 1.8 0 3.2 {w, 7.79, 3}{DJW removed} ; 8622 1 8656 34 parsed_1b4c 1 603 "{vw, 4.11, 1} 66ha1 also at 4.12, use 62ha since sees wk 62hn" 8660 1 8660 70 parsed_1b4c 1 604 ; {vw, 2.57, ~8*, amb}{modified from 62 to 63 beta-N; DJW} amb assign (segid="sbm1" and resid 29/65 and name he*/b1) (segid="sbm1" and resid 64 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 29/65 and name he*/b1) (segid="sbm2" and resid 64 and name hn) 1.8 0 4.2 {vw, 2.81, 4*, 0, amb} R assign (segid="sbm1" and resid 66 and name hn) (segid="sbm1" and resid 64 and name hn) 1.8 0 ? R assign (segid="sbm2" and resid 66 and name hn) (segid="sbm2" and resid 64 and name hn) 1.8 0 ? {?, 8.0, ?, 0} NOTES 3D NOESY: noesy100- 290 136 49 G66 NN+2 (hn4) 8.09ppm, (), could ovlp nn Asp 65 MED ; 8664 1 8682 5 parsed_1b4c 1 605 "{vw, 7.2, 4*}" 8685 1 8685 23 parsed_1b4c 1 606 "{w, 5.02, 3}{modified to 64 from 63; DJW}" 8689 1 8689 51 parsed_1b4c 1 607 "amb NOE that overlaps own beta, but it seems to fit; also own beta looks a little funny; DJW" 8693 9 8693 9 parsed_1b4c 1 608 ; NOTES 3D NOESY: noesy100- 274 129 38 NN (hn4) 8.09ppm, (24/2), could ovlp hn16 Gly 66 MED ; 8696 1 8704 5 parsed_1b4c 1 609 "{vw, 5.02, 7*, 0}, could be dispersive 67ha at 5.07, 63ha looks too far" 8707 1 8707 80 parsed_1b4c 1 610 ; {w, 7.95, 3, 0{DJW removed for now} NOTES 3D NOESY: noesy100- 274 129 47 D65 NN-1 (hn16) 8.09ppm, (), ovlps hn4 Glu 67 MED ; 8711 1 8721 5 parsed_1b4c 1 611 ; {?, 8.09, ?, 0} 66hn also at 8.09 assign (segid="sbm1" and resid 65 and name ha) (segid="sbm1" and resid 67 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 65 and name ha) (segid="sbm2" and resid 67 and name hn) 1.8 0 3.2 {vw, 4.91, 8*ovlp, 0} 65ha at 4.88 and K28ha 4.93, 65ha looks too far NOTES 3D NOESY: noesy100- 241 115 33 D65 NN-2 (hn16) 8.09ppm, (), could ovlp nn-1 Cys 68 MED NOTES 3D NOESY: noesy100- 164 82 31 X/Y= R20hg1,hg2 not in 4D NOESY, also observed for G66 NOTES 4D CN K26ha 4 ctrs in 4D 9* in 3D go with 2 K28ha 6ctrs in 4D 3 in 3D go with 4 Asp 69 MED SD? assign (segid="sbm1" and resid 67 and name ha) (segid="sbm1" and resid 69 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 67 and name ha) (segid="sbm2" and resid 69 and name hn) 1.8 0 4.2 {vw, 5.04, 3*, amb} ; 8724 1 8754 28 parsed_1b4c 1 612 "{vw, 7.95, 2*}" 8758 1 8758 23 parsed_1b4c 1 613 "{w, 8.36, 4}{DJW removed}" 8762 1 8762 34 parsed_1b4c 1 614 "{vw, 3.98, 8*, amb}" 8766 1 8766 28 parsed_1b4c 1 615 ; {mw?, 2.35, ~13/8, ncn} 72hg22 at 2.33 probably contributes RS assign (segid="sbm1" and resid 72 and name hb*) (segid="sbm1" and resid 69 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 72 and name hb*) (segid="sbm2" and resid 69 and name hn) 1.8 0 3.2 {w, 2.13, 8/6, ncn} 72hb2 at 7.09 ; 8770 1 8774 42 parsed_1b4c 1 616 ; {w, 2.49, 4/3, ncn} RS assign (segid="sbm1" and resid 72 and name hg*) (segid="sbm1" and resid 69 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 72 and name hg*) (segid="sbm2" and resid 69 and name hn) 1.8 0 3.2 {w, 2.34, ~13/5, ncn} NOTES 3D NOESY: noesy100- 233 111 27 Phe 70 MED ; 8778 1 8789 5 parsed_1b4c 1 617 "{w?, 3.33, ?, 1.0}" 8792 1 8792 27 parsed_1b4c 1 618 ; RS assign (segid="sbm1" and resid 73 and name hb*) (segid="sbm1" and resid 70 and name ha) 1.8 0 3.2 RS assign (segid="sbm2" and resid 73 and name hb*) (segid="sbm2" and resid 70 and name ha) 1.8 0 3.2 {w?, 3.22, ?, 1.0} NOTES 3D NOESY: noesy100- 181 89 32 Gln 71 MED ; 8797 1 8808 5 parsed_1b4c 1 619 "{w, 8.5, 4?, 0}" 8811 1 8811 25 parsed_1b4c 1 620 "{vw, 5.34, 7*, 0}" 8815 1 8815 26 parsed_1b4c 1 621 "{w, 2.79, 6, 1.0, amb} Z= F14hb2, N37hb1, F76hb2 from 4D - dont like any" 8819 1 8819 81 parsed_1b4c 1 622 "{w, 8.6, 4?, 0}" 8823 1 8823 25 parsed_1b4c 1 623 ; {w?, 1.44, 1*, 1.0} RS assign (segid="sbm1" and resid 74 and name hb*) (segid="sbm1" and resid 71 and name ha) 1.8 0 3.2 RS assign (segid="sbm2" and resid 74 and name hb*) (segid="sbm2" and resid 71 and name ha) 1.8 0 3.2 {w?, 1.44, 1*, 1.0} NOTES 3D NOESY: noesy100- 288 135 35 D69 NN-2 (hn78) 8.58ppm, (4/2), 110 could ovlp nn+2 F73 NN+2 (hn72) 8.62ppm, (4/2), 110 could ovlp nn-2 Glu 72 close to Q16 in 1H and 15N MED ; 8827 1 8843 5 parsed_1b4c 1 624 "{vw, 5.18, 2, 0} 51ha-16hn may contribute" 8846 1 8846 50 parsed_1b4c 1 625 "{vw, 2.84, ~8*, 1.0, amb} looks too far and may be only 69hb2 at 2.79" 8850 1 8850 78 parsed_1b4c 1 626 "{vw, 2.79, ~8*, 1.0, amb}{DJW removed}" 8854 1 8854 47 parsed_1b4c 1 627 "This noe is overlapped, but fits well; DJW" 8858 9 8858 9 parsed_1b4c 1 628 "{vw, 3.39, 8*, 0, amb}{DJW removed}" 8862 1 8862 45 parsed_1b4c 1 629 ; {w?, 8.0, ?, 0} art? assign (segid="sbm1" and resid 74 and name hb*) (segid="sbm1" and resid 72 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 74 and name hb*) (segid="sbm2" and resid 72 and name hn) 1.8 0 4.2 {vw, 1.48, 5*, 1.0, amb} R assign (segid="sbm1" and resid 75 and name hb*) (segid="sbm1" and resid 72 and name ha) 1.8 0 1.1 R assign (segid="sbm2" and resid 75 and name hb*) (segid="sbm2" and resid 72 and name ha) 1.8 0 1.1 {s?, 1.26, 10, 1.5} NOTES 3D NOESY: noesy100- 254 121 28 M74 NN+2 (hn32) 8.00ppm, () could ovlp nn-1 Phe 73 MED amb assign (segid="sbm1" and resid 68 and name ha) (segid="sbm1" and resid 73 and name ha) 1.8 0 3.2 amb assign (segid="sbm2" and resid 68 and name ha) (segid="sbm2" and resid 73 and name ha) 1.8 0 3.2 {w, 5.15, 4, 0, amb} looks too far assign (segid="sbm1" and resid 68 and name hb*) (segid="sbm1" and resid 73 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid 68 and name hb*) (segid="sbm2" and resid 73 and name hn) 1.8 0 3.2 {w, 2.84, 2ov, 1.0, amb}{DJW removed} ; 8866 1 8891 46 parsed_1b4c 1 630 ; {w?, 3.39, 6ov?, 0, amb} 73hb1/2-70ha assigned assign (segid="sbm1" and resid 71 and name hn) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 71 and name hn) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {w?, 7.93, 3?, 0, amb} ; 8895 1 8901 31 parsed_1b4c 1 631 ; {w, 3.55, 1, 0} assign (segid="sbm1" and resid 71 and name hb*) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 71 and name hb*) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 2.13, 6ov, 1.0, amb}{DJW removed} R assign (segid="sbm1" and resid 75 and name hn) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 75 and name hn) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 7.86ov, 3, 0} amb assign (segid="sbm1" and resid 75 and name hb*) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 75 and name hb*) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 1.24, 2ov, 1.5, amb} 75hb* looks too far, think its 32hd1* at 1.21 and 27hb2 at 1.26 amb assign (segid="sbm1" and resid 76 and name hb*) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 76 and name hb*) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 2.81, 2ov?, 1.0, amb} ; 8905 1 8921 35 parsed_1b4c 1 632 ; {mw?, 3.06, 4, 1.0} RS assign (segid="sbm1" and resid 76 and name hb*) (segid="sbm1" and resid 73 and name ha) 1.8 0 4.2 RS assign (segid="sbm2" and resid 76 and name hb*) (segid="sbm2" and resid 73 and name ha) 1.8 0 4.2 {w, 2.81, 5?, 1.0} NOTES 3D NOESY: noesy100- 229 110 29 Q71 NN-2 (hn28) 7.93ppm, (), could ovlp nn NOTES 4D CN: close to O1 in D1 so intensity greatly attenuated Met 74 MED ; 8925 1 8940 5 parsed_1b4c 1 633 ; {w, 3.39, 3?, 0, amb} assign (segid="sbm1" and resid 70 and name hd*) (segid="sbm1" and resid 74 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 70 and name hd*) (segid="sbm2" and resid 74 and name hn) 1.8 0 4.2 {vw, 6.30, 5*, 2.4, amb}{DJW removed} ; 8943 1 8947 46 parsed_1b4c 1 634 "{mw, 3.55, 7, 0, amb}" 8951 1 8951 30 parsed_1b4c 1 635 "{w, 8.36, 2, 0}" 8955 1 8955 25 parsed_1b4c 1 636 ; {w, 4.01, 1, 0} assign (segid="sbm1" and resid 72 and name hb*) (segid="sbm1" and resid 74 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 72 and name hb*) (segid="sbm2" and resid 74 and name hn) 1.8 0 4.2 {vw, 2.33, 7*, 1.0, amb}{DJW removed} ; 8959 1 8963 46 parsed_1b4c 1 637 "{w?, 7.99, ?, 0, amb}" 8967 1 8967 30 parsed_1b4c 1 638 "{m, 1.73, 7?, 0}, 74hg* also at 1.73, so may be weak" 8971 1 8971 61 parsed_1b4c 1 639 ; {m?, 0.77, 11, 3.0, vwk cfilt 0.79?} assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm1" and resid 74 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm2" and resid 74 and name hn) 1.8 0 4.2 {vw, 0.48, 7*ov, 1.5, amb}{DJW removed} ; 8975 1 8979 48 parsed_1b4c 1 640 ; {w, 0.48, 7, 3.0} NOTES 3D NOESY: noesy100- 282 133 34 F76 NN+2 (hn23) 7.99ppm, (), could ovlp M74 hn32 Ala 75 MED ; 8983 1 8993 5 parsed_1b4c 1 641 ; {w, 3.55, 2, 0} assign (segid="sbm1" and resid 71 and name hb*) (segid="sbm1" and resid 75 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 71 and name hb*) (segid="sbm2" and resid 75 and name hn) 1.8 0 4.2 {vw, 2.13, 1ov, 1, amb}{DJW removed} assign (segid="sbm1" and resid 71 and name hg*) (segid="sbm1" and resid 75 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 71 and name hg*) (segid="sbm2" and resid 75 and name hn) 1.8 0 4.2 {vw, 2.30, 1, 1.0, amb}[DJW removed} ; 8996 1 9004 45 parsed_1b4c 1 642 "{mw?, 4.01, 6, 0, cn}" 9008 1 9008 30 parsed_1b4c 1 643 "{s, 3.97, >10, 1.5}" 9012 1 9012 28 parsed_1b4c 1 644 ; {w, 8.63, 1, 0} assign (segid="sbm1" and resid 73 and name hd*) (segid="sbm1" and resid 75 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 73 and name hd*) (segid="sbm2" and resid 75 and name hn) 1.8 0 4.2 {vw, 6.92, 5*, 2.4, amb}{DJW removed} ; 9016 1 9020 46 parsed_1b4c 1 645 ; {w, 8.46, 9*, 0} assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm1" and resid 75 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm2" and resid 75 and name hn) 1.8 0 4.2 {vw, 0.48, 3*, 1.5, amb}{DJW removed} ; 9024 1 9028 46 parsed_1b4c 1 646 ; {m?, 3.95, 6?, 1.0} ovlps with 75ha NOTES 3D NOESY: noesy100- 294 138 22 M74 NN-1 (hn32) 8.00ppm, (14/2), 133 ovlps nn F76 NN (hn23) 7.99ppm, (14/2), 133 ovlps nn-1 Phe 76 MED ; 9032 1 9043 5 parsed_1b4c 1 647 "{w, 4.01, 8ov, 0, amb}" 9046 1 9046 31 parsed_1b4c 1 648 ; {mw?, 4.39, 4?, 0, amb} 76hb1/2-73ha assigned assign (segid="sbm1" and resid 74 and name ha) (segid="sbm1" and resid 76 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 74 and name ha) (segid="sbm2" and resid 76 and name hn) 1.8 0 4.2 {w, 3.68, 4, 0}{DJW removed} R assign (segid="sbm1" and resid 78 and name hn) (segid="sbm1" and resid 76 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 78 and name hn) (segid="sbm2" and resid 76 and name hn) 1.8 0 3.2 {w, 8.63, 4, 0} amb assign (segid="sbm1" and resid 78 and name hb*) (segid="sbm1" and resid 76 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 78 and name hb*) (segid="sbm2" and resid 76 and name hn) 1.8 0 4.2 {vw, 3.98, 8ov?, 1.0, amb} could be inter or intra, or not at all ; 9050 1 9064 74 parsed_1b4c 1 649 "{mw?, 2.20, 5?, 1.0} viol for med asbd9" 9068 1 9068 48 parsed_1b4c 1 650 ; NOTES 3D NOESY: noesy100- 283 133 35 ha vw in 3D NOESY and 10 ctrs in 4D go with 5 ctrs Val 77 MED ; 9073 1 9081 5 parsed_1b4c 1 651 ; {w, 4.39, 6*, 0, amb} assign (segid="sbm1" and resid 73 and name hd*) (segid="sbm1" and resid 77 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 73 and name hd*) (segid="sbm2" and resid 77 and name hn) 1.8 0 4.2 {vw, 6.92, 8*, 2.4, amb}{DJW removed} ; 9084 1 9088 46 parsed_1b4c 1 652 "{vw, 7.09, 1, 3.9}" 9092 1 9092 27 parsed_1b4c 1 653 "{vw, 7.11, 8*, 2.4, amb}" 9096 1 9096 33 parsed_1b4c 1 654 "{vw, 7.02, 2, 3.9}" 9100 1 9100 27 parsed_1b4c 1 655 "{w, 7.09, 3, 1.5}" 9104 1 9104 26 parsed_1b4c 1 656 "{mw, 3.68, 7, 0}" 9108 1 9108 25 parsed_1b4c 1 657 "{vw, 3.66, 3, 1.5}" 9112 1 9112 27 parsed_1b4c 1 658 ; {m, 3.66, 10/7, 1.5} assign (segid="sbm1" and resid 74 and name hb*) (segid="sbm1" and resid 77 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 74 and name hb*) (segid="sbm2" and resid 77 and name hn) 1.8 0 4.2 {vw, 1.48, 8*, 1.0, amb}{DJW removed} R assign (segid="sbm1" and resid 74 and name he*) (segid="sbm1" and resid 77 and name hg1*) 1.8 0 1.5 R assign (segid="sbm2" and resid 74 and name he*) (segid="sbm2" and resid 77 and name hg1*) 1.8 0 1.5 {m, 1.56, ~12, 3.0, no cfilt} R assign (segid="sbm1" and resid 75 and name hn) (segid="sbm1" and resid 77 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 75 and name hn) (segid="sbm2" and resid 77 and name hn) 1.8 0 3.2 {w?, 7.8, 5?, 0} assign (segid="sbm1" and resid 75 and name ha) (segid="sbm1" and resid 77 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 75 and name ha) (segid="sbm2" and resid 77 and name hn) 1.8 0 4.2 {w, 4.01, 4, 0, amb}{DJW removed} amb assign (segid="sbm1" and resid 75 and name hb*) (segid="sbm1" and resid 77 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 75 and name hb*) (segid="sbm2" and resid 77 and name hn) 1.8 0 3.2 {w, 1.24, 7ov?, 1.5, amb} looks like med to 32hd1* from model assign (segid="sbm1" and resid 78 and name hb*) (segid="sbm1" and resid 77 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 78 and name hb*) (segid="sbm2" and resid 77 and name hn) 1.8 0 4.2 {vw, 3.98, 4ov, 1.0, amb}{DJW removed} R assign (segid="sbm1" and resid 79 and name hn) (segid="sbm1" and resid 77 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 79 and name hn) (segid="sbm2" and resid 77 and name hn) 1.8 0 3.2 {w?, 7.8, 5?, 0} ; 9116 1 9144 25 parsed_1b4c 1 659 ; {mw?, 2.06, 6, 0} NOTES 3D NOESY: noesy100- 244 116 35 A75 NN-2 (hn87) 7.8ppm, (5/2), 139 could ovlp nn+2 M79 NN+2 (hn79) 7.8ppm, (5/2), 139 could ovlp nn-2 Ser 78 MED ; 9148 1 9159 5 parsed_1b4c 1 660 ; {w?, 3.66, 10ov?, 0, amb} 74ha at 3.68 ovlp own ha at 3.66? amb assign (segid="sbm1" and resid 74 and name hb*) (segid="sbm1" and resid 78 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 74 and name hb*) (segid="sbm2" and resid 78 and name hn) 1.8 0 4.2 {vw, 1.73, 10ov, 1.0, amb} 77hb at 1.73 amb assign (segid="sbm1" and resid 74 and name hb*) (segid="sbm1" and resid 78 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 74 and name hb*) (segid="sbm2" and resid 78 and name hn) 1.8 0 4.2 {vw, 1.48, 2, 1.0, amb} could have inter contribution ; 9162 1 9170 62 parsed_1b4c 1 661 ; {w, 1.62, 4, amb} Distance over 10 structures between: MET 74: HE3/HE2/HE1/ AND SER 78: HN/ intramolecular Average=5.61 Angtroms, stand. dev.=0.5718, min= 4.606, max= 6.552 Distance over 10 structures between: MET 74: HE3/HE2/HE1/ AND SER 78: HN/ intermolecular Average=6.763 Angtroms, stand. dev.=0.5707, min= 5.523, max= 7.459 ; 9176 1 9180 68 parsed_1b4c 1 662 ; {mw?, 4.01, 12ov, 0} 78hb ovlps, and could be some inter contribution but only w-vw amb assign (segid="sbm1" and resid 75 and name hn) (segid="sbm1" and resid 78 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 75 and name hn) (segid="sbm2" and resid 78 and name hn) 1.8 0 3.2 {vw, 7.85, 12ov, 0. amb} amb assign (segid="sbm1" and resid 75 and name hb*) (segid="sbm1" and resid 78 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 75 and name hb*) (segid="sbm2" and resid 78 and name hn) 1.8 0 3.2 {w, 1.24, 4, 1.5, amb} could be some inter but w-vw ; 9184 1 9192 60 parsed_1b4c 1 663 ; {w, 8.00, 3, 0} dont see 81hb-78ha or vice versa NOTES 3D NOESY: noesy100- 228 109 32 M79 NN (hn79) 7.85ppm, (12), 139 could ovlp nn+2 Met 79 MED ; 9196 1 9208 5 parsed_1b4c 1 664 ; {w?, 4.01, ?, 0, amb} could have inter contirbution amb assign (segid="sbm1" and resid 75 and name hb*) (segid="sbm1" and resid 79 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 75 and name hb*) (segid="sbm2" and resid 79 and name hn) 1.8 0 3.2 {w, 1.21, 5, 1.5, amb} could have inter contirbution, looks about same dist either way ; 9211 1 9215 95 parsed_1b4c 1 665 "{w, 4.31, 6*, 0}" 9219 1 9219 25 parsed_1b4c 1 666 ; {w, 4.31, 6, 1.5} assign (segid="sbm1" and resid 76 and name hb*) (segid="sbm1" and resid 79 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 76 and name hb*) (segid="sbm2" and resid 79 and name hn) 1.8 0 4.2 {vw, 3.06, 4*, 1.0, amb}{DJW removed} assign (segid="sbm1" and resid 76 and name hd*) (segid="sbm1" and resid 79 and name he*) 1.8 0 3.2 assign (segid="sbm2" and resid 76 and name hd*) (segid="sbm2" and resid 79 and name he*) 1.8 0 3.2 {w, 7.24, 3, 4.4}{DJW removed} ; 9223 1 9231 39 parsed_1b4c 1 667 "{w, 8.44, 5*, 0}" 9235 1 9235 26 parsed_1b4c 1 668 ; {w, 3.41, 2, 0} amb assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm1" and resid 79 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm2" and resid 79 and name hn) 1.8 0 4.2 {vw, 0.80, 3, 1.5, amb} could be to V77hg1* at 0.78 and/or 52hg2* at 0.83 assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm1" and resid 79 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm2" and resid 79 and name hn) 1.8 0 4.2 {vw, 0.50, 4*, 1.5, amb}{DJW removed} amb assign (segid="sbm1" and resid 82 and name hg2*) (segid="sbm1" and resid 79 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 82 and name hg2*) (segid="sbm2" and resid 79 and name hn) 1.8 0 4.2 {vw, 0.56, 4*, 1.5, amb} CS at 0.56 off from 0.59 for 82hg2* ; 9239 1 9251 69 parsed_1b4c 1 669 ; {vw, 3.28, 1*, 0, amb} vw, shows only at cl=0.12, and not seen by 79ha at d2=3.95 amb assign (segid="sbm1" and resid 82 and name hg2*) (segid="sbm1" and resid 79 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 82 and name hg2*) (segid="sbm2" and resid 79 and name he*) 1.8 0 4.2 {vw, 0.57, 2, 3.0} 82hg2* not see 79he* amb assign (segid="sbm1" and resid 84? and name ha) (segid="sbm1" and resid 79 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 84? and name ha) (segid="sbm2" and resid 79 and name hn) 1.8 0 4.2 {vw, 4.72, 5*, 0, amb} CS at 4.72 off from 4.75 for 84ha NOTES 3D NOESY: noesy100- 297 139 27 V80 NN (hn22) 7.80ppm, (25/2), ~139 could ovlp M79 hn79 Val 80 MED ; 9255 1 9273 5 parsed_1b4c 1 670 ; {w, 4.31, 5*ov, 0, amb} assign (segid="sbm1" and resid 76 and name ha) (segid="sbm1" and resid 80 and name hg1*) 1.8 0 4.2 assign (segid="sbm2" and resid 76 and name ha) (segid="sbm2" and resid 80 and name hg1*) 1.8 0 4.2 {w, 4.33, 2, 1.5}{DJW removed} ; 9276 1 9280 39 parsed_1b4c 1 671 ; {w?, 3.44, ov80ha?, 0, amb} amb assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm1" and resid 80 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm2" and resid 80 and name hn) 1.8 0 4.2 {vw, 0.77, 3/2, 1.5} 3hd2* could contribute ; 9284 1 9288 52 parsed_1b4c 1 672 "{w, 8.66, 4*, 0}" 9292 1 9292 25 parsed_1b4c 1 673 ; {w, 3.66, 3*, 0, amb} amb assign (segid="sbm1" and resid 82 and name hg2*) (segid="sbm1" and resid 80 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 82 and name hg2*) (segid="sbm2" and resid 80 and name hn) 1.8 0 4.2 {vw, 0.59, 5, 1.5} ; 9296 1 9300 27 parsed_1b4c 1 674 "{m?, 1.59, 5?, 1.5, amb}" 9304 1 9304 33 parsed_1b4c 1 675 ; {w, 4, 1.56, 3.0} NOTES 3D NOESY: noesy100- 298 139 36 M79 NN-1 (hn79) ppm, (22/2), ~139 ovlps V80 hn22 T81 NN+2 (hn) ppm, (), could ovlp hn22 NOTES 4D CN: M79 an-1 could also be R20, F88 Thr 81 MED ; 9308 1 9320 5 parsed_1b4c 1 676 "{w?, 3.41, 6ov, 0, amb} 77ha at 3.44" 9323 1 9323 45 parsed_1b4c 1 677 ; {mw?, 3.66, 6ov, 0, amb} syha at 3.66 amb assign (segid="sbm1" and resid 78 and name hb*) (segid="sbm1" and resid 81 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 78 and name hb*) (segid="sbm2" and resid 81 and name hn) 1.8 0 3.2 {w?, 3.98, 5ov, 0, amb} dont see 78ha-81hb or vice versa amb assign (segid="sbm1" and resid 79 and name hn) (segid="sbm1" and resid 81 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 79 and name hn) (segid="sbm2" and resid 81 and name hn) 1.8 0 3.2 {w?, 7.8, 10?, 0, amb} assign (segid="sbm1" and resid 79 and name ha) (segid="sbm1" and resid 81 and name hn) 1.8 0 2.4 assign (segid="sbm2" and resid 79 and name ha) (segid="sbm2" and resid 81 and name hn) 1.8 0 2.4 {mw?, 3.93, 5ov, 0, amb}{DJW removed} R assign (segid="sbm1" and resid 83 and name hn) (segid="sbm1" and resid 81 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 83 and name hn) (segid="sbm2" and resid 81 and name hn) 1.8 0 4.2 {vw, 7.25, 2*, 0} NOTES 3D NOESY: noesy100- ~270 ~127 38 V80 NN-1 (hn22) 7.80ppm, (10/3), ~139 could ovlp nn and nn-2 T82 NN (hn111) 7.87ppm, (10/3), ~139 could ovlp nn-1/-2 M79 NN-2 (hn79) 7.83ppm, (10/3), ~139 could ovlp nn and nn-1 NOTES 4D CN V80 aN-1 (hn22) and V77 aN-4 (hn29) 3.4ppm, ovlp @ C=67.23; could also be I11 or V53 S78an-3 could also be S41ha,hb or I47hb Thr 82 MED ; 9327 1 9360 5 parsed_1b4c 1 678 ; {w?, 3.66, 9*, amb} amb assign (segid="sbm1" and resid 78 and name hb*) (segid="sbm1" and resid 82 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 78 and name hb*) (segid="sbm2" and resid 82 and name hn) 1.8 0 3.2 {w, 3.96, 9*ov, amb} ; 9363 1 9367 29 parsed_1b4c 1 679 ; {w, 3.93, 9*ov, amb} amb/art? assign (segid="sbm1" and resid 79 and name hb*) (segid="sbm1" and resid 82 and name hg2*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 79 and name hb*) (segid="sbm2" and resid 82 and name hg2*) 1.8 0 4.2 {vw, 1.85, 1*} art? assign (segid="sbm1" and resid 79 and name hg*) (segid="sbm1" and resid 82 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 79 and name hg*) (segid="sbm2" and resid 82 and name hg2*) 1.8 0 4.2 {vw, 2.34, 2} ; 9371 1 9379 22 parsed_1b4c 1 680 "{w?, 7.80, ?, amb}" 9383 1 9383 27 parsed_1b4c 1 681 ; {w?, 3.39, 4*, amb} assign (segid="sbm1" and resid 80 and name hb) (segid="sbm1" and resid 82 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 80 and name hb) (segid="sbm2" and resid 82 and name hn) 1.8 0 4.2 {vw, 2.05, 6*, amb}{DJW removed} assign (segid="sbm1" and resid 83 and name hb*) (segid="sbm1" and resid 82 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 83 and name hb*) (segid="sbm2" and resid 82 and name hn) 1.8 0 4.2 {vw, 1.61, 5*, amb} R assign (segid="sbm1" and resid 84 and name hn) (segid="sbm1" and resid 82 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 84 and name hn) (segid="sbm2" and resid 82 and name hn) 1.8 0 4.2 {vw, 7.52, 4*} NOTES 3D NOESY: noesy100- 293 137 45 there was some uncertainty about the assignment of ha and hb however a unique noe was observed for A83 to 3.79,68.38 consistent with the current assignment of the ha and hb for T82 M79 aN-3 (hn79) 3.96ppm, vw(9), ~282 could ovlp an-4; strgr at 8.6ppm S78 aN-4 (hn49) 3.96ppm, vw(9), ~282 could ovlp an-3; strgr at 8.6ppm vw pk 100ms NOESY looks like two peaks 7.88/7.86 Ala 83 MED ; 9387 1 9413 5 parsed_1b4c 1 682 ; {w?, 3.93, 9*} assign (segid="sbm1" and resid 79 and name hb*) (segid="sbm1" and resid 83 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 79 and name hb*) (segid="sbm2" and resid 83 and name hn) 1.8 0 4.2 {vw, 1.92, 9*, amb}{DJW removed} assign (segid="sbm1" and resid 79 and name hb*) (segid="sbm1" and resid 83 and name hb*) 1.8 0 3.2 assign (segid="sbm2" and resid 79 and name hb*) (segid="sbm2" and resid 83 and name hb*) 1.8 0 3.2 {w, 1.92, 3}{DJW removed} ; 9416 1 9424 34 parsed_1b4c 1 683 ; {mw?, 3.39, 6ov} R assign (segid="sbm1" and resid 80 and name ha) (segid="sbm1" and resid 83 and name hb*) 1.8 0 1.5 R assign (segid="sbm2" and resid 80 and name ha) (segid="sbm2" and resid 83 and name hb*) 1.8 0 1.5 {m, 3.34, 9ov?