data_5858 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 5858 _Entry.Title ; Characterization of us-ms Dynamics of Proteins Using a Combined Analysis of 15N NMR Relaxation and Chemical Shift: Conformational Exchange in Plastocyanin Induced by Histidine Protonations ; _Entry.Type . _Entry.Version_type original _Entry.Submission_date 2003-07-04 _Entry.Accession_date 2003-07-07 _Entry.Last_release_date 2004-02-12 _Entry.Original_release_date 2004-02-12 _Entry.Origination author _Entry.NMR_STAR_version 3.1.1.61 _Entry.Original_NMR_STAR_version 2.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.Entry_ID 1 Mathias Hass . A.S. . 5858 2 Marianne Thuesen . H. . 5858 3 Hans Christensen . E.M. . 5858 4 Jens Led . J. . 5858 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 14 5858 heteronucl_T1_relaxation 8 5858 heteronucl_T2_relaxation 6 5858 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '1H chemical shifts' 1312 5858 '15N chemical shifts' 1312 5858 'T1 relaxation values' 742 5858 'T2 relaxation values' 570 5858 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2004-02-12 2003-07-04 original author . 5858 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 5505 'Chemical shifts and other data' 5858 stop_ save_ ############### # Citations # ############### save_entry_citation _Citation.Sf_category citations _Citation.Sf_framecode entry_citation _Citation.Entry_ID 5858 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 14733549 _Citation.Full_citation . _Citation.Title ; Characterization of us-ms Dynamics of Proteins Using a Combined Analysis of 15N NMR Relaxation and Chemical Shift: Conformational Exchange in Plastocyanin Induced by Histidine Protonations ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'J. Am. Chem. Soc.' _Citation.Journal_name_full . _Citation.Journal_volume 126 _Citation.Journal_issue 3 _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 753 _Citation.Page_last 765 _Citation.Year 2004 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Mathias Hass . A.S. . 5858 1 2 Marianne Thuesen . H. . 5858 1 3 Hans Christensen . E.M. . 5858 1 4 Jens Led . J. . 5858 1 stop_ save_ save_ref_1 _Citation.Sf_category citations _Citation.Sf_framecode ref_1 _Citation.Entry_ID 5858 _Citation.ID 2 _Citation.Class 'reference citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 12525159 _Citation.Full_citation ; Ma L, Hass MA, Vierick N, Kristensen SM, Ulstrup J, Led JJ. Biochemistry 2003, 42,320-330. ; _Citation.Title 'Backbone dynamics of reduced plastocyanin from the cyanobacterium Anabaena variabilis: regions involved in electron transfer have enhanced mobility.' _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev Biochemistry _Citation.Journal_name_full Biochemistry _Citation.Journal_volume 42 _Citation.Journal_issue 2 _Citation.Journal_ASTM . _Citation.Journal_ISSN 0006-2960 _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 320 _Citation.Page_last 330 _Citation.Year 2003 _Citation.Details ; The dynamics of the backbone of the electron-transfer protein plastocyanin from the cyanobacterium Anabaena variabilis were determined from the (15)N and (13)C(alpha) R(1) and R(2) relaxation rates and steady-state [(1)H]-(15)N and [(1)H]-(13)C nuclear Overhauser effects (NOEs) using the model-free approach. The (13)C relaxation studies were performed using (13)C in natural abundance. Overall, it is found that the protein backbone is rigid. However, the regions that are important for the function of the protein show moderate mobility primarily on the microsecond to millisecond time scale. These regions are the "northern" hydrophobic site close to the metal site, the metal site itself, and the "eastern" face of the molecule. In particular, the mobility of the latter region is interesting in light of recent findings indicating that residues also on the eastern face of plastocyanins from prokaryotes are important for the function of the protein. The study also demonstrates that relaxation rates and NOEs of the (13)C(alpha) nuclei of proteins are valuable supplements to the conventional (15)N relaxation measurements in studies of protein backbone dynamics. ; loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Lixin Ma L. . . 5858 2 2 'Mathias A S' Hass M. A. . 5858 2 3 Nanna Vierick N. . . 5858 2 4 'Soren M' Kristensen S. M. . 5858 2 5 Jens Ulstrup J. . . 5858 2 6 'Jens J' Led J. J. . 5858 2 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_system_A.v.PCu(I) _Assembly.Sf_category assembly _Assembly.Sf_framecode system_A.v.PCu(I) _Assembly.Entry_ID 5858 _Assembly.ID 1 _Assembly.Name 'Cu (I) Plastocyanin from Anabaena Variabilis' _Assembly.BMRB_code . _Assembly.Number_of_components . _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state 'all other bound' _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Assembly_type.Type _Assembly_type.Entry_ID _Assembly_type.Assembly_ID monomer 5858 1 stop_ loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 'plastocyanin monomer' 1 $plastocyanin . . . native . . . . . 5858 1 2 'COPPER (I) ION' 2 $CU1 . . . native . . . . . 5858 1 stop_ loop_ _Bond.ID _Bond.Type _Bond.Value_order _Bond.Assembly_atom_ID_1 _Bond.Entity_assembly_ID_1 _Bond.Entity_assembly_name_1 _Bond.Entity_ID_1 _Bond.Comp_ID_1 _Bond.Comp_index_ID_1 _Bond.Seq_ID_1 _Bond.Atom_ID_1 _Bond.Assembly_atom_ID_2 _Bond.Entity_assembly_ID_2 _Bond.Entity_assembly_name_2 _Bond.Entity_ID_2 _Bond.Comp_ID_2 _Bond.Comp_index_ID_2 _Bond.Seq_ID_2 _Bond.Atom_ID_2 _Bond.Auth_entity_assembly_ID_1 _Bond.Auth_entity_assembly_name_1 _Bond.Auth_seq_ID_1 _Bond.Auth_comp_ID_1 _Bond.Auth_atom_ID_1 _Bond.Auth_entity_assembly_ID_2 _Bond.Auth_entity_assembly_name_2 _Bond.Auth_seq_ID_2 _Bond.Auth_comp_ID_2 _Bond.Auth_atom_ID_2 _Bond.Entry_ID _Bond.Assembly_ID 1 coordination single . 1 . 1 CYS 90 90 SG . 2 . 2 CU1 1 1 CU . . . . . . . . . . 5858 1 stop_ loop_ _Assembly_common_name.Name _Assembly_common_name.Type _Assembly_common_name.Entry_ID _Assembly_common_name.Assembly_ID 'Cu (I) Plastocyanin from Anabaena Variabilis' system 5858 1 'A. v. PCu(I)' abbreviation 5858 1 stop_ loop_ _Assembly_bio_function.Biological_function _Assembly_bio_function.Entry_ID _Assembly_bio_function.Assembly_ID 'Electron transfer in photosynthesis' 5858 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_plastocyanin _Entity.Sf_category entity _Entity.Sf_framecode plastocyanin _Entity.Entry_ID 5858 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name 'Cu(II) Plastocyanin from Anabeana Variabilis' _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; METYTVKLGSDKGLLVFEPA KLTIKPGDTVEFLNNKVPPH NVVFDAALNPAKSADLAKSL SHKQLLMSPGQSTSTTFPAD APAGEYTFYCEPHRGAGMVG KITVAG ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states . _Entity.Ambiguous_chem_comp_sites . _Entity.Nstd_monomer . _Entity.Nstd_chirality . _Entity.Nstd_linkage . _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 106 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic . _Entity.Thiol_state 'all other bound' _Entity.Src_method . _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight 11900 _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date 2008-08-19 _Entity.DB_query_revised_last_date 2008-08-19 loop_ _Entity_db_link.Ordinal _Entity_db_link.Author_supplied _Entity_db_link.Database_code _Entity_db_link.Accession_code _Entity_db_link.Entry_mol_code _Entity_db_link.Entry_mol_name _Entity_db_link.Entry_experimental_method _Entity_db_link.Entry_structure_resolution _Entity_db_link.Entry_relation_type _Entity_db_link.Entry_details _Entity_db_link.Chimera_segment_ID _Entity_db_link.Seq_query_to_submitted_percent _Entity_db_link.Seq_subject_length _Entity_db_link.Seq_identity _Entity_db_link.Seq_positive _Entity_db_link.Seq_homology_expectation_val _Entity_db_link.Seq_align_begin _Entity_db_link.Seq_align_end _Entity_db_link.Seq_difference_details _Entity_db_link.Seq_alignment_details _Entity_db_link.Entry_ID _Entity_db_link.Entity_ID . . SWISS-PROT P46444 . 'Plastocyanin precursor' . . . . . 99.06 139 100.00 100.00 1.08e-55 . . . . 5858 1 . . SWISS-PROT P0C178 . Plastocyanin . . . . . 99.06 105 100.00 100.00 1.03e-54 . . . . 5858 1 . . SWISS-PROT O52830 . 'Plastocyanin precursor' . . . . . 99.06 139 100.00 100.00 1.08e-55 . . . . 5858 1 . . REF NP_484302 . 'plastocyanin [Nostoc sp. PCC 7120]' . . . . . 99.06 139 100.00 100.00 1.08e-55 . . . . 5858 1 . . PIR CUAI . 'plastocyanin - Anabaena variabilis' . . . . . 99.06 105 100.00 100.00 1.03e-54 . . . . 5858 1 . . GenBank AAA59364 . 'plastocyanin precursor' . . . . . 99.06 139 100.00 100.00 1.08e-55 . . . . 5858 1 . . EMBL CAA05338 . 'plastocyanin [Nostoc sp. PCC 7119]' . . . . . 99.06 139 100.00 100.00 1.08e-55 . . . . 5858 1 . . DBJ BAB77782 . 'plastocyanin precursor [Nostoc sp. PCC 7120]' . . . . . 99.06 139 100.00 100.00 1.08e-55 . . . . 5858 1 . . PDB 2GIM . '1.6 Angstrom Structure Of Plastocyanin From Anabaena Variabilis' . . . . . 100.00 106 100.00 100.00 2.18e-55 . . . . 5858 1 . . PDB 2CJ3 . 'Crystal Structure Of Plastocyanin From A Cyanobacterium, Anabaena Variabilis' . . . . . 97.17 105 100.00 100.00 1.94e-53 . . . . 5858 1 . . PDB 1TU2 . 'The Complex Of Nostoc Cytochrome F And Plastocyanin Determin With Paramagnetic Nmr. Based On The Structures Of Cytochrome F And Plastocyanin, 10 Structures' . . . . . 99.06 105 100.00 100.00 1.03e-54 . . . . 5858 1 . . PDB 1NIN . 'Plastocyanin From Anabaena Variabilis, Nmr, 20 Structures' . . . . . 99.06 105 100.00 100.00 1.03e-54 . . . . 5858 1 . . PDB 1FA4 . 'Elucidation Of The Paramagnetic Relaxation Of Heteronuclei And Protons In Cu(Ii) Plastocyanin From Anabaena Variabilis' . . . . . 99.06 105 100.00 100.00 1.03e-54 . . . . 5858 1 . . BMRB 5505 . 'Cu(II) Plastocyanin from Anabeana Variabilis' . . . . . 99.06 105 100.00 100.00 1.03e-54 . . . . 5858 1 . . BMRB 4738 . 'Plastocyanin from Anabena variabilis' . . . . . 99.06 105 100.00 100.00 1.03e-54 . . . . 5858 1 stop_ loop_ _Entity_common_name.Name _Entity_common_name.Type _Entity_common_name.Entry_ID _Entity_common_name.Entity_ID 'Cu(II) Plastocyanin from Anabeana Variabilis' common 5858 1 'A. v. PCu(I)' abbreviation 5858 1 stop_ loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 0 MET . 5858 1 2 1 GLU . 5858 1 3 2 THR . 5858 1 4 3 TYR . 5858 1 5 4 THR . 5858 1 6 5 VAL . 5858 1 7 6 LYS . 5858 1 8 7 LEU . 5858 1 9 8 GLY . 5858 1 10 9 SER . 5858 1 11 10 ASP . 5858 1 12 11 LYS . 5858 1 13 12 GLY . 5858 1 14 13 LEU . 5858 1 15 14 LEU . 5858 1 16 15 VAL . 5858 1 17 16 PHE . 5858 1 18 17 GLU . 5858 1 19 18 PRO . 5858 1 20 19 ALA . 5858 1 21 20 LYS . 5858 1 22 21 LEU . 5858 1 23 22 THR . 5858 1 24 23 ILE . 5858 1 25 24 LYS . 5858 1 26 25 PRO . 5858 1 27 26 GLY . 5858 1 28 27 ASP . 5858 1 29 28 THR . 5858 1 30 29 VAL . 5858 1 31 30 GLU . 5858 1 32 31 PHE . 5858 1 33 32 LEU . 5858 1 34 33 ASN . 5858 1 35 34 ASN . 5858 1 36 35 LYS . 5858 1 37 36 VAL . 5858 1 38 37 PRO . 5858 1 39 38 PRO . 5858 1 40 39 HIS . 5858 1 41 40 ASN . 5858 1 42 41 VAL . 5858 1 43 42 VAL . 5858 1 44 43 PHE . 5858 1 45 44 ASP . 5858 1 46 45 ALA . 5858 1 47 46 ALA . 5858 1 48 47 LEU . 5858 1 49 48 ASN . 5858 1 50 49 PRO . 5858 1 51 50 ALA . 5858 1 52 51 LYS . 5858 1 53 52 SER . 5858 1 54 53 ALA . 5858 1 55 54 ASP . 5858 1 56 55 LEU . 5858 1 57 56 ALA . 5858 1 58 57 LYS . 5858 1 59 58 SER . 5858 1 60 59 LEU . 5858 1 61 60 SER . 5858 1 62 61 HIS . 5858 1 63 62 LYS . 5858 1 64 63 GLN . 5858 1 65 64 LEU . 5858 1 66 65 LEU . 5858 1 67 66 MET . 5858 1 68 67 SER . 5858 1 69 68 PRO . 5858 1 70 69 GLY . 5858 1 71 70 GLN . 5858 1 72 71 SER . 5858 1 73 72 THR . 5858 1 74 73 SER . 5858 1 75 74 THR . 5858 1 76 75 THR . 5858 1 77 76 PHE . 5858 1 78 77 PRO . 5858 1 79 78 ALA . 5858 1 80 79 ASP . 5858 1 81 80 ALA . 5858 1 82 81 PRO . 5858 1 83 82 ALA . 5858 1 84 83 GLY . 5858 1 85 84 GLU . 5858 1 86 85 TYR . 5858 1 87 86 THR . 5858 1 88 87 PHE . 5858 1 89 88 TYR . 5858 1 90 89 CYS . 5858 1 91 90 GLU . 5858 1 92 91 PRO . 5858 1 93 92 HIS . 5858 1 94 93 ARG . 5858 1 95 94 GLY . 5858 1 96 95 ALA . 5858 1 97 96 GLY . 5858 1 98 97 MET . 5858 1 99 98 VAL . 5858 1 100 99 GLY . 5858 1 101 100 LYS . 5858 1 102 101 ILE . 5858 1 103 102 THR . 5858 1 104 103 VAL . 5858 1 105 104 ALA . 5858 1 106 105 GLY . 5858 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . MET 1 1 5858 1 . GLU 2 2 5858 1 . THR 3 3 5858 1 . TYR 4 4 5858 1 . THR 5 5 5858 1 . VAL 6 6 5858 1 . LYS 7 7 5858 1 . LEU 8 8 5858 1 . GLY 9 9 5858 1 . SER 10 10 5858 1 . ASP 11 11 5858 1 . LYS 12 12 5858 1 . GLY 13 13 5858 1 . LEU 14 14 5858 1 . LEU 15 15 5858 1 . VAL 16 16 5858 1 . PHE 17 17 5858 1 . GLU 18 18 5858 1 . PRO 19 19 5858 1 . ALA 20 20 5858 1 . LYS 21 21 5858 1 . LEU 22 22 5858 1 . THR 23 23 5858 1 . ILE 24 24 5858 1 . LYS 25 25 5858 1 . PRO 26 26 5858 1 . GLY 27 27 5858 1 . ASP 28 28 5858 1 . THR 29 29 5858 1 . VAL 30 30 5858 1 . GLU 31 31 5858 1 . PHE 32 32 5858 1 . LEU 33 33 5858 1 . ASN 34 34 5858 1 . ASN 35 35 5858 1 . LYS 36 36 5858 1 . VAL 37 37 5858 1 . PRO 38 38 5858 1 . PRO 39 39 5858 1 . HIS 40 40 5858 1 . ASN 41 41 5858 1 . VAL 42 42 5858 1 . VAL 43 43 5858 1 . PHE 44 44 5858 1 . ASP 45 45 5858 1 . ALA 46 46 5858 1 . ALA 47 47 5858 1 . LEU 48 48 5858 1 . ASN 49 49 5858 1 . PRO 50 50 5858 1 . ALA 51 51 5858 1 . LYS 52 52 5858 1 . SER 53 53 5858 1 . ALA 54 54 5858 1 . ASP 55 55 5858 1 . LEU 56 56 5858 1 . ALA 57 57 5858 1 . LYS 58 58 5858 1 . SER 59 59 5858 1 . LEU 60 60 5858 1 . SER 61 61 5858 1 . HIS 62 62 5858 1 . LYS 63 63 5858 1 . GLN 64 64 5858 1 . LEU 65 65 5858 1 . LEU 66 66 5858 1 . MET 67 67 5858 1 . SER 68 68 5858 1 . PRO 69 69 5858 1 . GLY 70 70 5858 1 . GLN 71 71 5858 1 . SER 72 72 5858 1 . THR 73 73 5858 1 . SER 74 74 5858 1 . THR 75 75 5858 1 . THR 76 76 5858 1 . PHE 77 77 5858 1 . PRO 78 78 5858 1 . ALA 79 79 5858 1 . ASP 80 80 5858 1 . ALA 81 81 5858 1 . PRO 82 82 5858 1 . ALA 83 83 5858 1 . GLY 84 84 5858 1 . GLU 85 85 5858 1 . TYR 86 86 5858 1 . THR 87 87 5858 1 . PHE 88 88 5858 1 . TYR 89 89 5858 1 . CYS 90 90 5858 1 . GLU 91 91 5858 1 . PRO 92 92 5858 1 . HIS 93 93 5858 1 . ARG 94 94 5858 1 . GLY 95 95 5858 1 . ALA 96 96 5858 1 . GLY 97 97 5858 1 . MET 98 98 5858 1 . VAL 99 99 5858 1 . GLY 100 100 5858 1 . LYS 101 101 5858 1 . ILE 102 102 5858 1 . THR 103 103 5858 1 . VAL 104 104 5858 1 . ALA 105 105 5858 1 . GLY 106 106 5858 1 stop_ save_ save_CU1 _Entity.Sf_category entity _Entity.Sf_framecode CU1 _Entity.Entry_ID 5858 _Entity.ID 2 _Entity.BMRB_code . _Entity.Name CU1 _Entity.Type non-polymer _Entity.Polymer_common_type . _Entity.Polymer_type . _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code . _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer . _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID CU1 _Entity.Nonpolymer_comp_label $chem_comp_CU1 _Entity.Number_of_monomers . _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic . _Entity.Thiol_state . _Entity.Src_method . _Entity.Parent_entity_ID 2 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . CU1 . 5858 2 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 5858 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Subvariant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Cellular_location _Entity_natural_src.Fragment _Entity_natural_src.Fraction _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Plasmid_details _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Dev_stage _Entity_natural_src.Details _Entity_natural_src.Citation_ID _Entity_natural_src.Citation_label _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $plastocyanin . 1172 organism . 'Anabaena variabilis' 'Anabaena variabilis' . . Eubacteria . Anabaena variabilis . . . . . . . . . . . . . . . . . . . . . 5858 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 5858 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_subvariant _Entity_experimental_src.Host_org_organ _Entity_experimental_src.Host_org_tissue _Entity_experimental_src.Host_org_tissue_fraction _Entity_experimental_src.Host_org_cell_line _Entity_experimental_src.Host_org_cell_type _Entity_experimental_src.Host_org_cellular_location _Entity_experimental_src.Host_org_organelle _Entity_experimental_src.Host_org_gene _Entity_experimental_src.Host_org_culture_collection _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Host_org_dev_stage _Entity_experimental_src.Details _Entity_experimental_src.Citation_ID _Entity_experimental_src.Citation_label _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $plastocyanin . 'recombinant technology' 'Escherichia coli' 'E. coli' . . Escherichia coli . . . . . . . . . . . . . plasmid . . BL21G(DE3) . . . . . . 