} ; 9428 1 9432 24 parsed_1b4c 1 684 ; {w, 1.07, 3} amb assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 83 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 83 and name hn) 1.8 0 4.2 {vw?, 0.94, 6} 53hg1* at 0.96 also ? ; 9436 1 9440 45 parsed_1b4c 1 685 "{w, 8.17, 5*}" 9444 1 9444 22 parsed_1b4c 1 686 ; {w, 3.68, 1, amb} NOTES 3D NOESY: noesy100- 347 160 29 ha dispersive in 3D NOESY; hb 17 ctrs in both expts so 9 ctrs used for ha Cys 84 - MED amb/art? assign (segid="sbm1" and resid 45/46 and name hb*/g*) (segid="sbm1" and resid 84 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 45/46 and name hb*/g*) (segid="sbm2" and resid 84 and name hn) 1.8 0 4.2 {vw, 2.24, 5*} amb assign (segid="sbm1" and resid 44/81 and name hn) (segid="sbm1" and resid 84 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 44/81 and name hn) (segid="sbm2" and resid 84 and name hn) 1.8 0 4.2 {vw, 8.14, 3*, amb} ; 9448 1 9464 28 parsed_1b4c 1 687 "{w, 3.68, 5*, amb}" 9468 1 9468 27 parsed_1b4c 1 688 ; {w, 3.39, 5*, amb} amb assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 84 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 84 and name hn) 1.8 0 4.2 {vw, 0.94, 7*} 53hg1 at 0.96 ; 9472 1 9476 37 parsed_1b4c 1 689 ; {w, 7.87, 6*} NOTES 3D NOESY: noesy100- 325 151 37 His 85? MED assign (segid="sbm1" and resid 83 and name ha) (segid="sbm1" and resid 85 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 83 and name ha) (segid="sbm2" and resid 85 and name hn) 1.8 0 4.2 alpha-N-2 (hn69) 4.42ppm, (3), ~265, dispersive in 100 and 200 ms (nh- 8.35ppm) hn119 seems to be multiple 8.35, 8.34, 8.33 nn region differs a little between 100 and 200 ms noesy100- ~254 ~121 48 alpha?- 3.68 ppm () ~292 ovlps has[3], could be 3.8 instead beta1- 2.16 ppm () 348 ovlps peak from G22(hn3) beta2- 1.89 ppm () 358 ovlps peak from G22 Glu 86? MED assign (segid="sbm1" and resid 84 and name ha) (segid="sbm1" and resid 86 and name hn) assign (segid="sbm2" and resid 84 and name ha) (segid="sbm2" and resid 86 and name hn) ??alpha-N-2 (hn110) 4.7ppm, (), dispersive peak in 200ms nothing in 100ms (nh- 8.01ppm) hn107 dispersive amide in 100ms close to E91 in 1H and 15N noesy100- 281 ~132 20 alpha- 4.36 ppm () missing in NOESY, present in TOCSY beta1- 2.22 ppm vw(8) 346 close to negative peak beta2- 1.86 ppm (4) 359 gamma1- 2.57 ppm vw(9) 340 gamma2- 2.38 ppm vw(6) 333 close to negative peak Phe 87 MED assign (segid="sbm1" and resid 85 and name ha) (segid="sbm1" and resid 87 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 85 and name ha) (segid="sbm2" and resid 87 and name hn) 1.8 0 4.2 alpha-N-2 (hn119) 3.68ppm, vw(6), ~292 (nh- 8.61ppm) hn122 noesy100- 229 ~109 25 alpha- 3.96 ppm (4) 282 beta1- 2.00 ppm (5) 354 beta2- 1.86 ppm (5) 359 could ovpl b2n-1 ??in tocsy- 1.56 ppm (3) Phe 88 MED NOTES 3D NOESY: noesy100- 329 ~153 40 E89 NN (hn60) 7.57ppm, (~6), ~149 ovlps F88 hn5 Glu 89 MED assign (segid="sbm1" and resid 87 and name hb*) (segid="sbm1" and resid 89 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 87 and name hb*) (segid="sbm2" and resid 89 and name hn) 1.8 0 4.2 {vw, 2.43, 7*, amb}{DJW removed} ; 9480 1 9559 41 parsed_1b4c 1 690 ; {vw, 6.13, 5*} amb assign (segid="sbm1" and resid 91 and name hg*) (segid="sbm1" and resid 89 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 91 and name hg*) (segid="sbm2" and resid 89 and name hn) 1.8 0 3.2 {w?, 2.16, 12ov?} NOTES 3D NOESY: noesy100-320 149 31 His 90 MED amb assign (segid="sbm1" and resid 88 and name hn) (segid="sbm1" and resid 90 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 88 and name hn) (segid="sbm2" and resid 90 and name hn) 1.8 0 4.2 {vw, 7.44, 3*, 0, amb} 88hn not see 90hn ; 9563 1 9579 50 parsed_1b4c 1 691 ; {vw, 7.33, 2*, amb} NOTES 3D NOESY: noesy100- 274 129 32 ha dispersive in 3D, stronger in 4D E91 NN (hn90) ppm, (17/2), ~129 could ovlp H90 hn114 Glu 91 MED amb assign (segid="sbm1" and resid 89 and name hn) (segid="sbm1" and resid 91 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 89 and name hn) (segid="sbm2" and resid 91 and name hn) 1.8 0 4.2 {vw, 7.60, 2*, amb} NOTES 3D NOESY noesy100- 273 129 20 H90 NN-1 (hn114) 8.0ppm, (), could ovlp E91 hn90 NOTES 4D CN H90ha 13 ctrs in 4D close to H2O in 3D go with 6 ctrs Note 1: number in parentheses are number of contours seen at lvl=0.02 of NOESY-HMQC for weak peaks and at lvl=0.1 for others Nilges et al. Biopolymers 29, 813-822, (1990). note 2: Naming- upfield = > , downfield = < previous naming was downfield "1" and upfield "2" Two beta protons are named downfield beta proton, hb1, and upfield beta proton, hb2; if degenerate, then hb*. For CH3 protons the protons hb11,hb12,hb13 and hb21,hb22,hb23. If degenerate, use hb1* for the downfield and hb2* for the upfield. Gamma, delta, epsilon, and eta, protons were treated in a similar manner. note 3a: Pseudo-corrections - NOT USED as of noe10.tbl, swith to sum averaging - ACD 971126 (a) CH3 groups add 1.0 A to the upper limit (b) CH2 group with degenerate protons add 1.0 A to the upper limit (c) degenerate CH3 groups for V, L add 1.7 A to the upper limit (d) aromatics add 2.3 A to the upper limit Conditions for 3D 100 ms NOESY-HSQC contour level = 0.1 # of levels= 20 level mult= 1.2 strong noe (>10 contour) = 1.8 0 0.9 (0 to 2.7 angstroms) strong noe (>10 contour) = 1.8 0 1.1 (0 to 2.9 angstroms for hn) medium noe (7-10 contours) = 1.8 0 1.5 (0 to 3.3 angstroms) medium noe (7-10 contours) = 1.8 0 1.7 (0 to 3.5 angstroms for hns) weak noe (3-6 countours) = 1.8 0 3.2 (0 to 5.0 angstroms) very weak noe (<3 countours) = 1.8 0 4.2 (0 to 6.0 angstroms) very weak(not seen at lvl=0.1) = 1.8 0 4.2 (0 to 6.0 angstroms) residue (nh- ppm) arbitrary assignment (destination residue) (origin residue) assign (segid="sbm1" and resid and name hn) (segid="sbm1" and resid and name hn) {s-m-w, dest'n ppm, # contours,correction} order: intraresidue sequentials medium range long range ordered by dest'n ppm value notes about questions Definitions of codes for commenting out NOEs !I!: all intraresidue NOEs commented out !viol!: comment out b/c violation in xplor run(s) !R!: redundant; weaker of two removed, if equal # levels first appearing removed !amb!: ambiguous and may not necessarily be resolved from any NOESY spectra ******************************************************************************************* **** DATA FROM 3D 13C-EDITED AND 4D 13C,13C-EDITED NOESY SPECTRA ************************** ******************************************************************************************* All parameters not mentioned here are same for the 13C-edited NOESY Conditions for 3D 13C-edited NOESY-HSQC contour level = 0.2 # of levels= 20 level mult= 1.2 strong noe (>10 contours) = 1.8 0 0.9 (0 to 2.7 angstroms) medium noe (7-10 contours) = 1.8 0 1.5 (0 to 3.3 angstroms) weak noe (3-6 countours) = 1.8 0 3.2 (0 to 5.0 angstroms) very weak noe (<3 countours) = 1.8 0 4.2 (0 to 6.0 angstroms) very weak(not seen at lvl=0.1) = 1.8 0 4.2 (0 to 6.0 angstroms) ******************************************************************************************* Ser 1a (nh-10.23; n= 121.93 ppm) hn104 no sidechain peaks in 3D TOCSY LONG NOTES 3D NOESY: noesy100-92 51 28 NOE, hn[], D2(pt), ovlp NN,98, could ovlp nn+2 N+2 (hn70/hn71), 98, could ovlp nn N+3 (hn55), 129 N+4 (hn26), 112 Ser 1b (nh-9.95ppm; n= 120.73) hn108 NOTES 3D NOESY: noesy100-115 61 30 no sidechain peaks in 3D TOCSY sc NOEs at 4.33, 2.27, 1.84, 1.73 NN, 98, could ovlp nn+2 N+2 (hn70/hn71) 98 N+3 (hn55) 128 N+4 (hn26) 112 NOTES 4D CN: signals stronger in 4D than 3D as exected in range of H2O Glu 2 LONG NOTES 3D NOESY (nh- 8.93ppm; n= 120.7) hn62 noesy100- 202 98 30 NN (hn70), 8.94, could ovlp hn62 NN+2 (hn55) 129 NN+3 (hn24/hn26?), 113 NOTES 4D CN: Y= S1 or F43 Leu 3a LONG Glu 4a LONG Lys 5a Ala 6a Met 7 LONG ; 9583 1 9748 6 parsed_1b4c 1 692 ; {w, 6.95, 4, 3.9, no cfilt} Val 8a LONG Ala 9 Leu 10a LONG amb/art? assign (segid="sbm1" and resid 70 and name he*) (segid="sbm1" and resid 10 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 70 and name he*) (segid="sbm2" and resid 10 and name hn) 1.8 0 4.2 {vw, 6.95, 4*} 70he* 6.95 but seems far based on model, 73hd* at 6.90 ; 9752 1 9775 78 parsed_1b4c 1 693 ; {d'', w, 5, 7.09, 5.3} amb b/c peak maxes at L3hd<, could be to F14hd* same CS SD? assign (segid="sbm1" and resid 73 and name hz) (segid="sbm1" and resid 10 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 73 and name hz) (segid="sbm2" and resid 10 and name hn) 1.8 0 4.2 {vw, 7.11, 9*, 0, amb}, could be 14he*, 70hz ; 9779 1 9783 53 parsed_1b4c 1 694 ; {d'', w, 7, 7.09, 2.9} amb b/c peak maxes at L3hd< R assign (segid="sbm1" and resid 74 and name he*) (segid="sbm1" and resid 10 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 74 and name he*) (segid="sbm2" and resid 10 and name hd*) 1.8 0 1.5 {d'', m, 1.56, >12, 4.4, wk cfilt} could be intermolecular contribution amb assign (segid="sbm1" and resid 74 and name hb*) (segid="sbm1" and resid 10 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 74 and name hb*) (segid="sbm2" and resid 10 and name hd*) 1.8 0 3.2 {d'', w, 3, 1.49, 3.9} vios w/ sani amb/RS assign (segid="sbm1" and resid 74 and name hb*) (segid="sbm1" and resid 10 and name hd*) 1.8 0 3.2 amb/RS assign (segid="sbm2" and resid 74 and name hb*) (segid="sbm2" and resid 10 and name hd*) 1.8 0 3.2 {d'', w, 3, 1.92, 3.9} ; 9787 1 9799 31 parsed_1b4c 1 695 ; {d>, m, 0.71, 9, 4.4} amb b/c peak maxes at L3hd< for test14 strucs, intramolecular was 6.6A and intermolecular was 9.2A when restraint was set for either ; 9803 1 9804 106 parsed_1b4c 1 696 ; {d>, w, 0.43??, 6} amb b/c peak maxes at L3hd< and 10hd to 77 could be intra or intermolecular Distance over 10 structures between: VAL 77: HG23/HG22/HG21/ AND LEU 10: HD23/HD22/HD21/HD13/HD12/HD11/ intra Average=7.624 Angtroms, stand. dev.=0.3483, min= 6.94, max= 8.033 Distance over 10 structures between: VAL 77: HG23/HG22/HG21/ AND LEU 10: HD23/HD22/HD21/HD13/HD12/HD11/ inter Average=11.62 Angtroms, stand. dev.=0.6026, min= 10.68, max= 12.63 Distance over 10 structures between: VAL 77: HG23/HG22/HG21/ AND LEU 3: HD23/HD22/HD21/HD13/HD12/HD11/ inter (assigned already) Average=6.681 Angtroms, stand. dev.=0.7836, min= 5.27, max= 8.108 NOTES 3D NOESY: noesy100- 257 122 32 Leu 10a (nh- 8.29ppm; n= 119.76) hn52; strgr of the pair in the HSQC Leu 10b (nh- 8.26ppm; n= 119.60) hn48 Ile 11a LONG NOTES 3D NOESY: noesy100- 246 117 29 Ile 11a (nh- 8.44ppm; n= 121.21) hn65 close to hn67 (V13), but wkr than hn67 Ile 11b (nh- 8.39ppm; n= 121.21) hn65a, wkr than hn65 NN (hn) 8.1ppm, (), could be ovlpd NN-1 (hn) 8.2ppm, (), could be ovlpd NOTES 4D CN: too weak Asp 12 LONG amb assign (segid="sbm1" and resid 70 and name he*) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 70 and name he*) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 6.95, 9*, 2.4} NOTES 3D NOESY: noesy100- 269 127 30 Illhb could also be K26hb* (nh- 8.15ppm; n= 120.73) hn64; in NOESY seems to have vw mult peak Val 13 LONG amb assign (segid="sbm1" and resid 35 and name ha) (segid="sbm1" and resid 13 and name hg1*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 35 and name ha) (segid="sbm2" and resid 13 and name hg1*) 1.8 0 4.2 {vw, 3.62, 2} amb 971118 ; 9808 1 9861 35 parsed_1b4c 1 697 ; {m, 0.57, 9} R assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 13 and name hg1*) 1.8 0 3.2 R assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 13 and name hg1*) 1.8 0 3.2 {w, 0.36, 5} SD? assign (segid="sbm1" and resid 73 and name hz) (segid="sbm1" and resid 13 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 73 and name hz) (segid="sbm2" and resid 13 and name hn) 1.8 0 4.2 {vw, 7.11, 6*, amb} ; 9865 1 9873 28 parsed_1b4c 1 698 ; {w, 7.02, 5} NOTES 3D NOESY (nh- 8.41ppm) hn67 noesy100- 248 118 29 F14 NN (hn50) 8.4ppm, could ovlp w/hn[67]- assumed f14hn-acd I11 NN-2 (hn65) 8.4ppm, could ovlp w/hn[67] NOTES HNH (clvl=0.1): 119.68 (7) F14 and 120.73 D12 Phe 14a Phe 14b LONG amb/art assign (segid="sbm1" and resid 26 and name ha) (segid="sbm1" and resid 14 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 26 and name ha) (segid="sbm2" and resid 14 and name hn) 1.8 0 4.2 {vw, 5.34-7, 2-4*, 0, amb} amb assign (segid="sbm1" and resid 26 and name ha) (segid="sbm1" and resid 14 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 26 and name ha) (segid="sbm2" and resid 14 and name hd*) 1.8 0 4.2 {vw, 5.40, 2, 2.4, amb, 2D} ; 9877 1 9899 36 parsed_1b4c 1 699 "{w, 0.64, 5, 5.3, 4D}" 9903 1 9903 30 parsed_1b4c 1 700 "{vw, 0.39, 7*, amb}" 9907 1 9907 28 parsed_1b4c 1 701 ; {w, 0.41, 6}, 35hd2* sees wk (4lvls) to 14ha R/amb assign (segid="sbm1" and resid ? and name hd*) (segid="sbm1" and resid 14 and name ha) 1.8 0 3.2 R/amb assign (segid="sbm2" and resid ? and name hd*) (segid="sbm2" and resid 14 and name ha) 1.8 0 3.2 {w, 0.59, 3, 1}, could be to 27hd** or to 35hd1*, both are already assigned ; 9911 1 9915 84 parsed_1b4c 1 702 "{vw, 2.61, 2, 3.4, amb, 2D}" 9919 1 9919 36 parsed_1b4c 1 703 ; {w, 6.33, 6, 4.8, 2D} amb assign (segid="sbm1" and resid 73 and name hd*) (segid="sbm1" and resid 14 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 73 and name hd*) (segid="sbm2" and resid 14 and name hn) 1.8 0 4.2 {vw, 6.92, 9*, 2.4, amb} amb 971205 amb assign (segid="sbm1" and resid 73 and name hz) (segid="sbm1" and resid 14 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 73 and name hz) (segid="sbm2" and resid 14 and name hn) 1.8 0 3.2 {w, 7.11, 5, 0, amb} could be to F73he* and F14he* NOTES 3D NOESY: noesy100- ~244 117 31 V13 NN-1 ovlps diag D12 NN-2 (hn64) 8.17ppm very weak but seems to be there NOTES 4D CN an-4 or G66 4.15 in 3D and 4.17 in 4D, 13C goes w/G66 not an-4 sofrom another cube ? Phe 14a (nh- 8.47ppm; n= 119.76) hn50 strgr of the pair Phe 14b (nh- 8.43ppm; n= 119.84) hn51 His 15 LONG amb assign (segid="sbm1" and resid 70 and name he*) (segid="sbm1" and resid 15 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 70 and name he*) (segid="sbm2" and resid 15 and name hn) 1.8 0 4.2 {vw, 6.92, 3*, 2.4, amb}, could be F73 hd* 6.90, 70 seems better from model NOTES 3D NOESY: noesy100- 219 106 35 bN-1 (hn50) 3.14ppm, (4/2), ovlps beta2 NN-2 (hn67) 8.4ppm, could ovlp NN-1 (nh- 8.74ppm; n= 117.42) hn109 - VERY WEAK SIGNAL FOR 3D AND 4D Gln 16 LONG NOTES 3D NOESY: noesy100- 255 120 27 F14 NN-2 (hn50) 8.4ppm, (),could ovlp diag (nh- 8.32ppm; n= 122.25) hn75; close in 15n/1H to hn74(E72) Tyr 17 LONG ; 9923 1 9972 6 parsed_1b4c 1 704 ; {w, 0.64, 6, 2.9, amb} could be 35hd1, amb 980105-acd 27hd*-17hn: Ave=7.26 Angtroms, stand. dev.=0.8448, min= 6.301, max= 9.17 980112 35hd*-17hn: Ave=6.497 Angtroms, stand. dev.=0.405, min= 5.439, max= 7.11 980112 ; 9975 1 9977 95 parsed_1b4c 1 705 ; {mw?, 0.59, 7/~9, 4.4} peak med in 4D to 17hb*, mw for vios - 980105 acd amb/art? assign (segid="sbm1" and resid 35 and name hb*) (segid="sbm1" and resid 17 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 35 and name hb*) (segid="sbm2" and resid 17 and name hn) 1.8 0 4.2 {vw, 1.65, 3*, 1.0, amb} ; 9981 1 9985 34 parsed_1b4c 1 706 "{w, 0.42, 4, 2.9, amb}" 9989 1 9989 31 parsed_1b4c 1 707 ; {w, 0.41, 3, 3.9} NOTES 3D NOESY (nh- 7.37ppm; n= 115.73) hn14 noesy100- 336 156 38 aN-2 (hn109) 5.15ppm, other signals are present in 4D CN at 5.1 that aren't H15 NOTES 4D CN aN-1 (hn75) 3.82ppm is only 1 contour not all Y17 peaks optimize at one 15N value Q16hg2 could alos be M79hb1 Ser 18 LONG ; 9993 1 10009 6 parsed_1b4c 1 708 ; {w, 0.61-4, 6*} NOTES 3D NOESY: noesy100- 140 72 29 (nh- 9.64ppm; n= 121.37) hn112 vwk peak, may be multiple seems to have mult peaks in NOESY 9.66, 9.63, 9.60 aN-4 (hn50) 3.49ppm, could ovlp beta NOTES 4D CN - too weak Gly 19 LONG amb assign (segid="sbm1" and resid 27 and name hd*) (segid="sbm1" and resid 19 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 27 and name hd*) (segid="sbm2" and resid 19 and name hn) 1.8 0 3.2 {w, 0.61, 5*, 3.4, ncn?}, L35hd1* vw peak at 23.80 in 4D, L27hd** @ 0.64 not see pk @ 8.02 27hd* makes most sense from model NOTES 3D NOESY: noesy100- 280 132 51 S18 aN-1 (hn112) 3.9ppm, could ovlp alpha1 (nh- 8.02ppm; n= 107.28) hn1, may be multiple Arg 20 LONG amb assign (segid="sbm1" and resid 31 and name hg*) (segid="sbm1" and resid 20 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 31 and name hg*) (segid="sbm2" and resid 20 and name hn) 1.8 0 4.2 {vw, 2.33, 2, 1.0, amb}, E31hg* sees 7.16; 4D 13C CS suggests E46hg*,E49hg1, or E58hg2 NOTES 3D NOESY: noesy100- 353 163 33 (nh- 7.17ppm; n= 118.63) hn38 Glu 21 LONG NOTES 3D NOESY: noesy100- ~302 142/143 38 G22 NN (hn3) 8.3ppm, could ovlp N37 nn (nh- 7.77ppm; n= 115.81) (hn15) - close N37 (hn13) in 1H and 15N Gly 22 LONG NOTES 3D NOESY: noesy100- 252 120 48 NOTES 4D CN (nh- 8.35ppm; n= 109.13) hn3 E21hb1 could also be K55hb1,E91hb1,K5hb*,M57hb2 E21hb2 could also be K55hb2,E91hb2,V52hb,V53hb,V80hb E21hg* could also be E46hg*,E49hg2 Asp 23 LONG NOTES 3D NOESY (nh- 8.61ppm; n= 125.47) hn86 noesy100- 229 110 23 NN (hn) 8.57ppm, could ovlp hn86 NOTES 4D CN: Close to O1 in D1, so signal not so good Lys 24 LONG NOTES 3D NOESY: noesy100- 232 111 22 NN-1 (hn86) 8.6ppm,could ovlp hn106 beta-N-1 (hn86) ovlps hn86 (D23) from 15N plane one up NOTES 4D CN: ha only sidechain atom of K24 present His 25 LONG amb assign (segid="sbm1" and resid 14 and name he*) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 14 and name he*) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 7.11, 7*, 0} F14&F73he*@7.11, Q16e21@7.11, F70hz@7.12, F88h?@7.13 amb assign (segid="sbm1" and resid 18 and name ha) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 18 and name ha) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 4.01, 2*, 0, amb} NOTES 3D NOESY: noesy100- 184 90 35 (nh- 9.14ppm; n= 117.50) hn25 close to hn21 (E51) in 1H and 15N K26 (NN) 7.71ppm, could ovlp E21(n-2) from next 15N plane, so use 6 ctrs vs. 9 8.57/7.11 are dispersive so intensity may be reduced 6.78/7.11 correspond to Q16 he22 and he21, both are present in 200 ms NOESY NOTES 4D CN: ha 7 ctrs in 4D 1 in 3D go with 4 ctrs Lys 26 - LONG ; 10012 1 10122 15 parsed_1b4c 1 709 "{vw, 7.30, 2, 0, amb} F14hz and 17hd* at 7.30, F76h? at 7.27/7.32, or F88h? at 7.34" 10125 1 10125 93 parsed_1b4c 1 710 ; {vw, 7.11, 7*, 2.4, amb} F14he* & F73he* @7.11/130.5, F73hz 7.09, F70hz@7.12 ?? assign (segid="sbm1" and resid 18 and name ha) (segid="sbm1" and resid 26 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 18 and name ha) (segid="sbm2" and resid 26 and name hn) 1.8 0 4.2 {vw, 4.01, 9*, amb} ; 10129 1 10133 28 parsed_1b4c 1 711 "{w, 3.50, 3, amb}" 10137 1 10137 26 parsed_1b4c 1 712 ; {mw?, 5.34, ?ovlps own ha - amb!, 0} 4D sees 69ha at 1 level when 26hb* at 3 levels NOTES 3D: noesy100- 309 144 35 H25 (NN-1) 9.17ppm, (9), 90, could also be F70; F70 has 7.11/7.30 NOTES 4D CN hb could also ovlp I11hb,Ihb hd 5 at H=596, 3 at H=595, split difference and use 4 contours hg1 could ovlp K5,K28,K55 hg2 could ovlp K33,K48 hd* could ovlp K48hd* NOTES 13C NOESY: 23hb1-26ha could also be 69hb2 (commented out above), but probably to 23hb1 33ha-26hb* could also be from s18b* or v8(ab)ha; viol!