5858 1 stop_ save_ ################################# # Polymer residues and ligands # ################################# save_chem_comp_CU1 _Chem_comp.Sf_category chem_comp _Chem_comp.Sf_framecode chem_comp_CU1 _Chem_comp.Entry_ID 5858 _Chem_comp.ID CU1 _Chem_comp.Provenance . _Chem_comp.Name 'COPPER (I) ION' _Chem_comp.Type non-polymer _Chem_comp.BMRB_code . _Chem_comp.PDB_code CU1 _Chem_comp.Ambiguous_flag no _Chem_comp.Initial_date 1999-07-08 _Chem_comp.Modified_date 2011-06-04 _Chem_comp.Release_status REL _Chem_comp.Replaced_by . _Chem_comp.Replaces . _Chem_comp.One_letter_code . _Chem_comp.Three_letter_code CU1 _Chem_comp.Number_atoms_all . _Chem_comp.Number_atoms_nh . _Chem_comp.PubChem_code . _Chem_comp.Subcomponent_list . _Chem_comp.InChI_code . _Chem_comp.Mon_nstd_flag . _Chem_comp.Mon_nstd_class . _Chem_comp.Mon_nstd_details . _Chem_comp.Mon_nstd_parent . _Chem_comp.Mon_nstd_parent_comp_ID . _Chem_comp.Std_deriv_one_letter_code . _Chem_comp.Std_deriv_three_letter_code . _Chem_comp.Std_deriv_BMRB_code . _Chem_comp.Std_deriv_PDB_code . _Chem_comp.Std_deriv_chem_comp_name . _Chem_comp.Synonyms . _Chem_comp.Formal_charge 1 _Chem_comp.Paramagnetic . _Chem_comp.Aromatic no _Chem_comp.Formula Cu _Chem_comp.Formula_weight 63.546 _Chem_comp.Formula_mono_iso_wt_nat . _Chem_comp.Formula_mono_iso_wt_13C . _Chem_comp.Formula_mono_iso_wt_15N . _Chem_comp.Formula_mono_iso_wt_13C_15N . _Chem_comp.Image_file_name . _Chem_comp.Image_file_format . _Chem_comp.Topo_file_name . _Chem_comp.Topo_file_format . _Chem_comp.Struct_file_name . _Chem_comp.Struct_file_format . _Chem_comp.Stereochem_param_file_name . _Chem_comp.Stereochem_param_file_format . _Chem_comp.Model_details . _Chem_comp.Model_erf . _Chem_comp.Model_source . _Chem_comp.Model_coordinates_details . _Chem_comp.Model_coordinates_missing_flag no _Chem_comp.Ideal_coordinates_details . _Chem_comp.Ideal_coordinates_missing_flag no _Chem_comp.Model_coordinates_db_code . _Chem_comp.Processing_site RCSB _Chem_comp.Vendor . _Chem_comp.Vendor_product_code . _Chem_comp.Details ; Information obtained from PDB's Chemical Component Dictionary at http://wwpdb-remediation.rutgers.edu/downloads.html Downloaded on Wed Jul 27 13:15:34 2011 ; _Chem_comp.DB_query_date . _Chem_comp.DB_last_query_revised_last_date . loop_ _Chem_comp_descriptor.Descriptor _Chem_comp_descriptor.Type _Chem_comp_descriptor.Program _Chem_comp_descriptor.Program_version _Chem_comp_descriptor.Entry_ID _Chem_comp_descriptor.Comp_ID [Cu+] SMILES ACDLabs 10.04 5858 CU1 [Cu+] SMILES_CANONICAL CACTVS 3.341 5858 CU1 [Cu+] SMILES CACTVS 3.341 5858 CU1 [Cu+] SMILES_CANONICAL 'OpenEye OEToolkits' 1.5.0 5858 CU1 [Cu+] SMILES 'OpenEye OEToolkits' 1.5.0 5858 CU1 InChI=1S/Cu/q+1 InChI InChI 1.03 5858 CU1 VMQMZMRVKUZKQL-UHFFFAOYSA-N InChIKey InChI 1.03 5858 CU1 stop_ loop_ _Chem_comp_identifier.Identifier _Chem_comp_identifier.Type _Chem_comp_identifier.Program _Chem_comp_identifier.Program_version _Chem_comp_identifier.Entry_ID _Chem_comp_identifier.Comp_ID copper(1+) 'SYSTEMATIC NAME' ACDLabs 10.04 5858 CU1 'copper(+1) cation' 'SYSTEMATIC NAME' 'OpenEye OEToolkits' 1.5.0 5858 CU1 stop_ loop_ _Chem_comp_atom.Atom_ID _Chem_comp_atom.BMRB_code _Chem_comp_atom.PDB_atom_ID _Chem_comp_atom.Alt_atom_ID _Chem_comp_atom.Auth_atom_ID _Chem_comp_atom.Type_symbol _Chem_comp_atom.Isotope_number _Chem_comp_atom.Chirality _Chem_comp_atom.Stereo_config _Chem_comp_atom.Charge _Chem_comp_atom.Partial_charge _Chem_comp_atom.Oxidation_number _Chem_comp_atom.Unpaired_electron_number _Chem_comp_atom.Align _Chem_comp_atom.Aromatic_flag _Chem_comp_atom.Leaving_atom_flag _Chem_comp_atom.Substruct_code _Chem_comp_atom.Ionizable _Chem_comp_atom.Drawing_2D_coord_x _Chem_comp_atom.Drawing_2D_coord_y _Chem_comp_atom.Model_Cartn_x _Chem_comp_atom.Model_Cartn_x_esd _Chem_comp_atom.Model_Cartn_y _Chem_comp_atom.Model_Cartn_y_esd _Chem_comp_atom.Model_Cartn_z _Chem_comp_atom.Model_Cartn_z_esd _Chem_comp_atom.Model_Cartn_x_ideal _Chem_comp_atom.Model_Cartn_y_ideal _Chem_comp_atom.Model_Cartn_z_ideal _Chem_comp_atom.PDBX_ordinal _Chem_comp_atom.Details _Chem_comp_atom.Entry_ID _Chem_comp_atom.Comp_ID CU . CU . . CU . . N 1 . . . . no no . . . . 0.000 . 0.000 . 0.000 . 0.000 0.000 0.000 1 . 5858 CU1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 5858 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system . _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'Cu(II) Plastocyanin from Anabeana Variabilis' '[U-95% 15N]' . . 1 $plastocyanin . . 1.0 0.8 1.2 mM . . . . 5858 1 2 'natrium ascorbate' . . . . . . . 0.1 . . mM . . . . 5858 1 stop_ save_ ####################### # Sample conditions # ####################### save_Condition_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_1 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 8.50 0.05 na 5858 1 temperature 298 0.1 K 5858 1 stop_ save_ save_Condition_2 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_2 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 2 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 7.80 0.05 na 5858 2 temperature 298 0.1 K 5858 2 stop_ save_ save_Condition_3 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_3 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 3 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 7.46 0.05 na 5858 3 temperature 298 0.1 K 5858 3 stop_ save_ save_Condition_4 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_4 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 4 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.96 0.05 na 5858 4 temperature 298 0.1 K 5858 4 stop_ save_ save_Condition_5 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_5 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 5 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.59 0.05 na 5858 5 temperature 298 0.1 K 5858 5 stop_ save_ save_Condition_6 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_6 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 6 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.05 0.05 na 5858 6 temperature 298 0.1 K 5858 6 stop_ save_ save_Condition_7 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_7 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 7 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 5.78 0.05 na 5858 7 temperature 298 0.1 K 5858 7 stop_ save_ save_Condition_8 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_8 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 8 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 5.35 0.05 na 5858 8 temperature 298 0.1 K 5858 8 stop_ save_ save_Condition_9 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_9 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 9 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 4.98 0.05 na 5858 9 temperature 298 0.1 K 5858 9 stop_ save_ save_Condition_10 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_10 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 10 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 4.60 0.05 na 5858 10 temperature 298 0.1 K 5858 10 stop_ save_ save_Condition_11 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_11 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 11 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 4.20 0.05 na 5858 11 temperature 298 0.1 K 5858 11 stop_ save_ save_Condition_12 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_12 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 12 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 5.78 0.05 na 5858 12 temperature 293 0.1 K 5858 12 stop_ save_ save_Condition_13 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_13 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 13 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 5.78 0.05 na 5858 13 temperature 303 0.1 K 5858 13 stop_ save_ save_Condition_14 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode Condition_14 _Sample_condition_list.Entry_ID 5858 _Sample_condition_list.ID 14 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 5.78 0.05 na 5858 14 temperature 308 0.1 K 5858 14 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer _NMR_spectrometer.Entry_ID 5858 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Varian _NMR_spectrometer.Model Inova _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 800 save_ save_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode spectrometer_list _NMR_spectrometer_list.Entry_ID 5858 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 NMR_spectrometer Varian Inova . 800 . . . 5858 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 5858 _Experiment_list.ID 1 _Experiment_list.Details ; 15N-HSQC using standard gradient enhanced pulse sequence." A CPMG pulse with a interpulse delay of 1 ms was applied in the R2 experiment. ; loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 15N-HSQC . . . . . . . . . . . 1 $sample_1 . . . . . . . . 1 $NMR_spectrometer . . . . . . . . . . . . . . . . 5858 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chemical_shift_reference _Chem_shift_reference.Entry_ID 5858 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Indirect_shift_ratio_cit_ID _Chem_shift_ref.Indirect_shift_ratio_cit_label _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Correction_val_cit_ID _Chem_shift_ref.Correction_val_cit_label _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 . . . . . . ppm . . . . . . . . . . . . . 5858 1 N 15 . . . . . . ppm . . . . . . . . . . . . . 5858 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_shift_set_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_1 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 15N-HSQC 1 $sample_1 . 5858 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 4 4 TYR N N 15 126.9 . . . . . . . . . . . 5858 1 2 . 1 1 4 4 TYR H H 1 8.83 . . . . . . . . . . . 5858 1 3 . 1 1 5 5 THR N N 15 118.6 . . . . . . . . . . . 5858 1 4 . 1 1 5 5 THR H H 1 8.58 . . . . . . . . . . . 5858 1 5 . 1 1 6 6 VAL N N 15 129.9 . . . . . . . . . . . 5858 1 6 . 1 1 6 6 VAL H H 1 9.36 . . . . . . . . . . . 5858 1 7 . 1 1 7 7 LYS N N 15 126.5 . . . . . . . . . . . 5858 1 8 . 1 1 7 7 LYS H H 1 9.06 . . . . . . . . . . . 5858 1 9 . 1 1 8 8 LEU N N 15 122.0 . . . . . . . . . . . 5858 1 10 . 1 1 8 8 LEU H H 1 8.87 . . . . . . . . . . . 5858 1 11 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 1 12 . 1 1 9 9 GLY H H 1 7.67 . . . . . . . . . . . 5858 1 13 . 1 1 10 10 SER N N 15 119.6 . . . . . . . . . . . 5858 1 14 . 1 1 10 10 SER H H 1 8.67 . . . . . . . . . . . 5858 1 15 . 1 1 13 13 GLY N N 15 108.9 . . . . . . . . . . . 5858 1 16 . 1 1 13 13 GLY H H 1 8.33 . . . . . . . . . . . 5858 1 17 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 1 18 . 1 1 14 14 LEU H H 1 7.46 . . . . . . . . . . . 5858 1 19 . 1 1 15 15 LEU N N 15 124.9 . . . . . . . . . . . 5858 1 20 . 1 1 15 15 LEU H H 1 8.38 . . . . . . . . . . . 5858 1 21 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 1 22 . 1 1 16 16 VAL H H 1 7.48 . . . . . . . . . . . 5858 1 23 . 1 1 17 17 PHE N N 15 120.0 . . . . . . . . . . . 5858 1 24 . 1 1 17 17 PHE H H 1 8.64 . . . . . . . . . . . 5858 1 25 . 1 1 18 18 GLU N N 15 122.1 . . . . . . . . . . . 5858 1 26 . 1 1 18 18 GLU H H 1 9.02 . . . . . . . . . . . 5858 1 27 . 1 1 20 20 ALA N N 15 117.1 . . . . . . . . . . . 5858 1 28 . 1 1 20 20 ALA H H 1 8.15 . . . . . . . . . . . 5858 1 29 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 1 30 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 1 31 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 1 32 . 1 1 22 22 LEU H H 1 7.78 . . . . . . . . . . . 5858 1 33 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 1 34 . 1 1 23 23 THR H H 1 8.22 . . . . . . . . . . . 5858 1 35 . 1 1 24 24 ILE N N 15 120.9 . . . . . . . . . . . 5858 1 36 . 1 1 24 24 ILE H H 1 8.92 . . . . . . . . . . . 5858 1 37 . 1 1 25 25 LYS N N 15 119.8 . . . . . . . . . . . 5858 1 38 . 1 1 25 25 LYS H H 1 9.03 . . . . . . . . . . . 5858 1 39 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 1 40 . 1 1 27 27 GLY H H 1 7.11 . . . . . . . . . . . 5858 1 41 . 1 1 28 28 ASP N N 15 119.9 . . . . . . . . . . . 5858 1 42 . 1 1 28 28 ASP H H 1 7.89 . . . . . . . . . . . 5858 1 43 . 1 1 29 29 THR N N 15 114.9 . . . . . . . . . . . 5858 1 44 . 1 1 29 29 THR H H 1 8.73 . . . . . . . . . . . 5858 1 45 . 1 1 30 30 VAL N N 15 126.5 . . . . . . . . . . . 5858 1 46 . 1 1 30 30 VAL H H 1 9.18 . . . . . . . . . . . 5858 1 47 . 1 1 31 31 GLU N N 15 128.7 . . . . . . . . . . . 5858 1 48 . 1 1 31 31 GLU H H 1 9.18 . . . . . . . . . . . 5858 1 49 . 1 1 32 32 PHE N N 15 126.1 . . . . . . . . . . . 5858 1 50 . 1 1 32 32 PHE H H 1 9.13 . . . . . . . . . . . 5858 1 51 . 1 1 33 33 LEU N N 15 125.2 . . . . . . . . . . . 5858 1 52 . 1 1 33 33 LEU H H 1 8.96 . . . . . . . . . . . 5858 1 53 . 1 1 34 34 ASN N N 15 127.5 . . . . . . . . . . . 5858 1 54 . 1 1 34 34 ASN H H 1 9.33 . . . . . . . . . . . 5858 1 55 . 1 1 35 35 ASN N N 15 129.8 . . . . . . . . . . . 5858 1 56 . 1 1 35 35 ASN H H 1 8.80 . . . . . . . . . . . 5858 1 57 . 1 1 36 36 LYS N N 15 116.7 . . . . . . . . . . . 5858 1 58 . 1 1 36 36 LYS H H 1 8.11 . . . . . . . . . . . 5858 1 59 . 1 1 37 37 VAL N N 15 115.3 . . . . . . . . . . . 5858 1 60 . 1 1 37 37 VAL H H 1 8.92 . . . . . . . . . . . 5858 1 61 . 1 1 40 40 HIS N N 15 112.7 . . . . . . . . . . . 5858 1 62 . 1 1 40 40 HIS H H 1 7.18 . . . . . . . . . . . 5858 1 63 . 1 1 41 41 ASN N N 15 123.1 . . . . . . . . . . . 5858 1 64 . 1 1 41 41 ASN H H 1 9.87 . . . . . . . . . . . 5858 1 65 . 1 1 42 42 VAL N N 15 109.4 . . . . . . . . . . . 5858 1 66 . 1 1 42 42 VAL H H 1 7.10 . . . . . . . . . . . 5858 1 67 . 1 1 43 43 VAL N N 15 128.1 . . . . . . . . . . . 5858 1 68 . 1 1 43 43 VAL H H 1 9.41 . . . . . . . . . . . 5858 1 69 . 1 1 44 44 PHE N N 15 125.6 . . . . . . . . . . . 5858 1 70 . 1 1 44 44 PHE H H 1 8.69 . . . . . . . . . . . 5858 1 71 . 1 1 45 45 ASP N N 15 124.1 . . . . . . . . . . . 5858 1 72 . 1 1 45 45 ASP H H 1 8.41 . . . . . . . . . . . 5858 1 73 . 1 1 46 46 ALA N N 15 128.2 . . . . . . . . . . . 5858 1 74 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 1 75 . 1 1 47 47 ALA N N 15 117.5 . . . . . . . . . . . 5858 1 76 . 1 1 47 47 ALA H H 1 8.45 . . . . . . . . . . . 5858 1 77 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 1 78 . 1 1 48 48 LEU H H 1 8.66 . . . . . . . . . . . 5858 1 79 . 1 1 49 49 ASN N N 15 114.5 . . . . . . . . . . . 5858 1 80 . 1 1 49 49 ASN H H 1 8.04 . . . . . . . . . . . 5858 1 81 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 1 82 . 1 1 51 51 ALA H H 1 7.01 . . . . . . . . . . . 5858 1 83 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 1 84 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 1 85 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 1 86 . 1 1 53 53 SER H H 1 8.21 . . . . . . . . . . . 5858 1 87 . 1 1 56 56 LEU N N 15 123.7 . . . . . . . . . . . 5858 1 88 . 1 1 56 56 LEU H H 1 8.13 . . . . . . . . . . . 5858 1 89 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 1 90 . 1 1 57 57 ALA H H 1 7.55 . . . . . . . . . . . 5858 1 91 . 1 1 58 58 LYS N N 15 120.6 . . . . . . . . . . . 5858 1 92 . 1 1 58 58 LYS H H 1 8.51 . . . . . . . . . . . 5858 1 93 . 1 1 59 59 SER N N 15 115.3 . . . . . . . . . . . 5858 1 94 . 1 1 59 59 SER H H 1 7.73 . . . . . . . . . . . 5858 1 95 . 1 1 60 60 LEU N N 15 120.9 . . . . . . . . . . . 5858 1 96 . 1 1 60 60 LEU H H 1 6.88 . . . . . . . . . . . 5858 1 97 . 1 1 61 61 SER N N 15 110.7 . . . . . . . . . . . 5858 1 98 . 1 1 61 61 SER H H 1 6.86 . . . . . . . . . . . 5858 1 99 . 1 1 62 62 HIS N N 15 122.8 . . . . . . . . . . . 5858 1 100 . 1 1 62 62 HIS H H 1 9.59 . . . . . . . . . . . 5858 1 101 . 1 1 63 63 LYS N N 15 122.5 . . . . . . . . . . . 5858 1 102 . 1 1 63 63 LYS H H 1 8.57 . . . . . . . . . . . 5858 1 103 . 1 1 64 64 GLN N N 15 120.1 . . . . . . . . . . . 5858 1 104 . 1 1 64 64 GLN H H 1 8.34 . . . . . . . . . . . 5858 1 105 . 1 1 65 65 LEU N N 15 121.1 . . . . . . . . . . . 5858 1 106 . 1 1 65 65 LEU H H 1 8.14 . . . . . . . . . . . 5858 1 107 . 1 1 66 66 LEU N N 15 125.1 . . . . . . . . . . . 5858 1 108 . 1 1 66 66 LEU H H 1 9.52 . . . . . . . . . . . 5858 1 109 . 1 1 67 67 MET N N 15 121.8 . . . . . . . . . . . 5858 1 110 . 1 1 67 67 MET H H 1 8.06 . . . . . . . . . . . 5858 1 111 . 1 1 68 68 SER N N 15 113.7 . . . . . . . . . . . 5858 1 112 . 1 1 68 68 SER H H 1 8.39 . . . . . . . . . . . 5858 1 113 . 1 1 70 70 GLY N N 15 112.9 . . . . . . . . . . . 5858 1 114 . 1 1 70 70 GLY H H 1 9.05 . . . . . . . . . . . 5858 1 115 . 1 1 71 71 GLN N N 15 120.0 . . . . . . . . . . . 5858 1 116 . 1 1 71 71 GLN H H 1 7.54 . . . . . . . . . . . 5858 1 117 . 1 1 72 72 SER N N 15 116.2 . . . . . . . . . . . 5858 1 118 . 1 1 72 72 SER H H 1 8.63 . . . . . . . . . . . 5858 1 119 . 1 1 73 73 THR N N 15 115.8 . . . . . . . . . . . 5858 1 120 . 1 1 73 73 THR H H 1 8.73 . . . . . . . . . . . 5858 1 121 . 1 1 75 75 THR N N 15 121.5 . . . . . . . . . . . 5858 1 122 . 1 1 75 75 THR H H 1 9.54 . . . . . . . . . . . 5858 1 123 . 1 1 76 76 THR N N 15 126.9 . . . . . . . . . . . 5858 1 124 . 1 1 76 76 THR H H 1 9.10 . . . . . . . . . . . 5858 1 125 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 1 126 . 1 1 77 77 PHE H H 1 9.20 . . . . . . . . . . . 5858 1 127 . 1 1 79 79 ALA N N 15 123.1 . . . . . . . . . . . 5858 1 128 . 1 1 79 79 ALA H H 1 8.81 . . . . . . . . . . . 5858 1 129 . 1 1 80 80 ASP N N 15 113.1 . . . . . . . . . . . 5858 1 130 . 1 1 80 80 ASP H H 1 8.00 . . . . . . . . . . . 5858 1 131 . 1 1 81 81 ALA N N 15 124.7 . . . . . . . . . . . 5858 1 132 . 1 1 81 81 ALA H H 1 7.59 . . . . . . . . . . . 5858 1 133 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 1 134 . 1 1 83 83 ALA H H 1 8.38 . . . . . . . . . . . 5858 1 135 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 1 136 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 1 137 . 1 1 85 85 GLU N N 15 119.7 . . . . . . . . . . . 5858 1 138 . 1 1 85 85 GLU H H 1 8.48 . . . . . . . . . . . 5858 1 139 . 1 1 86 86 TYR N N 15 125.6 . . . . . . . . . . . 5858 1 140 . 1 1 86 86 TYR H H 1 10.17 . . . . . . . . . . . 5858 1 141 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 1 142 . 1 1 87 87 THR H H 1 8.61 . . . . . . . . . . . 5858 1 143 . 1 1 88 88 PHE N N 15 126.3 . . . . . . . . . . . 5858 1 144 . 1 1 88 88 PHE H H 1 8.58 . . . . . . . . . . . 5858 1 145 . 1 1 89 89 TYR N N 15 115.4 . . . . . . . . . . . 5858 1 146 . 1 1 89 89 TYR H H 1 8.92 . . . . . . . . . . . 5858 1 147 . 1 1 90 90 CYS N N 15 125.2 . . . . . . . . . . . 5858 1 148 . 1 1 90 90 CYS H H 1 7.75 . . . . . . . . . . . 5858 1 149 . 1 1 91 91 GLU N N 15 125.6 . . . . . . . . . . . 5858 1 150 . 1 1 91 91 GLU H H 1 10.05 . . . . . . . . . . . 5858 1 151 . 1 1 93 93 HIS N N 15 115.9 . . . . . . . . . . . 5858 1 152 . 1 1 93 93 HIS H H 1 8.67 . . . . . . . . . . . 5858 1 153 . 1 1 94 94 ARG N N 15 129.4 . . . . . . . . . . . 5858 1 154 . 1 1 94 94 ARG H H 1 8.50 . . . . . . . . . . . 5858 1 155 . 1 1 96 96 ALA N N 15 121.7 . . . . . . . . . . . 5858 1 156 . 1 1 96 96 ALA H H 1 7.58 . . . . . . . . . . . 5858 1 157 . 1 1 97 97 GLY N N 15 106.4 . . . . . . . . . . . 5858 1 158 . 1 1 97 97 GLY H H 1 8.07 . . . . . . . . . . . 5858 1 159 . 1 1 98 98 MET N N 15 124.3 . . . . . . . . . . . 5858 1 160 . 1 1 98 98 MET H H 1 7.65 . . . . . . . . . . . 5858 1 161 . 1 1 99 99 VAL N N 15 125.8 . . . . . . . . . . . 5858 1 162 . 1 1 99 99 VAL H H 1 7.93 . . . . . . . . . . . 5858 1 163 . 1 1 100 100 GLY N N 15 118.2 . . . . . . . . . . . 5858 1 164 . 1 1 100 100 GLY H H 1 9.00 . . . . . . . . . . . 5858 1 165 . 1 1 101 101 LYS N N 15 117.6 . . . . . . . . . . . 5858 1 166 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 1 167 . 1 1 102 102 ILE N N 15 127.6 . . . . . . . . . . . 5858 1 168 . 1 1 102 102 ILE H H 1 9.47 . . . . . . . . . . . 5858 1 169 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 1 170 . 1 1 103 103 THR H H 1 9.26 . . . . . . . . . . . 5858 1 171 . 1 1 104 104 VAL N N 15 128.6 . . . . . . . . . . . 5858 1 172 . 1 1 104 104 VAL H H 1 9.32 . . . . . . . . . . . 5858 1 173 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 1 174 . 1 1 105 105 ALA H H 1 9.26 . . . . . . . . . . . 5858 1 175 . 1 1 106 106 GLY N N 15 113.9 . . . . . . . . . . . 5858 1 176 . 1 1 106 106 GLY H H 1 7.78 . . . . . . . . . . . 5858 1 stop_ save_ save_shift_set_2 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_2 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 2 _Assigned_chem_shift_list.Sample_condition_list_ID 2 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_2 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 2 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 4 4 TYR N N 15 127.0 . . . . . . . . . . . 5858 2 2 . 1 1 4 4 TYR H H 1 8.84 . . . . . . . . . . . 5858 2 3 . 1 1 5 5 THR N N 15 118.6 . . . . . . . . . . . 5858 2 4 . 1 1 5 5 THR H H 1 8.59 . . . . . . . . . . . 5858 2 5 . 1 1 6 6 VAL N N 15 129.9 . . . . . . . . . . . 5858 2 6 . 1 1 6 6 VAL H H 1 9.36 . . . . . . . . . . . 5858 2 7 . 1 1 7 7 LYS N N 15 126.5 . . . . . . . . . . . 5858 2 8 . 1 1 7 7 LYS H H 1 9.06 . . . . . . . . . . . 5858 2 9 . 1 1 8 8 LEU N N 15 122.0 . . . . . . . . . . . 5858 2 10 . 1 1 8 8 LEU H H 1 8.87 . . . . . . . . . . . 5858 2 11 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 2 12 . 1 1 9 9 GLY H H 1 7.67 . . . . . . . . . . . 5858 2 13 . 1 1 10 10 SER N N 15 119.6 . . . . . . . . . . . 5858 2 14 . 1 1 10 10 SER H H 1 8.67 . . . . . . . . . . . 5858 2 15 . 1 1 11 11 ASP N N 15 121.0 . . . . . . . . . . . 5858 2 16 . 1 1 11 11 ASP H H 1 9.48 . . . . . . . . . . . 5858 2 17 . 1 1 13 13 GLY N N 15 108.9 . . . . . . . . . . . 5858 2 18 . 1 1 13 13 GLY H H 1 8.33 . . . . . . . . . . . 5858 2 19 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 2 20 . 1 1 14 14 LEU H H 1 7.46 . . . . . . . . . . . 5858 2 21 . 1 1 15 15 LEU N N 15 124.9 . . . . . . . . . . . 5858 2 22 . 1 1 15 15 LEU H H 1 8.38 . . . . . . . . . . . 5858 2 23 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 2 24 . 1 1 16 16 VAL H H 1 7.48 . . . . . . . . . . . 5858 2 25 . 1 1 17 17 PHE N N 15 120.0 . . . . . . . . . . . 5858 2 26 . 1 1 17 17 PHE H H 1 8.64 . . . . . . . . . . . 5858 2 27 . 1 1 18 18 GLU N N 15 122.1 . . . . . . . . . . . 5858 2 28 . 1 1 18 18 GLU H H 1 9.02 . . . . . . . . . . . 5858 2 29 . 1 1 20 20 ALA N N 15 117.1 . . . . . . . . . . . 5858 2 30 . 1 1 20 20 ALA H H 1 8.14 . . . . . . . . . . . 5858 2 31 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 2 32 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 2 33 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 2 34 . 1 1 22 22 LEU H H 1 7.78 . . . . . . . . . . . 5858 2 35 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 2 36 . 1 1 23 23 THR H H 1 8.22 . . . . . . . . . . . 5858 2 37 . 1 1 24 24 ILE N N 15 120.9 . . . . . . . . . . . 5858 2 38 . 1 1 24 24 ILE H H 1 8.92 . . . . . . . . . . . 5858 2 39 . 1 1 25 25 LYS N N 15 119.7 . . . . . . . . . . . 5858 2 40 . 1 1 25 25 LYS H H 1 9.01 . . . . . . . . . . . 5858 2 41 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 2 42 . 1 1 27 27 GLY H H 1 7.11 . . . . . . . . . . . 5858 2 43 . 1 1 28 28 ASP N N 15 119.9 . . . . . . . . . . . 5858 2 44 . 1 1 28 28 ASP H H 1 7.90 . . . . . . . . . . . 5858 2 45 . 1 1 29 29 THR N N 15 114.8 . . . . . . . . . . . 5858 2 46 . 1 1 29 29 THR H H 1 8.70 . . . . . . . . . . . 5858 2 47 . 1 1 30 30 VAL N N 15 126.5 . . . . . . . . . . . 5858 2 48 . 1 1 30 30 VAL H H 1 9.18 . . . . . . . . . . . 5858 2 49 . 1 1 31 31 GLU N N 15 128.7 . . . . . . . . . . . 5858 2 50 . 1 1 31 31 GLU H H 1 9.19 . . . . . . . . . . . 5858 2 51 . 1 1 32 32 PHE N N 15 126.1 . . . . . . . . . . . 5858 2 52 . 1 1 32 32 PHE H H 1 9.13 . . . . . . . . . . . 5858 2 53 . 1 1 33 33 LEU N N 15 125.2 . . . . . . . . . . . 5858 2 54 . 1 1 33 33 LEU H H 1 8.96 . . . . . . . . . . . 5858 2 55 . 1 1 34 34 ASN N N 15 127.5 . . . . . . . . . . . 5858 2 56 . 1 1 34 34 ASN H H 1 9.33 . . . . . . . . . . . 5858 2 57 . 1 1 35 35 ASN N N 15 129.7 . . . . . . . . . . . 5858 2 58 . 1 1 35 35 ASN H H 1 8.81 . . . . . . . . . . . 5858 2 59 . 1 1 36 36 LYS N N 15 116.7 . . . . . . . . . . . 5858 2 60 . 1 1 36 36 LYS H H 1 8.12 . . . . . . . . . . . 5858 2 61 . 1 1 37 37 VAL N N 15 115.3 . . . . . . . . . . . 5858 2 62 . 1 1 37 37 VAL H H 1 8.92 . . . . . . . . . . . 5858 2 63 . 1 1 40 40 HIS N N 15 112.7 . . . . . . . . . . . 5858 2 64 . 1 1 40 40 HIS H H 1 7.18 . . . . . . . . . . . 5858 2 65 . 1 1 41 41 ASN N N 15 123.1 . . . . . . . . . . . 5858 2 66 . 1 1 41 41 ASN H H 1 9.88 . . . . . . . . . . . 5858 2 67 . 1 1 42 42 VAL N N 15 109.3 . . . . . . . . . . . 5858 2 68 . 1 1 42 42 VAL H H 1 7.08 . . . . . . . . . . . 5858 2 69 . 1 1 43 43 VAL N N 15 128.1 . . . . . . . . . . . 5858 2 70 . 1 1 43 43 VAL H H 1 9.42 . . . . . . . . . . . 5858 2 71 . 1 1 44 44 PHE N N 15 125.5 . . . . . . . . . . . 5858 2 72 . 1 1 44 44 PHE H H 1 8.69 . . . . . . . . . . . 5858 2 73 . 1 1 45 45 ASP N N 15 124.1 . . . . . . . . . . . 5858 2 74 . 1 1 45 45 ASP H H 1 8.40 . . . . . . . . . . . 5858 2 75 . 1 1 46 46 ALA N N 15 128.2 . . . . . . . . . . . 5858 2 76 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 2 77 . 1 1 47 47 ALA N N 15 117.5 . . . . . . . . . . . 5858 2 78 . 1 1 47 47 ALA H H 1 8.46 . . . . . . . . . . . 5858 2 79 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 2 80 . 1 1 48 48 LEU H H 1 8.66 . . . . . . . . . . . 5858 2 81 . 1 1 49 49 ASN N N 15 114.5 . . . . . . . . . . . 5858 2 82 . 1 1 49 49 ASN H H 1 8.05 . . . . . . . . . . . 5858 2 83 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 2 84 . 1 1 51 51 ALA H H 1 7.01 . . . . . . . . . . . 5858 2 85 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 2 86 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 2 87 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 2 88 . 1 1 53 53 SER H H 1 8.21 . . . . . . . . . . . 5858 2 89 . 1 1 56 56 LEU N N 15 123.7 . . . . . . . . . . . 5858 2 90 . 1 1 56 56 LEU H H 1 8.14 . . . . . . . . . . . 5858 2 91 . 1 1 57 57 ALA N N 15 119.6 . . . . . . . . . . . 5858 2 92 . 1 1 57 57 ALA H H 1 7.56 . . . . . . . . . . . 5858 2 93 . 1 1 58 58 LYS N N 15 120.7 . . . . . . . . . . . 5858 2 94 . 1 1 58 58 LYS H H 1 8.52 . . . . . . . . . . . 5858 2 95 . 1 1 59 59 SER N N 15 115.3 . . . . . . . . . . . 5858 2 96 . 1 1 59 59 SER H H 1 7.74 . . . . . . . . . . . 5858 2 97 . 1 1 60 60 LEU N N 15 120.8 . . . . . . . . . . . 5858 2 98 . 1 1 60 60 LEU H H 1 6.89 . . . . . . . . . . . 5858 2 99 . 1 1 61 61 SER N N 15 110.8 . . . . . . . . . . . 5858 2 100 . 1 1 61 61 SER H H 1 6.88 . . . . . . . . . . . 5858 2 101 . 1 1 62 62 HIS N N 15 122.4 . . . . . . . . . . . 5858 2 102 . 1 1 62 62 HIS H H 1 9.60 . . . . . . . . . . . 5858 2 103 . 1 1 63 63 LYS N N 15 122.6 . . . . . . . . . . . 5858 2 104 . 1 1 63 63 LYS H H 1 8.60 . . . . . . . . . . . 5858 2 105 . 1 1 64 64 GLN N N 15 120.1 . . . . . . . . . . . 5858 2 106 . 1 1 64 64 GLN H H 1 8.35 . . . . . . . . . . . 5858 2 107 . 1 1 65 65 LEU N N 15 121.2 . . . . . . . . . . . 5858 2 108 . 1 1 65 65 LEU H H 1 8.16 . . . . . . . . . . . 5858 2 109 . 1 1 66 66 LEU N N 15 125.1 . . . . . . . . . . . 5858 2 110 . 1 1 66 66 LEU H H 1 9.53 . . . . . . . . . . . 5858 2 111 . 1 1 67 67 MET N N 15 121.9 . . . . . . . . . . . 5858 2 112 . 1 1 67 67 MET H H 1 8.07 . . . . . . . . . . . 5858 2 113 . 1 1 68 68 SER N N 15 113.7 . . . . . . . . . . . 5858 2 114 . 1 1 68 68 SER H H 1 8.38 . . . . . . . . . . . 5858 2 115 . 1 1 70 70 GLY N N 15 112.9 . . . . . . . . . . . 5858 2 116 . 1 1 70 70 GLY H H 1 9.04 . . . . . . . . . . . 5858 2 117 . 1 1 71 71 GLN N N 15 120.0 . . . . . . . . . . . 5858 2 118 . 1 1 71 71 GLN H H 1 7.54 . . . . . . . . . . . 5858 2 119 . 1 1 72 72 SER N N 15 116.1 . . . . . . . . . . . 5858 2 120 . 1 1 72 72 SER H H 1 8.64 . . . . . . . . . . . 5858 2 121 . 1 1 73 73 THR N N 15 115.9 . . . . . . . . . . . 5858 2 122 . 1 1 73 73 THR H H 1 8.73 . . . . . . . . . . . 5858 2 123 . 1 1 74 74 SER N N 15 117.6 . . . . . . . . . . . 5858 2 124 . 1 1 74 74 SER H H 1 8.20 . . . . . . . . . . . 5858 2 125 . 1 1 75 75 THR N N 15 121.4 . . . . . . . . . . . 5858 2 126 . 1 1 75 75 THR H H 1 9.55 . . . . . . . . . . . 5858 2 127 . 1 1 76 76 THR N N 15 126.9 . . . . . . . . . . . 5858 2 128 . 1 1 76 76 THR H H 1 9.10 . . . . . . . . . . . 5858 2 129 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 2 130 . 1 1 77 77 PHE H H 1 9.19 . . . . . . . . . . . 5858 2 131 . 1 1 79 79 ALA N N 15 123.2 . . . . . . . . . . . 5858 2 132 . 1 1 79 79 ALA H H 1 8.82 . . . . . . . . . . . 5858 2 133 . 1 1 80 80 ASP N N 15 113.1 . . . . . . . . . . . 5858 2 134 . 1 1 80 80 ASP H H 1 8.00 . . . . . . . . . . . 5858 2 135 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 2 136 . 1 1 81 81 ALA H H 1 7.58 . . . . . . . . . . . 5858 2 137 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 2 138 . 1 1 83 83 ALA H H 1 8.38 . . . . . . . . . . . 5858 2 139 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 2 140 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 2 141 . 1 1 85 85 GLU N N 15 119.7 . . . . . . . . . . . 5858 2 142 . 1 1 85 85 GLU H H 1 8.48 . . . . . . . . . . . 5858 2 143 . 1 1 86 86 TYR N N 15 125.6 . . . . . . . . . . . 5858 2 144 . 1 1 86 86 TYR H H 1 10.17 . . . . . . . . . . . 5858 2 145 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 2 146 . 1 1 87 87 THR H H 1 8.62 . . . . . . . . . . . 5858 2 147 . 1 1 88 88 PHE N N 15 126.3 . . . . . . . . . . . 5858 2 148 . 1 1 88 88 PHE H H 1 8.58 . . . . . . . . . . . 5858 2 149 . 1 1 89 89 TYR N N 15 115.4 . . . . . . . . . . . 5858 2 150 . 1 1 89 89 TYR H H 1 8.92 . . . . . . . . . . . 5858 2 151 . 1 1 90 90 CYS N N 15 125.2 . . . . . . . . . . . 5858 2 152 . 1 1 90 90 CYS H H 1 7.75 . . . . . . . . . . . 5858 2 153 . 1 1 91 91 GLU N N 15 125.6 . . . . . . . . . . . 5858 2 154 . 1 1 91 91 GLU H H 1 10.04 . . . . . . . . . . . 5858 2 155 . 1 1 93 93 HIS N N 15 115.8 . . . . . . . . . . . 5858 2 156 . 1 1 93 93 HIS H H 1 8.67 . . . . . . . . . . . 5858 2 157 . 1 1 94 94 ARG N N 15 129.4 . . . . . . . . . . . 5858 2 158 . 1 1 94 94 ARG H H 1 8.50 . . . . . . . . . . . 5858 2 159 . 1 1 96 96 ALA N N 15 121.7 . . . . . . . . . . . 5858 2 160 . 1 1 96 96 ALA H H 1 7.58 . . . . . . . . . . . 5858 2 161 . 1 1 97 97 GLY N N 15 106.4 . . . . . . . . . . . 5858 2 162 . 1 1 97 97 GLY H H 1 8.07 . . . . . . . . . . . 5858 2 163 . 1 1 98 98 MET N N 15 124.4 . . . . . . . . . . . 5858 2 164 . 1 1 98 98 MET H H 1 7.65 . . . . . . . . . . . 5858 2 165 . 1 1 99 99 VAL N N 15 125.8 . . . . . . . . . . . 5858 2 166 . 1 1 99 99 VAL H H 1 7.94 . . . . . . . . . . . 5858 2 167 . 1 1 100 100 GLY N N 15 118.2 . . . . . . . . . . . 5858 2 168 . 1 1 100 100 GLY H H 1 9.00 . . . . . . . . . . . 5858 2 169 . 1 1 101 101 LYS N N 15 117.6 . . . . . . . . . . . 5858 2 170 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 2 171 . 1 1 102 102 ILE N N 15 127.5 . . . . . . . . . . . 5858 2 172 . 1 1 102 102 ILE H H 1 9.48 . . . . . . . . . . . 5858 2 173 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 2 174 . 1 1 103 103 THR H H 1 9.27 . . . . . . . . . . . 5858 2 175 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 2 176 . 1 1 104 104 VAL H H 1 9.32 . . . . . . . . . . . 5858 2 177 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 2 178 . 1 1 105 105 ALA H H 1 9.26 . . . . . . . . . . . 5858 2 179 . 1 1 106 106 GLY N N 15 113.8 . . . . . . . . . . . 5858 2 180 . 1 1 106 106 GLY H H 1 7.79 . . . . . . . . . . . 5858 2 stop_ save_ save_shift_set_3 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_3 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 3 _Assigned_chem_shift_list.Sample_condition_list_ID 3 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_3 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 3 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.7 . . . . . . . . . . . 5858 3 2 . 1 1 3 3 THR H H 1 8.75 . . . . . . . . . . . 5858 3 3 . 1 1 4 4 TYR N N 15 127.0 . . . . . . . . . . . 5858 3 4 . 1 1 4 4 TYR H H 1 8.84 . . . . . . . . . . . 5858 3 5 . 1 1 5 5 THR N N 15 118.6 . . . . . . . . . . . 5858 3 6 . 1 1 5 5 THR H H 1 8.60 . . . . . . . . . . . 5858 3 7 . 1 1 6 6 VAL N N 15 129.9 . . . . . . . . . . . 5858 3 8 . 1 1 6 6 VAL H H 1 9.35 . . . . . . . . . . . 5858 3 9 . 1 1 7 7 LYS N N 15 126.6 . . . . . . . . . . . 5858 3 10 . 1 1 7 7 LYS H H 1 9.07 . . . . . . . . . . . 5858 3 11 . 1 1 8 8 LEU N N 15 122.0 . . . . . . . . . . . 5858 3 12 . 1 1 8 8 LEU H H 1 8.87 . . . . . . . . . . . 5858 3 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 3 14 . 1 1 9 9 GLY H H 1 7.68 . . . . . . . . . . . 5858 3 15 . 1 1 10 10 SER N N 15 119.6 . . . . . . . . . . . 5858 3 16 . 1 1 10 10 SER H H 1 8.67 . . . . . . . . . . . 5858 3 17 . 1 1 11 11 ASP N N 15 121.0 . . . . . . . . . . . 5858 3 18 . 1 1 11 11 ASP H H 1 9.48 . . . . . . . . . . . 5858 3 19 . 1 1 13 13 GLY N N 15 108.9 . . . . . . . . . . . 5858 3 20 . 1 1 13 13 GLY H H 1 8.33 . . . . . . . . . . . 5858 3 21 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 3 22 . 1 1 14 14 LEU H H 1 7.46 . . . . . . . . . . . 5858 3 23 . 1 1 15 15 LEU N N 15 124.9 . . . . . . . . . . . 5858 3 24 . 1 1 15 15 LEU H H 1 8.39 . . . . . . . . . . . 5858 3 25 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 3 26 . 1 1 16 16 VAL H H 1 7.48 . . . . . . . . . . . 5858 3 27 . 1 1 17 17 PHE N N 15 120.0 . . . . . . . . . . . 5858 3 28 . 1 1 17 17 PHE H H 1 8.64 . . . . . . . . . . . 5858 3 29 . 1 1 18 18 GLU N N 15 122.1 . . . . . . . . . . . 5858 3 30 . 1 1 18 18 GLU H H 1 9.02 . . . . . . . . . . . 5858 3 31 . 1 1 20 20 ALA N N 15 117.1 . . . . . . . . . . . 5858 3 32 . 1 1 20 20 ALA H H 1 8.14 . . . . . . . . . . . 5858 3 33 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 3 34 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 3 35 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 3 36 . 1 1 22 22 LEU H H 1 7.77 . . . . . . . . . . . 5858 3 37 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 3 38 . 1 1 23 23 THR H H 1 8.22 . . . . . . . . . . . 5858 3 39 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 3 40 . 1 1 24 24 ILE H H 1 8.93 . . . . . . . . . . . 5858 3 41 . 1 1 25 25 LYS N N 15 119.7 . . . . . . . . . . . 5858 3 42 . 1 1 25 25 LYS H H 1 9.00 . . . . . . . . . . . 5858 3 43 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 3 44 . 1 1 27 27 GLY H H 1 7.11 . . . . . . . . . . . 5858 3 45 . 1 1 28 28 ASP N N 15 119.9 . . . . . . . . . . . 5858 3 46 . 1 1 28 28 ASP H H 1 7.90 . . . . . . . . . . . 5858 3 47 . 1 1 29 29 THR N N 15 114.8 . . . . . . . . . . . 5858 3 48 . 1 1 29 29 THR H H 1 8.69 . . . . . . . . . . . 5858 3 49 . 1 1 30 30 VAL N N 15 126.5 . . . . . . . . . . . 5858 3 50 . 1 1 30 30 VAL H H 1 9.18 . . . . . . . . . . . 5858 3 51 . 1 1 31 31 GLU N N 15 128.7 . . . . . . . . . . . 5858 3 52 . 1 1 31 31 GLU H H 1 9.20 . . . . . . . . . . . 