- now think above is 33ha-36hb, 36hb & K26hb* overlap 23hb1-26hg2 could also be intra to 26he2, which may be at 2.72(42.07) Leu 27 LONG amb/art assign (segid="sbm1" and resid 13 and name hb) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 13 and name hb) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 2.34, 2, 2.9} art? assign (segid="sbm1" and resid 14 and name ha) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 14 and name ha) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 3.48, 1, 2.9} ; 10141 1 10168 27 parsed_1b4c 1 713 "{w, 7.30, 4, 0, amb}, could be 17hd* both at 7.30 but 17 looks far, F76h? at 7.27/7.32" 10172 1 10172 95 parsed_1b4c 1 714 "{w, 7.30/133.7, 5}" 10176 1 10176 27 parsed_1b4c 1 715 ; {w, 4.00, 8, 2.9}, could also be to S30hb*!! art? assign (segid="sbm1" and resid 20 and name hb*) (segid="sbm1" and resid 27 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 20 and name hb*) (segid="sbm2" and resid 27 and name hn) 1.8 0 4.2 {vw, 1.86, 4, 1.0, amb} art? assign (segid="sbm1" and resid 20 and name hb*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 20 and name hb*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 1.78, 3, 3.9} R assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 1.5 {m, 0.36, 10, 5.8} SD? assign (segid="sbm1" and resid 60 and name hb*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 60 and name hb*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 1.63, 3, 3.9} ; 10180 1 10196 27 parsed_1b4c 1 716 "{vw, 5.07, 6*, 0}" 10200 1 10200 26 parsed_1b4c 1 717 "{m, 9.39, 8, 0}" 10204 1 10204 24 parsed_1b4c 1 718 "{w, 9.38, 4, 0}" 10208 1 10208 24 parsed_1b4c 1 719 ; {vw, 5.21, ~8*, 0} amb assign (segid="sbm1" and resid 68 and name hb*) (segid="sbm1" and resid 27 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 68 and name hb*) (segid="sbm2" and resid 27 and name hn) 1.8 0 4.2 {vw, 2.81, 2, 1.0, amb} ; 10212 1 10216 32 parsed_1b4c 1 720 "{vw, 2.81, 2, 3.9}" 10220 1 10220 27 parsed_1b4c 1 721 ; {w?, 5.37, ~17 ovlp?, 0, amb} D69ha@5.34/51.6, K26ha@5.37/54.3, 26ha sees w @8.62, 69ha sees vw @8.77 amb/art? assign (segid="sbm1" and resid 73 and name hb*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 73 and name hb*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 3.19, 1, 3.9} assign (segid="sbm1" and resid 73 and name hd*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 assign (segid="sbm2" and resid 73 and name hd*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 6.88, 3, 5.3{DJW removed 62698} amb assign (segid="sbm1" and resid 73 and name he*) (segid="sbm1" and resid 27 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 73 and name he*) (segid="sbm2" and resid 27 and name hn) 1.8 0 4.2 {vw, 7.11, 8*, 2.4, amb}, F14&F73he* @7.11/130.5, F70hz@7.12, F73hz@7.07 assign (segid="sbm1" and resid 73 and name he*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 assign (segid="sbm2" and resid 73 and name he*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 7.09, 2, 5.3}, could be F14hd* also {DJW removed} art? assign (segid="sbm1" and resid 77 and name hb) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 77 and name hb) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 1.78, 2, 2.9} art? assign (segid="sbm1" and resid 80 and name hg2*) (segid="sbm1" and resid 27 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 80 and name hg2*) (segid="sbm2" and resid 27 and name hd*) 1.8 0 4.2 {vw, 1.00, 1, 4.9} NOTES 3D NOESY: noesy100- 223 107 31 ha missing in 3D; very weak in 200ms NOTES 4D NOESY: too weak, in solvent ridge Lys 28 LONG ; 10224 1 10260 6 parsed_1b4c 1 722 ; {m?, 5.07, 8, 0} amb assign (segid="sbm1" and resid 67 and name hg*) (segid="sbm1" and resid 28 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 67 and name hg*) (segid="sbm2" and resid 28 and name hn) 1.8 0 3.2 {w, 2.35, 4ov?, 1.0, cn} dont like it based on model NOTES 3D NOESY: noesy100- 179 88 24 NN (hn89) 9.15ppm, vw(7), 91, nearly ovlps hn85 NOTES 4D CN: L27 an >10 in 4D vw in 3D go with 5 ctrs Lys 29 LONG ; 10263 1 10277 6 parsed_1b4c 1 723 "{vw, 0.07, 2, 2.9, ncn}" 10280 1 10280 32 parsed_1b4c 1 724 ; {w, 0.07, 5, 2.9} amb assign (segid="sbm1" and resid 65 and name hn) (segid="sbm1" and resid 29 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 65 and name hn) (segid="sbm2" and resid 29 and name hn) 1.8 0 4.2 {vw, 8.11, 9*, 0} amb assign (segid="sbm1" and resid 66 and name hn) (segid="sbm1" and resid 29 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 66 and name hn) (segid="sbm2" and resid 29 and name hn) 1.8 0 4.2 {vw, 8.11, 9*, 0, recip} ; 10284 1 10292 33 parsed_1b4c 1 725 "{vw, 8.47, 4*, 0, amb}" 10296 1 10296 31 parsed_1b4c 1 726 ; {w, 5.07, 3, 0, ncn} NOTES 3D NOESY: noesy100- 188 92 21 NN-1 (hn) ppm, (), ovlps hn89 NOTES 4D CN: ha NOEs fairly strong, the rest are weak NOTES 13C: K29ha close to S41(e)hb at 3.79(61.90) so could have some ambiguity Ser 30 LONG ; 10300 1 10312 6 parsed_1b4c 1 727 ; {vw, 0.07, 8*} sani assign (segid="sbm1" and resid 64 and name ha*) (segid="sbm1" and resid 30 and name hn) 1.8 0 3.2 sani assign (segid="sbm2" and resid 64 and name ha*) (segid="sbm2" and resid 30 and name hn) 1.8 0 3.2 {w, 3.92, 1disp/8, 1.0, ncn} not clear in 3D, vio w/ sani art? assign (segid="sbm1" and resid 64 and name hn) (segid="sbm1" and resid 30 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 64 and name hn) (segid="sbm2" and resid 30 and name hn) 1.8 0 4.2 {vw, 7.93, 6*, 0} amb assign (segid="sbm1" and resid 65 and name hn) (segid="sbm1" and resid 30 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 65 and name hn) (segid="sbm2" and resid 30 and name hn) 1.8 0 4.2 {vw, 8.09, 9*, 0}, 33hn@8.05 sees vw at 9.40, 65hn@8.09 sees vw @9.37, 66hn@8.09 not see 9.35 vios when sani rest added art? assign (segid="sbm1" and resid 67 and name ha) (segid="sbm1" and resid 30 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 67 and name ha) (segid="sbm2" and resid 30 and name hn) 1.8 0 4.2 {vw, 5.07, 6*, 0, amb} NOTES 3D NOESY: noesy100- 166 83 40 NOTES 4D CN: none of the NOEs to K29 are in the 4D Glu 31 LONG NOTES 3D NOESY: noesy100- 368 170 25 Leu 32 LONG amb assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 1.5 {d'', m, 0.64, 3 in LP, 5.8} looks too far and off in C13 CS, 40hd1* close to 32hd2* in 1h/13c CS ; 10315 1 10353 106 parsed_1b4c 1 728 "{d'', vw, 1.71, 3, 2.9}" 10357 1 10357 32 parsed_1b4c 1 729 ; {vw, 0.39, 2, 2.9, n} R assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 0.36, 3, 5.8} R assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 32 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 32 and name hn) 1.8 0 4.2 {vw, 0.07, 9*, 2.9, n} ; 10361 1 10369 31 parsed_1b4c 1 730 ; {d'', s, 0.08, 10, 5.8} SD? assign (segid="sbm1" and resid 67 and name ha) (segid="sbm1" and resid 32 and name hd*) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 67 and name ha) (segid="sbm2" and resid 32 and name hd*) 1.8 0 4.2 {d'', vw, 5.04, 1*, 2.9} amb assign (segid="sbm1" and resid 68 and name hb*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 68 and name hb*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 4.2 {d', vw, 2.84, 1, 4.9} pk very low in noise ; 10373 1 10381 52 parsed_1b4c 1 731 ; {d', mw, 4.4, 7, 2.9} R assign (segid="sbm1" and resid 73 and name ha) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 73 and name ha) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 4.4, 6, 2.9} ; 10385 1 10389 30 parsed_1b4c 1 732 ; {m/w, 6.88, 8, 5.3} SD? assign (segid="sbm1" and resid 73 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 SD? assign (segid="sbm2" and resid 73 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 6.88, 2, 5.4} ; 10393 1 10397 31 parsed_1b4c 1 733 ; {d'', w, 3.05, 3, 3.9} RS assign (segid="sbm1" and resid 76 and name hb*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 76 and name hb*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 2.77, 3, 3.9} ; 10401 1 10405 31 parsed_1b4c 1 734 ; {d'', w, 7.31, 5, 5.4} not sure if hd*/he*/hz of 76, hd* looks closest on model amb assign (segid="sbm1" and resid 77 and name ha) (segid="sbm1" and resid 32 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 77 and name ha) (segid="sbm2" and resid 32 and name hd*) 1.8 0 4.2 {d'', vw, 3.41, 2, 2.9} could be probably 77ha to 40hd1* art/SD? assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 art/SD? assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d', w, 0.77, 3, 4.4} art? assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 0.77, 7, 4.4} peak does not look real and looks too far on model R assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d', w, 0.43, 4, 4.4} amb assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 0.43, 6, 4.4} could be 77hg2* to 40hd1* and looks far on model art? assign (segid="sbm1" and resid 80 and name hg2*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 80 and name hg2*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 {d'', w, 1.07/23.3, 3, 4.4} not sure looks real, could be based on model NOTES 3D NOESY: noesy100- 249 118 27 Lys 33 LONG amb assign (segid="sbm1" and resid 27 and name hd*) (segid="sbm1" and resid 33 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 27 and name hd*) (segid="sbm2" and resid 33 and name hn) 1.8 0 3.2 {w, 0.64, 4, 3.4, n, amb} could be 35hd so !amb 980106-acd SD? assign (segid="sbm1" and resid 60 and name hn) (segid="sbm1" and resid 33 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 60 and name hn) (segid="sbm2" and resid 33 and name hn) 1.8 0 4.2 {vw, 7.82, 2, 0, amb} amb assign (segid="sbm1" and resid 60 and name ha) (segid="sbm1" and resid 33 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 60 and name ha) (segid="sbm2" and resid 33 and name hn) 1.8 0 4.2 {vw, 3.85, 3ov, 0, amb} ; 10409 1 10453 32 parsed_1b4c 1 735 ; {mw?, 0.39, 8/5, 2.9, ncn} R assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 33 and name hn) 1.8 0 3.2 R assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 33 and name hn) 1.8 0 3.2 {w, 0.07, 3, 2.9, n} ; 10457 1 10461 29 parsed_1b4c 1 736 ; {w, 0.41, 6, 2.9} amb assign (segid="sbm1" and resid 63 and name ha) (segid="sbm1" and resid 33 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 63 and name ha) (segid="sbm2" and resid 33 and name hn) 1.8 0 4.2 {vw, 4.94, 4*, 0, amb}, peak looks antiphase & thus could be 5.02-7 or 63ha, and 67ha amb assign (segid="sbm1" and resid 64 and name hn) (segid="sbm1" and resid 33 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 64 and name hn) (segid="sbm2" and resid 33 and name hn) 1.8 0 4.2 {vw, 7.93, 4ov, 0}, Q71hn, and 50he21 also possible, peak looks real NOTES 3D NOESY: noesy100- 278 131 31 NN-2 (hn84) 7.0ppm, (), could ovlp NN Glu 34 LONG art? assign (segid="sbm1" and resid 17 and name he*) (segid="sbm1" and resid 34 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 17 and name he*) (segid="sbm2" and resid 34 and name hn) 1.8 0 4.2 {vw, 6.70, 5*, amb} !art? - shoulder of autocorrelation and vwk ; 10465 1 10486 76 parsed_1b4c 1 737 ; {vw, 0.39, 2, n} NOTES 3D NOESY: noesy100- 375 173 34 Leu 35 LONG R assign (segid="sbm1" and resid 13 and name hg1*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 13 and name hg1*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 1.5 {d', m, 1.14, 10, 4.4} R assign (segid="sbm1" and resid 13 and name hg1*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 13 and name hg1*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 1.5 {d'', m, 1.14, 10, 4.4} SD/art? assign (segid="sbm1" and resid 14 and name ha) (segid="sbm1" and resid 35 and name hd*) 1.8 0 4.2 SD/art? assign (segid="sbm2" and resid 14 and name ha) (segid="sbm2" and resid 35 and name hd*) 1.8 0 4.2 {d', vw, 3.48, 1, 2.9} R assign (segid="sbm1" and resid 14 and name ha) (segid="sbm1" and resid 35 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 14 and name ha) (segid="sbm2" and resid 35 and name hd*) 1.8 0 3.2 {d''. w, 3.48, 4, 2.9} ; 10490 1 10515 31 parsed_1b4c 1 738 "{vw, 7.30, 2, 2.4}" 10519 1 10519 28 parsed_1b4c 1 739 ; {d', mw, 7.31, 7, 5.3} RS assign (segid="sbm1" and resid 17 and name hd*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 17 and name hd*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 3.2 {d'', w, 7.31, 7, 5.3} ; 10523 1 10527 31 parsed_1b4c 1 740 "{vw?, 6.68, 3, 2.4} sani vios as wk" 10531 1 10531 48 parsed_1b4c 1 741 ; {d', vw, 6.74, 3*, 5.4} art? assign (segid="sbm1" and resid 27 and name hd*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 27 and name hd*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 3.2 {d', w?, 0.64, ?, 5.8} should be close enough but doesnt show up with LP ; 10535 1 10539 81 parsed_1b4c 1 742 ; {d'', mw, 0.65, 8, 5.8} mw 980105 acd, peaks not totally convincing SD? assign (segid="sbm1" and resid 73 and name hd*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 73 and name hd*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 4.2 {d'', vw, 7.02, 2, 5.3} ; 10543 1 10547 32 parsed_1b4c 1 743 ; {d', mw, 7.11, 7, 5.4} RS assign (segid="sbm1" and resid 73 and name he*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 73 and name he*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 3.2 {d'', w, 6.92, 7, 5.4} ; 10551 1 10555 31 parsed_1b4c 1 744 ; {d', w, 7.07, 5, 2.9} R assign (segid="sbm1" and resid 73 and name hz) (segid="sbm1" and resid 35 and name hd*) 1.8 0 4.2 R assign (segid="sbm2" and resid 73 and name hz) (segid="sbm2" and resid 35 and name hd*) 1.8 0 4.2 {d'', vw, 7.02, 2, 2.9} amb/ridge assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 1.1 amb/ridge assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 1.1 {d', s, 0.48, ?, 4.4} NOTES 3D NOESY: noesy100- 268 127 28 NOTES 4D CN L32ha could also be L44, M57, E91 ha's L35ha could also overlap Q50ha, Q71ha L35bn-1 could overlap E49hb1, E72hb1 Ile 36 LONG art? assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 36 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 36 and name hd*) 1.8 0 4.2 {vw, 1.07, 3, 2.5} ; 10559 1 10584 27 parsed_1b4c 1 745 ; {m, 0.78, 10, 3.0} 52hg1 too far based on distance.inp in test14d strucs amb assign (segid="sbm1" and resid 56 and name hg1*) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 56 and name hg1*) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 3.2 {w?, 0.78, 15/ridge?, 3.0} peak wk in LP matrix R assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 36 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 36 and name hd*) 1.8 0 1.5 {m, 0.36, 9, 4.4} RS assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 36 and name hd*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 36 and name hd*) 1.8 0 3.2 {w, 0.07, 3, 4.4} art? assign (segid="sbm1" and resid 73 and name ha) (segid="sbm1" and resid 36 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 73 and name ha) (segid="sbm2" and resid 36 and name hn) 1.8 0 4.2 {vw, 4.39, 7*, 0, amb/art?} RS assign (segid="sbm1" and resid 76 and name hb*) (segid="sbm1" and resid 36 and name hd*) 1.8 0 4.2 RS assign (segid="sbm2" and resid 76 and name hb*) (segid="sbm2" and resid 36 and name hd*) 1.8 0 4.2 {vw, 3.05, 3, 2.5} ; 10588 1 10608 27 parsed_1b4c 1 746 "{w, 2.81, 5, 2.5}" 10612 1 10612 26 parsed_1b4c 1 747 ; {w, 3.48, 3.41/67.2, 4ovlp} R assign (segid="sbm1" and resid 80 and name hg2*) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 1.5 R assign (segid="sbm2" and resid 80 and name hg2*) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 1.5 {m, 1.07/23.3, 9, 3.0} ; 10616 1 10620 31 parsed_1b4c 1 748 ; {m, 0.85, 9, 3.0} art? assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 36 and name hd*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 36 and name hd*) 1.8 0 3.2 {w, 0.85, 3, 3.0} not sure its real NOTES 3D NOESY: noesy100- 235 112 29 NOTES 4D CN: V56hg2 signal doesn't max at H=522 Asn 37 LONG assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 0.39, 7*, 2.9, amb}{DJW removed} SD? assign (segid="sbm1" and resid 77 and name ha) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 77 and name ha) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 3.48/67.2, 5*/2, 0, ncn} 80ha 3.39/67.2, 77ha 3.44/67.2, 8ha 3.52/67.2, 3d sees 3.49 amb assign (segid="sbm1" and resid 80 and name hg2*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg2*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, ~1.1, 3, 1.5, amb} amb assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 0.90, 2, 1.5, amb} may ovlp L40hd1* at 0.90, makes sense from model NOTES 3D NOESY: noesy100- 300 141 38 Asn 38 LONG NOTES 3D NOESY: noesy100- 255 121 39 NOTES 4D CN: N37ha could also be E21ha no good evidence for 35ha-38hb1/2 NOE, but assigned 38hb2-35ha dont see 41hb*-38ha or vice versa, could be b/c 38ha at carrier frequencey Glu 39 LONG 3D NOESY: noesy100- 184 90 39 4D CN: hb1? Wk signal at 2.41, 30.32 which could ovlp hg2 in 3D 13C: 39hb*-36ha assigned, dont see 36ha-39hb* Leu 40 - LONG ; 10624 1 10685 15 parsed_1b4c 1 749 "{d', w, 3.19, 8ovlp, 2.9} could be to 80ha also, but 77ha based on dist.inp for test14d strucs" 10688 1 10688 96 parsed_1b4c 1 750 "{d', w, 1.63, 3, 2.9}" 10692 1 10692 30 parsed_1b4c 1 751 ; {d', m, 0.71, 9, 4.4} amb assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm1" and resid 40 and name hd*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm2" and resid 40 and name hd*) 1.8 0 1.5 {d'', m, 0.71, 11, 4.4} ; 10696 1 10700 32 parsed_1b4c 1 752 ; {d', w, 0.48, 6, 4.4} amb assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm1" and resid 40 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm2" and resid 40 and name hd*) 1.8 0 3.2 {d'', w, 0.50, 3, 4.4} R assign (segid="sbm1" and resid 80 and name hg2*) (segid="sbm1" and resid 40 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 80 and name hg2*) (segid="sbm2" and resid 40 and name hd*) 1.8 0 3.2 {d', w, 1.07, 6, 4.4} ; 10704 1 10712 30 parsed_1b4c 1 753 ; {d', m?, 0.85, 9, 4.4} R assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 40 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 40 and name hd*) 1.8 0 3.2 {d'', w, 0.85, 5, 4.4} ; 10716 1 10720 31 parsed_1b4c 1 754 ; {d', w, 1.99, 3, 2.9} NOTES 3D NOESY: noesy100- 298 139 33 Dont see 40hb*-37ha or 37ha-40hb* Ser 41d LONG amb assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 41 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 41 and name hn) 1.8 0 4.2 {vw, 0.94, 5*, 1.5, amb} could be 53hg1* at 0.96 ? NOTES 3D NOESY: noesy100- 394 181 44 (nh- 6.70ppm; n= 111.79) hn97 mult peak with 98/99 Ser 41e (nh- 6.71ppm; n= 112.27) hn98 NOTES 3D NOESY: noesy100- 393 ~181 43 7.41 is dispersive NOTES 4D CN: overlaps Ser 41d Ser 41f (nh- 6.78ppm; n= 112.75) hn99 NOTES 3D NOESY: noesy100- 387 ~178 43 7.41 is dipsersive NOTES 4D CN: Ser41f missing or too weak His 42d LONG NOTES 3D NOESY: noesy100- 135 70 27 His 42e (nh- 9.57ppm; n= 122.25) hn105 NOTES 3D NOESY: noesy100- 148 75 28 His 42f (nh- 9.46ppm; n= 121.37) hn100 NOTES 3D NOESY: noesy100- 157 79 29 Phe 43d LONG art? assign (segid="sbm1" and resid 57 and name he*) (segid="sbm1" and resid 43 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 57 and name he*) (segid="sbm2" and resid 43 and name hd*) 1.8 0 4.2 {vw, 1.99, 2, 3.9} amb assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 43 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 43 and name hd*) 1.8 0 3.2 {w, 0.85, 4, 3.9} looks too far NOTES 3D NOESY: noesy100- 242 116 25 ha dispersive Phe 43e (nh- 8.33ppm; n= 123.78) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Phe 43f (nh- 8.06ppm; n= 123.22) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Leu 44d LONG ; 10724 1 10797 6 parsed_1b4c 1 755 ; {mw, 0.92, 8} both 53hg1* or V80hg2* for test14d strucs: 53-44: Average=5.878 Angtroms, stand. dev.=0.9916, min= 4.34, max= 7.379 80-44: Average=5.352 Angtroms, stand. dev.=1.498, min= 3.227, max= 8.7 ; 10800 1 10802 79 parsed_1b4c 1 756 "{w, 1.92, 5, 4.9}" 10806 1 10806 26 parsed_1b4c 1 757 ; {w, 0.92, 8, 4.4} both 53hg1* or V80hg2* for test14d strucs: 53-44: Average=5.878 Angtroms, stand. dev.=0.9916, min= 4.34, max= 7.379 80-44: Average=5.352 Angtroms, stand. dev.