5858 3 53 . 1 1 32 32 PHE N N 15 126.0 . . . . . . . . . . . 5858 3 54 . 1 1 32 32 PHE H H 1 9.13 . . . . . . . . . . . 5858 3 55 . 1 1 33 33 LEU N N 15 125.2 . . . . . . . . . . . 5858 3 56 . 1 1 33 33 LEU H H 1 8.97 . . . . . . . . . . . 5858 3 57 . 1 1 34 34 ASN N N 15 127.5 . . . . . . . . . . . 5858 3 58 . 1 1 34 34 ASN H H 1 9.33 . . . . . . . . . . . 5858 3 59 . 1 1 35 35 ASN N N 15 129.8 . . . . . . . . . . . 5858 3 60 . 1 1 35 35 ASN H H 1 8.81 . . . . . . . . . . . 5858 3 61 . 1 1 36 36 LYS N N 15 116.7 . . . . . . . . . . . 5858 3 62 . 1 1 36 36 LYS H H 1 8.13 . . . . . . . . . . . 5858 3 63 . 1 1 37 37 VAL N N 15 115.3 . . . . . . . . . . . 5858 3 64 . 1 1 37 37 VAL H H 1 8.92 . . . . . . . . . . . 5858 3 65 . 1 1 40 40 HIS N N 15 112.7 . . . . . . . . . . . 5858 3 66 . 1 1 40 40 HIS H H 1 7.18 . . . . . . . . . . . 5858 3 67 . 1 1 41 41 ASN N N 15 123.1 . . . . . . . . . . . 5858 3 68 . 1 1 41 41 ASN H H 1 9.88 . . . . . . . . . . . 5858 3 69 . 1 1 42 42 VAL N N 15 109.2 . . . . . . . . . . . 5858 3 70 . 1 1 42 42 VAL H H 1 7.05 . . . . . . . . . . . 5858 3 71 . 1 1 43 43 VAL N N 15 128.2 . . . . . . . . . . . 5858 3 72 . 1 1 43 43 VAL H H 1 9.42 . . . . . . . . . . . 5858 3 73 . 1 1 44 44 PHE N N 15 125.5 . . . . . . . . . . . 5858 3 74 . 1 1 44 44 PHE H H 1 8.70 . . . . . . . . . . . 5858 3 75 . 1 1 45 45 ASP N N 15 124.1 . . . . . . . . . . . 5858 3 76 . 1 1 45 45 ASP H H 1 8.40 . . . . . . . . . . . 5858 3 77 . 1 1 46 46 ALA N N 15 128.2 . . . . . . . . . . . 5858 3 78 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 3 79 . 1 1 47 47 ALA N N 15 117.5 . . . . . . . . . . . 5858 3 80 . 1 1 47 47 ALA H H 1 8.46 . . . . . . . . . . . 5858 3 81 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 3 82 . 1 1 48 48 LEU H H 1 8.67 . . . . . . . . . . . 5858 3 83 . 1 1 49 49 ASN N N 15 114.5 . . . . . . . . . . . 5858 3 84 . 1 1 49 49 ASN H H 1 8.05 . . . . . . . . . . . 5858 3 85 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 3 86 . 1 1 51 51 ALA H H 1 7.01 . . . . . . . . . . . 5858 3 87 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 3 88 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 3 89 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 3 90 . 1 1 53 53 SER H H 1 8.21 . . . . . . . . . . . 5858 3 91 . 1 1 56 56 LEU N N 15 123.7 . . . . . . . . . . . 5858 3 92 . 1 1 56 56 LEU H H 1 8.14 . . . . . . . . . . . 5858 3 93 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 3 94 . 1 1 57 57 ALA H H 1 7.56 . . . . . . . . . . . 5858 3 95 . 1 1 58 58 LYS N N 15 120.7 . . . . . . . . . . . 5858 3 96 . 1 1 58 58 LYS H H 1 8.52 . . . . . . . . . . . 5858 3 97 . 1 1 59 59 SER N N 15 115.3 . . . . . . . . . . . 5858 3 98 . 1 1 59 59 SER H H 1 7.74 . . . . . . . . . . . 5858 3 99 . 1 1 60 60 LEU N N 15 120.8 . . . . . . . . . . . 5858 3 100 . 1 1 60 60 LEU H H 1 6.89 . . . . . . . . . . . 5858 3 101 . 1 1 61 61 SER N N 15 110.9 . . . . . . . . . . . 5858 3 102 . 1 1 61 61 SER H H 1 6.90 . . . . . . . . . . . 5858 3 103 . 1 1 62 62 HIS N N 15 122.2 . . . . . . . . . . . 5858 3 104 . 1 1 62 62 HIS H H 1 9.61 . . . . . . . . . . . 5858 3 105 . 1 1 63 63 LYS N N 15 122.7 . . . . . . . . . . . 5858 3 106 . 1 1 63 63 LYS H H 1 8.63 . . . . . . . . . . . 5858 3 107 . 1 1 64 64 GLN N N 15 120.1 . . . . . . . . . . . 5858 3 108 . 1 1 64 64 GLN H H 1 8.35 . . . . . . . . . . . 5858 3 109 . 1 1 65 65 LEU N N 15 121.3 . . . . . . . . . . . 5858 3 110 . 1 1 65 65 LEU H H 1 8.16 . . . . . . . . . . . 5858 3 111 . 1 1 66 66 LEU N N 15 125.0 . . . . . . . . . . . 5858 3 112 . 1 1 66 66 LEU H H 1 9.52 . . . . . . . . . . . 5858 3 113 . 1 1 67 67 MET N N 15 121.9 . . . . . . . . . . . 5858 3 114 . 1 1 67 67 MET H H 1 8.07 . . . . . . . . . . . 5858 3 115 . 1 1 68 68 SER N N 15 113.7 . . . . . . . . . . . 5858 3 116 . 1 1 68 68 SER H H 1 8.38 . . . . . . . . . . . 5858 3 117 . 1 1 70 70 GLY N N 15 112.9 . . . . . . . . . . . 5858 3 118 . 1 1 70 70 GLY H H 1 9.04 . . . . . . . . . . . 5858 3 119 . 1 1 71 71 GLN N N 15 120.0 . . . . . . . . . . . 5858 3 120 . 1 1 71 71 GLN H H 1 7.54 . . . . . . . . . . . 5858 3 121 . 1 1 72 72 SER N N 15 116.1 . . . . . . . . . . . 5858 3 122 . 1 1 72 72 SER H H 1 8.64 . . . . . . . . . . . 5858 3 123 . 1 1 73 73 THR N N 15 116.0 . . . . . . . . . . . 5858 3 124 . 1 1 73 73 THR H H 1 8.74 . . . . . . . . . . . 5858 3 125 . 1 1 74 74 SER N N 15 117.7 . . . . . . . . . . . 5858 3 126 . 1 1 74 74 SER H H 1 8.21 . . . . . . . . . . . 5858 3 127 . 1 1 75 75 THR N N 15 121.4 . . . . . . . . . . . 5858 3 128 . 1 1 75 75 THR H H 1 9.55 . . . . . . . . . . . 5858 3 129 . 1 1 76 76 THR N N 15 127.0 . . . . . . . . . . . 5858 3 130 . 1 1 76 76 THR H H 1 9.11 . . . . . . . . . . . 5858 3 131 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 3 132 . 1 1 77 77 PHE H H 1 9.18 . . . . . . . . . . . 5858 3 133 . 1 1 79 79 ALA N N 15 123.2 . . . . . . . . . . . 5858 3 134 . 1 1 79 79 ALA H H 1 8.82 . . . . . . . . . . . 5858 3 135 . 1 1 80 80 ASP N N 15 113.2 . . . . . . . . . . . 5858 3 136 . 1 1 80 80 ASP H H 1 8.00 . . . . . . . . . . . 5858 3 137 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 3 138 . 1 1 81 81 ALA H H 1 7.58 . . . . . . . . . . . 5858 3 139 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 3 140 . 1 1 83 83 ALA H H 1 8.38 . . . . . . . . . . . 5858 3 141 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 3 142 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 3 143 . 1 1 85 85 GLU N N 15 119.8 . . . . . . . . . . . 5858 3 144 . 1 1 85 85 GLU H H 1 8.48 . . . . . . . . . . . 5858 3 145 . 1 1 86 86 TYR N N 15 125.6 . . . . . . . . . . . 5858 3 146 . 1 1 86 86 TYR H H 1 10.17 . . . . . . . . . . . 5858 3 147 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 3 148 . 1 1 87 87 THR H H 1 8.62 . . . . . . . . . . . 5858 3 149 . 1 1 88 88 PHE N N 15 126.3 . . . . . . . . . . . 5858 3 150 . 1 1 88 88 PHE H H 1 8.58 . . . . . . . . . . . 5858 3 151 . 1 1 89 89 TYR N N 15 115.4 . . . . . . . . . . . 5858 3 152 . 1 1 89 89 TYR H H 1 8.92 . . . . . . . . . . . 5858 3 153 . 1 1 90 90 CYS N N 15 125.2 . . . . . . . . . . . 5858 3 154 . 1 1 90 90 CYS H H 1 7.75 . . . . . . . . . . . 5858 3 155 . 1 1 91 91 GLU N N 15 125.6 . . . . . . . . . . . 5858 3 156 . 1 1 91 91 GLU H H 1 10.04 . . . . . . . . . . . 5858 3 157 . 1 1 93 93 HIS N N 15 115.8 . . . . . . . . . . . 5858 3 158 . 1 1 93 93 HIS H H 1 8.66 . . . . . . . . . . . 5858 3 159 . 1 1 94 94 ARG N N 15 129.4 . . . . . . . . . . . 5858 3 160 . 1 1 94 94 ARG H H 1 8.50 . . . . . . . . . . . 5858 3 161 . 1 1 96 96 ALA N N 15 121.7 . . . . . . . . . . . 5858 3 162 . 1 1 96 96 ALA H H 1 7.57 . . . . . . . . . . . 5858 3 163 . 1 1 97 97 GLY N N 15 106.4 . . . . . . . . . . . 5858 3 164 . 1 1 97 97 GLY H H 1 8.07 . . . . . . . . . . . 5858 3 165 . 1 1 98 98 MET N N 15 124.3 . . . . . . . . . . . 5858 3 166 . 1 1 98 98 MET H H 1 7.65 . . . . . . . . . . . 5858 3 167 . 1 1 99 99 VAL N N 15 125.8 . . . . . . . . . . . 5858 3 168 . 1 1 99 99 VAL H H 1 7.94 . . . . . . . . . . . 5858 3 169 . 1 1 100 100 GLY N N 15 118.2 . . . . . . . . . . . 5858 3 170 . 1 1 100 100 GLY H H 1 8.99 . . . . . . . . . . . 5858 3 171 . 1 1 101 101 LYS N N 15 117.6 . . . . . . . . . . . 5858 3 172 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 3 173 . 1 1 102 102 ILE N N 15 127.5 . . . . . . . . . . . 5858 3 174 . 1 1 102 102 ILE H H 1 9.48 . . . . . . . . . . . 5858 3 175 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 3 176 . 1 1 103 103 THR H H 1 9.27 . . . . . . . . . . . 5858 3 177 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 3 178 . 1 1 104 104 VAL H H 1 9.32 . . . . . . . . . . . 5858 3 179 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 3 180 . 1 1 105 105 ALA H H 1 9.25 . . . . . . . . . . . 5858 3 181 . 1 1 106 106 GLY N N 15 113.8 . . . . . . . . . . . 5858 3 182 . 1 1 106 106 GLY H H 1 7.79 . . . . . . . . . . . 5858 3 stop_ save_ save_shift_set_4 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_4 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 4 _Assigned_chem_shift_list.Sample_condition_list_ID 4 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_4 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 4 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.7 . . . . . . . . . . . 5858 4 2 . 1 1 3 3 THR H H 1 8.77 . . . . . . . . . . . 5858 4 3 . 1 1 4 4 TYR N N 15 127.0 . . . . . . . . . . . 5858 4 4 . 1 1 4 4 TYR H H 1 8.84 . . . . . . . . . . . 5858 4 5 . 1 1 5 5 THR N N 15 118.6 . . . . . . . . . . . 5858 4 6 . 1 1 5 5 THR H H 1 8.60 . . . . . . . . . . . 5858 4 7 . 1 1 6 6 VAL N N 15 129.9 . . . . . . . . . . . 5858 4 8 . 1 1 6 6 VAL H H 1 9.34 . . . . . . . . . . . 5858 4 9 . 1 1 7 7 LYS N N 15 126.6 . . . . . . . . . . . 5858 4 10 . 1 1 7 7 LYS H H 1 9.07 . . . . . . . . . . . 5858 4 11 . 1 1 8 8 LEU N N 15 122.0 . . . . . . . . . . . 5858 4 12 . 1 1 8 8 LEU H H 1 8.87 . . . . . . . . . . . 5858 4 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 4 14 . 1 1 9 9 GLY H H 1 7.68 . . . . . . . . . . . 5858 4 15 . 1 1 10 10 SER N N 15 119.6 . . . . . . . . . . . 5858 4 16 . 1 1 10 10 SER H H 1 8.67 . . . . . . . . . . . 5858 4 17 . 1 1 11 11 ASP N N 15 121.0 . . . . . . . . . . . 5858 4 18 . 1 1 11 11 ASP H H 1 9.48 . . . . . . . . . . . 5858 4 19 . 1 1 13 13 GLY N N 15 108.9 . . . . . . . . . . . 5858 4 20 . 1 1 13 13 GLY H H 1 8.33 . . . . . . . . . . . 5858 4 21 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 4 22 . 1 1 14 14 LEU H H 1 7.46 . . . . . . . . . . . 5858 4 23 . 1 1 15 15 LEU N N 15 124.9 . . . . . . . . . . . 5858 4 24 . 1 1 15 15 LEU H H 1 8.39 . . . . . . . . . . . 5858 4 25 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 4 26 . 1 1 16 16 VAL H H 1 7.48 . . . . . . . . . . . 5858 4 27 . 1 1 17 17 PHE N N 15 120.0 . . . . . . . . . . . 5858 4 28 . 1 1 17 17 PHE H H 1 8.64 . . . . . . . . . . . 5858 4 29 . 1 1 18 18 GLU N N 15 122.1 . . . . . . . . . . . 5858 4 30 . 1 1 18 18 GLU H H 1 9.01 . . . . . . . . . . . 5858 4 31 . 1 1 20 20 ALA N N 15 117.1 . . . . . . . . . . . 5858 4 32 . 1 1 20 20 ALA H H 1 8.14 . . . . . . . . . . . 5858 4 33 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 4 34 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 4 35 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 4 36 . 1 1 22 22 LEU H H 1 7.77 . . . . . . . . . . . 5858 4 37 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 4 38 . 1 1 23 23 THR H H 1 8.22 . . . . . . . . . . . 5858 4 39 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 4 40 . 1 1 24 24 ILE H H 1 8.93 . . . . . . . . . . . 5858 4 41 . 1 1 25 25 LYS N N 15 119.6 . . . . . . . . . . . 5858 4 42 . 1 1 25 25 LYS H H 1 8.99 . . . . . . . . . . . 5858 4 43 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 4 44 . 1 1 27 27 GLY H H 1 7.10 . . . . . . . . . . . 5858 4 45 . 1 1 28 28 ASP N N 15 119.9 . . . . . . . . . . . 5858 4 46 . 1 1 28 28 ASP H H 1 7.91 . . . . . . . . . . . 5858 4 47 . 1 1 29 29 THR N N 15 114.8 . . . . . . . . . . . 5858 4 48 . 1 1 29 29 THR H H 1 8.68 . . . . . . . . . . . 5858 4 49 . 1 1 30 30 VAL N N 15 126.5 . . . . . . . . . . . 5858 4 50 . 1 1 30 30 VAL H H 1 9.17 . . . . . . . . . . . 5858 4 51 . 1 1 31 31 GLU N N 15 128.8 . . . . . . . . . . . 5858 4 52 . 1 1 31 31 GLU H H 1 9.21 . . . . . . . . . . . 5858 4 53 . 1 1 32 32 PHE N N 15 126.0 . . . . . . . . . . . 5858 4 54 . 1 1 32 32 PHE H H 1 9.14 . . . . . . . . . . . 5858 4 55 . 1 1 33 33 LEU N N 15 125.3 . . . . . . . . . . . 5858 4 56 . 1 1 33 33 LEU H H 1 8.97 . . . . . . . . . . . 5858 4 57 . 1 1 34 34 ASN N N 15 127.4 . . . . . . . . . . . 5858 4 58 . 1 1 34 34 ASN H H 1 9.33 . . . . . . . . . . . 5858 4 59 . 1 1 35 35 ASN N N 15 129.7 . . . . . . . . . . . 5858 4 60 . 1 1 35 35 ASN H H 1 8.81 . . . . . . . . . . . 5858 4 61 . 1 1 36 36 LYS N N 15 116.7 . . . . . . . . . . . 5858 4 62 . 1 1 36 36 LYS H H 1 8.13 . . . . . . . . . . . 5858 4 63 . 1 1 37 37 VAL N N 15 115.3 . . . . . . . . . . . 5858 4 64 . 1 1 37 37 VAL H H 1 8.93 . . . . . . . . . . . 5858 4 65 . 1 1 40 40 HIS N N 15 112.6 . . . . . . . . . . . 5858 4 66 . 1 1 40 40 HIS H H 1 7.18 . . . . . . . . . . . 5858 4 67 . 1 1 41 41 ASN N N 15 123.1 . . . . . . . . . . . 5858 4 68 . 1 1 41 41 ASN H H 1 9.88 . . . . . . . . . . . 5858 4 69 . 1 1 42 42 VAL N N 15 109.1 . . . . . . . . . . . 5858 4 70 . 1 1 42 42 VAL H H 1 7.01 . . . . . . . . . . . 5858 4 71 . 1 1 43 43 VAL N N 15 128.3 . . . . . . . . . . . 5858 4 72 . 1 1 43 43 VAL H H 1 9.43 . . . . . . . . . . . 5858 4 73 . 1 1 44 44 PHE N N 15 125.5 . . . . . . . . . . . 5858 4 74 . 1 1 44 44 PHE H H 1 8.71 . . . . . . . . . . . 5858 4 75 . 1 1 45 45 ASP N N 15 124.1 . . . . . . . . . . . 5858 4 76 . 1 1 45 45 ASP H H 1 8.39 . . . . . . . . . . . 5858 4 77 . 1 1 46 46 ALA N N 15 128.2 . . . . . . . . . . . 5858 4 78 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 4 79 . 1 1 47 47 ALA N N 15 117.6 . . . . . . . . . . . 5858 4 80 . 1 1 47 47 ALA H H 1 8.45 . . . . . . . . . . . 5858 4 81 . 1 1 48 48 LEU N N 15 123.2 . . . . . . . . . . . 5858 4 82 . 1 1 48 48 LEU H H 1 8.67 . . . . . . . . . . . 5858 4 83 . 1 1 49 49 ASN N N 15 114.5 . . . . . . . . . . . 5858 4 84 . 1 1 49 49 ASN H H 1 8.06 . . . . . . . . . . . 5858 4 85 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 4 86 . 1 1 51 51 ALA H H 1 7.01 . . . . . . . . . . . 5858 4 87 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 4 88 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 4 89 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 4 90 . 1 1 53 53 SER H H 1 8.22 . . . . . . . . . . . 5858 4 91 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 4 92 . 1 1 54 54 ALA H H 1 9.19 . . . . . . . . . . . 5858 4 93 . 1 1 55 55 ASP N N 15 120.0 . . . . . . . . . . . 5858 4 94 . 1 1 55 55 ASP H H 1 8.41 . . . . . . . . . . . 5858 4 95 . 1 1 56 56 LEU N N 15 123.7 . . . . . . . . . . . 5858 4 96 . 1 1 56 56 LEU H H 1 8.14 . . . . . . . . . . . 5858 4 97 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 4 98 . 1 1 57 57 ALA H H 1 7.57 . . . . . . . . . . . 5858 4 99 . 1 1 58 58 LYS N N 15 120.8 . . . . . . . . . . . 5858 4 100 . 1 1 58 58 LYS H H 1 8.53 . . . . . . . . . . . 5858 4 101 . 1 1 59 59 SER N N 15 115.3 . . . . . . . . . . . 5858 4 102 . 1 1 59 59 SER H H 1 7.74 . . . . . . . . . . . 5858 4 103 . 1 1 60 60 LEU N N 15 120.7 . . . . . . . . . . . 5858 4 104 . 1 1 60 60 LEU H H 1 6.89 . . . . . . . . . . . 5858 4 105 . 1 1 61 61 SER N N 15 111.0 . . . . . . . . . . . 5858 4 106 . 1 1 61 61 SER H H 1 6.92 . . . . . . . . . . . 5858 4 107 . 1 1 62 62 HIS N N 15 121.6 . . . . . . . . . . . 5858 4 108 . 1 1 62 62 HIS H H 1 9.62 . . . . . . . . . . . 5858 4 109 . 1 1 63 63 LYS N N 15 122.8 . . . . . . . . . . . 5858 4 110 . 1 1 63 63 LYS H H 1 8.69 . . . . . . . . . . . 5858 4 111 . 1 1 64 64 GLN N N 15 120.2 . . . . . . . . . . . 5858 4 112 . 1 1 64 64 GLN H H 1 8.36 . . . . . . . . . . . 5858 4 113 . 1 1 65 65 LEU N N 15 121.5 . . . . . . . . . . . 5858 4 114 . 1 1 65 65 LEU H H 1 8.19 . . . . . . . . . . . 5858 4 115 . 1 1 66 66 LEU N N 15 125.0 . . . . . . . . . . . 5858 4 116 . 1 1 66 66 LEU H H 1 9.52 . . . . . . . . . . . 5858 4 117 . 1 1 67 67 MET N N 15 121.9 . . . . . . . . . . . 5858 4 118 . 1 1 67 67 MET H H 1 8.08 . . . . . . . . . . . 5858 4 119 . 1 1 68 68 SER N N 15 113.7 . . . . . . . . . . . 5858 4 120 . 1 1 68 68 SER H H 1 8.37 . . . . . . . . . . . 5858 4 121 . 1 1 70 70 GLY N N 15 112.8 . . . . . . . . . . . 5858 4 122 . 1 1 70 70 GLY H H 1 9.04 . . . . . . . . . . . 5858 4 123 . 1 1 71 71 GLN N N 15 119.9 . . . . . . . . . . . 5858 4 124 . 1 1 71 71 GLN H H 1 7.53 . . . . . . . . . . . 5858 4 125 . 1 1 72 72 SER N N 15 116.0 . . . . . . . . . . . 5858 4 126 . 1 1 72 72 SER H H 1 8.65 . . . . . . . . . . . 5858 4 127 . 1 1 73 73 THR N N 15 116.2 . . . . . . . . . . . 5858 4 128 . 1 1 73 73 THR H H 1 8.74 . . . . . . . . . . . 5858 4 129 . 1 1 74 74 SER N N 15 118.0 . . . . . . . . . . . 5858 4 130 . 1 1 74 74 SER H H 1 8.18 . . . . . . . . . . . 5858 4 131 . 1 1 75 75 THR N N 15 121.2 . . . . . . . . . . . 5858 4 132 . 1 1 75 75 THR H H 1 9.55 . . . . . . . . . . . 5858 4 133 . 1 1 76 76 THR N N 15 127.0 . . . . . . . . . . . 5858 4 134 . 1 1 76 76 THR H H 1 9.11 . . . . . . . . . . . 5858 4 135 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 4 136 . 1 1 77 77 PHE H H 1 9.18 . . . . . . . . . . . 5858 4 137 . 1 1 79 79 ALA N N 15 123.2 . . . . . . . . . . . 5858 4 138 . 1 1 79 79 ALA H H 1 8.82 . . . . . . . . . . . 5858 4 139 . 1 1 80 80 ASP N N 15 113.2 . . . . . . . . . . . 5858 4 140 . 1 1 80 80 ASP H H 1 8.01 . . . . . . . . . . . 5858 4 141 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 4 142 . 1 1 81 81 ALA H H 1 7.58 . . . . . . . . . . . 5858 4 143 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 4 144 . 1 1 83 83 ALA H H 1 8.38 . . . . . . . . . . . 5858 4 145 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 4 146 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 4 147 . 1 1 85 85 GLU N N 15 119.8 . . . . . . . . . . . 5858 4 148 . 1 1 85 85 GLU H H 1 8.48 . . . . . . . . . . . 5858 4 149 . 1 1 86 86 TYR N N 15 125.6 . . . . . . . . . . . 