=1.498, min= 3.227, max= 8.7 NOTES 3D NOESY: noesy100- ~254 ~120 39 alpha- 4.04 ppm (8) ~279 ovlps N38 an-4[9/31] & M7 an-4[8/70] beta- 1.75 ppm (10) 363 ovlps M7 bn-1[8/83] NN-1 (hn102) 8.50ppm, (9/2), 115 ovlps nn[43] Leu 44e (nh- 8.28ppm; n= 115.41) hn12 NOTES 3D NOESY: noesy100- ~257 ~122 39 NN-1 (hn103) 8.33ppm, (), could ovlp hn12 Leu 44f (nh- 8.15ppm; n= 115.33) hn11 NOTES 3D NOESY: noesy100- 268 ~128 39 NN-1 (hn123)8.06ppm, (5), 131 nearly ovlps hn11 NOTES 4D CN: too weak and overlapped Glu 45 LONG art? assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 0.94, 6*, 1.5} 4D 0.90/22.3 = 80hg2*, 53hg2 0.90, 53hg2 0.96 40hd1* 0.93, 3hg1* ~0.91 amb/art? assign (segid="sbm1" and resid 80 and name ha) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 80 and name ha) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 3.39, 2, 0, amb}, 43hb* at 3.41/3.44, 53hb 3.36 NOTES 3D NOESY: noesy100- 338 157 33 Glu 45e (nh- 7.35ppm; n= 118.63) hn36 NOTES 3D NOESY: noesy100- 338 157 33 NOE to 8.15 verifies that d/f overlap Glu 45f (nh- 7.32ppm; n= 118.63) hn37 NOTES 3D NOESY: noesy100- 340 159 33 NN-2 (hn103) 8.3ppm, (), could ovlp nn-1! Glu 46d Glu 46e Glu 46f LONG NOTES 3D NOESY: noesy100- 313 ~146 32 NN (hn116) 7.82ppm, (8/2), ~140 nearly ovlps hn45 beta-N-1 (hn36) 2.22ppm, (10/2), could ovlp beta Ile 47 LONG ; 10810 1 10872 6 parsed_1b4c 1 758 "{w?, 2.06, 7} w b/c 52hb may contribute" 10875 1 10875 48 parsed_1b4c 1 759 "{w, 2.06, 3}" 10879 1 10879 21 parsed_1b4c 1 760 "{mw?, 0.85, 8}, ran as 53hg1 or 80hg1 for test14b - 53hg1 closer by 2 A" 10883 1 10883 80 parsed_1b4c 1 761 ; {s, 0.85, 14} amb assign (segid="sbm1" and resid 53 and name hg1*) (segid="sbm1" and resid 47 and name hd*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 53 and name hg1*) (segid="sbm2" and resid 47 and name hd*) 1.8 0 1.5 {m, 0.85, 9/3LP} ; 10887 1 10891 25 parsed_1b4c 1 762 ; {mw, 0.85, 9ovlp/5LP} art? assign (segid="sbm1" and resid 57 and name hb*) (segid="sbm1" and resid 47 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 57 and name hb*) (segid="sbm2" and resid 47 and name hd*) 1.8 0 4.2 {vw, 1.85, 1} ; 10895 1 10899 22 parsed_1b4c 1 763 ; {m, 1.56, 8} amb/art? assign (segid="sbm1" and resid 84 and name ha) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 84 and name ha) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 4.2 {vw, 4.68, 2} NOTES 3D NOESY: noesy100-302 141 28 (values from HOHAHA-HSQC) hn too weak to observe in 3D or 4D Ile 47e? (nh- 7.81ppm) N= 122.25 hn116 very weak peak NOTES 4D CN: too weak Lys 48 nitrogen data too weak INTRA SEQ MED LONG INTER AMB NOTES 3D NOESY: noesy100- 217 105 20 an-1 and he could overlap NOTES 4D CN: too weak Glu 49 LONG amb assign (segid="sbm1" and resid 83 and name ha) (segid="sbm1" and resid 49 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 83 and name ha) (segid="sbm2" and resid 49 and name hn) 1.8 0 4.2 {vw, 4.48, 3?, 0, cn, in 3D ?} not in 3D? ; 10903 1 10947 50 parsed_1b4c 1 764 ; {w, 1.58, 9ov/6, 1.5} w-971120 NOTES 3D NOESY: noesy100- 304 ~141 31 NN (hn88) 8.5ppm, , ~113 ovlps nn-1 NN-2 (hn116) 7.8ppm, (), could ovlp hn59 NOTES 4D CN: plane overlaps K55, so any NOEs from the CN could be to K55hn Gln 50 LONG NOTES 3D NOESY: noesy100- 237 113 22 NOTES 4D CN: close to D23 in H and N, baseline troulbes at N=11, h=515-525 Glu 51 LONG NOTES 3D NOESY: noesy100- 184 90 36 NN-2 (hn59) 7.71ppm, (6), 144 ovlps hn[25]H25 nn[27] beta-N-1 (hn88) 1.9ppm, (), could ovlp beta, beta and beta-1 carbons also overlap Val 52 LONG amb/SD? assign (segid="sbm1" and resid 79 and name ha) (segid="sbm1" and resid 52 and name hn) 1.8 0 4.2 amb/SD? assign (segid="sbm2" and resid 79 and name ha) (segid="sbm2" and resid 52 and name hn) 1.8 0 4.2 {vw, 3.93, 7*, 0, amb} could be 47ha but 79 looks closer amb assign (segid="sbm1" and resid 79 and name ha) (segid="sbm1" and resid 52 and name hg2*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 79 and name ha) (segid="sbm2" and resid 52 and name hg2*) 1.8 0 4.2 {g1, vw, 3.90, 2, 2.9} amb 980105-acd amb assign (segid="sbm1" and resid 79 and name he*) (segid="sbm1" and resid 52 and name hg1*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 79 and name he*) (segid="sbm2" and resid 52 and name hg1*) 1.8 0 3.2 {g1, w, 1.85, 5, 4.4}, max at other plane and off in 13c CS ; 10951 1 10997 68 parsed_1b4c 1 765 ; {g1, w, 3.38, 5?} amb assign (segid="sbm1" and resid 83 and name hb*) (segid="sbm1" and resid 52 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 83 and name hb*) (segid="sbm2" and resid 52 and name hn) 1.8 0 3.2 {w, 1.65, 6ov, amb} amb 980112 b/c off slightly in CS, 83hb at 1.62 ; 11001 1 11005 80 parsed_1b4c 1 766 ; {g1, w, 1.56, 8?shoulder, 4.4} art? assign (segid="sbm1" and resid 84 and name hb*) (segid="sbm1" and resid 52 and name hg1*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 84 and name hb*) (segid="sbm2" and resid 52 and name hg1*) 1.8 0 4.2 {g1, vw, 2.70, 3, 3.9} AMB NOTES 3D NOESY: noesy100- 365 168 34 Val 53 LONG amb assign (segid="sbm1" and resid 41 and name ha) (segid="sbm1" and resid 53 and name hg1*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 41 and name ha) (segid="sbm2" and resid 53 and name hg1*) 1.8 0 4.2 {vw, 3.97, 3 oivlp?, 1.5, amb} looks too far on model for test21: Average=9.127 Angtroms, stand. dev.=0.5104, min= 8.286, max= 9.724 amb assign (segid="sbm1" and resid 44 and name hg) (segid="sbm1" and resid 53 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 44 and name hg) (segid="sbm2" and resid 53 and name hg2*) 1.8 0 3.2 {w, 1.56, 5, 1.5} not sure about 44hg assignment - 980119 R assign (segid="sbm1" and resid 44 and name hd*) (segid="sbm1" and resid 53 and name hg1*) 1.8 0 1.5 R assign (segid="sbm2" and resid 44 and name hd*) (segid="sbm2" and resid 53 and name hg1*) 1.8 0 1.5 {m, 0.71, 11, 4.4} R assign (segid="sbm1" and resid 47 and name hg2*) (segid="sbm1" and resid 53 and name hg2*) 1.8 0 3.2 R assign (segid="sbm2" and resid 47 and name hg2*) (segid="sbm2" and resid 53 and name hg2*) 1.8 0 3.2 {w, 0.71, 6, 3.0} ; 11009 1 11040 26 parsed_1b4c 1 767 ; {vw, 1.78, 2, 2.5} SD? assign (segid="sbm1" and resid 47 and name hg1*) (segid="sbm1" and resid 53 and name hg2*) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 47 and name hg1*) (segid="sbm2" and resid 53 and name hg2*) 1.8 0 4.2 {vw, 1.00, *, 2.5} ; 11044 1 11048 27 parsed_1b4c 1 768 ; {w, 0.92, 5, 3.0} art? assign (segid="sbm1" and resid 82 and name hg2*) (segid="sbm1" and resid 53 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 82 and name hg2*) (segid="sbm2" and resid 53 and name hg2*) 1.8 0 4.2 {vw, 0.50, 2, 3.0} ; 11052 1 11056 27 parsed_1b4c 1 769 "{w, 1.65, 3/1, 1.5, cn}" 11060 1 11060 33 parsed_1b4c 1 770 ; {s, 1.63, 15, 3.0} NOTES 3D NOESY: noesy100- 387 178 32 beta-N-1 (hn2.0) 2.0ppm, (10/2),could ovlp beta, ovlps in Carbon as well Asp 54 LONG NOTES 3D NOESY: noesy100- 227 108 31 V52 alpha-N-2 (hn34) 3.66ppm, (9/2), 293 could ovlp an-4 Q50 alpha-N-4 (hn88) 3.66ppm, (9/2), 293 could ovlp an-2 NOTES 4D CN: close to O1 in D1 Lys 55 LONG NOTES 3D NOESY: noesy100- 302 141 31 NOTES 4D CN: plane overlaps E49, so NOEs from 4D CN could be to E49 instead Val 56 LONG amb assign (segid="sbm1" and resid 36 and name hd*) (segid="sbm1" and resid 56 and name hg2*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 36 and name hd*) (segid="sbm2" and resid 56 and name hg2*) 1.8 0 4.2 {vw, 0.59, 3, 3.0} amb - not see 56hg2 to 36hd art? assign (segid="sbm1" and resid 75 and name hb*) (segid="sbm1" and resid 56 and name hg2*) 1.8 0 1.5 art? assign (segid="sbm2" and resid 75 and name hb*) (segid="sbm2" and resid 56 and name hg2*) 1.8 0 1.5 {m, 1.21, 7, 2.5} ; 11064 1 11103 26 parsed_1b4c 1 771 "{vw, 4.33, 5, 1.5} vw for sani" 11107 1 11107 44 parsed_1b4c 1 772 "{m, 7.31, 8, 4.4, 76hd,e,z???} add 1A for ambigu 76he closest for test14c structures 980108" 11111 1 11111 100 parsed_1b4c 1 773 "{w, 3.90, 6} viol with wk for asbd9" 11115 1 11115 44 parsed_1b4c 1 774 ; {w, 2.20, 4} R assign (segid="sbm1" and resid 79 and name hb*) (segid="sbm1" and resid 56 and name hg2*) 1.8 0 3.2 R assign (segid="sbm2" and resid 79 and name hb*) (segid="sbm2" and resid 56 and name hg2*) 1.8 0 3.2 {w, 1.84, 6} amb/sani assign (segid="sbm1" and resid 79 and name hg*) (segid="sbm1" and resid 56 and name hg2*) 1.8 0 3.2 amb/sani assign (segid="sbm2" and resid 79 and name hg*) (segid="sbm2" and resid 56 and name hg2*) 1.8 0 3.2 {w, 2.48, 7, 2.5} 56hg*-79he* assigened amb assign (segid="sbm1" and resid 80 and name ha) (segid="sbm1" and resid 56 and name hg2*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 80 and name ha) (segid="sbm2" and resid 56 and name hg2*) 1.8 0 1.5 {m, 3.34, 11, 1.5} 80ha or 53ha - both make sense from model? ; 11119 1 11133 70 parsed_1b4c 1 775 ; {vw, 1.07, 2, 1.5, amb} NOTES 3D NOESY: noesy100- 278 131 27 E58 NN+2 (hn39) 8.27ppm, (), could ovlp nn V52 alpha-N-4 (hn34) 3.66ppm, (10/2), ~293, could ovlp ha Met 57 LONG ; 11137 1 11148 6 parsed_1b4c 1 776 "{w, 3.49, 6, 1.5}" 11151 1 11151 26 parsed_1b4c 1 777 ; {w, 1.21, 4, 2.5} RS assign (segid="sbm1" and resid 33 and name hg*) (segid="sbm1" and resid 57 and name he*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 33 and name hg*) (segid="sbm2" and resid 57 and name he*) 1.8 0 3.2 {w, 1.21, 5, 2.5} ; 11155 1 11159 26 parsed_1b4c 1 778 "{w, 1.71, 7, 1.5}" 11163 1 11163 26 parsed_1b4c 1 779 "{mw, 0.50, 9, 3.0} 57he to 36hd onlt 7 lvls" 11167 1 11167 57 parsed_1b4c 1 780 "{m, 0.78, >15 ridge, 3.0}" 11171 1 11171 34 parsed_1b4c 1 781 ; {w, 4.19, 3, 1.5} R assign (segid="sbm1" and resid 44 and name hd*) (segid="sbm1" and resid 57 and name he*) 1.8 0 3.2 R assign (segid="sbm2" and resid 44 and name hd*) (segid="sbm2" and resid 57 and name he*) 1.8 0 3.2 {w?, 0.71, 9, 4.4} 44 sees as weak ; 11175 1 11179 43 parsed_1b4c 1 782 "{vw, 1.07, 7*, 1.5, amb}" 11183 1 11183 34 parsed_1b4c 1 783 ; {w, 1.07, 7, 3.0} amb assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 57 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 57 and name hn) 1.8 0 4.2 {vw?, 0.94, 6, 1.5, amb} 53hg1* at 0.96 NOTES 3D NOESY: noesy100- 256 ~121 37 E58 NN (hn39) 8.27ppm, (>10/2), ~123 ovlps hn19 V56 beta-N-1 (hn80) 2.33ppm, (10/2), ovlps hb2 in H and C Glu 58 LONG amb assign (segid="sbm1" and resid 80 and name hg2*) (segid="sbm1" and resid 58 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg2*) (segid="sbm2" and resid 58 and name hn) 1.8 0 4.2 {vw, 1.07, 8*, 1.5, amb} amb assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm1" and resid 58 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm2" and resid 58 and name hn) 1.8 0 4.2 {vw, 0.96, 7*, 1.5, amb} could be 53hg1* at 0.96 NOTES 3D NOESY: noesy100- 260 123 33 NOTES 4D CN M57 NN-1 (hn19) 8.30ppm, (), could ovlp hn39 T59 NN (hn18) 8.04ppm, (12), 132 could ovlp nn-2[80] Thr 59 LONG amb assign (segid="sbm1" and resid 29 and name hb*) (segid="sbm1" and resid 59 and name hg2*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 29 and name hb*) (segid="sbm2" and resid 59 and name hg2*) 1.8 0 4.2 {vw, 2.27, 3, 2.5} amb assign (segid="sbm1" and resid 76 and name hz) (segid="sbm1" and resid 59 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 76 and name hz) (segid="sbm2" and resid 59 and name hn) 1.8 0 4.2 {vw, 7.30, 8*, 0, amb} ; 11187 1 11228 31 parsed_1b4c 1 784 ; {w, 7.24-31, 6, 1.5} 2-3 aromatics in 4D, not sure which 1H of 76 so used hz b/c looks closest on model - 3/28/96 amb assign (segid="sbm1" and resid 76 and name hd*) (segid="sbm1" and resid 59 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 76 and name hd*) (segid="sbm2" and resid 59 and name hg2*) 1.8 0 3.2 {w, 7.24-31, 6, 3.9} amb assign (segid="sbm1" and resid 76 and name he*) (segid="sbm1" and resid 59 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 76 and name he*) (segid="sbm2" and resid 59 and name hg2*) 1.8 0 3.2 {w, 7.24-31, 6, 3.9} NOTES 3D NOESY: noesy100- 281 132 37 NN-1 (hn39) 8.2ppm, (14), 123 could ovlp nn-2[19] NN-2 (hn19) 8.3ppm, (14/2), could ovlp nn-1[39] Leu 60 LONG DL assign (segid="sbm1" and resid 28 and name hd*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 4.2 DL assign (segid="sbm2" and resid 28 and name hd*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 4.2 {d'', vw, 1.49, 3, 3.9} R assign (segid="sbm1" and resid 29 and name ha) (segid="sbm1" and resid 60 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 29 and name ha) (segid="sbm2" and resid 60 and name hd*) 1.8 0 3.2 {d'', w, 3.76, 5, 2.9} amb/art? assign (segid="sbm1" and resid 29 and name hb*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 29 and name hb*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 4.2 {d'', vw, 2.27, 2, 3.9} amb/art? assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 4.2 {d'', vw, 1.49, 1, 3.9} amb/art? assign (segid="sbm1" and resid 29 and name hd*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 29 and name hd*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 4.2 {d'', vw, 1.07, 1, 3.9} amb assign (segid="sbm1" and resid 32 and name hb*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 32 and name hb*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 4.2 {d', vw, 1.42, 2, 3.9} R assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 1.5 {d', m, 0.85, 9, 5.8} R assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 3.2 {d', w, 0.85, 3, 5.8} R assign (segid="sbm1" and resid 33 and name ha) (segid="sbm1" and resid 60 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 33 and name ha) (segid="sbm2" and resid 60 and name hd*) 1.8 0 1.5 {d', m, 3.48, 8, 2.9} ; 11232 1 11288 30 parsed_1b4c 1 785 ; {d', w, 1.63, 3, 3.9} RS assign (segid="sbm1" and resid 33 and name hb*) (segid="sbm1" and resid 60 and name hd*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 33 and name hb*) (segid="sbm2" and resid 60 and name hd*) 1.8 0 3.2 {d', w, 1.63, 3, 3.9} ; 11292 1 11296 30 parsed_1b4c 1 786 ; {d', m, 0.59, 8, 4.4} amb assign (segid="sbm1" and resid 37 and name ha) (segid="sbm1" and resid 60 and name hd*) 1.8 0 7.1 amb assign (segid="sbm2" and resid 37 and name ha) (segid="sbm2" and resid 60 and name hd*) 1.8 0 7.1 {d'', vw, 4.26, 2, 2.9} off in CS for 37ha ; 11300 1 11304 51 parsed_1b4c 1 787 ; {vw, 7.30, 8*, 0, amb} not sure which 1H of 76, used hz b/c looks closest on model - 3/28/96 NOTES 3D NOESY: noesy100- 298 140 29 D61 NN (hn20) 7.7ppm, (11), ovlps L60 hn[68] Asp 61 LONG amb assign (segid="sbm1" and resid 33 and name he*) (segid="sbm1" and resid 61 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 33 and name he*) (segid="sbm2" and resid 61 and name hn) 1.8 0 4.2 {vw, 3.05, 5*, 0, amb}, 33he* unassigned for sure (2.9 possible), and Lys he usually about 3.0 NOTES 3D NOESY: noesy100- 304 142 36 NN-1 (hn68) 7.81ppm, (25/3), could ovlp D61 hn20 NN (hn53) 7.78ppm, (25/3), could ovlp D61 hn20 Glu 62 LONG NOTES 3D NOESY: noesy100- 301 141 32 NN-1 (hn20) 7.74ppm, (), ovlps E62 hn53 NN-2 (hn68) 7.81ppm, (), ovlps E62 hn53 Asp 63 LONG NOTES 3D NOESY: noesy100- 350 162 34 E62 NN-1 (hn53) 7.79ppm, (14/2), 141 could ovlp nn-2[20] D61 NN-2 (hn20) 7.74ppm, (14/2), 141 could ovlp nn-1[53] ; 11308 1 11347 65 parsed_1b4c 1 788 ; Gly 64 LONG assign (segid="sbm1" and resid 29 and name hb*) (segid="sbm1" and resid 64 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 29 and name hb*) (segid="sbm2" and resid 64 and name hn) 1.8 0 4.2 {vw, 2.30, 7*, 1.0, amb} 58hg2 2.27 but looks too far {DJW removed} amb assign (segid="sbm1" and resid 30 and name hn) (segid="sbm1" and resid 64 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 30 and name hn) (segid="sbm2" and resid 64 and name hn) 1.8 0 4.2 {vw, 9.36, 3*, 0} NOTES 3D NOESY: noesy100- 290 136 49 G66 NN+2 (hn4) 8.09ppm, (), could ovlp nn Asp 65 LONG NOTES 3D NOESY: noesy100- 274 129 38 NN (hn4) 8.09ppm, (24/2), could ovlp hn16 Gly 66 LONG R assign (segid="sbm1" and resid 29 and name hn) (segid="sbm1" and resid 66 and name hn) 1.8 0 4.2 R assign (segid="sbm2" and resid 29 and name hn) (segid="sbm2" and resid 66 and name hn) 1.8 0 4.2 {vw?, 9.10, 3*} ; 11355 1 11386 24 parsed_1b4c 1 789 "{w, 2.30, 2, amb{DJW removed}" 11390 1 11390 38 parsed_1b4c 1 790 ; assign (segid="sbm1" and resid 29 and name hg*) (segid="sbm1" and resid 66 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 29 and name hg*) (segid="sbm2" and resid 66 and name hn) 1.8 0 4.2 {vw, 1.78, 2, amb}{DJW removed} ; 11395 1 11397 40 parsed_1b4c 1 791 ; {vw, 1.54, 2, amb} not sure on CS assignment for 29hd1 NOTES 3D NOESY: noesy100- 274 129 47 D65 NN-1 (hn16) 8.09ppm, (), ovlps hn4 Glu 67 LONG ; 11401 1 11411 6 parsed_1b4c 1 792 "{vw, 4.91, 8*ov, 0, amb}, could be 65ha at 4.88" 11414 1 11414 56 parsed_1b4c 1 793 ; amb assign (segid="sbm1" and resid 28 and name hb*) (segid="sbm1" and resid 67 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 28 and name hb*) (segid="sbm2" and resid 67 and name hn) 1.8 0 4.2 {vw, 2.38, 8ov 67hg, 1.0} ; 11419 1 11421 34 parsed_1b4c 1 794 ; {vw, 9.10, ~5*, 0, amb} amb assign (segid="sbm1" and resid 28/29 and name hd?) (segid="sbm1" and resid 67 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 28/29 and name hd?) (segid="sbm2" and resid 67 and name hn) 1.8 0 4.2 {vw, 1.51, 1, 0, amb} amb assign (segid="sbm1" and resid 29 and name he*) (segid="sbm1" and resid 67 and name hn) 1.8 0 5.2 amb assign (segid="sbm2" and resid 29 and name he*) (segid="sbm2" and resid 67 and name hn) 1.8 0 5.2 {vw, 2.81, 2, 1.0, amb}, 29he* or 65hb1, 65hb1 looks too far NOTES 3D NOESY: noesy100- 241 115 33 D65 NN-2 (hn16) 8.09ppm, (), could ovlp nn-1 Cys 68 LONG ; 11425 1 11443 6 parsed_1b4c 1 795 "{vw, 5.37, 2/*, 0, ncn}" 11446 1 11446 32 parsed_1b4c 1 796 "{vw, 1.73, 8ov, 1.0, amb} looks far for 26hb*, but too strong for 28hb2 alone or 28hd*" 11450 1 11450 95 parsed_1b4c 1 797 "{m, 8.71, 9, 0}" 11454 1 11454 24 parsed_1b4c 1 798 ; {w, 1.51, 6, 1.0, n} 26hd*, 26hg1, 27hb1, and 32hg all @ 1.51, 27hb1 looks closest RS assign (segid="sbm1" and resid 27 and name hb*) (segid="sbm1" and resid 68 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 27 and name hb*) (segid="sbm2" and resid 68 and name hn) 1.8 0 4.2 {vw, 1.26, ~8*, 1.0, amb} ; 11458 1 11462 34 parsed_1b4c 1 799 "{vw, 0.64, ~9*, 3.4, amb}" 11466 1 11466 34 parsed_1b4c 1 800 "{vw, 9.26, 3, 0, amb}" 11470 1 11470 30 parsed_1b4c 1 801 "{w, 4.91, 4, 0, ncn}" 11474 1 11474 29 parsed_1b4c 1 802 ; {w, 2.35, 5ov?, 1.0, amb} 67hg1 at 2.38? RS assign (segid="sbm1" and resid 28 and name hb*) (segid="sbm1" and resid 68 and name hn) 1.8 0 3.2 RS assign (segid="sbm2" and resid 28 and name hb*) (segid="sbm2" and resid 68 and name hn) 1.8 0 3.2 {w, 1.73, 8ov?, 1.0, amb} could also be 28hd* and 26hb* but they look too far ; 11478 1 11482 86 parsed_1b4c 1 803 ; {vw, 9.11, 1, 0, amb} NOTES 3D NOESY: noesy100- 164 82 31 X/Y= R20hg1,hg2 not in 4D NOESY, also observed for G66 NOTES 4D CN K26ha 4 ctrs in 4D 9* in 3D go with 2 K28ha 6ctrs in 4D 3 in 3D go with 4 Asp 69 LONG ; 11486 1 11499 6 parsed_1b4c 1 804 ; {vw, 1.73, 4*, 1.0, amb} amb assign (segid="sbm1" and resid 27/26 and name hb2/g2) (segid="sbm1" and resid 69 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 27/26 and name hb2/g2) (segid="sbm2" and resid 69 and name hn) 1.8 0 4.2 {vw, 1.26, 4*, 0, amb} NOTES 3D NOESY: noesy100- 233 111 27 Phe 70 - LONG ; 11502 1 11514 15 parsed_1b4c 1 805 "{w, 7.11, 2} lots possibilities at 7.11" 11517 1 11517 48 parsed_1b4c 1 806 ; {w, 7.30, 8*, amb}could be 71he21 at 7.32 but dont see he22 at 6.70 amb/anis 980106-acd b/c of large vio for 70 N-HN anis NOTES 3D NOESY: noesy100- 181 89 32 ; 11524 1 11526 37 parsed_1b4c 1 807 ; Gln 71 LONG NOTES 3D NOESY: noesy100- 288 135 35 D69 NN-2 (hn78) 8.58ppm, (4/2), 110 could ovlp nn+2 F73 NN+2 (hn72) 8.62ppm, (4/2), 110 could ovlp nn-2 Glu 72 close to Q16 in 1H and 15N LONG NOTES 3D NOESY: noesy100- 254 121 28 M74 NN+2 (hn32) 8.00ppm, () could ovlp nn-1 Phe 73 - LONG SD? assign (segid="sbm1" and resid 14 and name hd*) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 SD? assign (segid="sbm2" and resid 14 and name hd*) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 6.24, 4*, 2.4, amb} amb assign (segid="sbm1" and resid 14 and name he*) (segid="sbm1" and resid 73 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 14 and name he*) (segid="sbm2" and resid 73 and name hn) 1.8 0 3.2 {w, 7.11, 2, 2.4, amb} 73he* also at 7.11, but it could not be wk to 73hn b/c too far away amb assign (segid="sbm1" and resid 14 and name hz) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 14 and name hz) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 7.30-3, 6*, 0} 76ring 7.27 and 7.30 but far away, 88ring 7.34 could be close? assign (segid="sbm1" and resid 27 and name hd*) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 27 and name hd*) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 0.64, 5*, 3.4, amb assign (segid="sbm1" and resid 27 and name hb*) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 27 and name hb*) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 1.51, ~15*, amb} 26hg1, 26hd*, and 32hg also at 1.51 RS assign (segid="sbm1" and resid 27 and name hb*) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 RS assign (segid="sbm2" and resid 27 and name hb*) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 1.24, 2ov, 1.5, amb} 75hb* looks too far, think its 32hd1* at 1.21 and 27hb2 at 1.26 amb assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 73 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 73 and name hn) 1.8 0 4.2 {vw, 1.24, 2ov, 2.9, amb} could be 75hb* at 1.24 R assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 73 and name ha) 1.8 0 3.2 R assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 73 and name ha) 1.8 0 3.2 {w, 1.21, 4, 2.9, nv 0} R assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 73 and name hb*) 1.8 0 4.2 R assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 73 and name hb*) 1.8 0 4.2 {vw, 1.21, 2*, 3.9} NOTES 3D NOESY: noesy100- 229 110 29 Q71 NN-2 (hn28) 7.93ppm, (), could ovlp nn NOTES 4D CN: close to O1 in D1 so intensity greatly attenuated Met 74 - LONG ; 11533 1 11601 15 parsed_1b4c 1 808 ; {m, 2.06, 13, 3.0, md cfilt} med as both intra and inter Dist over 10 (test_rama3) strucs intra: Average=5.324 Angtroms, stand. dev.