5858 4 150 . 1 1 86 86 TYR H H 1 10.17 . . . . . . . . . . . 5858 4 151 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 4 152 . 1 1 87 87 THR H H 1 8.62 . . . . . . . . . . . 5858 4 153 . 1 1 88 88 PHE N N 15 126.3 . . . . . . . . . . . 5858 4 154 . 1 1 88 88 PHE H H 1 8.58 . . . . . . . . . . . 5858 4 155 . 1 1 89 89 TYR N N 15 115.4 . . . . . . . . . . . 5858 4 156 . 1 1 89 89 TYR H H 1 8.93 . . . . . . . . . . . 5858 4 157 . 1 1 90 90 CYS N N 15 125.2 . . . . . . . . . . . 5858 4 158 . 1 1 90 90 CYS H H 1 7.75 . . . . . . . . . . . 5858 4 159 . 1 1 91 91 GLU N N 15 125.6 . . . . . . . . . . . 5858 4 160 . 1 1 91 91 GLU H H 1 10.04 . . . . . . . . . . . 5858 4 161 . 1 1 93 93 HIS N N 15 115.7 . . . . . . . . . . . 5858 4 162 . 1 1 93 93 HIS H H 1 8.65 . . . . . . . . . . . 5858 4 163 . 1 1 94 94 ARG N N 15 129.4 . . . . . . . . . . . 5858 4 164 . 1 1 94 94 ARG H H 1 8.50 . . . . . . . . . . . 5858 4 165 . 1 1 95 95 GLY N N 15 107.6 . . . . . . . . . . . 5858 4 166 . 1 1 95 95 GLY H H 1 9.10 . . . . . . . . . . . 5858 4 167 . 1 1 96 96 ALA N N 15 121.7 . . . . . . . . . . . 5858 4 168 . 1 1 96 96 ALA H H 1 7.57 . . . . . . . . . . . 5858 4 169 . 1 1 97 97 GLY N N 15 106.4 . . . . . . . . . . . 5858 4 170 . 1 1 97 97 GLY H H 1 8.07 . . . . . . . . . . . 5858 4 171 . 1 1 98 98 MET N N 15 124.3 . . . . . . . . . . . 5858 4 172 . 1 1 98 98 MET H H 1 7.65 . . . . . . . . . . . 5858 4 173 . 1 1 99 99 VAL N N 15 125.8 . . . . . . . . . . . 5858 4 174 . 1 1 99 99 VAL H H 1 7.94 . . . . . . . . . . . 5858 4 175 . 1 1 100 100 GLY N N 15 118.2 . . . . . . . . . . . 5858 4 176 . 1 1 100 100 GLY H H 1 8.99 . . . . . . . . . . . 5858 4 177 . 1 1 101 101 LYS N N 15 117.6 . . . . . . . . . . . 5858 4 178 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 4 179 . 1 1 102 102 ILE N N 15 127.5 . . . . . . . . . . . 5858 4 180 . 1 1 102 102 ILE H H 1 9.48 . . . . . . . . . . . 5858 4 181 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 4 182 . 1 1 103 103 THR H H 1 9.27 . . . . . . . . . . . 5858 4 183 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 4 184 . 1 1 104 104 VAL H H 1 9.32 . . . . . . . . . . . 5858 4 185 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 4 186 . 1 1 105 105 ALA H H 1 9.25 . . . . . . . . . . . 5858 4 187 . 1 1 106 106 GLY N N 15 113.8 . . . . . . . . . . . 5858 4 188 . 1 1 106 106 GLY H H 1 7.80 . . . . . . . . . . . 5858 4 stop_ save_ save_shift_set_5 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_5 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 5 _Assigned_chem_shift_list.Sample_condition_list_ID 5 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_5 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 5 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.7 . . . . . . . . . . . 5858 5 2 . 1 1 3 3 THR H H 1 8.78 . . . . . . . . . . . 5858 5 3 . 1 1 4 4 TYR N N 15 127.0 . . . . . . . . . . . 5858 5 4 . 1 1 4 4 TYR H H 1 8.84 . . . . . . . . . . . 5858 5 5 . 1 1 5 5 THR N N 15 118.5 . . . . . . . . . . . 5858 5 6 . 1 1 5 5 THR H H 1 8.61 . . . . . . . . . . . 5858 5 7 . 1 1 6 6 VAL N N 15 129.8 . . . . . . . . . . . 5858 5 8 . 1 1 6 6 VAL H H 1 9.33 . . . . . . . . . . . 5858 5 9 . 1 1 7 7 LYS N N 15 126.6 . . . . . . . . . . . 5858 5 10 . 1 1 7 7 LYS H H 1 9.07 . . . . . . . . . . . 5858 5 11 . 1 1 8 8 LEU N N 15 122.0 . . . . . . . . . . . 5858 5 12 . 1 1 8 8 LEU H H 1 8.86 . . . . . . . . . . . 5858 5 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 5 14 . 1 1 9 9 GLY H H 1 7.68 . . . . . . . . . . . 5858 5 15 . 1 1 10 10 SER N N 15 119.7 . . . . . . . . . . . 5858 5 16 . 1 1 10 10 SER H H 1 8.68 . . . . . . . . . . . 5858 5 17 . 1 1 11 11 ASP N N 15 121.0 . . . . . . . . . . . 5858 5 18 . 1 1 11 11 ASP H H 1 9.48 . . . . . . . . . . . 5858 5 19 . 1 1 12 12 LYS N N 15 115.9 . . . . . . . . . . . 5858 5 20 . 1 1 12 12 LYS H H 1 7.50 . . . . . . . . . . . 5858 5 21 . 1 1 13 13 GLY N N 15 108.9 . . . . . . . . . . . 5858 5 22 . 1 1 13 13 GLY H H 1 8.33 . . . . . . . . . . . 5858 5 23 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 5 24 . 1 1 14 14 LEU H H 1 7.46 . . . . . . . . . . . 5858 5 25 . 1 1 15 15 LEU N N 15 124.9 . . . . . . . . . . . 5858 5 26 . 1 1 15 15 LEU H H 1 8.40 . . . . . . . . . . . 5858 5 27 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 5 28 . 1 1 16 16 VAL H H 1 7.48 . . . . . . . . . . . 5858 5 29 . 1 1 17 17 PHE N N 15 120.0 . . . . . . . . . . . 5858 5 30 . 1 1 17 17 PHE H H 1 8.65 . . . . . . . . . . . 5858 5 31 . 1 1 18 18 GLU N N 15 122.1 . . . . . . . . . . . 5858 5 32 . 1 1 18 18 GLU H H 1 9.01 . . . . . . . . . . . 5858 5 33 . 1 1 20 20 ALA N N 15 117.1 . . . . . . . . . . . 5858 5 34 . 1 1 20 20 ALA H H 1 8.13 . . . . . . . . . . . 5858 5 35 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 5 36 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 5 37 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 5 38 . 1 1 22 22 LEU H H 1 7.77 . . . . . . . . . . . 5858 5 39 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 5 40 . 1 1 23 23 THR H H 1 8.22 . . . . . . . . . . . 5858 5 41 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 5 42 . 1 1 24 24 ILE H H 1 8.93 . . . . . . . . . . . 5858 5 43 . 1 1 25 25 LYS N N 15 119.6 . . . . . . . . . . . 5858 5 44 . 1 1 25 25 LYS H H 1 8.99 . . . . . . . . . . . 5858 5 45 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 5 46 . 1 1 27 27 GLY H H 1 7.10 . . . . . . . . . . . 5858 5 47 . 1 1 28 28 ASP N N 15 119.9 . . . . . . . . . . . 5858 5 48 . 1 1 28 28 ASP H H 1 7.91 . . . . . . . . . . . 5858 5 49 . 1 1 29 29 THR N N 15 114.8 . . . . . . . . . . . 5858 5 50 . 1 1 29 29 THR H H 1 8.67 . . . . . . . . . . . 5858 5 51 . 1 1 30 30 VAL N N 15 126.5 . . . . . . . . . . . 5858 5 52 . 1 1 30 30 VAL H H 1 9.16 . . . . . . . . . . . 5858 5 53 . 1 1 31 31 GLU N N 15 128.8 . . . . . . . . . . . 5858 5 54 . 1 1 31 31 GLU H H 1 9.22 . . . . . . . . . . . 5858 5 55 . 1 1 32 32 PHE N N 15 125.9 . . . . . . . . . . . 5858 5 56 . 1 1 32 32 PHE H H 1 9.15 . . . . . . . . . . . 5858 5 57 . 1 1 33 33 LEU N N 15 125.3 . . . . . . . . . . . 5858 5 58 . 1 1 33 33 LEU H H 1 8.97 . . . . . . . . . . . 5858 5 59 . 1 1 34 34 ASN N N 15 127.4 . . . . . . . . . . . 5858 5 60 . 1 1 34 34 ASN H H 1 9.33 . . . . . . . . . . . 5858 5 61 . 1 1 35 35 ASN N N 15 129.7 . . . . . . . . . . . 5858 5 62 . 1 1 35 35 ASN H H 1 8.81 . . . . . . . . . . . 5858 5 63 . 1 1 36 36 LYS N N 15 116.7 . . . . . . . . . . . 5858 5 64 . 1 1 36 36 LYS H H 1 8.13 . . . . . . . . . . . 5858 5 65 . 1 1 37 37 VAL N N 15 115.4 . . . . . . . . . . . 5858 5 66 . 1 1 37 37 VAL H H 1 8.93 . . . . . . . . . . . 5858 5 67 . 1 1 40 40 HIS N N 15 112.6 . . . . . . . . . . . 5858 5 68 . 1 1 40 40 HIS H H 1 7.18 . . . . . . . . . . . 5858 5 69 . 1 1 41 41 ASN N N 15 123.0 . . . . . . . . . . . 5858 5 70 . 1 1 41 41 ASN H H 1 9.88 . . . . . . . . . . . 5858 5 71 . 1 1 42 42 VAL N N 15 109.0 . . . . . . . . . . . 5858 5 72 . 1 1 42 42 VAL H H 1 6.97 . . . . . . . . . . . 5858 5 73 . 1 1 43 43 VAL N N 15 128.4 . . . . . . . . . . . 5858 5 74 . 1 1 43 43 VAL H H 1 9.44 . . . . . . . . . . . 5858 5 75 . 1 1 44 44 PHE N N 15 125.5 . . . . . . . . . . . 5858 5 76 . 1 1 44 44 PHE H H 1 8.71 . . . . . . . . . . . 5858 5 77 . 1 1 45 45 ASP N N 15 124.0 . . . . . . . . . . . 5858 5 78 . 1 1 45 45 ASP H H 1 8.39 . . . . . . . . . . . 5858 5 79 . 1 1 46 46 ALA N N 15 128.2 . . . . . . . . . . . 5858 5 80 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 5 81 . 1 1 47 47 ALA N N 15 117.6 . . . . . . . . . . . 5858 5 82 . 1 1 47 47 ALA H H 1 8.45 . . . . . . . . . . . 5858 5 83 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 5 84 . 1 1 48 48 LEU H H 1 8.66 . . . . . . . . . . . 5858 5 85 . 1 1 49 49 ASN N N 15 114.6 . . . . . . . . . . . 5858 5 86 . 1 1 49 49 ASN H H 1 8.06 . . . . . . . . . . . 5858 5 87 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 5 88 . 1 1 51 51 ALA H H 1 7.01 . . . . . . . . . . . 5858 5 89 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 5 90 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 5 91 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 5 92 . 1 1 53 53 SER H H 1 8.22 . . . . . . . . . . . 5858 5 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 5 94 . 1 1 54 54 ALA H H 1 9.19 . . . . . . . . . . . 5858 5 95 . 1 1 55 55 ASP N N 15 120.0 . . . . . . . . . . . 5858 5 96 . 1 1 55 55 ASP H H 1 8.41 . . . . . . . . . . . 5858 5 97 . 1 1 56 56 LEU N N 15 123.7 . . . . . . . . . . . 5858 5 98 . 1 1 56 56 LEU H H 1 8.14 . . . . . . . . . . . 5858 5 99 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 5 100 . 1 1 57 57 ALA H H 1 7.57 . . . . . . . . . . . 5858 5 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 5 102 . 1 1 58 58 LYS H H 1 8.54 . . . . . . . . . . . 5858 5 103 . 1 1 59 59 SER N N 15 115.3 . . . . . . . . . . . 5858 5 104 . 1 1 59 59 SER H H 1 7.74 . . . . . . . . . . . 5858 5 105 . 1 1 60 60 LEU N N 15 120.6 . . . . . . . . . . . 5858 5 106 . 1 1 60 60 LEU H H 1 6.89 . . . . . . . . . . . 5858 5 107 . 1 1 61 61 SER N N 15 111.1 . . . . . . . . . . . 5858 5 108 . 1 1 61 61 SER H H 1 6.94 . . . . . . . . . . . 5858 5 109 . 1 1 62 62 HIS N N 15 121.1 . . . . . . . . . . . 5858 5 110 . 1 1 62 62 HIS H H 1 9.63 . . . . . . . . . . . 5858 5 111 . 1 1 63 63 LYS N N 15 123.1 . . . . . . . . . . . 5858 5 112 . 1 1 63 63 LYS H H 1 8.74 . . . . . . . . . . . 5858 5 113 . 1 1 64 64 GLN N N 15 120.3 . . . . . . . . . . . 5858 5 114 . 1 1 64 64 GLN H H 1 8.37 . . . . . . . . . . . 5858 5 115 . 1 1 65 65 LEU N N 15 121.7 . . . . . . . . . . . 5858 5 116 . 1 1 65 65 LEU H H 1 8.20 . . . . . . . . . . . 5858 5 117 . 1 1 66 66 LEU N N 15 125.0 . . . . . . . . . . . 5858 5 118 . 1 1 66 66 LEU H H 1 9.51 . . . . . . . . . . . 5858 5 119 . 1 1 67 67 MET N N 15 121.9 . . . . . . . . . . . 5858 5 120 . 1 1 67 67 MET H H 1 8.09 . . . . . . . . . . . 5858 5 121 . 1 1 68 68 SER N N 15 113.6 . . . . . . . . . . . 5858 5 122 . 1 1 68 68 SER H H 1 8.36 . . . . . . . . . . . 5858 5 123 . 1 1 70 70 GLY N N 15 112.8 . . . . . . . . . . . 5858 5 124 . 1 1 70 70 GLY H H 1 9.03 . . . . . . . . . . . 5858 5 125 . 1 1 71 71 GLN N N 15 119.9 . . . . . . . . . . . 5858 5 126 . 1 1 71 71 GLN H H 1 7.52 . . . . . . . . . . . 5858 5 127 . 1 1 72 72 SER N N 15 115.9 . . . . . . . . . . . 5858 5 128 . 1 1 72 72 SER H H 1 8.65 . . . . . . . . . . . 5858 5 129 . 1 1 73 73 THR N N 15 116.3 . . . . . . . . . . . 5858 5 130 . 1 1 73 73 THR H H 1 8.74 . . . . . . . . . . . 5858 5 131 . 1 1 74 74 SER N N 15 118.2 . . . . . . . . . . . 5858 5 132 . 1 1 74 74 SER H H 1 8.17 . . . . . . . . . . . 5858 5 133 . 1 1 75 75 THR N N 15 121.1 . . . . . . . . . . . 5858 5 134 . 1 1 75 75 THR H H 1 9.55 . . . . . . . . . . . 5858 5 135 . 1 1 76 76 THR N N 15 127.1 . . . . . . . . . . . 5858 5 136 . 1 1 76 76 THR H H 1 9.11 . . . . . . . . . . . 5858 5 137 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 5 138 . 1 1 77 77 PHE H H 1 9.18 . . . . . . . . . . . 5858 5 139 . 1 1 79 79 ALA N N 15 123.2 . . . . . . . . . . . 5858 5 140 . 1 1 79 79 ALA H H 1 8.82 . . . . . . . . . . . 5858 5 141 . 1 1 80 80 ASP N N 15 113.2 . . . . . . . . . . . 5858 5 142 . 1 1 80 80 ASP H H 1 8.01 . . . . . . . . . . . 5858 5 143 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 5 144 . 1 1 81 81 ALA H H 1 7.58 . . . . . . . . . . . 5858 5 145 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 5 146 . 1 1 83 83 ALA H H 1 8.38 . . . . . . . . . . . 5858 5 147 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 5 148 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 5 149 . 1 1 85 85 GLU N N 15 119.8 . . . . . . . . . . . 5858 5 150 . 1 1 85 85 GLU H H 1 8.48 . . . . . . . . . . . 5858 5 151 . 1 1 86 86 TYR N N 15 125.6 . . . . . . . . . . . 5858 5 152 . 1 1 86 86 TYR H H 1 10.17 . . . . . . . . . . . 5858 5 153 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 5 154 . 1 1 87 87 THR H H 1 8.62 . . . . . . . . . . . 5858 5 155 . 1 1 88 88 PHE N N 15 126.3 . . . . . . . . . . . 5858 5 156 . 1 1 88 88 PHE H H 1 8.58 . . . . . . . . . . . 5858 5 157 . 1 1 89 89 TYR N N 15 115.3 . . . . . . . . . . . 5858 5 158 . 1 1 89 89 TYR H H 1 8.94 . . . . . . . . . . . 5858 5 159 . 1 1 90 90 CYS N N 15 125.2 . . . . . . . . . . . 5858 5 160 . 1 1 90 90 CYS H H 1 7.75 . . . . . . . . . . . 5858 5 161 . 1 1 91 91 GLU N N 15 125.6 . . . . . . . . . . . 5858 5 162 . 1 1 91 91 GLU H H 1 10.03 . . . . . . . . . . . 5858 5 163 . 1 1 93 93 HIS N N 15 115.7 . . . . . . . . . . . 5858 5 164 . 1 1 93 93 HIS H H 1 8.62 . . . . . . . . . . . 5858 5 165 . 1 1 94 94 ARG N N 15 129.3 . . . . . . . . . . . 5858 5 166 . 1 1 94 94 ARG H H 1 8.49 . . . . . . . . . . . 5858 5 167 . 1 1 95 95 GLY N N 15 107.6 . . . . . . . . . . . 5858 5 168 . 1 1 95 95 GLY H H 1 9.09 . . . . . . . . . . . 5858 5 169 . 1 1 96 96 ALA N N 15 121.7 . . . . . . . . . . . 5858 5 170 . 1 1 96 96 ALA H H 1 7.57 . . . . . . . . . . . 5858 5 171 . 1 1 97 97 GLY N N 15 106.4 . . . . . . . . . . . 5858 5 172 . 1 1 97 97 GLY H H 1 8.07 . . . . . . . . . . . 5858 5 173 . 1 1 98 98 MET N N 15 124.3 . . . . . . . . . . . 5858 5 174 . 1 1 98 98 MET H H 1 7.65 . . . . . . . . . . . 5858 5 175 . 1 1 99 99 VAL N N 15 125.8 . . . . . . . . . . . 5858 5 176 . 1 1 99 99 VAL H H 1 7.94 . . . . . . . . . . . 5858 5 177 . 1 1 100 100 GLY N N 15 118.2 . . . . . . . . . . . 5858 5 178 . 1 1 100 100 GLY H H 1 8.98 . . . . . . . . . . . 5858 5 179 . 1 1 101 101 LYS N N 15 117.6 . . . . . . . . . . . 5858 5 180 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 5 181 . 1 1 102 102 ILE N N 15 127.5 . . . . . . . . . . . 5858 5 182 . 1 1 102 102 ILE H H 1 9.48 . . . . . . . . . . . 5858 5 183 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 5 184 . 1 1 103 103 THR H H 1 9.27 . . . . . . . . . . . 5858 5 185 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 5 186 . 1 1 104 104 VAL H H 1 9.33 . . . . . . . . . . . 5858 5 187 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 5 188 . 1 1 105 105 ALA H H 1 9.25 . . . . . . . . . . . 5858 5 189 . 1 1 106 106 GLY N N 15 113.8 . . . . . . . . . . . 5858 5 190 . 1 1 106 106 GLY H H 1 7.80 . . . . . . . . . . . 5858 5 stop_ save_ save_shift_set_6 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_6 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 6 _Assigned_chem_shift_list.Sample_condition_list_ID 6 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_6 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 6 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.6 . . . . . . . . . . . 5858 6 2 . 1 1 3 3 THR H H 1 8.79 . . . . . . . . . . . 5858 6 3 . 1 1 4 4 TYR N N 15 127.0 . . . . . . . . . . . 5858 6 4 . 1 1 4 4 TYR H H 1 8.84 . . . . . . . . . . . 5858 6 5 . 1 1 5 5 THR N N 15 118.4 . . . . . . . . . . . 5858 6 6 . 1 1 5 5 THR H H 1 8.62 . . . . . . . . . . . 5858 6 7 . 1 1 6 6 VAL N N 15 129.7 . . . . . . . . . . . 5858 6 8 . 1 1 6 6 VAL H H 1 9.32 . . . . . . . . . . . 5858 6 9 . 1 1 7 7 LYS N N 15 126.6 . . . . . . . . . . . 5858 6 10 . 1 1 7 7 LYS H H 1 9.08 . . . . . . . . . . . 5858 6 11 . 1 1 8 8 LEU N N 15 121.9 . . . . . . . . . . . 5858 6 12 . 1 1 8 8 LEU H H 1 8.86 . . . . . . . . . . . 5858 6 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 6 14 . 1 1 9 9 GLY H H 1 7.67 . . . . . . . . . . . 5858 6 15 . 1 1 10 10 SER N N 15 119.7 . . . . . . . . . . . 5858 6 16 . 1 1 10 10 SER H H 1 8.68 . . . . . . . . . . . 5858 6 17 . 1 1 11 11 ASP N N 15 121.0 . . . . . . . . . . . 5858 6 18 . 1 1 11 11 ASP H H 1 9.48 . . . . . . . . . . . 5858 6 19 . 1 1 12 12 LYS N N 15 115.9 . . . . . . . . . . . 5858 6 20 . 1 1 12 12 LYS H H 1 7.51 . . . . . . . . . . . 5858 6 21 . 1 1 13 13 GLY N N 15 108.9 . . . . . . . . . . . 5858 6 22 . 1 1 13 13 GLY H H 1 8.33 . . . . . . . . . . . 5858 6 23 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 6 24 . 1 1 14 14 LEU H H 1 7.47 . . . . . . . . . . . 5858 6 25 . 1 1 15 15 LEU N N 15 125.0 . . . . . . . . . . . 5858 6 26 . 1 1 15 15 LEU H H 1 8.43 . . . . . . . . . . . 5858 6 27 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 6 28 . 1 1 16 16 VAL H H 1 7.50 . . . . . . . . . . . 5858 6 29 . 1 1 17 17 PHE N N 15 120.1 . . . . . . . . . . . 5858 6 30 . 1 1 17 17 PHE H H 1 8.67 . . . . . . . . . . . 5858 6 31 . 1 1 18 18 GLU N N 15 122.1 . . . . . . . . . . . 5858 6 32 . 1 1 18 18 GLU H H 1 9.01 . . . . . . . . . . . 5858 6 33 . 1 1 20 20 ALA N N 15 117.0 . . . . . . . . . . . 5858 6 34 . 1 1 20 20 ALA H H 1 8.12 . . . . . . . . . . . 5858 6 35 . 1 1 21 21 LYS N N 15 115.8 . . . . . . . . . . . 5858 6 36 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 6 37 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 6 38 . 1 1 22 22 LEU H H 1 7.76 . . . . . . . . . . . 5858 6 39 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 6 40 . 1 1 23 23 THR H H 1 8.23 . . . . . . . . . . . 5858 6 41 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 6 42 . 1 1 24 24 ILE H H 1 8.93 . . . . . . . . . . . 5858 6 43 . 1 1 25 25 LYS N N 15 119.6 . . . . . . . . . . . 5858 6 44 . 1 1 25 25 LYS H H 1 8.98 . . . . . . . . . . . 5858 6 45 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 6 46 . 