=0.4607, min= 4.231, max= 6.081 Dist over 10 (test_rama3) strucs inter: Average=5.691 Angtroms, stand. dev.=0.7689, min= 4.542, max= 6.957 ; 11604 1 11606 109 parsed_1b4c 1 809 ; {mw, 1.00, 16, med cfilt?} mw b/c some inter contribution amb assign (segid="sbm1" and resid 10 and name hd*) (segid="sbm1" and resid 74 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 10 and name hd*) (segid="sbm2" and resid 74 and name hn) 1.8 0 4.2 {vw, 0.97, 3*, 2.9} RS assign (segid="sbm1" and resid 10 and name hd*) (segid="sbm1" and resid 74 and name he*) 1.8 0 1.5 RS assign (segid="sbm2" and resid 10 and name hd*) (segid="sbm2" and resid 74 and name he*) 1.8 0 1.5 {m?, 0.92, >12 ovlp L3hd1*?, 4.4, wk cfilt 1.00} amb assign (segid="sbm1" and resid 10 and name ha) (segid="sbm1" and resid 74 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 10 and name ha) (segid="sbm2" and resid 74 and name he*) 1.8 0 4.2 {vw, 4.11, 2, 1.5} amb 980112 b/c off in CS amb assign (segid="sbm1" and resid 25 and name ha) (segid="sbm1" and resid 74 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 25 and name ha) (segid="sbm2" and resid 74 and name hn) 1.8 0 4.2 {vw, 4.88, 4*, 0, amb}, 25ha at 4.91 to 25hn so CS off amb assign (segid="sbm1" and resid 27 and name hd*) (segid="sbm1" and resid 74 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 27 and name hd*) (segid="sbm2" and resid 74 and name hn) 1.8 0 4.2 {vw, 0.61, ~9*, 3.4, amb} NOTES 3D NOESY: noesy100- 282 133 34 F76 NN+2 (hn23) 7.99ppm, (), could ovlp M74 hn32 Ala 75 NOTES 3D NOESY: noesy100- 294 138 22 M74 NN-1 (hn32) 8.00ppm, (14/2), 133 ovlps nn F76 NN (hn23) 7.99ppm, (14/2), 133 ovlps nn-1 Phe 76 LONG assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 76 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 76 and name hn) 1.8 0 4.2 {vw, 0.94, 3, 2.9, amb}{DJW removed} art? assign (segid="sbm1" and resid 56 and name hg2*) (segid="sbm1" and resid 76 and name hn) 1.8 0 3.2 art? assign (segid="sbm2" and resid 56 and name hg2*) (segid="sbm2" and resid 76 and name hn) 1.8 0 3.2 {w, 1.15/23.4, 5, 1.5, cn} off in CS fro 56hg1* and looks too far amb assign (segid="sbm1" and resid 56 and name hg1*) (segid="sbm1" and resid 76 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 56 and name hg1*) (segid="sbm2" and resid 76 and name hn) 1.8 0 4.2 {vw, 0.80, 2ov, 1.5} 77hg1 at 0.78, 56hg2* at 0.83, could be both?, 77hg1* looks too far NOTES 3D NOESY: noesy100- 283 133 35 ha vw in 3D NOESY and 10 ctrs in 4D go with 5 ctrs Val 77 LONG amb assign (segid="sbm1" and resid 10 and name hd*) (segid="sbm1" and resid 77 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 10 and name hd*) (segid="sbm2" and resid 77 and name hn) 1.8 0 4.2 {vw, 1.07, 9*ov, 2.9} R/amb assign (segid="sbm1" and resid 10 and name hd*) (segid="sbm1" and resid 77 and name hg1*) 1.8 0 1.5 R/amb assign (segid="sbm2" and resid 10 and name hd*) (segid="sbm2" and resid 77 and name hg1*) 1.8 0 1.5 {m, 0.92/25.6, 12ov?, 4.4} could be to both L3hd< and L10hd>, see L10 long ; 11610 1 11677 88 parsed_1b4c 1 810 ; {w?, 1.24, 7ov?, 2.9, amb} 75hb* at 1.24, dist to 32hd* = 7.4A, 5.1A to 75hb* assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 77 and name hg2*) 1.8 0 3.2 assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 77 and name hg2*) 1.8 0 3.2 {w, 1.13, 7, 4.4}{DJW removed} amb/RS assign (segid="sbm1" and resid 32 and name hd*) (segid="sbm1" and resid 77 and name hn) 1.8 0 3.2 amb/RS assign (segid="sbm2" and resid 32 and name hd*) (segid="sbm2" and resid 77 and name hn) 1.8 0 3.2 {w, 0.94, 5, 2.9, amb} L10hd2* 0.97 also?, it should be there ; 11681 1 11689 70 parsed_1b4c 1 811 "{vw, 0.61, 4ov, amb}" 11693 1 11693 29 parsed_1b4c 1 812 ; {w, 0.57, 5, 3.0} R assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 77 and name hg1*) 1.8 0 1.5 R assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 77 and name hg1*) 1.8 0 1.5 {m, 0.85, 11ov?, 4.4} R/amb assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 77 and name hg2*) 1.8 0 3.2 R/amb assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 77 and name hg2*) 1.8 0 3.2 {w?, 0.94, 8, 4.4} art? assign (segid="sbm1" and resid 40? and name hd2*) (segid="sbm1" and resid 77 and name hg1*) 1.8 0 1.5 art? assign (segid="sbm2" and resid 40? and name hd2*) (segid="sbm2" and resid 77 and name hg1*) 1.8 0 1.5 {m, 0.57, 8, 3.0} off in CS for 40hd2* amb assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 77 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 77 and name hg2*) 1.8 0 3.2 {w, 0.94, 9, 4.4} looks too far for 40hd2*, probably to L3hd2* NOTES 3D NOESY: noesy100- 244 116 35 A75 NN-2 (hn87) 7.8ppm, (5/2), 139 could ovlp nn+2 M79 NN+2 (hn79) 7.8ppm, (5/2), 139 could ovlp nn-2 Ser 78 LONG NOTES 3D NOESY: noesy100- 228 109 32 M79 NN (hn79) 7.85ppm, (12), 139 could ovlp nn+2 Met 79 - LONG amb assign (segid="sbm1" and resid 52 and name hg*) (segid="sbm1" and resid 79 and name hn) 1.8 0 5.7 amb assign (segid="sbm2" and resid 52 and name hg*) (segid="sbm2" and resid 79 and name hn) 1.8 0 5.7 {vw, 0.80, 3, 1.5, amb} could be to V77hg1* at 0.78 and/or 52hg2* at 0.83 ; 11697 1 11737 82 parsed_1b4c 1 813 ; {w, 0.78/20.7, 10, 3.0 may be to both 52hg2* and 56hg2*, at least weak to 56hg2* amb assign (segid="sbm1" and resid 55 and name hg*) (segid="sbm1" and resid 79 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 55 and name hg*) (segid="sbm2" and resid 79 and name he*) 1.8 0 4.2 {vw, 1.42/24.5, 3, 2.5} ; 11741 1 11745 32 parsed_1b4c 1 814 "{m, 1.14/23.3, 10}{lowered 1 A since ambiguous}" 11749 1 11749 56 parsed_1b4c 1 815 ; {w, 0.78/20.7, 10, 3.0} may be to both 52hg2* and 56hg2*, at least weak to 56hg2* NOTES 3D NOESY: noesy100- 297 139 27 V80 NN (hn22) 7.80ppm, (25/2), ~139 could ovlp M79 hn79 Val 80 - LONG ; 11753 1 11761 15 parsed_1b4c 1 816 "{m, 0.78, 9}" 11764 1 11764 25 parsed_1b4c 1 817 "{m, 0.59, 9}" 11768 1 11768 25 parsed_1b4c 1 818 ; {w, 0.85, 6} amb assign (segid="sbm1" and resid 52 and name ha) (segid="sbm1" and resid 80 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 52 and name ha) (segid="sbm2" and resid 80 and name hg2*) 1.8 0 3.2 {w, 3.28, 4} ; 11772 1 11776 21 parsed_1b4c 1 819 ; {m?, 0.78, >15} could be to both 56hg1 and 52hg1, for test14d structures with OR assignment: 56hg1#-80hg2#: Ave=4.196 Angtroms, stand. dev.=0.3527, min= 3.476, max= 4.705 52hg1#-80hg2#: Ave=7.136 Angtroms, stand. dev.=0.2377, min= 6.701, max= 7.538 since it could be partially from both, I lowered it from 1.1 to 3.2 DJW amb assign (segid="sbm1" and resid 60 and name hd*) (segid="sbm1" and resid 80 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 60 and name hd*) (segid="sbm2" and resid 80 and name hg2*) 1.8 0 3.2 {w, 0.36/25.6, 4} NOTES 3D NOESY: noesy100- 298 139 36 M79 NN-1 (hn79) ppm, (22/2), ~139 ovlps V80 hn22 T81 NN+2 (hn) ppm, (), could ovlp hn22 NOTES 4D CN: M79 an-1 could also be R20, F88 Thr 81 LONG art? assign (segid="sbm1" and resid 40 and name ha) (segid="sbm1" and resid 81 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 40 and name ha) (segid="sbm2" and resid 81 and name hn) 1.8 0 4.2 {vw, 5.04, 2*, 0, amb} amb assign (segid="sbm1" and resid 43 and name hd*) (segid="sbm1" and resid 81 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 43 and name hd*) (segid="sbm2" and resid 81 and name hg2*) 1.8 0 3.2 {w, 7.17, 3, 4.4} ; 11780 1 11806 26 parsed_1b4c 1 820 ; {w, 7.38, 5, 4.4} NOTES 3D NOESY: noesy100- ~270 ~127 38 V80 NN-1 (hn22) 7.80ppm, (10/3), ~139 could ovlp nn and nn-2 T82 NN (hn111) 7.87ppm, (10/3), ~139 could ovlp nn-1/-2 M79 NN-2 (hn79) 7.83ppm, (10/3), ~139 could ovlp nn and nn-1 NOTES 4D CN V80 aN-1 (hn22) and V77 aN-4 (hn29) 3.4ppm, ovlp @ C=67.23; could also be I11 or V53 S78an-3 could also be S41ha,hb or I47hb Thr 82 LONG amb assign (segid="sbm1" and resid 48 and name hb*) (segid="sbm1" and resid 82 and name hg2*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 48 and name hb*) (segid="sbm2" and resid 82 and name hg2*) 1.8 0 4.2 {vw, 1.71, 2, 2.5} amb assign (segid="sbm1" and resid 53 and name hg2*) (segid="sbm1" and resid 82 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 53 and name hg2*) (segid="sbm2" and resid 82 and name hg2*) 1.8 0 3.2 {w, 0.78, 6, 3.0} amb assign (segid="sbm1" and resid 53 and name hg1*) (segid="sbm1" and resid 82 and name hg2*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 53 and name hg1*) (segid="sbm2" and resid 82 and name hg2*) 1.8 0 1.5 {m, 0.92, 8, 3.0} NOTES 3D NOESY: noesy100- 293 137 45 there was some uncertainty about the assignment of ha and hb however a unique noe was observed for A83 to 3.79,68.38 consistent with the current assignment of the ha and hb for T82 M79 aN-3 (hn79) 3.96ppm, vw(9), ~282 could ovlp an-4; strgr at 8.6ppm S78 aN-4 (hn49) 3.96ppm, vw(9), ~282 could ovlp an-3; strgr at 8.6ppm vw pk 100ms NOESY looks like two peaks 7.88/7.86 Ala 83 LONG amb/art? assign (segid="sbm1" and resid 44 and name hd*) (segid="sbm1" and resid 83 and name hb*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 44 and name hd*) (segid="sbm2" and resid 83 and name hb*) 1.8 0 4.2 {vw, 0.64, 1} ; 11810 1 11855 22 parsed_1b4c 1 821 "{mw?, 1.92, 8}" 11859 1 11859 23 parsed_1b4c 1 822 "{w, 2.13, 3}" 11863 1 11863 21 parsed_1b4c 1 823 "{vw, 3.62, 3}" 11867 1 11867 22 parsed_1b4c 1 824 "{vw, 2.11, 3, amb}" 11871 1 11871 27 parsed_1b4c 1 825 ; {m, 2.06, 10ov}{Lowered to 3.2 since ambiguous; DJW lowered} R assign (segid="sbm1" and resid 52 and name hg*) (segid="sbm1" and resid 83 and name hb*) 1.8 0 1.5 R assign (segid="sbm2" and resid 52 and name hg*) (segid="sbm2" and resid 83 and name hb*) 1.8 0 1.5 {m, 0.99, 10} ; 11875 1 11879 22 parsed_1b4c 1 826 "{w, 0.83, 5/2} looks OK 971125" 11883 1 11883 40 parsed_1b4c 1 827 "{s?, 0.78/20.7, 16/ridge}" 11887 1 11887 34 parsed_1b4c 1 828 "{mw?, 3.34, 9ov?}" 11891 1 11891 26 parsed_1b4c 1 829 ; {w?, 2.06, 10ov} amb assign (segid="sbm1" and resid 53 and name hg1*) (segid="sbm1" and resid 83 and name hb*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 53 and name hg1*) (segid="sbm2" and resid 83 and name hb*) 1.8 0 3.2 {w?, 0.99, 10?, 3.0} NOTES 3D NOESY: noesy100- 347 160 29 ha dispersive in 3D NOESY; hb 17 ctrs in both expts so 9 ctrs used for ha Cys 84 LONG amb assign (segid="sbm1" and resid 53 and name ha) (segid="sbm1" and resid 84 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 53 and name ha) (segid="sbm2" and resid 84 and name hn) 1.8 0 4.2 {vw, 3.33, 5*, amb} art? assign (segid="sbm1" and resid 53 and name hb) (segid="sbm1" and resid 84 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 53 and name hb) (segid="sbm2" and resid 84 and name hn) 1.8 0 4.2 {vw, 2.08, 3*, amb} NOTES 3D NOESY: noesy100- 325 151 37 His 85? INTRA LONG (nh- 8.35ppm) hn119 seems to be multiple 8.35, 8.34, 8.33 nn region differs a little between 100 and 200 ms noesy100- ~254 ~121 48 alpha?- 3.68 ppm () ~292 ovlps has[3], could be 3.8 instead beta1- 2.16 ppm () 348 ovlps peak from G22(hn3) beta2- 1.89 ppm () 358 ovlps peak from G22 Glu 86? LONG (nh- 8.01ppm) hn107 dispersive amide in 100ms close to E91 in 1H and 15N noesy100- 281 ~132 20 alpha- 4.36 ppm () missing in NOESY, present in TOCSY beta1- 2.22 ppm vw(8) 346 close to negative peak beta2- 1.86 ppm (4) 359 gamma1- 2.57 ppm vw(9) 340 gamma2- 2.38 ppm vw(6) 333 close to negative peak Phe 87 INTRA LONG amb assign (segid="sbm1" and resid 81 and name hg2*) (segid="sbm1" and resid 87 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 81 and name hg2*) (segid="sbm2" and resid 87 and name hd*) 1.8 0 3.2 {w, 1.05, 4, 2D amb} 10hd1* at 1.08 ; 11895 1 11962 44 parsed_1b4c 1 830 ; {w, 0.62, 4, 2D amb} (nh- 8.61ppm) hn122 noesy100- 229 ~109 25 alpha- 3.96 ppm (4) 282 beta1- 2.00 ppm (5) 354 beta2- 1.86 ppm (5) 359 could ovpl b2n-1 ??in tocsy- 1.56 ppm (3) Phe 88 LONG NOTES 3D NOESY: noesy100- 329 ~153 40 E89 NN (hn60) 7.57ppm, (~6), ~149 ovlps F88 hn5 Glu 89 LONG amb assign (segid="sbm1" and resid 43 and name hd*) (segid="sbm1" and resid 89 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 43 and name hd*) (segid="sbm2" and resid 89 and name hn) 1.8 0 4.2 {vw, 7.19, 8*, amb} NOTES 3D NOESY: noesy100-320 149 31 His 90 LONG NOTES 3D NOESY: noesy100- 274 129 32 ha dispersive in 3D, stronger in 4D E91 NN (hn90) ppm, (17/2), ~129 could ovlp H90 hn114 Glu 91 LONG NOTES 3D NOESY noesy100- 273 129 20 H90 NN-1 (hn114) 8.0ppm, (), could ovlp E91 hn90 NOTES 4D CN H90ha 13 ctrs in 4D close to H2O in 3D go with 6 ctrs Note 1: number in parentheses are number of contours seen at lvl=0.02 of NOESY-HMQC for weak peaks and at lvl=0.1 for others Nilges et al. Biopolymers 29, 813-822, (1990). note 2: Naming- upfield = > , downfield = < previous naming was downfield "1" and upfield "2" Two beta protons are named downfield beta proton, hb1, and upfield beta proton, hb2; if degenerate, then hb*. For CH3 protons the protons hb11,hb12,hb13 and hb21,hb22,hb23. If degenerate, use hb1* for the downfield and hb2* for the upfield. Gamma, delta, epsilon, and eta, protons were treated in a similar manner. note 3a: Pseudo-corrections - NOT USED as of noe10.tbl, swith to sum averaging - ACD 971126 (a) CH3 groups add 1.0 A to the upper limit (b) CH2 group with degenerate protons add 1.0 A to the upper limit (c) degenerate CH3 groups for V, L add 1.7 A to the upper limit (d) aromatics add 2.3 A to the upper limit Conditions for 3D 100 ms NOESY-HSQC contour level = 0.1 # of levels= 20 level mult= 1.2 strong noe (>10 contour) = 1.8 0 0.9 (0 to 2.7 angstroms) strong noe (>10 contour) = 1.8 0 1.1 (0 to 2.9 angstroms for hn) medium noe (7-10 contours) = 1.8 0 1.5 (0 to 3.3 angstroms) medium noe (7-10 contours) = 1.8 0 1.7 (0 to 3.5 angstroms for hns) weak noe (3-6 countours) = 1.8 0 3.2 (0 to 5.0 angstroms) very weak noe (<3 countours) = 1.8 0 4.2 (0 to 6.0 angstroms) very weak(not seen at lvl=0.1) = 1.8 0 4.2 (0 to 6.0 angstroms) residue (nh- ppm) arbitrary assignment (destination residue) (origin residue) assign (segid="sbm1" and resid and name hn) (segid="sbm1" and resid and name hn) {s-m-w, dest'n ppm, # contours,correction} order: intraresidue sequentials medium range long range ordered by dest'n ppm value notes about questions Definitions of codes for commenting out NOEs !I!: all intraresidue NOEs commented out !viol!: comment out b/c violation in xplor run(s) !R!: redundant; weaker of two removed, if equal # levels first appearing removed !amb!: ambiguous and may not necessarily be resolved from any NOESY spectra ******************************************************************************************* **** DATA FROM 3D 13C-EDITED AND 4D 13C,13C-EDITED NOESY SPECTRA ************************** ******************************************************************************************* All parameters not mentioned here are same for the 13C-edited NOESY Conditions for 3D 13C-edited NOESY-HSQC contour level = 0.2 # of levels= 20 level mult= 1.2 strong noe (>10 contours) = 1.8 0 0.9 (0 to 2.7 angstroms) medium noe (7-10 contours) = 1.8 0 1.5 (0 to 3.3 angstroms) weak noe (3-6 countours) = 1.8 0 3.2 (0 to 5.0 angstroms) very weak noe (<3 countours) = 1.8 0 4.2 (0 to 6.0 angstroms) very weak(not seen at lvl=0.1) = 1.8 0 4.2 (0 to 6.0 angstroms) ******************************************************************************************* Ser 1a (nh-10.23; n= 121.93 ppm) hn104 no sidechain peaks in 3D TOCSY INTER AMB amb assign (segid="sbm1" and resid and name h) (segid="sbm1" and resid 1 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid and name h) (segid="sbm2" and resid 1 and name hn) 1.8 0 ? {, 0.61, 2*, } amb assign (segid="sbm1" and resid ? and name h) (segid="sbm1" and resid 1 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid ? and name h) (segid="sbm2" and resid 1 and name hn) 1.8 0 ? {, 1.70, ?*, } amb assign (segid="sbm1" and resid ? and name h) (segid="sbm1" and resid 1 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid ? and name h) (segid="sbm2" and resid 1 and name hn) 1.8 0 ? {, 2.60, 4*, } amb assign (segid="sbm1" and resid ? and name h) (segid="sbm1" and resid 1 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid ? and name h) (segid="sbm2" and resid 1 and name hn) 1.8 0 ? {, 8.39, 3*, } NOTES 3D NOESY: noesy100-92 51 28 NOE, hn[], D2(pt), ovlp NN,98, could ovlp nn+2 N+2 (hn70/hn71), 98, could ovlp nn N+3 (hn55), 129 N+4 (hn26), 112 Ser 1b (nh-9.95ppm; n= 120.73) hn108 NOTES 3D NOESY: noesy100-115 61 30 no sidechain peaks in 3D TOCSY sc NOEs at 4.33, 2.27, 1.84, 1.73 NN, 98, could ovlp nn+2 N+2 (hn70/hn71) 98 N+3 (hn55) 128 N+4 (hn26) 112 NOTES 4D CN: signals stronger in 4D than 3D as exected in range of H2O Glu 2 INTER ; 11966 1 12144 7 parsed_1b4c 1 831 ; {w, 1.21, 4, 2.9, cn} AMB amb assign (segid="sbm1" and resid 43 and name ha) (segid="sbm1" and resid 2 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 43 and name ha) (segid="sbm2" and resid 2 and name hn) 1.8 0 3.2 {w, 4.66, 11?, 0, cn}, probably S1ha as assigned above remove 1ha-2hn b/c dispersive and very weak in 3d NOTES 3D NOESY (nh- 8.93ppm; n= 120.7) hn62 noesy100- 202 98 30 NN (hn70), 8.94, could ovlp hn62 NN+2 (hn55) 129 NN+3 (hn24/hn26?), 113 NOTES 4D CN: Y= S1 or F43 Leu 3a INTER amb assign (segid="sbm1" and resid 9 and name hb*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 9 and name hb*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d<, w, 1.65, 12, 4.4, w cfilt} could have intra contribution from A6hb* amb 980108 b/c pk stronger to L10hd>, and 10hd* to 6hb* much closer from model ; 12147 1 12173 80 parsed_1b4c 1 832 "{d<, w, 4.12, >15ov, 2.9, wk cfilt}" 12177 1 12177 44 parsed_1b4c 1 833 ; {d<, w, 1.99, 9, 2.9, wk cfilt} R assign (segid="sbm1" and resid 10 and name hd*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 10 and name hd*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d>, w, 0.92, 8ovlp, 5.8, wk cfilt at 0.95} ; 12181 1 12185 52 parsed_1b4c 1 834 ; {mw, 1.21-4, 8, 2.9, ncn} R assign (segid="sbm1" and resid 13 and name hg*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 1.1 R assign (segid="sbm2" and resid 13 and name hg*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 1.1 {d<, s, 1.22, 15, 5.8} R assign (segid="sbm1" and resid 13 and name hg*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 13 and name hg*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 1.5 {d>, m, 1.22, 9, 5.8} ; 12189 1 12197 30 parsed_1b4c 1 835 ; {d<, w, 2.30, 7, 2.9, wk cfilt} R assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d<, w?, 0.61, 9, 5.8, wk? cfilt} R assign (segid="sbm1" and resid 36 and name hg*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 36 and name hg*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 1.5 {d>, m, 0.84, 9ov, 5.8, cfilt} amb/R assign (segid="sbm1" and resid 37 and name ha) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 amb/R assign (segid="sbm2" and resid 37 and name ha) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d>, w, 4.20, 10, 1.5, vwk cfilt}, 37ha sees m pk at 0.77 in cfilt ; 12201 1 12213 75 parsed_1b4c 1 836 ; {d>, w, 1.71, 7, 3.9, wk cfilt ov 3hb2} amb assign (segid="sbm1" and resid 40 and name hb*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 40 and name hb*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 4.2 {d>, vw, 2.06, 2, 3.9, no cfilt} amb/RS assign (segid="sbm1" and resid 40 and name hb*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 4.2 amb/RS assign (segid="sbm2" and resid 40 and name hb*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 4.2 {d>, vw, 1.78, 2, 3.9, ov l3hb cfilt} amb assign (segid="sbm1" and resid 40 and name hg) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 40 and name hg) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d>, w, 1.49, >12ov, 2.9, wk cfilt} amb assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d>, w?, 0.92, >12 ridge, 5.8, wk cfilt 0.90} assign (segid="sbm1" and resid 41 and name hb*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 4.2 assign (segid="sbm2" and resid 41 and name hb*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 4.2 {d'', vw?, 3.85, 7, 3.9, wk cfilt} could be s1hb*??, its hb* is amb, but shouldnt see cfilt s41hb* at 3.86/61.7 in cfilt sees m-w pk at 0.77 ; 12217 1 12238 57 parsed_1b4c 1 837 "{d<, w, 7.09/131.2-6, 6, 5.3, m cfilt at 7.09-11} - 73he*/z ? at 7.11/130.5" 12242 1 12242 84 parsed_1b4c 1 838 ; {d<, w, 7.09/128.1, 9, 2.9} 73hz/e* ? at 7.09/128.4 amb assign (segid="sbm1" and resid 74 and name he*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 74 and name he*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d<, w?, 1.64, 7, 4.4, w cfilt} amb 980108 b/c 10hd close to 3hd in CS R assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 1.5 R assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 1.5 {d<, m, 0.77, 12, 4.4, s cfilt ovlps 3hd2*} R/amb assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 R/amb assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d'', w, 0.77, 15?, 4.4, art?}, ovlps L3hd2* in cfilt R assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d<, w, 0.48, 7, 4.4, wk cfilt} R assign (segid="sbm1" and resid 77 and name hg2*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 77 and name hg2*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 3.2 {d>, w, 0.48, 6, 4.4, wk cfilt} amb assign (segid="sbm1" and resid 80 and name hg1*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg1*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 4.2 {d>, vw, 0.92, 8ov, 4.4, wk cfilt at 0.95} vw b/c looks far in model amb assign (segid="sbm1" and resid 80 and name hg2*) (segid="sbm2" and resid 3 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 80 and name hg2*) (segid="sbm1" and resid 3 and name hd*) 1.8 0 4.2 {d>, vw, 0.99, 3, 4.4, vw cfilt} AMB amb assign (segid="sbm1" and resid 16 and name hb*) (segid="sbm2" and resid 3 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 16 and name hb*) (segid="sbm1" and resid 3 and name hn) 1.8 0 4.2 {vw, 2.41, 9*, 1.0}, 58hg1, 62hg*, 67hg1 at 2.38, 16hb1 at 2.41, 34hg1, 2hg* at 2.46, max at 2.43 for 3bhn; wk at 2.40 in cfilt NOTES 3D NOESY: noesy100- 201 98 29 ovlps hn62(E2) in 1H and one 15N plane away NN (hn55) 129, ovlps hn62(E2) (nh- 8.94; n= 121.37) hn70 Leu 3b (nh- 9.01ppm) hn73 NOTES 3D NOESY: noesy100- 194 95 28 NN (hn35) 7.76ppm, vw(9), 142 NOTES 4D CN: could not find Leu 3c (nh- 8.92; n= 121.62) hn71 overlaps L3a in 1H and 15N in 3D Glu 4a INTER amb assign (segid="sbm1" and resid 17 and name he*) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 17 and name he*) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 {vw, 6.70-8, 5*, 2.4, amb, seen by both 4a/b hn, 41hn not see 4a/bhn amb/M assign (segid="sbm1" and resid 42 and name hb*) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 amb/M assign (segid="sbm2" and resid 42 and name hb*) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 {vw, 3.52, 9*, 1.0} 4b does not see 3.52 amb assign (segid="sbm1" and resid 43 and name he*) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 43 and name he*) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 {vw, 7.41, *5, 2.4, amb}, this peak clear to 4a_hn, but a shoulder at 4b_hn AMB amb assign (segid="sbm1" and resid 45 and name hb*) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 45 and name hb*) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 {vw, 2.28/35.6, 3, 1.0, cn}, 45hb* makes sense for intramolecular, 34hg2 closest for inter amb /M assign (segid="sbm1" and resid 81 and name hb) (segid="sbm1" and resid 4 and name hn) 1.8 0 4.2 amb /M assign (segid="sbm2" and resid 81 and name hb) (segid="sbm2" and resid 4 and name hn) 1.8 0 4.2 {vw, 4.28, 5*, 0, amb} amb assign (segid="sbm1" and resid 13 and name hg*) (segid="sbm1" and resid 4 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 13 and name hg*) (segid="sbm2" and resid 4 and name hn) 1.8 0 3.2 {w, 1.21-4, 5, 1.7}, not seen by E4bhn NOTES 3D NOESY: noesy100-273 129 31 NN-1 (hn70/71) 98, could ovlp nn-2 NN-2 (hn62), could ovlp nn-1 Glu 4b (nh- 7.73ppm; n= 118.47) hn35 NOTES 3D NOESY: noesy100- 305 142 33 K5 NN (hn30) 7.89ppm, (~3), ~137 ovlps E4b hn35 NOTES 4D CN: could not find ha=3.33 Lys 5a INTER AMB amb/DL assign (segid="sbm1" and resid 44 and name hg) (segid="sbm1" and resid 5 and name hn) 1.8 0 3.2 amb/DL assign (segid="sbm2" and resid 44 and name hg) (segid="sbm2" and resid 5 and name hn) 1.8 0 3.2 {w, 1.65, 4, cn} amb/M assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 5 and name hn) 1.8 0 4.2 amb/M assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 5 and name hn) 1.8 0 4.2 {vw, 5.18, 6*, 0}, H15hn or C68hn, neither make sense, not seen by 5chn amb/M assign (segid="sbm1" and resid ? and name h) (segid="sbm1" and resid 5 and name hn) 1.8 0 ? amb/M assign (segid="sbm2" and resid ? and name h) (segid="sbm2" and resid 5 and name hn) 1.8 0 ? {vw, 5.48, 2*, , amb} NOTES 3D NOESY: noesy100- 233 112 35 (nh- 8.57ppm; n= 117.59) hn24; multiple with hn26 and hn30 A6a NN (hn83) 131, could ovlp nn-1 NN-2 (hn70/71) 97, could ovlp NN-3, not ovlpd in hn70/71 strip NN-3 (hn62) 97, could ovlp NN-2 Lys5c (nh- 8.51ppm; n= 117.59) hn26 3D NOESY: noesy100- 238 114 35 NN-1 (hn55), could ovlp nn NN (hn83) 131, could ovlp nn-1 NN-2 (hn70/71) 98, could ovlp NN-3 NN-3 (hn62) 98, could ovlp NN-2 4D CN: 1.65 may be hd and hg Lys 5b (nh- 7.88ppm; n= 118.15) hn30 NOTES 3D NOESY: noesy100- 292 137 34 Ala 6a INTER ; 12246 1 12377 7 parsed_1b4c 1 839 "{w? , , , , } stg cfilt at 4.30, 9hb*-6ha and 6hb*-9ha also poss but look less likely" 12380 1 12380 94 parsed_1b4c 1 840 "{w? , , , , } wk cfilt at 4.15, check 4D for 10ha" 12384 1 12384 58 parsed_1b4c 1 841 "{w? , , , , } m-w cfilt at 2.52, check 4D for 10b*" 12388 1 12388 59 parsed_1b4c 1 842 ; {w? , , , , } wk cfilt at 1.81 and med at 2.00, both poss l10hg, check 4D for 10hg AMB amb assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm1" and resid 6 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm2" and resid 6 and name hn) 1.8 0 4.2 {vw, 0.99, 5, 2.9, amb}, could be inter to L10hd2*, vw b/c vw to 6b-hn amb assign (segid="sbm1" and resid 41 and name ha) (segid="sbm1" and resid 6 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 41 and name ha) (segid="sbm2" and resid 6 and name hn) 1.8 0 4.2 {vw#, 4.07, 2, 0} amb assign (segid="sbm1" and resid 42f and name hn) (segid="sbm1" and resid 6a and name hn) 1.8 3.2 amb assign (segid="sbm2" and resid 42f and name hn) (segid="sbm2" and resid 6a and name hn) 1.8 3.2 {w, 9.48, 3,1.8 0 ?, to F43-hn multiple near 6a-hn ?? amb/M assign (segid="sbm1" and resid 43 and name hd*) (segid="sbm1" and resid 6 and name hn) 1.8 0 4.2 amb/M assign (segid="sbm2" and resid 43 and name hd*) (segid="sbm2" and resid 6 and name hn) 1.8 0 4.2 {vw, 7.17, 9*, 2.4} amb/M assign (segid="sbm1" and resid 43 and name he*/z?) (segid="sbm1" and resid 6 and name hn) 1.8 0 4.2 amb/M assign (segid="sbm2" and resid 43 and name he*/z?) (segid="sbm2" and resid 6 and name hn) 1.8 0 4.2 {vw, 7.38, 8*, 2.4}, F43-hn may have multiple near 6a-hn, and these could be to F88 ring NOTES 3D NOESY: noesy100- 279 131 26 aN-2 (hn55) 3.3ppm,~304, ovlpd w/another peak Ala 6b (nh- 8.18ppm) hn82 NOTES 3D NOESY: noesy100- 267 126 26 M7 NN (hn8) 8.33ppm, (2), 121 could ovlp V8 nn+2 K5 aN-1 (hn30) 4.01ppm, (2), 280 could ovlp an-3,an-4 V8 NN+2 (hn42) 8.34ppm, (), could ovlp M7 nn L3b aN-3 (hn70/71) 4.01ppm, (2), 280 could ovlp an-1/-4 E2 aN-4 (hn62) 4.01ppm, (2), 280 could ovlp an-1/-3 NOTES 4D CN: could not find Met 7 INTER ; 12392 1 12432 7 parsed_1b4c 1 843 ; {w, 1.08, 12, 4.4, med cfilt} weak b/c could be some intramolecular contribution RS assign (segid="sbm1" and resid 10 and name hd*) (segid="sbm2" and resid 7 and name he*) 1.8 0 3.2 RS assign (segid="sbm2" and resid 10 and name hd*) (segid="sbm1" and resid 7 and name he*) 1.8 0 3.2 {w, 0.98, 8, 2.5, med cfilt}, weak b/c could be some intramolecular contribution amb assign (segid="sbm1" and resid 43 and name hd*) (segid="sbm2" and resid 7 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 43 and name hd*) (segid="sbm1" and resid 7 and name he*) 1.8 0 4.2 {vw, 7.16, 5, 3.9, vwk cfilt} amb 980107 amb assign (segid="sbm1" and resid 73 and name hz) (segid="sbm2" and resid 7 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 73 and name hz) (segid="sbm1" and resid 7 and name he*) 1.8 0 4.2 {vw, 7.16, 5, 3.9, vwk cfilt} amb 980107 R assign (segid="sbm1" and resid 74 and name he*) (segid="sbm2" and resid 7 and name he*) 1.8 0 0.9 R assign (segid="sbm2" and resid 74 and name he*) (segid="sbm1" and resid 7 and name he*) 1.8 0 0.9 {s, 1.56, >12, 3.0, stg cfilt} R assign (segid="sbm1" and resid 77 and name hg1*) (segid="sbm2" and resid 7 and name he*) 1.8 0 1.5 R assign (segid="sbm2" and resid 77 and name hg1*) (segid="sbm1" and resid 7 and name he*) 1.8 0 1.5 {m, 0.77, 13, 3.0, med cfilt} ; 12436 1 12456 38 parsed_1b4c 1 844 "{w, 0.49, 7, 3.0, wk cfilt}" 12460 1 12460 36 parsed_1b4c 1 845 ; {vw, 3.62, 3, 1.5, vw cfilt} amb assign (segid="sbm1" and resid 81 and name ha) (segid="sbm2" and resid 7 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 81 and name ha) (segid="sbm1" and resid 7 and name he*) 1.8 0 4.2 {vw, 3.68, 2, 1.5, no cfilt} ; 12464 1 12468 37 parsed_1b4c 1 846 ; {w, 4.26, 7, 2.5, wk cfilt} R assign (segid="sbm1" and resid 81 and name hg2*) (segid="sbm2" and resid 7 and name he*) 1.8 0 1.5 R assign (segid="sbm2" and resid 81 and name hg2*) (segid="sbm1" and resid 7 and name he*) 1.8 0 1.5 {m, 1.05, 12, 3.0, med cfilt} amb assign (segid="sbm1" and resid 82 and name hg2*) (segid="sbm2" and resid 7 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 82 and name hg2*) (segid="sbm1" and resid 7 and name he*) 1.8 0 4.2 {vw, 0.50, 2, 3.0, no cfilt} AMB amb assign (segid="sbm1" and resid 11 and name hd*/g2*) (segid="sbm1" and resid 7 and name he*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 11 and name hd*/g2*) (segid="sbm2" and resid 7 and name he*) 1.8 0 3.2 {w, 0.07, 4, 2.5, no cfilt} amb assign (segid="sbm1" and resid 11 and name ha) (segid="sbm1" and resid 7 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 11 and name ha) (segid="sbm2" and resid 7 and name he*) 1.8 0 4.2 {vw, 3.41, 1, 1.5, 4d, wk cfilt} NOTES 3D NOESY noesy100- 254 121 39 (nh- 8.33ppm; n= 115.25) hn8 close to hn9[N38], L44d&e V8 NN (hn43) 114, could ovlp K5 nn-2, as well as L44,N38 K5 bN-1 (hn83) 365, ovlps L44hb and hg K5 NN-2 (hn24), could ovlp nn, as well as L44,N38 A9 NN+2 9 (hn81) 140, could ovlp hn[9]N38 nn-1[13] L3 aN-4 (hn70) (9/3), 279, could ovlp other peaks hn9[N38]an-4, ha12[L44a], ha10[L44] NOTES 4D CN same coordinates as N38 ha dispersive in 3D 5 ctrs in 4D go with 3 Val 8a INTER ; 12472 1 12507 7 parsed_1b4c 1 847 "{w, 7.41, 8, wk cfilt}" 12510 1 12510 31 parsed_1b4c 1 848 "{w, 7.36, 8, wk cfilt}" 12514 1 12514 31 parsed_1b4c 1 849 ; {vw, 7.41, 9*, 2.4, amb}, could be 43he*, 17hn, 88hn ?? AMB NOTES 3D NOESY: noesy100- 239 113 33 (nh- 8.50ppm; n= 199.20) hn43 NN-1 (hn8) 8.33, 121, could ovlp NN+2 NN+2 (hn52) 8.29, could ovlp nn-1 aN-3 (hn24) 3.90ppm, ovlps hn40[E67] an-1/an-3, but it's real NOTES 4D CN: V8 is in same cube as E67 Val 8b (nh- 8.34ppm; n= 119.20) hn42, wkr than hn43 NOTES 3D NOESY: noesy100- 253 120 32 NN-1 (hn) 8.33ppm, (),could ovlp hn42 NN+2 (hn65) 8.4ppm, (), could ovlp hn42 Ala 9 INTER amb assign (segid="sbm2" and resid 2 and name hg*) (segid="sbm1" and resid 9 and name hb*) 1.8 0 3.2 amb assign (segid="sbm1" and resid 2 and name hg*) (segid="sbm2" and resid 9 and name hb*) 1.8 0 3.2 {w? , , , , } w-m cfilt at 2.47, check 4D for 2hg* AMB amb/art assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 7.57, ~6*, 0} amb/art assign (segid="sbm1" and resid 38 and name hd2*) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 38 and name hd2*) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 7.08, 1*, 1.0, @.015} amb/art assign (segid="sbm1" and resid 43 and name hz) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 43 and name hz) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 7.41, 13*, 0} amb assign (segid="sbm1" and resid 52 and name hb) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 52 and name hb) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 2.11, 1, 0, cn} amb assign (segid="sbm1" and resid 84 and name hn) (segid="sbm1" and resid 9 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 84 and name hn) (segid="sbm2" and resid 9 and name hn) 1.8 0 4.2 {vw, 7.49, 8*, 0, amb} NOTES 3D NOESY: noesy100- 307 143 27 (nh- 7.71ppm; n= 122.98) hn81 V8a or b NN-1 (hn43) 114, could ovlp nn+2 L10 or b NN (hn52) 8.31ppm,, 122, could ovlp nn-2 M7 NN-2 (hn8) 8.33ppm, could ovlp nn I11 NN+2 (hn65) 8.4ppm, could ovlp nn-1 Leu 10a INTER ; 12518 1 12579 7 parsed_1b4c 1 850 ; {d>, w, >12ov, 4.03, 2.9, wk cfilt} R assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 10 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 10 and name hd*) 1.8 0 3.2 {w, 0.71, 7, 4.4, wk cfilt at 0.77} ; 12582 1 12586 44 parsed_1b4c 1 851 "{d<, m?, 1.67, 11, 4.4, med cfilt} some might be due to intramolecular A9hb* but w-vw" 12590 1 12590 94 parsed_1b4c 1 852 ; {d<, w, >12ov, 1.92, 2.9, wk cfilt at 1.99} cfilt looks too strong for intra only amb/R assign (segid="sbm1" and resid 74 and name he*) (segid="sbm2" and resid 10 and name hd*) 1.8 0 3.2 amb/R assign (segid="sbm2" and resid 74 and name he*) (segid="sbm1" and resid 10 and name hd*) 1.8 0 3.2 {d<, w, 1.63, >12, 4.4, wk cfilt} amb/R assign (segid="sbm1" and resid 74 and name he*) (segid="sbm2" and resid 10 and name hd*) 1.8 0 3.2 amb/R assign (segid="sbm2" and resid 74 and name he*) (segid="sbm1" and resid 10 and name hd*) 1.8 0 3.2 {d>, w, 1.56, >12, 4.4, wk cfilt}, weak b/c mostly intramolecular contribution AMB amb/DL assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 10 and name hd*) 1.8 0 3.2 amb/DL assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 10 and name hd*) 1.8 0 3.2 {w, 0.77, >12 ridge, 5.8, med cfilt} could be inter to V77hg1*, L3hd2* looks too far amb assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 10 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 10 and name hn) 1.8 0 4.2 {vw, 5.18, 2*, 0}, H15,C68 NOTES 3D NOESY: noesy100- 257 122 32 Leu 10a (nh- 8.29ppm; n= 119.76) hn52; strgr of the pair in the HSQC Leu 10b (nh- 8.26ppm; n= 119.60) hn48 Ile 11a INTER amb assign (segid="sbm1" and resid 81 and name hg2*) (segid="sbm2" and resid 11 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 81 and name hg2*) (segid="sbm1" and resid 11 and name hd*) 1.8 0 3.2 {w, 1.00, 7, 3.0}, not sure if resonance at 0.12/12.7 is 11hd* or hg2*, think hd* based on 13C CS of I36 and I47, and hard to find 0.12/12.7 in cfilt AMB amb assign (segid="sbm1" and resid ? and name h?*) (segid="sbm1" and resid 11 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name h?*) (segid="sbm2" and resid 11 and name hn) 1.8 0 4.2 {vw, 0.61, 6*, 1.5}, could be 35hd1*, 27hd**, or 82hg2* - think 82hg2* best choice NOTES 3D NOESY: noesy100- 246 117 29 Ile 11a (nh- 8.44ppm; n= 121.21) hn65 close to hn67 (V13), but wkr than hn67 Ile 11b (nh- 8.39ppm; n= 121.21) hn65a, wkr than hn65 NN (hn) 8.1ppm, (), could be ovlpd NN-1 (hn) 8.2ppm, (), could be ovlpd NOTES 4D CN: too weak Asp 12 INTER AMB amb assign (segid="sbm1" and resid 35 and name hd*) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 35 and name hd*) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 0.39-42, 6*, 2.9, amb} amb assign (segid="sbm1" and resid ? and name h) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name h) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 2.13, 10*, 0, amb} amb assign (segid="sbm1" and resid 48 and name hg*?) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 48 and name hg*?) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 1.35, 3*, 1, amb} amb assign (segid="sbm1" and resid ? and name h) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name h) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 1.51, 4*, , amb} amb assign (segid="sbm1" and resid 89 and name ha) (segid="sbm1" and resid 12 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 89 and name ha) (segid="sbm2" and resid 12 and name hn) 1.8 0 4.2 {vw, 4.17, 6*, 0, amb} amb assign (segid="sbm1" and resid Z and name ha) (segid="sbm2" and resid 12 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid Z and name ha) (segid="sbm1" and resid 12 and name hn) 1.8 0 3.2 {w, 3.98, 5, 0}, Z= L3, R20(R20b sees 8.20), E72, M79, or F88 (F88 close in 1h and 13C) NOTES 3D NOESY: noesy100- 269 127 30 Illhb could also be K26hb* (nh- 8.15ppm; n= 120.73) hn64; in NOESY seems to have vw mult peak Val 13 INTER ; 12594 1 12683 7 parsed_1b4c 1 853 "{m, 2.08, 11, 1.5, wk cfilt 2.10}" 12686 1 12686 42 parsed_1b4c 1 854 "{w, 2.08, 6, 1.5, wk cfilt 2.10}" 12690 1 12690 41 parsed_1b4c 1 855 "{mw?, 2.46, 8, 2.5, mw cfilt 2.42}" 12694 1 12694 43 parsed_1b4c 1 856 "{vw, 2.46, 3, 2.5, no cfilt ? 2.42}" 12698 1 12698 44 parsed_1b4c 1 857 "{w, 4.04, 9, 1.5, wk cfilt 4.04}" 12702 1 12702 41 parsed_1b4c 1 858 "{w, 1.89, 7, 1.5, wk cfilt}" 12706 1 12706 36 parsed_1b4c 1 859 ; {w, 1.89, 5, 1.5, wk cfilt} amb assign (segid="sbm1" and resid 3 and name hg) (segid="sbm2" and resid 13 and name hg2*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hg) (segid="sbm1" and resid 13 and name hg2*) 1.8 0 4.2 {vw, 1.56, 3, 1.5, wk cfilt 1.49} amb assign (segid="sbm1" and resid 3 and name hg) (segid="sbm2" and resid 13 and name hg1*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hg) (segid="sbm1" and resid 13 and name hg1*) 1.8 0 4.2 {vw, 1.56, 3, 1.5, wk cfilt 1.49} R assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 13 and name hg2*) 1.8 0 1.5 R assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 13 and name hg2*) 1.8 0 1.5 {m, 1.02, 10, 3.0, stg cfilt} ; 12710 1 12722 38 parsed_1b4c 1 860 ; {s, 1.02, 13, 4.4, stg cfilt} S assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 13 and name hg1*) 1.8 0 3.2 S assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 13 and name hg1*) 1.8 0 3.2 {w?, 0.77, 8, 4.4, med cfilt} amb/DL assign (segid="sbm1" and resid 5 and name hd*) (segid="sbm2" and resid 13 and name hg2*) 1.8 0 4.2 amb/DL assign (segid="sbm2" and resid 5 and name hd*) (segid="sbm1" and resid 13 and name hg2*) 1.8 0 4.2 {vw, 1.56, 4, 1.5, wk cfilt 1.65} ; 12726 1 12734 42 parsed_1b4c 1 861 ; {w, 1.56, 10, 3.0, wk cfilt 1.65}, could be mostly intramolecular to A9hb* amb assign (segid="sbm1" and resid 87 and name hz) (segid="sbm2" and resid 13 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 87 and name hz) (segid="sbm1" and resid 13 and name hn) 1.8 0 4.2 {vw, 7.00?, 2, 0, amb} AMB art? assign (segid="sbm1" and resid Y and name h?) (segid="sbm1" and resid 13 and name hn) 1.8 0 ? art? assign (segid="sbm2" and resid Y and name h?) (segid="sbm2" and resid 13 and name hn) 1.8 0 ? {w, 2.34, 4, ?}, Y= K28hd*, E49hb1, E72hb1 NOTES 3D NOESY (nh- 8.41ppm) hn67 noesy100- 248 118 29 F14 NN (hn50) 8.4ppm, could ovlp w/hn[67]- assumed f14hn-acd I11 NN-2 (hn65) 8.4ppm, could ovlp w/hn[67] NOTES HNH (clvl=0.1): 119.68 (7) F14 and 120.73 D12 Phe 14a Phe 14b - INTER ; 12738 1 12761 17 parsed_1b4c 1 862 ; {vw, 0.99, >10*, 2.9, amb} amb assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 14 and name hd*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 14 and name hd*) 1.8 0 4.2 {vw, 1.03, 3, 5.3, 4D} amb assign (segid="sbm1" and resid 87 and name hb*) (segid="sbm2" and resid 14 and name hb*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 87 and name hb*) (segid="sbm1" and resid 14 and name hb*) 1.8 0 3.2 {w, 2.43, 4, 2.0, amb} not yet checked cfilt amb assign (segid="sbm1" and resid 87 and name hd*) (segid="sbm2" and resid 14 and name hb*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 87 and name hd*) (segid="sbm1" and resid 14 and name hb*) 1.8 0 4.2 {vw, 6.07, 2, 3.4, not ck cfilt} R assign (segid="sbm1" and resid 87 and name he*) (segid="sbm2" and resid 14 and name hd*) 1.8 0 3.2 R assign (segid="sbm2" and resid 87 and name he*) (segid="sbm1" and resid 14 and name hd*) 1.8 0 3.2 {w, 6.50, 4, 4.8, 2D, not ck cfilt} ; 12764 1 12780 44 parsed_1b4c 1 863 ; {w, 7.00, 3, 2D, have not ck'd cfilt} AMB amb assign (segid="sbm1" and resid 73/4 and name hb1/a) (segid="sbm1" and resid 14 and name ha) 1.8 0 3.2 amb assign (segid="sbm2" and resid 73/4 and name hb1/a) (segid="sbm2" and resid 14 and name ha) 1.8 0 3.2 {w, 3.33, ~8, 0} NOTES 3D NOESY: noesy100- ~244 117 31 V13 NN-1 ovlps diag D12 NN-2 (hn64) 8.17ppm very weak but seems to be there NOTES 4D CN an-4 or G66 4.15 in 3D and 4.17 in 4D, 13C goes w/G66 not an-4 sofrom another cube ? Phe 14a (nh- 8.47ppm; n= 119.76) hn50 strgr of the pair Phe 14b (nh- 8.43ppm; n= 119.84) hn51 His 15 INTER AMB NOTES 3D NOESY: noesy100- 219 106 35 bN-1 (hn50) 3.14ppm, (4/2), ovlps beta2 NN-2 (hn67) 8.4ppm, could ovlp NN-1 (nh- 8.74ppm; n= 117.42) hn109 - VERY WEAK SIGNAL FOR 3D AND 4D Gln 16 INTER AMB NOTES 3D NOESY: noesy100- 255 120 27 F14 NN-2 (hn50) 8.4ppm, (),could ovlp diag (nh- 8.32ppm; n= 122.25) hn75; close in 15n/1H to hn74(E72) Tyr 17 INTER amb assign (segid="sbm1" and resid 2 and name hb*) (segid="sbm2" and resid 17 and name hb*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 2 and name hb*) (segid="sbm1" and resid 17 and name hb*) 1.8 0 3.2 {w, 2.06, 3, 2.0, amb} NO cfilt found near 2.65/40.6 amb assign (segid="sbm1" and resid 3 and name hb*) (segid="sbm2" and resid 17 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hb*) (segid="sbm1" and resid 17 and name hn) 1.8 0 4.2 {b'', vw, 1.78, 3*, 1.0, amb} could be to 20hg1 amb assign (segid="sbm1" and resid 4 and name hb*) (segid="sbm2" and resid 17 and name he*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 4 and name hb*) (segid="sbm1" and resid 17 and name he*) 1.8 0 3.2 {w?, 2.29, 11/~4, 3.4} 4D sees 2.20/29.4 could be to 34hg2 ?? AMB amb assign (segid="sbm1" and resid ? and name hb2) (segid="sbm1" and resid 17 and name ha) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name hb2) (segid="sbm2" and resid 17 and name ha) 1.8 0 3.2 {w, 1.82, 4, 0}, 12hg, 20hb*, 89hb2 NOTES 3D NOESY (nh- 7.37ppm; n= 115.73) hn14 noesy100- 336 156 38 aN-2 (hn109) 5.15ppm, other signals are present in 4D CN at 5.1 that aren't H15 NOTES 4D CN aN-1 (hn75) 3.82ppm is only 1 contour not all Y17 peaks optimize at one 15N value Q16hg2 could alos be M79hb1 Ser 18 INTER AMB ? assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 18 and name hn) 1.8 0 ? ? assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 18 and name hn) 1.8 0 ? {vw, 2.38, 6*, ?