1 1 27 27 GLY H H 1 7.10 . . . . . . . . . . . 5858 6 47 . 1 1 28 28 ASP N N 15 119.8 . . . . . . . . . . . 5858 6 48 . 1 1 28 28 ASP H H 1 7.91 . . . . . . . . . . . 5858 6 49 . 1 1 29 29 THR N N 15 114.7 . . . . . . . . . . . 5858 6 50 . 1 1 29 29 THR H H 1 8.67 . . . . . . . . . . . 5858 6 51 . 1 1 30 30 VAL N N 15 126.4 . . . . . . . . . . . 5858 6 52 . 1 1 30 30 VAL H H 1 9.16 . . . . . . . . . . . 5858 6 53 . 1 1 31 31 GLU N N 15 128.8 . . . . . . . . . . . 5858 6 54 . 1 1 31 31 GLU H H 1 9.23 . . . . . . . . . . . 5858 6 55 . 1 1 32 32 PHE N N 15 125.9 . . . . . . . . . . . 5858 6 56 . 1 1 32 32 PHE H H 1 9.16 . . . . . . . . . . . 5858 6 57 . 1 1 33 33 LEU N N 15 125.3 . . . . . . . . . . . 5858 6 58 . 1 1 33 33 LEU H H 1 8.98 . . . . . . . . . . . 5858 6 59 . 1 1 34 34 ASN N N 15 127.3 . . . . . . . . . . . 5858 6 60 . 1 1 34 34 ASN H H 1 9.34 . . . . . . . . . . . 5858 6 61 . 1 1 35 35 ASN N N 15 129.7 . . . . . . . . . . . 5858 6 62 . 1 1 35 35 ASN H H 1 8.79 . . . . . . . . . . . 5858 6 63 . 1 1 36 36 LYS N N 15 116.8 . . . . . . . . . . . 5858 6 64 . 1 1 36 36 LYS H H 1 8.14 . . . . . . . . . . . 5858 6 65 . 1 1 37 37 VAL N N 15 115.6 . . . . . . . . . . . 5858 6 66 . 1 1 37 37 VAL H H 1 8.95 . . . . . . . . . . . 5858 6 67 . 1 1 40 40 HIS N N 15 112.4 . . . . . . . . . . . 5858 6 68 . 1 1 40 40 HIS H H 1 7.21 . . . . . . . . . . . 5858 6 69 . 1 1 41 41 ASN N N 15 122.9 . . . . . . . . . . . 5858 6 70 . 1 1 41 41 ASN H H 1 9.85 . . . . . . . . . . . 5858 6 71 . 1 1 42 42 VAL N N 15 108.9 . . . . . . . . . . . 5858 6 72 . 1 1 42 42 VAL H H 1 6.95 . . . . . . . . . . . 5858 6 73 . 1 1 43 43 VAL N N 15 128.5 . . . . . . . . . . . 5858 6 74 . 1 1 43 43 VAL H H 1 9.43 . . . . . . . . . . . 5858 6 75 . 1 1 44 44 PHE N N 15 125.5 . . . . . . . . . . . 5858 6 76 . 1 1 44 44 PHE H H 1 8.72 . . . . . . . . . . . 5858 6 77 . 1 1 45 45 ASP N N 15 124.0 . . . . . . . . . . . 5858 6 78 . 1 1 45 45 ASP H H 1 8.39 . . . . . . . . . . . 5858 6 79 . 1 1 46 46 ALA N N 15 128.2 . . . . . . . . . . . 5858 6 80 . 1 1 46 46 ALA H H 1 8.63 . . . . . . . . . . . 5858 6 81 . 1 1 47 47 ALA N N 15 117.6 . . . . . . . . . . . 5858 6 82 . 1 1 47 47 ALA H H 1 8.46 . . . . . . . . . . . 5858 6 83 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 6 84 . 1 1 48 48 LEU H H 1 8.67 . . . . . . . . . . . 5858 6 85 . 1 1 49 49 ASN N N 15 114.5 . . . . . . . . . . . 5858 6 86 . 1 1 49 49 ASN H H 1 8.06 . . . . . . . . . . . 5858 6 87 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 6 88 . 1 1 51 51 ALA H H 1 7.01 . . . . . . . . . . . 5858 6 89 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 6 90 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 6 91 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 6 92 . 1 1 53 53 SER H H 1 8.22 . . . . . . . . . . . 5858 6 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 6 94 . 1 1 54 54 ALA H H 1 9.19 . . . . . . . . . . . 5858 6 95 . 1 1 55 55 ASP N N 15 120.0 . . . . . . . . . . . 5858 6 96 . 1 1 55 55 ASP H H 1 8.42 . . . . . . . . . . . 5858 6 97 . 1 1 56 56 LEU N N 15 123.7 . . . . . . . . . . . 5858 6 98 . 1 1 56 56 LEU H H 1 8.15 . . . . . . . . . . . 5858 6 99 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 6 100 . 1 1 57 57 ALA H H 1 7.58 . . . . . . . . . . . 5858 6 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 6 102 . 1 1 58 58 LYS H H 1 8.55 . . . . . . . . . . . 5858 6 103 . 1 1 59 59 SER N N 15 115.3 . . . . . . . . . . . 5858 6 104 . 1 1 59 59 SER H H 1 7.75 . . . . . . . . . . . 5858 6 105 . 1 1 60 60 LEU N N 15 120.5 . . . . . . . . . . . 5858 6 106 . 1 1 60 60 LEU H H 1 6.90 . . . . . . . . . . . 5858 6 107 . 1 1 61 61 SER N N 15 111.1 . . . . . . . . . . . 5858 6 108 . 1 1 61 61 SER H H 1 6.97 . . . . . . . . . . . 5858 6 109 . 1 1 62 62 HIS N N 15 120.7 . . . . . . . . . . . 5858 6 110 . 1 1 62 62 HIS H H 1 9.63 . . . . . . . . . . . 5858 6 111 . 1 1 63 63 LYS N N 15 123.3 . . . . . . . . . . . 5858 6 112 . 1 1 63 63 LYS H H 1 8.78 . . . . . . . . . . . 5858 6 113 . 1 1 64 64 GLN N N 15 120.3 . . . . . . . . . . . 5858 6 114 . 1 1 64 64 GLN H H 1 8.38 . . . . . . . . . . . 5858 6 115 . 1 1 65 65 LEU N N 15 121.8 . . . . . . . . . . . 5858 6 116 . 1 1 65 65 LEU H H 1 8.23 . . . . . . . . . . . 5858 6 117 . 1 1 66 66 LEU N N 15 124.9 . . . . . . . . . . . 5858 6 118 . 1 1 66 66 LEU H H 1 9.49 . . . . . . . . . . . 5858 6 119 . 1 1 67 67 MET N N 15 121.9 . . . . . . . . . . . 5858 6 120 . 1 1 67 67 MET H H 1 8.11 . . . . . . . . . . . 5858 6 121 . 1 1 68 68 SER N N 15 113.7 . . . . . . . . . . . 5858 6 122 . 1 1 68 68 SER H H 1 8.37 . . . . . . . . . . . 5858 6 123 . 1 1 70 70 GLY N N 15 112.8 . . . . . . . . . . . 5858 6 124 . 1 1 70 70 GLY H H 1 9.02 . . . . . . . . . . . 5858 6 125 . 1 1 71 71 GLN N N 15 119.8 . . . . . . . . . . . 5858 6 126 . 1 1 71 71 GLN H H 1 7.52 . . . . . . . . . . . 5858 6 127 . 1 1 72 72 SER N N 15 115.8 . . . . . . . . . . . 5858 6 128 . 1 1 72 72 SER H H 1 8.66 . . . . . . . . . . . 5858 6 129 . 1 1 73 73 THR N N 15 116.2 . . . . . . . . . . . 5858 6 130 . 1 1 73 73 THR H H 1 8.73 . . . . . . . . . . . 5858 6 131 . 1 1 74 74 SER N N 15 118.3 . . . . . . . . . . . 5858 6 132 . 1 1 74 74 SER H H 1 8.16 . . . . . . . . . . . 5858 6 133 . 1 1 75 75 THR N N 15 121.0 . . . . . . . . . . . 5858 6 134 . 1 1 75 75 THR H H 1 9.55 . . . . . . . . . . . 5858 6 135 . 1 1 76 76 THR N N 15 127.1 . . . . . . . . . . . 5858 6 136 . 1 1 76 76 THR H H 1 9.12 . . . . . . . . . . . 5858 6 137 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 6 138 . 1 1 77 77 PHE H H 1 9.17 . . . . . . . . . . . 5858 6 139 . 1 1 79 79 ALA N N 15 123.1 . . . . . . . . . . . 5858 6 140 . 1 1 79 79 ALA H H 1 8.83 . . . . . . . . . . . 5858 6 141 . 1 1 80 80 ASP N N 15 113.1 . . . . . . . . . . . 5858 6 142 . 1 1 80 80 ASP H H 1 8.00 . . . . . . . . . . . 5858 6 143 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 6 144 . 1 1 81 81 ALA H H 1 7.58 . . . . . . . . . . . 5858 6 145 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 6 146 . 1 1 83 83 ALA H H 1 8.39 . . . . . . . . . . . 5858 6 147 . 1 1 84 84 GLY N N 15 107.3 . . . . . . . . . . . 5858 6 148 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 6 149 . 1 1 85 85 GLU N N 15 119.7 . . . . . . . . . . . 5858 6 150 . 1 1 85 85 GLU H H 1 8.49 . . . . . . . . . . . 5858 6 151 . 1 1 86 86 TYR N N 15 125.5 . . . . . . . . . . . 5858 6 152 . 1 1 86 86 TYR H H 1 10.17 . . . . . . . . . . . 5858 6 153 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 6 154 . 1 1 87 87 THR H H 1 8.63 . . . . . . . . . . . 5858 6 155 . 1 1 88 88 PHE N N 15 126.2 . . . . . . . . . . . 5858 6 156 . 1 1 88 88 PHE H H 1 8.58 . . . . . . . . . . . 5858 6 157 . 1 1 89 89 TYR N N 15 115.2 . . . . . . . . . . . 5858 6 158 . 1 1 89 89 TYR H H 1 8.96 . . . . . . . . . . . 5858 6 159 . 1 1 90 90 CYS N N 15 125.1 . . . . . . . . . . . 5858 6 160 . 1 1 90 90 CYS H H 1 7.75 . . . . . . . . . . . 5858 6 161 . 1 1 91 91 GLU N N 15 125.6 . . . . . . . . . . . 5858 6 162 . 1 1 91 91 GLU H H 1 10.03 . . . . . . . . . . . 5858 6 163 . 1 1 93 93 HIS N N 15 115.3 . . . . . . . . . . . 5858 6 164 . 1 1 93 93 HIS H H 1 8.58 . . . . . . . . . . . 5858 6 165 . 1 1 94 94 ARG N N 15 129.2 . . . . . . . . . . . 5858 6 166 . 1 1 94 94 ARG H H 1 8.46 . . . . . . . . . . . 5858 6 167 . 1 1 95 95 GLY N N 15 107.6 . . . . . . . . . . . 5858 6 168 . 1 1 95 95 GLY H H 1 9.09 . . . . . . . . . . . 5858 6 169 . 1 1 96 96 ALA N N 15 121.6 . . . . . . . . . . . 5858 6 170 . 1 1 96 96 ALA H H 1 7.56 . . . . . . . . . . . 5858 6 171 . 1 1 97 97 GLY N N 15 106.3 . . . . . . . . . . . 5858 6 172 . 1 1 97 97 GLY H H 1 8.08 . . . . . . . . . . . 5858 6 173 . 1 1 98 98 MET N N 15 124.0 . . . . . . . . . . . 5858 6 174 . 1 1 98 98 MET H H 1 7.63 . . . . . . . . . . . 5858 6 175 . 1 1 99 99 VAL N N 15 125.9 . . . . . . . . . . . 5858 6 176 . 1 1 99 99 VAL H H 1 7.95 . . . . . . . . . . . 5858 6 177 . 1 1 100 100 GLY N N 15 118.1 . . . . . . . . . . . 5858 6 178 . 1 1 100 100 GLY H H 1 8.97 . . . . . . . . . . . 5858 6 179 . 1 1 101 101 LYS N N 15 117.6 . . . . . . . . . . . 5858 6 180 . 1 1 101 101 LYS H H 1 8.28 . . . . . . . . . . . 5858 6 181 . 1 1 102 102 ILE N N 15 127.4 . . . . . . . . . . . 5858 6 182 . 1 1 102 102 ILE H H 1 9.48 . . . . . . . . . . . 5858 6 183 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 6 184 . 1 1 103 103 THR H H 1 9.27 . . . . . . . . . . . 5858 6 185 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 6 186 . 1 1 104 104 VAL H H 1 9.33 . . . . . . . . . . . 5858 6 187 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 6 188 . 1 1 105 105 ALA H H 1 9.25 . . . . . . . . . . . 5858 6 189 . 1 1 106 106 GLY N N 15 113.8 . . . . . . . . . . . 5858 6 190 . 1 1 106 106 GLY H H 1 7.81 . . . . . . . . . . . 5858 6 stop_ save_ save_shift_set_7 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_7 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 7 _Assigned_chem_shift_list.Sample_condition_list_ID 7 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_7 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 7 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.6 . . . . . . . . . . . 5858 7 2 . 1 1 3 3 THR H H 1 8.79 . . . . . . . . . . . 5858 7 3 . 1 1 4 4 TYR N N 15 127.0 . . . . . . . . . . . 5858 7 4 . 1 1 4 4 TYR H H 1 8.84 . . . . . . . . . . . 5858 7 5 . 1 1 5 5 THR N N 15 118.5 . . . . . . . . . . . 5858 7 6 . 1 1 5 5 THR H H 1 8.63 . . . . . . . . . . . 5858 7 7 . 1 1 6 6 VAL N N 15 129.7 . . . . . . . . . . . 5858 7 8 . 1 1 6 6 VAL H H 1 9.31 . . . . . . . . . . . 5858 7 9 . 1 1 7 7 LYS N N 15 126.6 . . . . . . . . . . . 5858 7 10 . 1 1 7 7 LYS H H 1 9.09 . . . . . . . . . . . 5858 7 11 . 1 1 8 8 LEU N N 15 121.9 . . . . . . . . . . . 5858 7 12 . 1 1 8 8 LEU H H 1 8.86 . . . . . . . . . . . 5858 7 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 7 14 . 1 1 9 9 GLY H H 1 7.66 . . . . . . . . . . . 5858 7 15 . 1 1 10 10 SER N N 15 119.7 . . . . . . . . . . . 5858 7 16 . 1 1 10 10 SER H H 1 8.69 . . . . . . . . . . . 5858 7 17 . 1 1 11 11 ASP N N 15 121.0 . . . . . . . . . . . 5858 7 18 . 1 1 11 11 ASP H H 1 9.47 . . . . . . . . . . . 5858 7 19 . 1 1 12 12 LYS N N 15 115.9 . . . . . . . . . . . 5858 7 20 . 1 1 12 12 LYS H H 1 7.51 . . . . . . . . . . . 5858 7 21 . 1 1 13 13 GLY N N 15 108.9 . . . . . . . . . . . 5858 7 22 . 1 1 13 13 GLY H H 1 8.33 . . . . . . . . . . . 5858 7 23 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 7 24 . 1 1 14 14 LEU H H 1 7.46 . . . . . . . . . . . 5858 7 25 . 1 1 15 15 LEU N N 15 125.1 . . . . . . . . . . . 5858 7 26 . 1 1 15 15 LEU H H 1 8.44 . . . . . . . . . . . 5858 7 27 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 7 28 . 1 1 16 16 VAL H H 1 7.50 . . . . . . . . . . . 5858 7 29 . 1 1 17 17 PHE N N 15 120.2 . . . . . . . . . . . 5858 7 30 . 1 1 17 17 PHE H H 1 8.69 . . . . . . . . . . . 5858 7 31 . 1 1 18 18 GLU N N 15 122.2 . . . . . . . . . . . 5858 7 32 . 1 1 18 18 GLU H H 1 9.00 . . . . . . . . . . . 5858 7 33 . 1 1 20 20 ALA N N 15 116.9 . . . . . . . . . . . 5858 7 34 . 1 1 20 20 ALA H H 1 8.10 . . . . . . . . . . . 5858 7 35 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 7 36 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 7 37 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 7 38 . 1 1 22 22 LEU H H 1 7.77 . . . . . . . . . . . 5858 7 39 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 7 40 . 1 1 23 23 THR H H 1 8.23 . . . . . . . . . . . 5858 7 41 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 7 42 . 1 1 24 24 ILE H H 1 8.93 . . . . . . . . . . . 5858 7 43 . 1 1 25 25 LYS N N 15 119.6 . . . . . . . . . . . 5858 7 44 . 1 1 25 25 LYS H H 1 8.98 . . . . . . . . . . . 5858 7 45 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 7 46 . 1 1 27 27 GLY H H 1 7.10 . . . . . . . . . . . 5858 7 47 . 1 1 28 28 ASP N N 15 119.8 . . . . . . . . . . . 5858 7 48 . 1 1 28 28 ASP H H 1 7.91 . . . . . . . . . . . 5858 7 49 . 1 1 29 29 THR N N 15 114.8 . . . . . . . . . . . 5858 7 50 . 1 1 29 29 THR H H 1 8.67 . . . . . . . . . . . 5858 7 51 . 1 1 30 30 VAL N N 15 126.4 . . . . . . . . . . . 5858 7 52 . 1 1 30 30 VAL H H 1 9.16 . . . . . . . . . . . 5858 7 53 . 1 1 31 31 GLU N N 15 128.8 . . . . . . . . . . . 5858 7 54 . 1 1 31 31 GLU H H 1 9.23 . . . . . . . . . . . 5858 7 55 . 1 1 32 32 PHE N N 15 126.0 . . . . . . . . . . . 5858 7 56 . 1 1 32 32 PHE H H 1 9.16 . . . . . . . . . . . 5858 7 57 . 1 1 33 33 LEU N N 15 125.3 . . . . . . . . . . . 5858 7 58 . 1 1 33 33 LEU H H 1 8.97 . . . . . . . . . . . 5858 7 59 . 1 1 34 34 ASN N N 15 127.3 . . . . . . . . . . . 5858 7 60 . 1 1 34 34 ASN H H 1 9.34 . . . . . . . . . . . 5858 7 61 . 1 1 35 35 ASN N N 15 129.7 . . . . . . . . . . . 5858 7 62 . 1 1 35 35 ASN H H 1 8.78 . . . . . . . . . . . 5858 7 63 . 1 1 36 36 LYS N N 15 116.8 . . . . . . . . . . . 5858 7 64 . 1 1 36 36 LYS H H 1 8.16 . . . . . . . . . . . 5858 7 65 . 1 1 37 37 VAL N N 15 115.6 . . . . . . . . . . . 5858 7 66 . 1 1 37 37 VAL H H 1 8.96 . . . . . . . . . . . 5858 7 67 . 1 1 40 40 HIS N N 15 112.3 . . . . . . . . . . . 5858 7 68 . 1 1 40 40 HIS H H 1 7.22 . . . . . . . . . . . 5858 7 69 . 1 1 41 41 ASN N N 15 122.9 . . . . . . . . . . . 5858 7 70 . 1 1 41 41 ASN H H 1 9.83 . . . . . . . . . . . 5858 7 71 . 1 1 42 42 VAL N N 15 108.9 . . . . . . . . . . . 5858 7 72 . 1 1 42 42 VAL H H 1 6.95 . . . . . . . . . . . 5858 7 73 . 1 1 43 43 VAL N N 15 128.5 . . . . . . . . . . . 5858 7 74 . 1 1 43 43 VAL H H 1 9.42 . . . . . . . . . . . 5858 7 75 . 1 1 44 44 PHE N N 15 125.5 . . . . . . . . . . . 5858 7 76 . 1 1 44 44 PHE H H 1 8.73 . . . . . . . . . . . 5858 7 77 . 1 1 45 45 ASP N N 15 124.0 . . . . . . . . . . . 5858 7 78 . 1 1 45 45 ASP H H 1 8.39 . . . . . . . . . . . 5858 7 79 . 1 1 46 46 ALA N N 15 128.2 . . . . . . . . . . . 5858 7 80 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 7 81 . 1 1 47 47 ALA N N 15 117.6 . . . . . . . . . . . 5858 7 82 . 1 1 47 47 ALA H H 1 8.46 . . . . . . . . . . . 5858 7 83 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 7 84 . 1 1 48 48 LEU H H 1 8.66 . . . . . . . . . . . 5858 7 85 . 1 1 49 49 ASN N N 15 114.6 . . . . . . . . . . . 5858 7 86 . 1 1 49 49 ASN H H 1 8.07 . . . . . . . . . . . 5858 7 87 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 7 88 . 1 1 51 51 ALA H H 1 7.00 . . . . . . . . . . . 5858 7 89 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 7 90 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 7 91 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 7 92 . 1 1 53 53 SER H H 1 8.22 . . . . . . . . . . . 5858 7 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 7 94 . 1 1 54 54 ALA H H 1 9.19 . . . . . . . . . . . 5858 7 95 . 1 1 55 55 ASP N N 15 120.0 . . . . . . . . . . . 5858 7 96 . 1 1 55 55 ASP H H 1 8.42 . . . . . . . . . . . 5858 7 97 . 1 1 56 56 LEU N N 15 123.8 . . . . . . . . . . . 5858 7 98 . 1 1 56 56 LEU H H 1 8.14 . . . . . . . . . . . 5858 7 99 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 7 100 . 1 1 57 57 ALA H H 1 7.57 . . . . . . . . . . . 5858 7 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 7 102 . 1 1 58 58 LYS H H 1 8.55 . . . . . . . . . . . 5858 7 103 . 1 1 59 59 SER N N 15 115.4 . . . . . . . . . . . 5858 7 104 . 1 1 59 59 SER H H 1 7.75 . . . . . . . . . . . 5858 7 105 . 1 1 60 60 LEU N N 15 120.5 . . . . . . . . . . . 5858 7 106 . 1 1 60 60 LEU H H 1 6.90 . . . . . . . . . . . 5858 7 107 . 1 1 61 61 SER N N 15 111.2 . . . . . . . . . . . 5858 7 108 . 1 1 61 61 SER H H 1 6.97 . . . . . . . . . . . 5858 7 109 . 1 1 62 62 HIS N N 15 120.6 . . . . . . . . . . . 5858 7 110 . 1 1 62 62 HIS H H 1 9.63 . . . . . . . . . . . 5858 7 111 . 1 1 63 63 LYS N N 15 123.4 . . . . . . . . . . . 5858 7 112 . 1 1 63 63 LYS H H 1 8.79 . . . . . . . . . . . 5858 7 113 . 1 1 64 64 GLN N N 15 120.4 . . . . . . . . . . . 5858 7 114 . 1 1 64 64 GLN H H 1 8.39 . . . . . . . . . . . 5858 7 115 . 1 1 65 65 LEU N N 15 121.8 . . . . . . . . . . . 5858 7 116 . 1 1 65 65 LEU H H 1 8.23 . . . . . . . . . . . 5858 7 117 . 1 1 66 66 LEU N N 15 124.9 . . . . . . . . . . . 5858 7 118 . 1 1 66 66 LEU H H 1 9.48 . . . . . . . . . . . 5858 7 119 . 1 1 67 67 MET N N 15 122.0 . . . . . . . . . . . 5858 7 120 . 1 1 67 67 MET H H 1 8.11 . . . . . . . . . . . 5858 7 121 . 1 1 68 68 SER N N 15 113.7 . . . . . . . . . . . 5858 7 122 . 1 1 68 68 SER H H 1 8.38 . . . . . . . . . . . 5858 7 123 . 1 1 70 70 GLY N N 15 112.8 . . . . . . . . . . . 5858 7 124 . 1 1 70 70 GLY H H 1 9.02 . . . . . . . . . . . 5858 7 125 . 1 1 71 71 GLN N N 15 119.8 . . . . . . . . . . . 5858 7 126 . 1 1 71 71 GLN H H 1 7.51 . . . . . . . . . . . 5858 7 127 . 1 1 72 72 SER N N 15 115.8 . . . . . . . . . . . 5858 7 128 . 1 1 72 72 SER H H 1 8.67 . . . . . . . . . . . 5858 7 129 . 1 1 73 73 THR N N 15 116.3 . . . . . . . . . . . 5858 7 130 . 1 1 73 73 THR H H 1 8.74 . . . . . . . . . . . 5858 7 131 . 1 1 74 74 SER N N 15 118.3 . . . . . . . . . . . 5858 7 132 . 1 1 74 74 SER H H 1 8.16 . . . . . . . . . . . 5858 7 133 . 1 1 75 75 THR N N 15 121.0 . . . . . . . . . . . 5858 7 134 . 1 1 75 75 THR H H 1 9.55 . . . . . . . . . . . 5858 7 135 . 1 1 76 76 THR N N 15 127.2 . . . . . . . . . . . 