}, Q16hb1 2.41, E31hg* 2.35 (E31hg* not see pk @ 9.64), or Y17hb2? NOTES 3D NOESY: noesy100- 140 72 29 (nh- 9.64ppm; n= 121.37) hn112 vwk peak, may be multiple seems to have mult peaks in NOESY 9.66, 9.63, 9.60 aN-4 (hn50) 3.49ppm, could ovlp beta NOTES 4D CN - too weak Gly 19 INTER AMB amb/art assign (segid="sbm1" and resid 31 and name hg*) (segid="sbm1" and resid 19 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 31 and name hg*) (segid="sbm2" and resid 19 and name hn) 1.8 0 4.2 {vw, 2.38, 3*, 1.0, amb}, could be 16hb1 2.41 ?, 31hg* at 2.35 NOTES 3D NOESY: noesy100- 280 132 51 S18 aN-1 (hn112) 3.9ppm, could ovlp alpha1 (nh- 8.02ppm; n= 107.28) hn1, may be multiple Arg 20 INTER AMB amb/DL assign (segid="sbm1" and resid 34 and name hb*) (segid="sbm1" and resid 20 and name hn) 1.8 0 3.2 amb/DL assign (segid="sbm2" and resid 34 and name hb*) (segid="sbm2" and resid 20 and name hn) 1.8 0 3.2 {w, 2.22, 6, 1.0, cn}, 4D 2.22/28.8 and E34hb2 at 2.19/29.0, 3D sees 2.19; E4hb* & E49hb1 poss amb assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 20 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 20 and name hn) 1.8 0 3.2 {vw, 2.09/31.0, 3, 0, cn, amb}, 31 hb2 not see 20hn and off in CS NOTES 3D NOESY: noesy100- 353 163 33 (nh- 7.17ppm; n= 118.63) hn38 Glu 21 INTER AMB NOTES 3D NOESY: noesy100- ~302 142/143 38 G22 NN (hn3) 8.3ppm, could ovlp N37 nn (nh- 7.77ppm; n= 115.81) (hn15) - close N37 (hn13) in 1H and 15N Gly 22 INTER AMB NOTES 3D NOESY: noesy100- 252 120 48 NOTES 4D CN (nh- 8.35ppm; n= 109.13) hn3 E21hb1 could also be K55hb1,E91hb1,K5hb*,M57hb2 E21hb2 could also be K55hb2,E91hb2,V52hb,V53hb,V80hb E21hg* could also be E46hg*,E49hg2 Asp 23 INTER AMB amb/art assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 23 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 23 and name hn) 1.8 0 4.2 {vw, 4.69, 4*, 0, amb} NOTES 3D NOESY (nh- 8.61ppm; n= 125.47) hn86 noesy100- 229 110 23 NN (hn) 8.57ppm, could ovlp hn86 NOTES 4D CN: Close to O1 in D1, so signal not so good Lys 24 INTER AMB art? assign (segid="sbm1" and resid ? and name ?) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name ?) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 {vw, 0.72-5, 1, 1.5, amb}, 40hd2* 0.72, 3hd2* 0.75, 44hd** 0.75, 77hg1*, 0.77 art? assign (segid="sbm1" and resid ? and name ?) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name ?) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 7.08, 2*, 0} , could be 14hd* at 7.11 art? assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 2.22, ~5*, 0, amb} art? assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 24 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 24 and name hn) 1.8 0 4.2 {vw, 2.43, 1*, 0, amb} NOTES 3D NOESY: noesy100- 232 111 22 NN-1 (hn86) 8.6ppm,could ovlp hn106 beta-N-1 (hn86) ovlps hn86 (D23) from 15N plane one up NOTES 4D CN: ha only sidechain atom of K24 present His 25 INTER AMB art? assign (segid="sbm1" and resid 14 and name ha) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 14 and name ha) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 3.52, 3*, 0, amb} amb assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 25 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 25 and name hn) 1.8 0 4.2 {vw, 5.34, 7*, 0} , D69ha sees wk pk @ 9.10, K26ha sees vw pk @ 9.19 - ?? NOTES 3D NOESY: noesy100- 184 90 35 (nh- 9.14ppm; n= 117.50) hn25 close to hn21 (E51) in 1H and 15N K26 (NN) 7.71ppm, could ovlp E21(n-2) from next 15N plane, so use 6 ctrs vs. 9 8.57/7.11 are dispersive so intensity may be reduced 6.78/7.11 correspond to Q16 he22 and he21, both are present in 200 ms NOESY NOTES 4D CN: ha 7 ctrs in 4D 1 in 3D go with 4 ctrs Lys 26 INTER AMB NOTES 3D: noesy100- 309 144 35 H25 (NN-1) 9.17ppm, (9), 90, could also be F70; F70 has 7.11/7.30 NOTES 4D CN hb could also ovlp I11hb,Ihb hd 5 at H=596, 3 at H=595, split difference and use 4 contours hg1 could ovlp K5,K28,K55 hg2 could ovlp K33,K48 hd* could ovlp K48hd* NOTES 13C NOESY: 23hb1-26ha could also be 69hb2 (commented out above), but probably to 23hb1 33ha-26hb* could also be from s18b* or v8(ab)ha; viol!- now think above is 33ha-36hb, 36hb & K26hb* overlap 23hb1-26hg2 could also be intra to 26he2, which may be at 2.72(42.07) Leu 27 INTER AMB NOTES 3D NOESY: noesy100- 223 107 31 ha missing in 3D; very weak in 200ms NOTES 4D NOESY: too weak, in solvent ridge Lys 28 INTER AMB amb/art assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 28 and name hn) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 28 and name hn) 1.8 0 4.2 {vw, 3.82, 1*, 0}, 13ha 3.82, 16ha 3.82, 60ha 3.85, 29ha 3.77 NOTES 3D NOESY: noesy100- 179 88 24 NN (hn89) 9.15ppm, vw(7), 91, nearly ovlps hn85 NOTES 4D CN: L27 an >10 in 4D vw in 3D go with 5 ctrs Lys 29 INTER AMB NOTES 3D NOESY: noesy100- 188 92 21 NN-1 (hn) ppm, (), ovlps hn89 NOTES 4D CN: ha NOEs fairly strong, the rest are weak NOTES 13C: K29ha close to S41(e)hb at 3.79(61.90) so could have some ambiguity Ser 30 INTER AMB NOTES 3D NOESY: noesy100- 166 83 40 NOTES 4D CN: none of the NOEs to K29 are in the 4D Glu 31 INTER AMB NOTES 3D NOESY: noesy100- 368 170 25 Leu 32 INTER amb assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 32 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 32 and name hd*) 1.8 0 3.2 {d', w, 1.00, ?, 5.8}, wk/amb cfilt at 1.00, 3hd1* could be in ridge of 4Dcc AMB art? assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 32 and name hd*) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 32 and name hd*) 1.8 0 4.2 {d'', vw, 7.31, 1, 3.9} 76h? NOTES 3D NOESY: noesy100- 249 118 27 Lys 33 INTER AMB NOTES 3D NOESY: noesy100- 278 131 31 NN-2 (hn84) 7.0ppm, (), could ovlp NN Glu 34 INTER AMB amb assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 34 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 34 and name hn) 1.8 0 3.2 {w, 2.07, 5, 0, cn}, seen in 4Dcn, but not clear in 3D NOTES 3D NOESY: noesy100- 375 173 34 Leu 35 INTER S assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 2.4 S assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 2.4 {d<, mw, 1.02, 7, 5.8, m/w? cfilt} amb assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 35 and name hd*) 1.8 0 1.5 amb assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 35 and name hd*) 1.8 0 1.5 {d<, mw, 0.76, 13ov, 5.8, stg cfilt} ovlps 35hg AMB NOTES 3D NOESY: noesy100- 268 127 28 NOTES 4D CN L32ha could also be L44, M57, E91 ha's L35ha could also overlap Q50ha, Q71ha L35bn-1 could overlap E49hb1, E72hb1 Ile 36 art? assign (segid="sbm1" and resid 2 and name ha) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid 2 and name ha) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 4.2 {vw, 4.05, 2, 1.5} amb assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 3.2 {w, 0.71, 6, 4.4, stg cfilt} vios w/ sani art/SD? assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 36 and name hd*) 1.8 0 4.2 art/SD? assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 36 and name hd*) 1.8 0 4.2 {vw, 0.64, 3, 4.4, wk cfilt} amb assign (segid="sbm1" and resid 47 and name hd*) (segid="sbm2" and resid 36 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 47 and name hd*) (segid="sbm1" and resid 36 and name hg2*) 1.8 0 3.2 {w, 0.92, 4, 3.0, cfilt?} this peak tp 47hg2* close in CS to 36hg2* AMB NOTES 3D NOESY: noesy100- 235 112 29 NOTES 4D CN: V56hg2 signal doesn't max at H=522 Asn 37 INTER amb assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 37 and name ha) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 37 and name ha) 1.8 0 4.2 {vw, 0.78, 11, 2.9, med cfilt} vwk b/c no cfilt in L3hd2* strip, but med 37ha in 3hd2* plane AMB amb assign (segid="sbm1" and resid ? and name hg*) (segid="sbm1" and resid 37 and name ha) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name hg*) (segid="sbm2" and resid 37 and name ha) 1.8 0 4.2 {w, 2.15, 3, 1.0} amb assign (segid="sbm1" and resid 3 and name hb*) (segid="sbm1" and resid 37 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hb*) (segid="sbm2" and resid 37 and name hn) 1.8 0 4.2 {vw, 1.78, 3, 1.0, cn} 4D gives 1.78/40.96: L3hb2 at 1.78/41.5; L44hb* at 1.78/40.5 NOTES 3D NOESY: noesy100- 300 141 38 Asn 38 INTER AMB NOTES 3D NOESY: noesy100- 255 121 39 NOTES 4D CN: N37ha could also be E21ha no good evidence for 35ha-38hb1/2 NOE, but assigned 38hb2-35ha dont see 41hb*-38ha or vice versa, could be b/c 38ha at carrier frequencey Glu 39 INTER amb assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 39 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 39 and name hn) 1.8 0 3.2 {w, 0.78, 5, 2.9, amb} V77hg1*, I36hg2*,47hg2, 44hd also at ~0.77 amb 980107-acd AMB amb assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 39 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 39 and name hn) 1.8 0 4.2 {vw, 4.09, 9*, 0} amb assign (segid="sbm1" and resid ? and name hg?) (segid="sbm1" and resid 39 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name hg?) (segid="sbm2" and resid 39 and name hn) 1.8 0 3.2 {w, 2.35, 4, ?, ncn} E31,E51,E58hg1/2,E62,E45hg2,E67hg1,E72hg1 amb assign (segid="sbm1" and resid ? and name hb?) (segid="sbm1" and resid 39 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name hb?) (segid="sbm2" and resid 39 and name hn) 1.8 0 3.2 {w, 2.09, 5, ?, ncn} 51hb*, Q16hb2,Q71hb*,Q50hb1,E2hb*,E51hb*,M7hb2 3D NOESY: noesy100- 184 90 39 4D CN: hb1? Wk signal at 2.41, 30.32 which could ovlp hg2 in 3D 13C: 39hb*-36ha assigned, dont see 36ha-39hb* Leu 40 INTER amb assign (segid="sbm1" and resid 4 and name ha) (segid="sbm2" and resid 40 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 4 and name ha) (segid="sbm1" and resid 40 and name hd*) 1.8 0 3.2 {d>, w, 3.26, 3, no cfilt} ; 12784 1 13270 35 parsed_1b4c 1 864 ; {d<, vw, 1.21, 3, wk cfilt 1.27} art? assign (segid="sbm1" and resid 8 and name hg2*) (segid="sbm2" and resid 40 and name hd*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 8 and name hg2*) (segid="sbm1" and resid 40 and name hd*) 1.8 0 3.2 {d>, w, 1.21, 4, amb no cfilt} AMB art? assign (segid="sbm1" and resid 61 and name hb*) (segid="sbm1" and resid 40 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 61 and name hb*) (segid="sbm2" and resid 40 and name hn) 1.8 0 4.2 {vw, 2.65, 4*, 1.0, amb}, could also be 23hb2 2.62, 17hb* 2.65, 54hb* 2.65, 14hb2 2.68 ?? NOTES 3D NOESY: noesy100- 298 139 33 Dont see 40hb*-37ha or 37ha-40hb* Ser 41d INTER amb assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 41 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 41 and name hn) 1.8 0 3.2 {w, 0.75, 3, 2.9, amb} amb 980107 b/c 40hd2* 0.75 is closer for test14b structures by 2A AMB amb assign (segid="sbm1" and resid ? and name hn) (segid="sbm1" and resid 41 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name hn) (segid="sbm2" and resid 41 and name hn) 1.8 0 4.2 {vw, 8.33, 5*, 0}, 7hn, 38hn, F43hn, or L44hn ?? ?!assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 41 and name hn) 1.8 0 4.2 ?!assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 41 and name hn) 1.8 0 4.2 {vw, 1.73-5, 8*, 0}, too many choices - all 41 multiples see it NOTES 3D NOESY: noesy100- 394 181 44 (nh- 6.70ppm; n= 111.79) hn97 mult peak with 98/99 Ser 41e (nh- 6.71ppm; n= 112.27) hn98 NOTES 3D NOESY: noesy100- 393 ~181 43 7.41 is dispersive NOTES 4D CN: overlaps Ser 41d Ser 41f (nh- 6.78ppm; n= 112.75) hn99 NOTES 3D NOESY: noesy100- 387 ~178 43 7.41 is dipsersive NOTES 4D CN: Ser41f missing or too weak His 42d INTER AMB M assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 42 and name hn) 1.8 0 4.2 M assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 42 and name hn) 1.8 0 4.2 {vw, 0.74, 4*, ?} , too many choices NOTES 3D NOESY: noesy100- 135 70 27 His 42e (nh- 9.57ppm; n= 122.25) hn105 NOTES 3D NOESY: noesy100- 148 75 28 His 42f (nh- 9.46ppm; n= 121.37) hn100 NOTES 3D NOESY: noesy100- 157 79 29 Phe 43d INTER amb assign (segid="sbm1" and resid 4 and name ha) (segid="sbm2" and resid 43 and name hd*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 4 and name ha) (segid="sbm1" and resid 43 and name hd*) 1.8 0 3.2 {w, 3.19, 3, 2.4} RS/SD? assign (segid="sbm1" and resid 8 and name hg1*) (segid="sbm2" and resid 43 and name hd*) 1.8 0 4.2 RS/SD? assign (segid="sbm2" and resid 8 and name hg1*) (segid="sbm1" and resid 43 and name hd*) 1.8 0 4.2 {vw, 0.92, 1, 5.4} 43hz and 43he* assigned to 8hg1* ; 13274 1 13353 60 parsed_1b4c 1 865 ; {vw, 0.92??, 2, 5.4} art? assign (segid="sbm1" and resid 14 and name he*) (segid="sbm2" and resid 43 and name hd*) 1.8 0 3.2 art? assign (segid="sbm2" and resid 14 and name he*) (segid="sbm1" and resid 43 and name hd*) 1.8 0 3.2 {w, 6.24, 4, 4.8} AMB NOTES 3D NOESY: noesy100- 242 116 25 ha dispersive Phe 43e (nh- 8.33ppm; n= 123.78) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Phe 43f (nh- 8.06ppm; n= 123.22) hn103 NOTES 3D NOESY: noesy100- 254 ~120 26 Leu 44d INTER AMB 43hn - 44hn assign weak b/c may overlap w/hn[115] NOTES 3D NOESY: noesy100- ~254 ~120 39 alpha- 4.04 ppm (8) ~279 ovlps N38 an-4[9/31] & M7 an-4[8/70] beta- 1.75 ppm (10) 363 ovlps M7 bn-1[8/83] NN-1 (hn102) 8.50ppm, (9/2), 115 ovlps nn[43] Leu 44e (nh- 8.28ppm; n= 115.41) hn12 NOTES 3D NOESY: noesy100- ~257 ~122 39 NN-1 (hn103) 8.33ppm, (), could ovlp hn12 Leu 44f (nh- 8.15ppm; n= 115.33) hn11 NOTES 3D NOESY: noesy100- 268 ~128 39 NN-1 (hn123)8.06ppm, (5), 131 nearly ovlps hn11 NOTES 4D CN: too weak and overlapped Glu 45 INTER AMB amb/art? assign (segid="sbm1" and resid 84 and name ha) (segid="sbm1" and resid 45 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 84 and name ha) (segid="sbm2" and resid 45 and name hn) 1.8 0 4.2 {vw, 4.68, 5, 0, cn}, chem shift 84ha not in 3D; could be 42ha as assigned NOTES 3D NOESY: noesy100- 338 157 33 Glu 45e (nh- 7.35ppm; n= 118.63) hn36 NOTES 3D NOESY: noesy100- 338 157 33 NOE to 8.15 verifies that d/f overlap Glu 45f (nh- 7.32ppm; n= 118.63) hn37 NOTES 3D NOESY: noesy100- 340 159 33 NN-2 (hn103) 8.3ppm, (), could ovlp nn-1! Glu 46d Glu 46e Glu 46f INTER AMB amb assign (segid="sbm1" and resid C and name hb?) (segid="sbm1" and resid 46 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid C and name hb?) (segid="sbm2" and resid 46 and name hn) 1.8 0 1.7 {m, 1.97, 9, 0, cn} , E91hb1, 5hb*, 55hb*, 31hb2 amb/art? assign (segid="sbm1" and resid 47 and name hg1*) (segid="sbm1" and resid 46 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 47 and name hg1*) (segid="sbm2" and resid 46 and name hn) 1.8 0 4.2 {vw, 1.10, 6*, 1.0}, could be 80hg1* at 1.10; 47hg12 at 1.07 amb assign (segid="sbm1" and resid and name h?) (segid="sbm1" and resid 46 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid and name h?) (segid="sbm2" and resid 46 and name hn) 1.8 0 ? {w, 1.78, 5, , }, 44hg, 47hb, or 47hg11 NOTES 3D NOESY: noesy100- 313 ~146 32 NN (hn116) 7.82ppm, (8/2), ~140 nearly ovlps hn45 beta-N-1 (hn36) 2.22ppm, (10/2), could ovlp beta Ile 47 INTER AMB art? assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 47 and name hg2*) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 47 and name hg2*) 1.8 0 4.2 {vw, 3.83, 2, 1.5} NOTES 3D NOESY: noesy100-302 141 28 (values from HOHAHA-HSQC) hn too weak to observe in 3D or 4D Ile 47e? (nh- 7.81ppm) N= 122.25 hn116 very weak peak NOTES 4D CN: too weak Lys 48 INTER AMB NOTES 3D NOESY: noesy100- 217 105 20 an-1 and he could overlap NOTES 4D CN: too weak Glu 49 INTER AMB art? assign (segid="sbm1" and resid ? and name hn) (segid="sbm1" and resid 49 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name hn) (segid="sbm2" and resid 49 and name hn) 1.8 0 4.2 {vw, 7.27, 7*, 0, amb} amb/art? assign (segid="sbm1" and resid 46 and name ha) (segid="sbm1" and resid 49 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 46 and name ha) (segid="sbm2" and resid 49 and name hn) 1.8 0 4.2 {vw, 4.61, 2, 0, cn} assign (segid="sbm1" and resid X and name ha) (segid="sbm1" and resid 49 and name hn) 1.8 0 3.2 assign (segid="sbm2" and resid X and name ha) (segid="sbm2" and resid 49 and name hn) 1.8 0 3.2 {w, 4.23, 3, 0, cn}, X= A6,A9,E21,N37 ha's; based on 3D NOESY probly goes with K55 art? assign (segid="sbm1" and resid B and name hb2) (segid="sbm1" and resid 49 and name hn) 1.8 0 3.2 art? assign (segid="sbm2" and resid B and name hb2) (segid="sbm2" and resid 49 and name hn) 1.8 0 3.2 {w, 1.65, 4, 0} , B= K28hb2, K33hb2 ?? or could be to L55hn?? NOTES 3D NOESY: noesy100- 304 ~141 31 NN (hn88) 8.5ppm, , ~113 ovlps nn-1 NN-2 (hn116) 7.8ppm, (), could ovlp hn59 NOTES 4D CN: plane overlaps K55, so any NOEs from the CN could be to K55hn Gln 50 INTER AMB NOTES 3D NOESY: noesy100- 237 113 22 NOTES 4D CN: close to D23 in H and N, baseline troulbes at N=11, h=515-525 Glu 51 INTER AMB art? assign (segid="sbm1" and resid X and name hb?) (segid="sbm1" and resid 51 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid X and name hb?) (segid="sbm2" and resid 51 and name hn) 1.8 0 4.2 {vw, 2.79, 2, 0, ncn}, X= N37hb1, N38hb2, F76hb2 - dont like any NOTES 3D NOESY: noesy100- 184 90 36 NN-2 (hn59) 7.71ppm, (6), 144 ovlps hn[25]H25 nn[27] beta-N-1 (hn88) 1.9ppm, (), could ovlp beta, beta and beta-1 carbons also overlap Val 52 INTER amb assign (segid="sbm1" and resid 71 and name hb*) (segid="sbm2" and resid 52 and name hg1*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 71 and name hb*) (segid="sbm1" and resid 52 and name hg1*) 1.8 0 3.2 {g', w, 2.13, 4, 3.9}, wk cfilt but 52hb at 2.13 also amb assign (segid="sbm1" and resid 75 and name hb*) (segid="sbm2" and resid 52 and name hg1*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 75 and name hb*) (segid="sbm1" and resid 52 and name hg1*) 1.8 0 4.2 {g', vw, 1.26, 3, vw cfilt 1.27} AMB NOTES 3D NOESY: noesy100- 365 168 34 Val 53 INTER AMB NOTES 3D NOESY: noesy100- 387 178 32 beta-N-1 (hn2.0) 2.0ppm, (10/2),could ovlp beta, ovlps in Carbon as well Asp 54 INTER AMB art? assign (segid="sbm1" and resid 76 and name he*) (segid="sbm1" and resid 54 and name hn) 1.8 0 6.6 art? assign (segid="sbm2" and resid 76 and name he*) (segid="sbm2" and resid 54 and name hn) 1.8 0 6.6 {vw, 7.30, 7*, 2.4}, shoulder of bigger peak NOTES 3D NOESY: noesy100- 227 108 31 V52 alpha-N-2 (hn34) 3.66ppm, (9/2), 293 could ovlp an-4 Q50 alpha-N-4 (hn88) 3.66ppm, (9/2), 293 could ovlp an-2 NOTES 4D CN: close to O1 in D1 Lys 55 INTER AMB amb assign (segid="sbm1" and resid X and name ha) (segid="sbm1" and resid 55 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid X and name ha) (segid="sbm2" and resid 55 and name hn) 1.8 0 3.2 {w, 4.23, 3, 0, cn} , X= A6,A9,E21,N37 ha's amb assign (segid="sbm1" and resid B and name hb2) (segid="sbm1" and resid 55 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid B and name hb2) (segid="sbm2" and resid 55 and name hn) 1.8 0 3.2 {w, 1.65, 4, 0} , B= K28hb2, K33hb2 ?? NOTES 3D NOESY: noesy100- 302 141 31 NOTES 4D CN: plane overlaps E49, so NOEs from 4D CN could be to E49 instead Val 56 INTER AMB amb/DL assign (segid="sbm1" and resid 48 and name hd*) (segid="sbm1" and resid 56 and name hg?*) 1.8 0 3.2 amb/DL assign (segid="sbm2" and resid 48 and name hd*) (segid="sbm2" and resid 56 and name hg?*) 1.8 0 3.2 {w, 1.42, 6, 2.5} inter? amb assign (segid="sbm1" and resid ? and name hb1) (segid="sbm1" and resid 56 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name hb1) (segid="sbm2" and resid 56 and name hg2*) 1.8 0 3.2 {w, 3.19, 3, 1.5} art? assign (segid="sbm1" and resid X and name ha) (segid="sbm1" and resid 56 and name hn) 1.8 0 3.2 art? assign (segid="sbm2" and resid X and name ha) (segid="sbm2" and resid 56 and name hn) 1.8 0 3.2 {w, 4.67, 3, 0, ncn}, X= N38, H90 ha's; 2 ctrs in 4D 6 in 3D go with 3; but dont like either NOTES 3D NOESY: noesy100- 278 131 27 E58 NN+2 (hn39) 8.27ppm, (), could ovlp nn V52 alpha-N-4 (hn34) 3.66ppm, (10/2), ~293, could ovlp ha Met 57 INTER AMB NOTES 3D NOESY: noesy100- 256 ~121 37 E58 NN (hn39) 8.27ppm, (>10/2), ~123 ovlps hn19 V56 beta-N-1 (hn80) 2.33ppm, (10/2), ovlps hb2 in H and C Glu 58 INTER AMB amb assign (segid="sbm1" and resid ? and name hb2) (segid="sbm1" and resid 58 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name hb2) (segid="sbm2" and resid 58 and name hn) 1.8 0 3.2 {w, 1.67, 5, 1, ncn} art? assign (segid="sbm1" and resid ? and name hn) (segid="sbm1" and resid 58 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name hn) (segid="sbm2" and resid 58 and name hn) 1.8 0 4.2 {vw, 7.44, 3*, 0, amb}, 88hn not see 8.27 amb assign (segid="sbm1" and resid Z and name hb*) (segid="sbm1" and resid 58 and name hn) 1.8 0 1.7 amb assign (segid="sbm2" and resid Z and name hb*) (segid="sbm2" and resid 58 and name hn) 1.8 0 1.7 {m, 2.22, 9, 1, ncn} , Z= V8, K29,E45 hb's - dont like any NOTES 3D NOESY: noesy100- 260 123 33 NOTES 4D CN M57 NN-1 (hn19) 8.30ppm, (), could ovlp hn39 T59 NN (hn18) 8.04ppm, (12), 132 could ovlp nn-2[80] Thr 59 INTER AMB art? assign (segid="sbm1" and resid A and name h?) (segid="sbm1" and resid 59 and name hn) 1.8 0 ? art? assign (segid="sbm2" and resid A and name h?) (segid="sbm2" and resid 59 and name hn) 1.8 0 ? {m, 1.65, 7, ?, ncn} , A= A6hb*,A9hb*, 6 ctrs in 4D 8 in 3D go with 7 - dont like any NOTES 3D NOESY: noesy100- 281 132 37 NN-1 (hn39) 8.2ppm, (14), 123 could ovlp nn-2[19] NN-2 (hn19) 8.3ppm, (14/2), could ovlp nn-1[39] Leu 60 INTER AMB NOTES 3D NOESY: noesy100- 298 140 29 D61 NN (hn20) 7.7ppm, (11), ovlps L60 hn[68] Asp 61 INTER AMB art? assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 61 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 61 and name hn) 1.8 0 4.2 {vw, 4.66/?, 4*, 0, amb}, could be SD or possibly noise fm carrier (4.68) art? assign (segid="sbm1" and resid Y and name h?) (segid="sbm1" and resid 61 and name hn) 1.8 0 1.5? art? assign (segid="sbm2" and resid Y and name h?) (segid="sbm2" and resid 61 and name hn) 1.8 0 1.5? {m, 2.09/31.5, 6, 0, ncn} , Y= M0hb missing,E21hg,E46hg,E49hg; may not be in this plane - dont like any NOTES 3D NOESY: noesy100- 304 142 36 NN-1 (hn68) 7.81ppm, (25/3), could ovlp D61 hn20 NN (hn53) 7.78ppm, (25/3), could ovlp D61 hn20 Glu 62 INTER AMB art? assign (segid="sbm1" and resid 38 and name ha) (segid="sbm1" and resid 62 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 38 and name ha) (segid="sbm2" and resid 62 and name hn) 1.8 0 4.2 {vw, 4.66, 2, 0, cn}, 90ha also at 4.66, neither make sense-artifact at 1H carrier (4.66) ? art? assign (segid="sbm1" and resid 90 and name hb*) (segid="sbm1" and resid 62 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 90 and name hb*) (segid="sbm2" and resid 62 and name hn) 1.8 0 4.2 {vw, 3.17, 4*, 1.0, amb} amb assign (segid="sbm1" and resid Y and name hb?) (segid="sbm1" and resid 62 and name hn) 1.8 0 1.5? amb assign (segid="sbm2" and resid Y and name hb?) (segid="sbm2" and resid 62 and name hn) 1.8 0 1.5? {m, 2.66, 8, ?, ncn}, Y= F14,Y17,D54,F70 hb's; C=39.82 - dont like any NOTES 3D NOESY: noesy100- 301 141 32 NN-1 (hn20) 7.74ppm, (), ovlps E62 hn53 NN-2 (hn68) 7.81ppm, (), ovlps E62 hn53 Asp 63 INTER AMB NOTES 3D NOESY: noesy100- 350 162 34 E62 NN-1 (hn53) 7.79ppm, (14/2), 141 could ovlp nn-2[20] D61 NN-2 (hn20) 7.74ppm, (14/2), 141 could ovlp nn-1[53] Gly 64 INTER AMB NOTES 3D NOESY: noesy100- 290 136 49 G66 NN+2 (hn4) 8.09ppm, (), could ovlp nn Asp 65 INTER AMB NOTES 3D NOESY: noesy100- 274 129 38 NN (hn4) 8.09ppm, (24/2), could ovlp hn16 Gly 66 INTER AMB amb assign (segid="sbm1" and resid ? and name hb) (segid="sbm1" and resid 66 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name hb) (segid="sbm2" and resid 66 and name hn) 1.8 0 4.2 {vw, 2.13-16, 3ov, 1.0} 62hb* 2.11, 58hb* 2.13, 49hg1/b1 2.13, or 32hb1 2.16 NOTES 3D NOESY: noesy100- 274 129 47 D65 NN-1 (hn16) 8.09ppm, (), ovlps hn4 Glu 67 INTER AMB SD? assign (segid="sbm1" and resid ? and name ha) (segid="sbm1" and resid 67 and name hn) 1.8 0 ? SD? assign (segid="sbm2" and resid ? and name ha) (segid="sbm2" and resid 67 and name hn) 1.8 0 ? {vw, 5.37-40, ~8*, 0, amb} 26ha or 69ha - both seem too far away NOTES 3D NOESY: noesy100- 241 115 33 D65 NN-2 (hn16) 8.09ppm, (), could ovlp nn-1 Cys 68 INTER AMB NOTES 3D NOESY: noesy100- 164 82 31 X/Y= R20hg1,hg2 not in 4D NOESY, also observed for G66 NOTES 4D CN K26ha 4 ctrs in 4D 9* in 3D go with 2 K28ha 6ctrs in 4D 3 in 3D go with 4 Asp 69 INTER AMB amb assign (segid="sbm1" and resid 88/14 and name he*/z?) (segid="sbm1" and resid 69 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid 88/14 and name he*/z?) (segid="sbm2" and resid 69 and name hn) 1.8 0 ? {vw, 7.33, 5*, 2.4} F14 7.30, F71 he21 7.32 but looks too far as does 76 ring (~7.27 and ~7.32) ? assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 69 and name hn) 1.8 0 4.2 ? assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 69 and name hn) 1.8 0 4.2 {vw, 5.48, 3*, 0} unassigned peak NOTES 3D NOESY: noesy100- 233 111 27 Phe 70 INTER assign (segid="sbm1" and resid 82 and name hg2*) (segid="sbm2" and resid 70 and name hn) 1.8 0 4.2 assign (segid="sbm2" and resid 82 and name hg2*) (segid="sbm1" and resid 70 and name hn) 1.8 0 4.2 {vw, 0.59, 3*} 82hg2*-71hn assigned so could be SD? for test_rama3 structures (10): Average=7.145 Angtroms, stand. dev.=0.6799, min= 5.731, max= 7.841 AMB {DJW removed} NOTES 3D NOESY: noesy100- 181 89 32 Gln 71 INTER ; 13357 1 13855 7 parsed_1b4c 1 866 ; {w, 0.59, 3} 82hg2*, 36hd*, 35d1*, or 27hd** ??? for test_rama3: Average=6.007 Angtroms, stand. dev.=0.4205, min= 5.1, max= 6.743 amb assign (segid="sbm1" and resid 88 and name he*) (segid="sbm2" and resid 71 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 88 and name he*) (segid="sbm1" and resid 71 and name hn) 1.8 0 4.2 {vw, 7.14, 4*, amb} could be F70hz 7.12, F14he* and F73he* 7.11 AMB amb assign (segid="sbm1" and resid 70/73 and name he/d*) (segid="sbm1" and resid 71 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 70/73 and name he/d*) (segid="sbm2" and resid 71 and name hn) 1.8 0 4.2 {vw, 6.92, 8*, 2.4} 73hd* closer in CS, and 73hd* at 6.92 for 73h ? assign (segid="sbm1" and resid 39 and name ha) (segid="sbm1" and resid 71 and name hn) 1.8 0 4.2 ? assign (segid="sbm2" and resid 39 and name ha) (segid="sbm2" and resid 71 and name hn) 1.8 0 4.2 {vw, 4.83, 5*, 0, ncn} NOTES 3D NOESY: noesy100- 288 135 35 D69 NN-2 (hn78) 8.58ppm, (4/2), 110 could ovlp nn+2 F73 NN+2 (hn72) 8.62ppm, (4/2), 110 could ovlp nn-2 Glu 72 INTER AMB NOTES 3D NOESY: noesy100- 254 121 28 M74 NN+2 (hn32) 8.00ppm, () could ovlp nn-1 Phe 73 INTER AMB NOTES 3D NOESY: noesy100- 229 110 29 Q71 NN-2 (hn28) 7.93ppm, (), could ovlp nn NOTES 4D CN: close to O1 in D1 so intensity greatly attenuated Met 74 INTER amb/R assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 74 and name he*) 1.8 0 4.2 amb/R assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 74 and name he*) 1.8 0 4.2 {w, 0.92, >12ovlp, 4.4, wk cfilt at 1.00} ; 13858 1 13911 50 parsed_1b4c 1 867 ; {m, 2.06, 13, 3.0, md cfilt} med as both intra and inter Dist over 10 (test_rama3) strucs intra: Average=5.324 Angtroms, stand. dev.=0.4607, min= 4.231, max= 6.081 Dist over 10 (test_rama3) strucs inter: Average=5.691 Angtroms, stand. dev.=0.7689, min= 4.542, max= 6.957 ; 13915 1 13917 109 parsed_1b4c 1 868 "{mw, 1.00, 16, 4.4, med cfilt?} mw b/c some intra contribution from model" 13921 1 13921 82 parsed_1b4c 1 869 ; {w, 3.90, 3, 2.5, wk cfilt 3.99} AMB amb/DL assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 74 and name hn) 1.8 0 4.2 amb/DL assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 74 and name hn) 1.8 0 4.2 {vw, 0.78, 3*, 2.9, amb}, probably 77hg1* at 0.77 amb assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 74 and name he*) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 74 and name he*) 1.8 0 3.2 {w, 7.38/130.0, 3, no cfilt} amb assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 74 and name he*) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 74 and name he*) 1.8 0 3.2 {w, 7.09/131.6, 2, 1.5, no cfilt}, 73hz, 14he*, 88h? NOTES 3D NOESY: noesy100- 282 133 34 F76 NN+2 (hn23) 7.99ppm, (), could ovlp M74 hn32 Ala 75 INTER amb assign (segid="sbm1" and resid 78 and name hb*) (segid="sbm2" and resid 75 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 78 and name hb*) (segid="sbm1" and resid 75 and name hn) 1.8 0 3.2 {w, 3.66-8?, 6ov?, 1.0} AMB ?!assign (segid="sbm1" and resid 14 and name hz) (segid="sbm1" and resid 75 and name hb*) 1.8 0 4.2 ?!assign (segid="sbm2" and resid 14 and name hz) (segid="sbm2" and resid 75 and name hb*) 1.8 0 4.2 {vw, 7.24, 1, 1.5, 4d} lloks far on model but could be art? assign (segid="sbm1" and resid 53 and name hg2*) (segid="sbm1" and resid 75 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 53 and name hg2*) (segid="sbm2" and resid 75 and name hn) 1.8 0 4.2 {vw, 0.91, 2*, 1.5, amb} amb assign (segid="sbm1" and resid and name h) (segid="sbm1" and resid 75 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid and name h) (segid="sbm2" and resid 75 and name hn) 1.8 0 ? {vw, 7.33, 6*, , amb} 14hz 7.30, 76h? 7.32, 71he21 7.32, 88h ring? 7.33 NOTES 3D NOESY: noesy100- 294 138 22 M74 NN-1 (hn32) 8.00ppm, (14/2), 133 ovlps nn F76 NN (hn23) 7.99ppm, (14/2), 133 ovlps nn-1 Phe 76 INTER AMB amb assign (segid="sbm1" and resid 79 and name hg*) (segid="sbm1" and resid 76 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 79 and name hg*) (segid="sbm2" and resid 76 and name hn) 1.8 0 4.2 {vw, 2.52, 7*, 1.0, amb} could be inter? NOTES 3D NOESY: noesy100- 283 133 35 ha vw in 3D NOESY and 10 ctrs in 4D go with 5 ctrs Val 77 INTER amb assign (segid="sbm1" and resid 3 and name hg) (segid="sbm2" and resid 77 and name hg1*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 3 and name hg) (segid="sbm1" and resid 77 and name hg1*) 1.8 0 4.2 {vw, 1.49, 3, 1.5, amb, wk cfilt} amb 980108 off in CS for 3hg ; 13925 1 13995 77 parsed_1b4c 1 870 ; {mw, 0.92, 11ov?, 4.4, med cfilt} amb/R assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 77 and name hg1*) 1.8 0 3.2 amb/R assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 77 and name hg1*) 1.8 0 3.2 {w, 0.65, 8, 4.4, amb} off in CS for 3hd2* or 40hd2*, 40hd2* may contribute ; 13999 1 14003 84 parsed_1b4c 1 871 ; {w, 0.71/26.8, 7, 4.4, amb, wk cfilt} amb/R assign (segid="sbm1" and resid 3 and name hd*) (segid="sbm2" and resid 77 and name hg2*) 1.8 0 3.2 amb/R assign (segid="sbm2" and resid 3 and name hd*) (segid="sbm1" and resid 77 and name hg2*) 1.8 0 3.2 {w, 0.92, 7, 4.4, amb, wk cfilt} ; 14007 1 14011 41 parsed_1b4c 1 872 ; {m, 2.06, ~12, 3.0, med cfilt} AMB art/SD? assign (segid="sbm1" and resid 10 and name ha) (segid="sbm1" and resid 77 and name hn) 1.8 0 4.2 art/SD? assign (segid="sbm2" and resid 10 and name ha) (segid="sbm2" and resid 77 and name hn) 1.8 0 4.2 {vw, 4.12, 9*, 0, cn} 10 looks too far art? assign (segid="sbm1" and resid 10 and name hb*) (segid="sbm1" and resid 77 and name hn) 1.8 0 4.2 art? assign (segid="sbm2" and resid 10 and name hb*) (segid="sbm2" and resid 77 and name hn) 1.8 0 4.2 {vw, 2.49, 3*, 1.0} 10hb* looks too far NOTES 3D NOESY: noesy100- 244 116 35 A75 NN-2 (hn87) 7.8ppm, (5/2), 139 could ovlp nn+2 M79 NN+2 (hn79) 7.8ppm, (5/2), 139 could ovlp nn-2 Ser 78 INTER AMB amb assign (segid="sbm1" and resid x and name h) (segid="sbm1" and resid 78 and name hn) 1.8 0 4.7 amb assign (segid="sbm2" and resid x and name h) (segid="sbm2" and resid 78 and name hn) 1.8 0 4.7 {w, 0.83, 4, , cn} 0.83/24.18 in 4Dcn: nothing matches well, V53hg2, I47hg, L44hd; 1 ctr in 4D 8 ctrs in 3D go with 4 - dont like any NOTES 3D NOESY: noesy100- 228 109 32 M79 NN (hn79) 7.85ppm, (12), 139 could ovlp nn+2 Met 79 INTER ; 14015 1 14050 7 parsed_1b4c 1 873 ; {vw, 7.32, 8*, 0} 71he21, 88h?, 45hn, 76h?, 17d*, 14hz ?? {vw, 6.70, 3*, 0} 17he*, 41hn, or 71he22 ?? amb assign (segid="sbm1" and resid 75 and name hb*) (segid="sbm2" and resid 79 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 75 and name hb*) (segid="sbm1" and resid 79 and name hn) 1.8 0 3.2 {w, 1.21, 5, 1.5, amb} could have intra contirbution AMB amb assign (segid="sbm1" and resid ? and name h?) (segid="sbm1" and resid 79 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid ? and name h?) (segid="sbm2" and resid 79 and name he*) 1.8 0 4.2 {vw, 0.93/24.1, 2, 3.0} 53hg2* not see 79he* NOTES 3D NOESY: noesy100- 297 139 27 V80 NN (hn22) 7.80ppm, (25/2), ~139 could ovlp M79 hn79 Val 80 INTER AMB art? assign (segid="sbm1" and resid 43 and name hd*) (segid="sbm1" and resid 80 and name hg2*) 1.8 0 8.6 art? assign (segid="sbm2" and resid 43 and name hd*) (segid="sbm2" and resid 80 and name hg2*) 1.8 0 8.6 {vw, 7.17, 1, 4.4} NOTES 3D NOESY: noesy100- 298 139 36 M79 NN-1 (hn79) ppm, (22/2), ~139 ovlps V80 hn22 T81 NN+2 (hn) ppm, (), could ovlp hn22 NOTES 4D CN: M79 an-1 could also be R20, F88 Thr 81 INTER ; 14053 1 14090 7 parsed_1b4c 1 874 ; {m, 2.06, >10, 3.0, med cfilt} amb assign (segid="sbm1" and resid 7 and name hb*) (segid="sbm2" and resid 81 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 7 and name hb*) (segid="sbm1" and resid 81 and name hg2*) 1.8 0 3.2 {w, 2.06, 5, wk cfilt} amb b/c 8hg1 close to 81hg2 in CS and maxes in other plane amb assign (segid="sbm1" and resid 8 and name ha) (segid="sbm2" and resid 81 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 8 and name ha) (segid="sbm1" and resid 81 and name hg2*) 1.8 0 3.2 {w, 3.48, 6, 1.5, NO cfilt?} amb b/c 8hg1 close to 81hg2 in CS amb assign (segid="sbm1" and resid 8 and name hb) (segid="sbm2" and resid 81 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 8 and name hb) (segid="sbm1" and resid 81 and name hg2*) 1.8 0 3.2 {w?, 2.13, 13, 1.5, wk cfilt} amb - off in 1H ppm for V8 amb assign (segid="sbm1" and resid 8 and name hg2*) (segid="sbm2" and resid 81 and name hg2*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 8 and name hg2*) (segid="sbm1" and resid 81 and name hg2*) 1.8 0 3.2 {w?, 1.21, ~15 max other plane} cfilt at 1.23 amb b/c 8hg1 close to 81hg2 in CS ; 14093 1 14109 90 parsed_1b4c 1 875 ; {w, 0.07, 9, no cfilt?} amb b/c 8hg1 close to 81hg2 in CS AMB amb assign (segid="sbm1" and resid 53/8 and name hg?*) (segid="sbm2" and resid 81 and name hn) 1.8 0 4.2 amb assign (segid="sbm2" and resid 53/8 and name hg?*) (segid="sbm1" and resid 81 and name hn) 1.8 0 4.2 {vw, 0.96, 8&3, 1.5, cn} looks real in 4D at 0.96/21.4 amb/art? assign (segid="sbm1" and resid 73 and name hz) (segid="sbm2" and resid 81 and name hg2*) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 73 and name hz) (segid="sbm1" and resid 81 and name hg2*) 1.8 0 4.2 {vw, 7.02, 1, 1.5} NOTES 3D NOESY: noesy100- ~270 ~127 38 V80 NN-1 (hn22) 7.80ppm, (10/3), ~139 could ovlp nn and nn-2 T82 NN (hn111) 7.87ppm, (10/3), ~139 could ovlp nn-1/-2 M79 NN-2 (hn79) 7.83ppm, (10/3), ~139 could ovlp nn and nn-1 NOTES 4D CN V80 aN-1 (hn22) and V77 aN-4 (hn29) 3.4ppm, ovlp @ C=67.23; could also be I11 or V53 S78an-3 could also be S41ha,hb or I47hb Thr 82 INTER amb/art assign (segid="sbm1" and resid 14 and name hd*) (segid="sbm2" and resid 82 and name hg2*) 1.8 0 4.2 amb/art assign (segid="sbm2" and resid 14 and name hd*) (segid="sbm1" and resid 82 and name hg2*) 1.8 0 4.2 {vw, 6.17, 2ovlp, 4.4, cfilt at 6.30} ; 14113 1 14140 46 parsed_1b4c 1 876 ; {m, 6.31, 8, 3.9, cfilt at 6.34} AMB NOTES 3D NOESY: noesy100- 293 137 45 there was some uncertainty about the assignment of ha and hb however a unique noe was observed for A83 to 3.79,68.38 consistent with the current assignment of the ha and hb for T82 M79 aN-3 (hn79) 3.96ppm, vw(9), ~282 could ovlp an-4; strgr at 8.6ppm S78 aN-4 (hn49) 3.96ppm, vw(9), ~282 could ovlp an-3; strgr at 8.6ppm vw pk 100ms NOESY looks like two peaks 7.88/7.86 Ala 83 INTER AMB inter?!assign (segid="sbm1" and resid 6 and name hb*) (segid="sbm1" and resid 83 and name hb*) 1.8 0 1.5 inter?!assign (segid="sbm2" and resid 6 and name hb*) (segid="sbm2" and resid 83 and name hb*) 1.8 0 1.5 {m?, 1.56, >15, 3.0} NOTES 3D NOESY: noesy100- 347 160 29 ha dispersive in 3D NOESY; hb 17 ctrs in both expts so 9 ctrs used for ha Cys 84 INTER His 85? INTER AMB assign (segid="sbm1" and resid and name hn) (segid="sbm1" and resid 85 and name hn) assign (segid="sbm2" and resid and name hn) (segid="sbm2" and resid 85 and name hn) NN+2 (hn122) 8.61ppm, vw(), ~110 (nh- 8.35ppm) hn119 seems to be multiple 8.35, 8.34, 8.33 nn region differs a little between 100 and 200 ms noesy100- ~254 ~121 48 alpha?- 3.68 ppm () ~292 ovlps has[3], could be 3.8 instead beta1- 2.16 ppm () 348 ovlps peak from G22(hn3) beta2- 1.89 ppm () 358 ovlps peak from G22 Glu 86? INTER AMB (nh- 8.01ppm) hn107 dispersive amide in 100ms close to E91 in 1H and 15N noesy100- 281 ~132 20 alpha- 4.36 ppm () missing in NOESY, present in TOCSY beta1- 2.22 ppm vw(8) 346 close to negative peak beta2- 1.86 ppm (4) 359 gamma1- 2.57 ppm vw(9) 340 gamma2- 2.38 ppm vw(6) 333 close to negative peak Phe 87 INTER amb assign (segid="sbm1" and resid 14 and name hb*) (segid="sbm2" and resid 87 and name he*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 14 and name hb*) (segid="sbm1" and resid 87 and name he*) 1.8 0 3.2 {w, 2.71, 4} ; 14144 1 14224 21 parsed_1b4c 1 877 ; {w, 6.24, 5} amb assign (segid="sbm1" and resid 25 and name hb*) (segid="sbm2" and resid 87 and name he*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 25 and name hb*) (segid="sbm1" and resid 87 and name he*) 1.8 0 3.2 {w, 3.24, 4} ; 14228 1 14232 21 parsed_1b4c 1 878 "{w, 2.61, 4}" 14236 1 14236 21 parsed_1b4c 1 879 "{w, 6.31, 3}" 14240 1 14240 21 parsed_1b4c 1 880 "{mw, 6.33, 6}" 14244 1 14244 22 parsed_1b4c 1 881 ; {w, 6.95, 3} amb/sani assign (segid="sbm1" and resid 71 and name ha) (segid="sbm2" and resid 87 and name he*) 1.8 0 4.2 amb/sani assign (segid="sbm2" and resid 71 and name ha) (segid="sbm1" and resid 87 and name he*) 1.8 0 4.2 {vw, 3.55, 2} AMB assign (segid="sbm1" and resid and name hn) (segid="sbm1" and resid 87 and name hn) assign (segid="sbm2" and resid and name hn) (segid="sbm2" and resid 87 and name hn) NONE NN+2 (hn) ppm, (), assign (segid="sbm1" and resid and name hn) (segid="sbm1" and resid 87 and name hn) assign (segid="sbm2" and resid and name hn) (segid="sbm2" and resid 87 and name hn) NONE NN-2 (hn) ppm, (), assign (segid="sbm1" and resid and name ha) (segid="sbm1" and resid 87 and name hn) assign (segid="sbm2" and resid and name ha) (segid="sbm2" and resid 87 and name hn) NONE alpha-N-1 (hn) ppm, (), assign (segid="sbm1" and resid and name ha) (segid="sbm1" and resid 87 and name hn) assign (segid="sbm2" and resid and name ha) (segid="sbm2" and resid 87 and name hn) NONE alpha-N-3 (hn) ppm, (), assign (segid="sbm1" and resid and name ha) (segid="sbm1" and resid 87 and name hn) assign (segid="sbm2" and resid and name ha) (segid="sbm2" and resid 87 and name hn) NONE alpha-N-4 (hn) ppm, (), (nh- 8.61ppm) hn122 noesy100- 229 ~109 25 alpha- 3.96 ppm (4) 282 beta1- 2.00 ppm (5) 354 beta2- 1.86 ppm (5) 359 could ovpl b2n-1 ??in tocsy- 1.56 ppm (3) Phe 88 INTER ; 14248 1 14288 7 parsed_1b4c 1 882 "{vw, 0.15, 4*, amb}" 14291 1 14291 28 parsed_1b4c 1 883 ; {m, 6.27, ~10, 2Droe, amb} amb assign (segid="sbm1" and resid 25 and name hb*) (segid="sbm2" and resid 88 and name he*) 1.8 0 4.2 amb assign (segid="sbm2" and resid 25 and name hb*) (segid="sbm1" and resid 88 and name he*) 1.8 0 4.2 {vw, 3.25, 2, 2Droe, amb} ; 14295 1 14299 34 parsed_1b4c 1 884 ; {s, 6.96, >10, 2Droe, amb therefore lower category, DJW} amb assign (segid="sbm1" and resid 74 and name he*) (segid="sbm2" and resid 88 and name he*) 1.8 0 3.2 amb assign (segid="sbm2" and resid 74 and name he*) (segid="sbm1" and resid 88 and name he*) 1.8 0 3.2 {w, 1.64, ~3, 2Droe, 3.9, amb} NOTES 3D NOESY: noesy100- 329 ~153 40 E89 NN (hn60) 7.57ppm, (~6), ~149 ovlps F88 hn5 Glu 89 INTER AMB amb/art? assign (segid="sbm1" and resid 37 and name hb*) (segid="sbm1" and resid 89 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 37 and name hb*) (segid="sbm2" and resid 89 and name hn) 1.8 0 4.2 {vw, 2.68, 4*, 1.0, amb} amb/art? assign (segid="sbm1" and resid 61 and name hb*) (segid="sbm1" and resid 89 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 61 and name hb*) (segid="sbm2" and resid 89 and name hn) 1.8 0 4.2 {vw, 2.65, 4*, 1.0, amb} amb assign (segid="sbm1" and resid ? and name hb1) (segid="sbm1" and resid 89 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid ? and name hb1) (segid="sbm2" and resid 89 and name hn) 1.8 0 3.2 {w?, 1.94/31.5, 8, 0, cn} 33hb1 1.94/32.3, 5bhb* 1.92/32.3, 55hb* 1.97/31.3, 91hb1 2.00/30.9 amb assign (segid="sbm1" and resid 58 and name hb*) (segid="sbm1" and resid 89 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 58 and name hb*) (segid="sbm2" and resid 89 and name hn) 1.8 0 3.2 {w, 2.13/29.2, 7, 1, cn} amb assign (segid="sbm1" and resid 62 and name ha) (segid="sbm1" and resid 89 and name hn) 1.8 0 3.2 amb assign (segid="sbm2" and resid 62 and name ha) (segid="sbm2" and resid 89 and name hn) 1.8 0 3.2 {w, 4.17/58.5, 7, 0, cn} 55ha 4.15/58.6 plus others amb assign (segid="sbm1" and resid and name h) (segid="sbm1" and resid 89 and name hn) 1.8 0 ? amb assign (segid="sbm2" and resid and name h) (segid="sbm2" and resid 89 and name hn) 1.8 0 ? {vw, 4.45, 5*, } NOTES 3D NOESY: noesy100-320 149 31 His 90 INTER AMB amb/art? assign (segid="sbm1" and resid 40 and name hd*) (segid="sbm1" and resid 90 and name hn) 1.8 0 4.2 amb/art? assign (segid="sbm2" and resid 40 and name hd*) (segid="sbm2" and resid 90 and name hn) 1.8 0 4.2 {vw, 0.94, 8*, 2.9} viol for 32hd2* and 40hd1*, probably artifact NOTES 3D NOESY: noesy100- 274 129 32 ha dispersive in 3D, stronger in 4D E91 NN (hn90) ppm, (17/2), ~129 could ovlp H90 hn114 Glu 91 INTER AMB NOTES 3D NOESY noesy100- 273 129 20 H90 NN-1 (hn114) 8.0ppm, (), could ovlp E91 hn90 NOTES 4D CN H90ha 13 ctrs in 4D close to H2O in 3D go with 6 ctrs ; 14303 1 14374 62 parsed_1b4c 1 stop_ save_
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