5858 7 136 . 1 1 76 76 THR H H 1 9.12 . . . . . . . . . . . 5858 7 137 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 7 138 . 1 1 77 77 PHE H H 1 9.18 . . . . . . . . . . . 5858 7 139 . 1 1 79 79 ALA N N 15 123.1 . . . . . . . . . . . 5858 7 140 . 1 1 79 79 ALA H H 1 8.84 . . . . . . . . . . . 5858 7 141 . 1 1 80 80 ASP N N 15 113.2 . . . . . . . . . . . 5858 7 142 . 1 1 80 80 ASP H H 1 8.01 . . . . . . . . . . . 5858 7 143 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 7 144 . 1 1 81 81 ALA H H 1 7.58 . . . . . . . . . . . 5858 7 145 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 7 146 . 1 1 83 83 ALA H H 1 8.38 . . . . . . . . . . . 5858 7 147 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 7 148 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 7 149 . 1 1 85 85 GLU N N 15 119.8 . . . . . . . . . . . 5858 7 150 . 1 1 85 85 GLU H H 1 8.48 . . . . . . . . . . . 5858 7 151 . 1 1 86 86 TYR N N 15 125.5 . . . . . . . . . . . 5858 7 152 . 1 1 86 86 TYR H H 1 10.17 . . . . . . . . . . . 5858 7 153 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 7 154 . 1 1 87 87 THR H H 1 8.63 . . . . . . . . . . . 5858 7 155 . 1 1 88 88 PHE N N 15 126.2 . . . . . . . . . . . 5858 7 156 . 1 1 88 88 PHE H H 1 8.58 . . . . . . . . . . . 5858 7 157 . 1 1 89 89 TYR N N 15 115.3 . . . . . . . . . . . 5858 7 158 . 1 1 89 89 TYR H H 1 8.97 . . . . . . . . . . . 5858 7 159 . 1 1 90 90 CYS N N 15 125.1 . . . . . . . . . . . 5858 7 160 . 1 1 90 90 CYS H H 1 7.75 . . . . . . . . . . . 5858 7 161 . 1 1 91 91 GLU N N 15 125.7 . . . . . . . . . . . 5858 7 162 . 1 1 91 91 GLU H H 1 10.03 . . . . . . . . . . . 5858 7 163 . 1 1 93 93 HIS N N 15 115.1 . . . . . . . . . . . 5858 7 164 . 1 1 93 93 HIS H H 1 8.54 . . . . . . . . . . . 5858 7 165 . 1 1 94 94 ARG N N 15 129.1 . . . . . . . . . . . 5858 7 166 . 1 1 94 94 ARG H H 1 8.44 . . . . . . . . . . . 5858 7 167 . 1 1 95 95 GLY N N 15 107.7 . . . . . . . . . . . 5858 7 168 . 1 1 95 95 GLY H H 1 9.10 . . . . . . . . . . . 5858 7 169 . 1 1 96 96 ALA N N 15 121.6 . . . . . . . . . . . 5858 7 170 . 1 1 96 96 ALA H H 1 7.54 . . . . . . . . . . . 5858 7 171 . 1 1 97 97 GLY N N 15 106.4 . . . . . . . . . . . 5858 7 172 . 1 1 97 97 GLY H H 1 8.08 . . . . . . . . . . . 5858 7 173 . 1 1 98 98 MET N N 15 123.9 . . . . . . . . . . . 5858 7 174 . 1 1 98 98 MET H H 1 7.61 . . . . . . . . . . . 5858 7 175 . 1 1 99 99 VAL N N 15 126.0 . . . . . . . . . . . 5858 7 176 . 1 1 99 99 VAL H H 1 7.96 . . . . . . . . . . . 5858 7 177 . 1 1 100 100 GLY N N 15 118.0 . . . . . . . . . . . 5858 7 178 . 1 1 100 100 GLY H H 1 8.97 . . . . . . . . . . . 5858 7 179 . 1 1 101 101 LYS N N 15 117.6 . . . . . . . . . . . 5858 7 180 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 7 181 . 1 1 102 102 ILE N N 15 127.4 . . . . . . . . . . . 5858 7 182 . 1 1 102 102 ILE H H 1 9.47 . . . . . . . . . . . 5858 7 183 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 7 184 . 1 1 103 103 THR H H 1 9.27 . . . . . . . . . . . 5858 7 185 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 7 186 . 1 1 104 104 VAL H H 1 9.32 . . . . . . . . . . . 5858 7 187 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 7 188 . 1 1 105 105 ALA H H 1 9.25 . . . . . . . . . . . 5858 7 189 . 1 1 106 106 GLY N N 15 113.8 . . . . . . . . . . . 5858 7 190 . 1 1 106 106 GLY H H 1 7.81 . . . . . . . . . . . 5858 7 stop_ save_ save_shift_set_8 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_8 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 8 _Assigned_chem_shift_list.Sample_condition_list_ID 8 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_8 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 8 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.5 . . . . . . . . . . . 5858 8 2 . 1 1 3 3 THR H H 1 8.79 . . . . . . . . . . . 5858 8 3 . 1 1 4 4 TYR N N 15 127.1 . . . . . . . . . . . 5858 8 4 . 1 1 4 4 TYR H H 1 8.85 . . . . . . . . . . . 5858 8 5 . 1 1 5 5 THR N N 15 118.2 . . . . . . . . . . . 5858 8 6 . 1 1 5 5 THR H H 1 8.62 . . . . . . . . . . . 5858 8 7 . 1 1 6 6 VAL N N 15 129.5 . . . . . . . . . . . 5858 8 8 . 1 1 6 6 VAL H H 1 9.29 . . . . . . . . . . . 5858 8 9 . 1 1 7 7 LYS N N 15 126.6 . . . . . . . . . . . 5858 8 10 . 1 1 7 7 LYS H H 1 9.10 . . . . . . . . . . . 5858 8 11 . 1 1 8 8 LEU N N 15 121.7 . . . . . . . . . . . 5858 8 12 . 1 1 8 8 LEU H H 1 8.86 . . . . . . . . . . . 5858 8 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 8 14 . 1 1 9 9 GLY H H 1 7.62 . . . . . . . . . . . 5858 8 15 . 1 1 10 10 SER N N 15 119.8 . . . . . . . . . . . 5858 8 16 . 1 1 10 10 SER H H 1 8.70 . . . . . . . . . . . 5858 8 17 . 1 1 11 11 ASP N N 15 120.9 . . . . . . . . . . . 5858 8 18 . 1 1 11 11 ASP H H 1 9.46 . . . . . . . . . . . 5858 8 19 . 1 1 12 12 LYS N N 15 115.9 . . . . . . . . . . . 5858 8 20 . 1 1 12 12 LYS H H 1 7.51 . . . . . . . . . . . 5858 8 21 . 1 1 13 13 GLY N N 15 108.8 . . . . . . . . . . . 5858 8 22 . 1 1 13 13 GLY H H 1 8.31 . . . . . . . . . . . 5858 8 23 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 8 24 . 1 1 14 14 LEU H H 1 7.47 . . . . . . . . . . . 5858 8 25 . 1 1 15 15 LEU N N 15 125.2 . . . . . . . . . . . 5858 8 26 . 1 1 15 15 LEU H H 1 8.50 . . . . . . . . . . . 5858 8 27 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 8 28 . 1 1 16 16 VAL H H 1 7.53 . . . . . . . . . . . 5858 8 29 . 1 1 17 17 PHE N N 15 120.4 . . . . . . . . . . . 5858 8 30 . 1 1 17 17 PHE H H 1 8.73 . . . . . . . . . . . 5858 8 31 . 1 1 18 18 GLU N N 15 122.3 . . . . . . . . . . . 5858 8 32 . 1 1 18 18 GLU H H 1 9.00 . . . . . . . . . . . 5858 8 33 . 1 1 20 20 ALA N N 15 116.9 . . . . . . . . . . . 5858 8 34 . 1 1 20 20 ALA H H 1 8.10 . . . . . . . . . . . 5858 8 35 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 8 36 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 8 37 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 8 38 . 1 1 22 22 LEU H H 1 7.76 . . . . . . . . . . . 5858 8 39 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 8 40 . 1 1 23 23 THR H H 1 8.23 . . . . . . . . . . . 5858 8 41 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 8 42 . 1 1 24 24 ILE H H 1 8.93 . . . . . . . . . . . 5858 8 43 . 1 1 25 25 LYS N N 15 119.6 . . . . . . . . . . . 5858 8 44 . 1 1 25 25 LYS H H 1 8.96 . . . . . . . . . . . 5858 8 45 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 8 46 . 1 1 27 27 GLY H H 1 7.11 . . . . . . . . . . . 5858 8 47 . 1 1 28 28 ASP N N 15 119.8 . . . . . . . . . . . 5858 8 48 . 1 1 28 28 ASP H H 1 7.91 . . . . . . . . . . . 5858 8 49 . 1 1 29 29 THR N N 15 114.7 . . . . . . . . . . . 5858 8 50 . 1 1 29 29 THR H H 1 8.66 . . . . . . . . . . . 5858 8 51 . 1 1 30 30 VAL N N 15 126.4 . . . . . . . . . . . 5858 8 52 . 1 1 30 30 VAL H H 1 9.16 . . . . . . . . . . . 5858 8 53 . 1 1 31 31 GLU N N 15 128.6 . . . . . . . . . . . 5858 8 54 . 1 1 31 31 GLU H H 1 9.24 . . . . . . . . . . . 5858 8 55 . 1 1 32 32 PHE N N 15 126.0 . . . . . . . . . . . 5858 8 56 . 1 1 32 32 PHE H H 1 9.18 . . . . . . . . . . . 5858 8 57 . 1 1 33 33 LEU N N 15 125.3 . . . . . . . . . . . 5858 8 58 . 1 1 33 33 LEU H H 1 8.96 . . . . . . . . . . . 5858 8 59 . 1 1 34 34 ASN N N 15 127.3 . . . . . . . . . . . 5858 8 60 . 1 1 34 34 ASN H H 1 9.35 . . . . . . . . . . . 5858 8 61 . 1 1 35 35 ASN N N 15 129.6 . . . . . . . . . . . 5858 8 62 . 1 1 35 35 ASN H H 1 8.73 . . . . . . . . . . . 5858 8 63 . 1 1 36 36 LYS N N 15 116.8 . . . . . . . . . . . 5858 8 64 . 1 1 36 36 LYS H H 1 8.16 . . . . . . . . . . . 5858 8 65 . 1 1 37 37 VAL N N 15 116.0 . . . . . . . . . . . 5858 8 66 . 1 1 37 37 VAL H H 1 9.00 . . . . . . . . . . . 5858 8 67 . 1 1 40 40 HIS N N 15 112.0 . . . . . . . . . . . 5858 8 68 . 1 1 40 40 HIS H H 1 7.27 . . . . . . . . . . . 5858 8 69 . 1 1 41 41 ASN N N 15 122.7 . . . . . . . . . . . 5858 8 70 . 1 1 41 41 ASN H H 1 9.74 . . . . . . . . . . . 5858 8 71 . 1 1 42 42 VAL N N 15 109.1 . . . . . . . . . . . 5858 8 72 . 1 1 42 42 VAL H H 1 6.95 . . . . . . . . . . . 5858 8 73 . 1 1 43 43 VAL N N 15 128.5 . . . . . . . . . . . 5858 8 74 . 1 1 43 43 VAL H H 1 9.41 . . . . . . . . . . . 5858 8 75 . 1 1 44 44 PHE N N 15 125.6 . . . . . . . . . . . 5858 8 76 . 1 1 44 44 PHE H H 1 8.74 . . . . . . . . . . . 5858 8 77 . 1 1 45 45 ASP N N 15 124.0 . . . . . . . . . . . 5858 8 78 . 1 1 45 45 ASP H H 1 8.40 . . . . . . . . . . . 5858 8 79 . 1 1 46 46 ALA N N 15 128.2 . . . . . . . . . . . 5858 8 80 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 8 81 . 1 1 47 47 ALA N N 15 117.6 . . . . . . . . . . . 5858 8 82 . 1 1 47 47 ALA H H 1 8.46 . . . . . . . . . . . 5858 8 83 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 8 84 . 1 1 48 48 LEU H H 1 8.66 . . . . . . . . . . . 5858 8 85 . 1 1 49 49 ASN N N 15 114.6 . . . . . . . . . . . 5858 8 86 . 1 1 49 49 ASN H H 1 8.06 . . . . . . . . . . . 5858 8 87 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 8 88 . 1 1 51 51 ALA H H 1 7.00 . . . . . . . . . . . 5858 8 89 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 8 90 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 8 91 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 8 92 . 1 1 53 53 SER H H 1 8.22 . . . . . . . . . . . 5858 8 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 8 94 . 1 1 54 54 ALA H H 1 9.19 . . . . . . . . . . . 5858 8 95 . 1 1 55 55 ASP N N 15 120.0 . . . . . . . . . . . 5858 8 96 . 1 1 55 55 ASP H H 1 8.42 . . . . . . . . . . . 5858 8 97 . 1 1 56 56 LEU N N 15 123.7 . . . . . . . . . . . 5858 8 98 . 1 1 56 56 LEU H H 1 8.15 . . . . . . . . . . . 5858 8 99 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 8 100 . 1 1 57 57 ALA H H 1 7.58 . . . . . . . . . . . 5858 8 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 8 102 . 1 1 58 58 LYS H H 1 8.55 . . . . . . . . . . . 5858 8 103 . 1 1 59 59 SER N N 15 115.4 . . . . . . . . . . . 5858 8 104 . 1 1 59 59 SER H H 1 7.74 . . . . . . . . . . . 5858 8 105 . 1 1 60 60 LEU N N 15 120.5 . . . . . . . . . . . 5858 8 106 . 1 1 60 60 LEU H H 1 6.90 . . . . . . . . . . . 5858 8 107 . 1 1 61 61 SER N N 15 111.2 . . . . . . . . . . . 5858 8 108 . 1 1 61 61 SER H H 1 6.97 . . . . . . . . . . . 5858 8 109 . 1 1 62 62 HIS N N 15 120.4 . . . . . . . . . . . 5858 8 110 . 1 1 62 62 HIS H H 1 9.61 . . . . . . . . . . . 5858 8 111 . 1 1 63 63 LYS N N 15 123.5 . . . . . . . . . . . 5858 8 112 . 1 1 63 63 LYS H H 1 8.82 . . . . . . . . . . . 5858 8 113 . 1 1 64 64 GLN N N 15 120.5 . . . . . . . . . . . 5858 8 114 . 1 1 64 64 GLN H H 1 8.41 . . . . . . . . . . . 5858 8 115 . 1 1 65 65 LEU N N 15 121.8 . . . . . . . . . . . 5858 8 116 . 1 1 65 65 LEU H H 1 8.25 . . . . . . . . . . . 5858 8 117 . 1 1 66 66 LEU N N 15 124.8 . . . . . . . . . . . 5858 8 118 . 1 1 66 66 LEU H H 1 9.44 . . . . . . . . . . . 5858 8 119 . 1 1 67 67 MET N N 15 122.0 . . . . . . . . . . . 5858 8 120 . 1 1 67 67 MET H H 1 8.13 . . . . . . . . . . . 5858 8 121 . 1 1 68 68 SER N N 15 113.9 . . . . . . . . . . . 5858 8 122 . 1 1 68 68 SER H H 1 8.38 . . . . . . . . . . . 5858 8 123 . 1 1 70 70 GLY N N 15 112.8 . . . . . . . . . . . 5858 8 124 . 1 1 70 70 GLY H H 1 9.00 . . . . . . . . . . . 5858 8 125 . 1 1 71 71 GLN N N 15 119.8 . . . . . . . . . . . 5858 8 126 . 1 1 71 71 GLN H H 1 7.51 . . . . . . . . . . . 5858 8 127 . 1 1 72 72 SER N N 15 115.8 . . . . . . . . . . . 5858 8 128 . 1 1 72 72 SER H H 1 8.68 . . . . . . . . . . . 5858 8 129 . 1 1 73 73 THR N N 15 116.1 . . . . . . . . . . . 5858 8 130 . 1 1 73 73 THR H H 1 8.73 . . . . . . . . . . . 5858 8 131 . 1 1 74 74 SER N N 15 118.3 . . . . . . . . . . . 5858 8 132 . 1 1 74 74 SER H H 1 8.16 . . . . . . . . . . . 5858 8 133 . 1 1 75 75 THR N N 15 121.0 . . . . . . . . . . . 5858 8 134 . 1 1 75 75 THR H H 1 9.53 . . . . . . . . . . . 5858 8 135 . 1 1 76 76 THR N N 15 127.2 . . . . . . . . . . . 5858 8 136 . 1 1 76 76 THR H H 1 9.12 . . . . . . . . . . . 5858 8 137 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 8 138 . 1 1 77 77 PHE H H 1 9.17 . . . . . . . . . . . 5858 8 139 . 1 1 79 79 ALA N N 15 123.2 . . . . . . . . . . . 5858 8 140 . 1 1 79 79 ALA H H 1 8.83 . . . . . . . . . . . 5858 8 141 . 1 1 80 80 ASP N N 15 113.1 . . . . . . . . . . . 5858 8 142 . 1 1 80 80 ASP H H 1 7.99 . . . . . . . . . . . 5858 8 143 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 8 144 . 1 1 81 81 ALA H H 1 7.58 . . . . . . . . . . . 5858 8 145 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 8 146 . 1 1 83 83 ALA H H 1 8.38 . . . . . . . . . . . 5858 8 147 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 8 148 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 8 149 . 1 1 85 85 GLU N N 15 119.7 . . . . . . . . . . . 5858 8 150 . 1 1 85 85 GLU H H 1 8.49 . . . . . . . . . . . 5858 8 151 . 1 1 86 86 TYR N N 15 125.5 . . . . . . . . . . . 5858 8 152 . 1 1 86 86 TYR H H 1 10.17 . . . . . . . . . . . 5858 8 153 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 8 154 . 1 1 87 87 THR H H 1 8.63 . . . . . . . . . . . 5858 8 155 . 1 1 88 88 PHE N N 15 126.1 . . . . . . . . . . . 5858 8 156 . 1 1 88 88 PHE H H 1 8.58 . . . . . . . . . . . 5858 8 157 . 1 1 89 89 TYR N N 15 115.2 . . . . . . . . . . . 5858 8 158 . 1 1 89 89 TYR H H 1 8.99 . . . . . . . . . . . 5858 8 159 . 1 1 90 90 CYS N N 15 124.8 . . . . . . . . . . . 5858 8 160 . 1 1 90 90 CYS H H 1 7.76 . . . . . . . . . . . 5858 8 161 . 1 1 91 91 GLU N N 15 125.7 . . . . . . . . . . . 5858 8 162 . 1 1 91 91 GLU H H 1 10.03 . . . . . . . . . . . 5858 8 163 . 1 1 94 94 ARG N N 15 128.9 . . . . . . . . . . . 5858 8 164 . 1 1 94 94 ARG H H 1 8.37 . . . . . . . . . . . 5858 8 165 . 1 1 95 95 GLY N N 15 107.7 . . . . . . . . . . . 5858 8 166 . 1 1 95 95 GLY H H 1 9.08 . . . . . . . . . . . 5858 8 167 . 1 1 96 96 ALA N N 15 121.4 . . . . . . . . . . . 5858 8 168 . 1 1 96 96 ALA H H 1 7.50 . . . . . . . . . . . 5858 8 169 . 1 1 97 97 GLY N N 15 106.3 . . . . . . . . . . . 5858 8 170 . 1 1 97 97 GLY H H 1 8.11 . . . . . . . . . . . 5858 8 171 . 1 1 98 98 MET N N 15 123.4 . . . . . . . . . . . 5858 8 172 . 1 1 98 98 MET H H 1 7.56 . . . . . . . . . . . 5858 8 173 . 1 1 99 99 VAL N N 15 126.2 . . . . . . . . . . . 5858 8 174 . 1 1 99 99 VAL H H 1 7.96 . . . . . . . . . . . 5858 8 175 . 1 1 100 100 GLY N N 15 117.9 . . . . . . . . . . . 5858 8 176 . 1 1 100 100 GLY H H 1 8.95 . . . . . . . . . . . 5858 8 177 . 1 1 101 101 LYS N N 15 117.6 . . . . . . . . . . . 5858 8 178 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 8 179 . 1 1 102 102 ILE N N 15 127.4 . . . . . . . . . . . 5858 8 180 . 1 1 102 102 ILE H H 1 9.47 . . . . . . . . . . . 5858 8 181 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 8 182 . 1 1 103 103 THR H H 1 9.27 . . . . . . . . . . . 5858 8 183 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 8 184 . 1 1 104 104 VAL H H 1 9.33 . . . . . . . . . . . 5858 8 185 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 8 186 . 1 1 105 105 ALA H H 1 9.24 . . . . . . . . . . . 5858 8 187 . 1 1 106 106 GLY N N 15 113.7 . . . . . . . . . . . 5858 8 188 . 1 1 106 106 GLY H H 1 7.82 . . . . . . . . . . . 5858 8 stop_ save_ save_shift_set_9 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_9 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 9 _Assigned_chem_shift_list.Sample_condition_list_ID 9 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_9 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 9 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.4 . . . . . . . . . . . 5858 9 2 . 1 1 3 3 THR H H 1 8.78 . . . . . . . . . . . 5858 9 3 . 1 1 4 4 TYR N N 15 127.1 . . . . . . . . . . . 5858 9 4 . 1 1 4 4 TYR H H 1 8.86 . . . . . . . . . . . 5858 9 5 . 1 1 5 5 THR N N 15 118.1 . . . . . . . . . . . 5858 9 6 . 1 1 5 5 THR H H 1 8.63 . . . . . . . . . . . 5858 9 7 . 1 1 6 6 VAL N N 15 129.4 . . . . . . . . . . . 5858 9 8 . 1 1 6 6 VAL H H 1 9.28 . . . . . . . . . . . 5858 9 9 . 1 1 7 7 LYS N N 15 126.6 . . . . . . . . . . . 5858 9 10 . 1 1 7 7 LYS H H 1 9.11 . . . . . . . . . . . 5858 9 11 . 1 1 8 8 LEU N N 15 121.6 . . . . . . . . . . . 5858 9 12 . 1 1 8 8 LEU H H 1 8.87 . . . . . . . . . . . 5858 9 13 . 1 1 9 9 GLY N N 15 114.8 . . . . . . . . . . . 5858 9 14 . 1 1 9 9 GLY H H 1 7.59 . . . . . . . . . . . 5858 9 15 . 1 1 10 10 SER N N 15 119.8 . . . . . . . . . . . 5858 9 16 . 1 1 10 10 SER H H 1 8.72 . . . . . . . . . . . 5858 9 17 . 1 1 11 11 ASP N N 15 120.9 . . . . . . . . . . . 5858 9 18 . 1 1 11 11 ASP H H 1 9.42 . . . . . . . . . . . 5858 9 19 . 1 1 12 12 LYS N N 15 115.9 . . . . . . . . . . . 5858 9 20 . 1 1 12 12 LYS H H 1 7.50 . . . . . . . . . . . 5858 9 21 . 1 1 13 13 GLY N N 15 108.7 . . . . . . . . . . . 5858 9 22 . 1 1 13 13 GLY H H 1 8.30 . . . . . . . . . . . 5858 9 23 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 9 24 . 1 1 14 14 LEU H H 1 7.48 . . . . . . . . . . . 5858 9 25 . 1 1 15 15 LEU N N 15 125.4 . . . . . . . . . . . 5858 9 26 . 1 1 15 15 LEU H H 1 8.57 . . . . . . . . . . . 5858 9 27 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 9 28 . 1 1 16 16 VAL H H 1 7.56 . . . . . . . . . . . 5858 9 29 . 1 1 17 17 PHE N N 15 120.8 . . . . . . . . . . . 5858 9 30 . 1 1 17 17 PHE H H 1 8.78 . . . . . . . . . . . 5858 9 31 . 1 1 18 18 GLU N N 15 122.4 . . . . . . . . . . . 5858 9 32 . 1 1 18 18 GLU H H 1 9.00 . . . . . . . . . . . 5858 9 33 . 1 1 20 20 ALA N N 15 116.6 . . . . . . . . . . . 5858 9 34 . 1 1 20 20 ALA H H 1 8.04 . . . . . . . . . . . 5858 9 35 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 9 36 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 9 37 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 9 38 . 1 1 22 22 LEU H H 1 7.75 . . . . . . . . . . . 5858 9 39 . 1 1 23 23 THR N N 15 121.2 . . . . . . . . . . . 5858 9 40 . 1 1 23 23 THR H H 1 8.23 . . . . . . . . . . . 5858 9 41 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 9 42 . 1 1 24 24 ILE H H 1 8.93 . . . . . . . . . . . 5858 9 43 . 1 1 25 25 LYS N N 15 119.5 . . . . . . . . . . . 5858 9 44 . 1 1 25 25 LYS H H 1 8.94 . . . . . . . . . . . 5858 9 45 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 9 46 . 1 1 27 27 GLY H H 1 7.11 . . . . . . . . . . . 5858 9 47 . 1 1 28 28 ASP N N 15 119.8 . . . . . . . . . . . 5858 9 48 . 1 1 28 28 ASP H H 1 7.91 . . . . . . . . . . . 5858 9 49 . 1 1 29 29 THR N N 15 114.7 . . . . . . . . . . . 5858 9 50 . 1 1 29 29 THR H H 1 8.64 . . . . . . . . . . . 5858 9 51 . 1 1 30 30 VAL N N 15 126.4 . . . . . . . . . . . 5858 9 52 . 1 1 30 30 VAL H H 1 9.18 . . . . . . . . . . . 5858 9 53 . 1 1 31 31 GLU N N 15 128.5 . . . . . . . . . . . 5858 9 54 . 1 1 31 31 GLU H H 1 9.25 . . . . . . . . . . . 5858 9 55 . 1 1 32 32 PHE N N 15 126.1 . . . . . . . . . . . 5858 9 56 . 1 1 32 32 PHE H H 1 9.20 . . . . . . . . . . . 5858 9 57 . 1 1 33 33 LEU N N 15 125.2 . . . . . . . . . . . 5858 9 58 . 1 1 33 33 LEU H H 1 8.95 . . . . . . . . . . . 5858 9 59 . 1 1 34 34 ASN N N 15 127.2 . . . . . . . . . . . 5858 9 60 . 1 1 34 34 ASN H H 1 9.36 . . . . . . . . . . . 5858 9 61 . 1 1 35 35 ASN N N 15 129.6 . . . . . . . . . . . 5858 9 62 . 1 1 35 35 ASN H H 1 8.68 . . . . . . . . . . . 5858 9 63 . 1 1 36 36 LYS N N 15 116.9 . . . . . . . . . . . 5858 9 64 . 1 1 36 36 LYS H H 1 8.13 . . . . . . . . . . . 5858 9 65 . 1 1 37 37 VAL N N 15 116.3 . . . . . . . . . . . 5858 9 66 . 1 1 37 37 VAL H H 1 9.04 . . . . . . . . . . . 5858 9 67 . 1 1 40 40 HIS N N 15 111.7 . . . . . . . . . . . 5858 9 68 . 1 1 40 40 HIS H H 1 7.33 . . . . . . . . . . . 5858 9 69 . 1 1 41 41 ASN N N 15 122.5 . . . . . . . . . . . 5858 9 70 . 1 1 41 41 ASN H H 1 9.65 . . . . . . . . . . . 5858 9 71 . 1 1 42 42 VAL N N 15 109.2 . . . . . . . . . . . 5858 9 72 . 1 1 42 42 VAL H H 1 6.96 . . . . . . . . . . . 5858 9 73 . 1 1 43 43 VAL N N 15 128.5 . . . . . . . . . . . 5858 9 74 . 1 1 43 43 VAL H H 1 9.38 . . . . . . . . . . . 5858 9 75 . 1 1 44 44 PHE N N 15 125.7 . . . . . . . . . . . 5858 9 76 . 1 1 44 44 PHE H H 1 8.76 . . . . . . . . . . . 5858 9 77 . 1 1 45 45 ASP N N 15 124.1 . . . . . . . . . . . 5858 9 78 . 1 1 45 45 ASP H H 1 8.40 . . . . . . . . . . . 5858 9 79 . 1 1 46 46 ALA N N 15 128.3 . . . . . . . . . . . 5858 9 80 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 9 81 . 1 1 47 47 ALA N N 15 117.5 . . . . . . . . . . . 5858 9 82 . 1 1 47 47 ALA H H 1 8.47 . . . . . . . . . . . 5858 9 83 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 9 84 . 1 1 48 48 LEU H H 1 8.65 . . . . . . . . . . . 5858 9 85 . 1 1 49 49 ASN N N 15 114.6 . . . . . . . . . . . 5858 9 86 . 1 1 49 49 ASN H H 1 8.06 . . . . . . . . . . . 5858 9 87 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 9 88 . 1 1 51 51 ALA H H 1 7.01 . . . . . . . . . . . 5858 9 89 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 9 90 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 9 91 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 9 92 . 1 1 53 53 SER H H 1 8.22 . . . . . . . . . . . 5858 9 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 9 94 . 1 1 54 54 ALA H H 1 9.19 . . . . . . . . . . . 5858 9 95 . 1 1 55 55 ASP N N 15 120.0 . . . . . . . . . . . 5858 9 96 . 1 1 55 55 ASP H H 1 8.43 . . . . . . . . . . . 5858 9 97 . 1 1 56 56 LEU N N 15 123.8 . . . . . . . . . . . 5858 9 98 . 1 1 56 56 LEU H H 1 8.15 . . . . . . . . . . . 5858 9 99 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 9 100 . 1 1 57 57 ALA H H 1 7.59 . . . . . . . . . . . 5858 9 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 9 102 . 1 1 58 58 LYS H H 1 8.55 . . . . . . . . . . . 5858 9 103 . 1 1 59 59 SER N N 15 115.4 . . . . . . . . . . . 5858 9 104 . 1 1 59 59 SER H H 1 7.75 . . . . . . . . . . . 5858 9 105 . 1 1 60 60 LEU N N 15 120.5 . . . . . . . . . . . 5858 9 106 . 1 1 60 60 LEU H H 1 6.90 . . . . . . . . . . . 5858 9 107 . 1 1 61 61 SER N N 15 111.2 . . . . . . . . . . . 5858 9 108 . 1 1 61 61 SER H H 1 6.98 . . . . . . . . . . . 5858 9 109 . 1 1 62 62 HIS N N 15 120.3 . . . . . . . . . . . 5858 9 110 . 1 1 62 62 HIS H H 1 9.59 . . . . . . . . . . . 5858 9 111 . 1 1 63 63 LYS N N 15 123.6 . . . . . . . . . . . 5858 9 112 . 1 1 63 63 LYS H H 1 8.85 . . . . . . . . . . . 5858 9 113 . 1 1 64 64 GLN N N 15 120.6 . . . . . . . . . . . 5858 9 114 . 1 1 64 64 GLN H H 1 8.44 . . . . . . . . . . . 5858 9 115 . 1 1 65 65 LEU N N 15 121.8 . . . . . . . . . . . 5858 9 116 . 1 1 65 65 LEU H H 1 8.27 . . . . . . . . . . . 5858 9 117 . 1 1 66 66 LEU N N 15 124.7 . . . . . . . . . . . 5858 9 118 . 1 1 66 66 LEU H H 1 9.41 . . . . . . . . . . . 5858 9 119 . 1 1 67 67 MET N N 15 122.0 . . . . . . . . . . . 5858 9 120 . 1 1 67 67 MET H H 1 8.16 . . . . . . . . . . . 5858 9 121 . 1 1 68 68 SER N N 15 114.2 . . . . . . . . . . . 5858 9 122 . 1 1 68 68 SER H H 1 8.41 . . . . . . . . . . . 5858 9 123 . 1 1 70 70 GLY N N 15 112.7 . . . . . . . . . . . 5858 9 124 . 1 1 70 70 GLY H H 1 8.98 . . . . . . . . . . . 5858 9 125 . 1 1 71 71 GLN N N 15 119.8 . . . . . . . . . . . 5858 9 126 . 1 1 71 71 GLN H H 1 7.51 . . . . . . . . . . . 5858 9 127 . 1 1 72 72 SER N N 15 115.7 . . . . . . . . . . . 5858 9 128 . 1 1 72 72 SER H H 1 8.68 . . . . . . . . . . . 5858 9 129 . 1 1 73 73 THR N N 15 115.8 . . . . . . . . . . . 5858 9 130 . 1 1 73 73 THR H H 1 8.74 . . . . . . . . . . . 5858 9 131 . 1 1 74 74 SER N N 15 118.4 . . . . . . . . . . . 5858 9 132 . 1 1 74 74 SER H H 1 8.16 . . . . . . . . . . . 5858 9 133 . 1 1 75 75 THR N N 15 121.0 . . . . . . . . . . . 5858 9 134 . 1 1 75 75 THR H H 1 9.51 . . . . . . . . . . . 5858 9 135 . 1 1 76 76 THR N N 15 127.2 . . . . . . . . . . . 5858 9 136 . 1 1 76 76 THR H H 1 9.13 . . . . . . . . . . . 5858 9 137 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 9 138 . 1 1 77 77 PHE H H 1 9.17 . . . . . . . . . . . 5858 9 139 . 1 1 79 79 ALA N N 15 123.2 . . . . . . . . . . . 5858 9 140 . 1 1 79 79 ALA H H 1 8.83 . . . . . . . . . . . 5858 9 141 . 1 1 80 80 ASP N N 15 113.0 . . . . . . . . . . . 5858 9 142 . 1 1 80 80 ASP H H 1 7.98 . . . . . . . . . . . 5858 9 143 . 1 1 81 81 ALA N N 15 124.7 . . . . . . . . . . . 5858 9 144 . 1 1 81 81 ALA H H 1 7.59 . . . . . . . . . . . 5858 9 145 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 9 146 . 1 1 83 83 ALA H H 1 8.39 . . . . . . . . . . . 5858 9 147 . 1 1 84 84 GLY N N 15 107.3 . . . . . . . . . . . 5858 9 148 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 9 149 . 1 1 85 85 GLU N N 15 119.7 . . . . . . . . . . . 5858 9 150 . 1 1 85 85 GLU H H 1 8.49 . . . . . . . . . . . 5858 9 151 . 1 1 86 86 TYR N N 15 125.5 . . . . . . . . . . . 5858 9 152 . 1 1 86 86 TYR H H 1 10.17 . . . . . . . . . . . 5858 9 153 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 9 154 . 1 1 87 87 THR H H 1 8.64 . . . . . . . . . . . 5858 9 155 . 1 1 88 88 PHE N N 15 126.0 . . . . . . . . . . . 5858 9 156 . 1 1 88 88 PHE H H 1 8.57 . . . . . . . . . . . 5858 9 157 . 1 1 89 89 TYR N N 15 115.2 . . . . . . . . . . . 5858 9 158 . 1 1 89 89 TYR H H 1 9.03 . . . . . . . . . . . 5858 9 159 . 1 1 90 90 CYS N N 15 124.5 . . . . . . . . . . . 5858 9 160 . 1 1 90 90 CYS H H 1 7.77 . . . . . . . . . . . 5858 9 161 . 1 1 91 91 GLU N N 15 125.8 . . . . . . . . . . . 5858 9 162 . 1 1 91 91 GLU H H 1 10.04 . . . . . . . . . . . 5858 9 163 . 1 1 93 93 HIS N N 15 113.4 . . . . . . . . . . . 5858 9 164 . 1 1 93 93 HIS H H 1 8.32 . . . . . . . . . . . 5858 9 165 . 1 1 94 94 ARG N N 15 128.7 . . . . . . . . . . . 5858 9 166 . 1 1 94 94 ARG H H 1 8.29 . . . . . . . . . . . 5858 9 167 . 1 1 95 95 GLY N N 15 107.8 . . . . . . . . . . . 5858 9 168 . 1 1 95 95 GLY H H 1 9.07 . . . . . . . . . . . 5858 9 169 . 1 1 96 96 ALA N N 15 121.3 . . . . . . . . . . . 5858 9 170 . 1 1 96 96 ALA H H 1 7.46 . . . . . . . . . . . 5858 9 171 . 1 1 97 97 GLY N N 15 106.2 . . . . . . . . . . . 5858 9 172 . 1 1 97 97 GLY H H 1 8.13 . . . . . . . . . . . 5858 9 173 . 1 1 98 98 MET N N 15 122.9 . . . . . . . . . . . 5858 9 174 . 1 1 98 98 MET H H 1 7.51 . . . . . . . . . . . 5858 9 175 . 1 1 99 99 VAL N N 15 126.4 . . . . . . . . . . . 5858 9 176 . 1 1 99 99 VAL H H 1 7.98 . . . . . . . . . . . 5858 9 177 . 1 1 100 100 GLY N N 15 117.8 . . . . . . . . . . . 5858 9 178 . 1 1 100 100 GLY H H 1 8.94 . . . . . . . . . . . 5858 9 179 . 1 1 101 101 LYS N N 15 117.7 . . . . . . . . . . . 5858 9 180 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 9 181 . 1 1 102 102 ILE N N 15 127.4 . . . . . . . . . . . 5858 9 182 . 1 1 102 102 ILE H H 1 9.47 . . . . . . . . . . . 5858 9 183 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 9 184 . 1 1 103 103 THR H H 1 9.26 . . . . . . . . . . . 5858 9 185 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 9 186 . 1 1 104 104 VAL H H 1 9.33 . . . . . . . . . . . 5858 9 187 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 9 188 . 1 1 105 105 ALA H H 1 9.24 . . . . . . . . . . . 5858 9 189 . 1 1 106 106 GLY N N 15 113.5 . . . . . . . . . . . 5858 9 190 . 1 1 106 106 GLY H H 1 7.84 . . . . . . . . . . . 5858 9 stop_ save_ save_shift_set_10 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_10 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 10 _Assigned_chem_shift_list.Sample_condition_list_ID 10 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_10 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 10 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.2 . . . . . . . . . . . 5858 10 2 . 1 1 3 3 THR H H 1 8.76 . . . . . . . . . . . 5858 10 3 . 1 1 4 4 TYR N N 15 127.1 . . . . . . . . . . . 5858 10 4 . 1 1 4 4 TYR H H 1 8.87 . . . . . . . . . . . 5858 10 5 . 1 1 5 5 THR N N 15 117.9 . . . . . . . . . . . 5858 10 6 . 1 1 5 5 THR H H 1 8.64 . . . . . . . . . . . 5858 10 7 . 1 1 6 6 VAL N N 15 129.3 . . . . . . . . . . . 5858 10 8 . 1 1 6 6 VAL H H 1 9.27 . . . . . . . . . . . 5858 10 9 . 1 1 7 7 LYS N N 15 126.7 . . . . . . . . . . . 5858 10 10 . 1 1 7 7 LYS H H 1 9.12 . . . . . . . . . . . 5858 10 11 . 1 1 8 8 LEU N N 15 121.5 . . . . . . . . . . . 5858 10 12 . 1 1 8 8 LEU H H 1 8.87 . . . . . . . . . . . 5858 10 13 . 1 1 9 9 GLY N N 15 114.8 . . . . . . . . . . . 5858 10 14 . 1 1 9 9 GLY H H 1 7.54 . . . . . . . . . . . 5858 10 15 . 1 1 10 10 SER N N 15 119.8 . . . . . . . . . . . 5858 10 16 . 1 1 10 10 SER H H 1 8.75 . . . . . . . . . . . 5858 10 17 . 1 1 11 11 ASP N N 15 120.8 . . . . . . . . . . . 5858 10 18 . 1 1 11 11 ASP H H 1 9.35 . . . . . . . . . . . 5858 10 19 . 1 1 12 12 LYS N N 15 115.9 . . . . . . . . . . . 5858 10 20 . 1 1 12 12 LYS H H 1 7.50 . . . . . . . . . . . 5858 10 21 . 1 1 13 13 GLY N N 15 108.6 . . . . . . . . . . . 5858 10 22 . 1 1 13 13 GLY H H 1 8.28 . . . . . . . . . . . 5858 10 23 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 10 24 . 1 1 14 14 LEU H H 1 7.49 . . . . . . . . . . . 5858 10 25 . 1 1 15 15 LEU N N 15 125.5 . . . . . . . . . . . 5858 10 26 . 1 1 15 15 LEU H H 1 8.63 . . . . . . . . . . . 5858 10 27 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 10 28 . 1 1 16 16 VAL H H 1 7.59 . . . . . . . . . . . 5858 10 29 . 1 1 17 17 PHE N N 15 121.0 . . . . . . . . . . . 5858 10 30 . 1 1 17 17 PHE H H 1 8.83 . . . . . . . . . . . 5858 10 31 . 1 1 18 18 GLU N N 15 122.5 . . . . . . . . . . . 5858 10 32 . 1 1 18 18 GLU H H 1 9.00 . . . . . . . . . . . 5858 10 33 . 1 1 20 20 ALA N N 15 116.5 . . . . . . . . . . . 5858 10 34 . 1 1 20 20 ALA H H 1 8.00 . . . . . . . . . . . 5858 10 35 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 10 36 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 10 37 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 10 38 . 1 1 22 22 LEU H H 1 7.74 . . . . . . . . . . . 5858 10 39 . 1 1 23 23 THR N N 15 121.2 . . . . . . . . . . . 5858 10 40 . 1 1 23 23 THR H H 1 8.23 . . . . . . . . . . . 5858 10 41 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 10 42 . 1 1 24 24 ILE H H 1 8.93 . . . . . . . . . . . 5858 10 43 . 1 1 25 25 LYS N N 15 119.5 . . . . . . . . . . . 5858 10 44 . 1 1 25 25 LYS H H 1 8.90 . . . . . . . . . . . 5858 10 45 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 10 46 . 1 1 27 27 GLY H H 1 7.12 . . . . . . . . . . . 5858 10 47 . 1 1 28 28 ASP N N 15 119.8 . . . . . . . . . . . 5858 10 48 . 1 1 28 28 ASP H H 1 7.91 . . . . . . . . . . . 5858 10 49 . 1 1 29 29 THR N N 15 114.7 . . . . . . . . . . . 5858 10 50 . 1 1 29 29 THR H H 1 8.61 . . . . . . . . . . . 5858 10 51 . 1 1 30 30 VAL N N 15 126.4 . . . . . . . . . . . 5858 10 52 . 1 1 30 30 VAL H H 1 9.18 . . . . . . . . . . . 5858 10 53 . 1 1 31 31 GLU N N 15 128.3 . . . . . . . . . . . 5858 10 54 . 1 1 31 31 GLU H H 1 9.25 . . . . . . . . . . . 5858 10 55 . 1 1 32 32 PHE N N 15 126.3 . . . . . . . . . . . 5858 10 56 . 1 1 32 32 PHE H H 1 9.22 . . . . . . . . . . . 5858 10 57 . 1 1 33 33 LEU N N 15 125.2 . . . . . . . . . . . 5858 10 58 . 1 1 33 33 LEU H H 1 8.94 . . . . . . . . . . . 5858 10 59 . 1 1 34 34 ASN N N 15 127.2 . . . . . . . . . . . 5858 10 60 . 1 1 34 34 ASN H H 1 9.37 . . . . . . . . . . . 5858 10 61 . 1 1 35 35 ASN N N 15 129.5 . . . . . . . . . . . 5858 10 62 . 1 1 35 35 ASN H H 1 8.63 . . . . . . . . . . . 5858 10 63 . 1 1 36 36 LYS N N 15 116.8 . . . . . . . . . . . 5858 10 64 . 1 1 36 36 LYS H H 1 8.13 . . . . . . . . . . . 5858 10 65 . 1 1 37 37 VAL N N 15 116.6 . . . . . . . . . . . 5858 10 66 . 1 1 37 37 VAL H H 1 9.08 . . . . . . . . . . . 5858 10 67 . 1 1 40 40 HIS N N 15 111.4 . . . . . . . . . . . 5858 10 68 . 1 1 40 40 HIS H H 1 7.38 . . . . . . . . . . . 5858 10 69 . 1 1 41 41 ASN N N 15 122.2 . . . . . . . . . . . 5858 10 70 . 1 1 41 41 ASN H H 1 9.56 . . . . . . . . . . . 5858 10 71 . 1 1 42 42 VAL N N 15 109.4 . . . . . . . . . . . 5858 10 72 . 1 1 42 42 VAL H H 1 6.97 . . . . . . . . . . . 5858 10 73 . 1 1 43 43 VAL N N 15 128.5 . . . . . . . . . . . 5858 10 74 . 1 1 43 43 VAL H H 1 9.36 . . . . . . . . . . . 5858 10 75 . 1 1 44 44 PHE N N 15 125.7 . . . . . . . . . . . 5858 10 76 . 1 1 44 44 PHE H H 1 8.78 . . . . . . . . . . . 5858 10 77 . 1 1 45 45 ASP N N 15 124.1 . . . . . . . . . . . 5858 10 78 . 1 1 45 45 ASP H H 1 8.41 . . . . . . . . . . . 5858 10 79 . 1 1 46 46 ALA N N 15 128.4 . . . . . . . . . . . 5858 10 80 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 10 81 . 1 1 47 47 ALA N N 15 117.5 . . . . . . . . . . . 5858 10 82 . 1 1 47 47 ALA H H 1 8.47 . . . . . . . . . . . 5858 10 83 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 10 84 . 1 1 48 48 LEU H H 1 8.63 . . . . . . . . . . . 5858 10 85 . 1 1 49 49 ASN N N 15 114.6 . . . . . . . . . . . 5858 10 86 . 1 1 49 49 ASN H H 1 8.06 . . . . . . . . . . . 5858 10 87 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 10 88 . 1 1 51 51 ALA H H 1 7.00 . . . . . . . . . . . 5858 10 89 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 10 90 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 10 91 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 10 92 . 1 1 53 53 SER H H 1 8.22 . . . . . . . . . . . 5858 10 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 10 94 . 1 1 54 54 ALA H H 1 9.19 . . . . . . . . . . . 5858 10 95 . 1 1 55 55 ASP N N 15 120.0 . . . . . . . . . . . 5858 10 96 . 1 1 55 55 ASP H H 1 8.44 . . . . . . . . . . . 5858 10 97 . 1 1 56 56 LEU N N 15 123.8 . . . . . . . . . . . 5858 10 98 . 1 1 56 56 LEU H H 1 8.15 . . . . . . . . . . . 5858 10 99 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 10 100 . 1 1 57 57 ALA H H 1 7.58 . . . . . . . . . . . 5858 10 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 10 102 . 1 1 58 58 LYS H H 1 8.55 . . . . . . . . . . . 5858 10 103 . 1 1 59 59 SER N N 15 115.3 . . . . . . . . . . . 5858 10 104 . 1 1 59 59 SER H H 1 7.75 . . . . . . . . . . . 5858 10 105 . 1 1 60 60 LEU N N 15 120.5 . . . . . . . . . . . 5858 10 106 . 1 1 60 60 LEU H H 1 6.90 . . . . . . . . . . . 5858 10 107 . 1 1 61 61 SER N N 15 111.3 . . . . . . . . . . . 5858 10 108 . 1 1 61 61 SER H H 1 6.98 . . . . . . . . . . . 5858 10 109 . 1 1 62 62 HIS N N 15 120.2 . . . . . . . . . . . 5858 10 110 . 1 1 62 62 HIS H H 1 9.57 . . . . . . . . . . . 5858 10 111 . 1 1 63 63 LYS N N 15 123.7 . . . . . . . . . . . 5858 10 112 . 1 1 63 63 LYS H H 1 8.87 . . . . . . . . . . . 5858 10 113 . 1 1 64 64 GLN N N 15 120.7 . . . . . . . . . . . 5858 10 114 . 1 1 64 64 GLN H H 1 8.46 . . . . . . . . . . . 5858 10 115 . 1 1 65 65 LEU N N 15 121.7 . . . . . . . . . . . 5858 10 116 . 1 1 65 65 LEU H H 1 8.28 . . . . . . . . . . . 5858 10 117 . 1 1 66 66 LEU N N 15 124.6 . . . . . . . . . . . 5858 10 118 . 1 1 66 66 LEU H H 1 9.37 . . . . . . . . . . . 5858 10 119 . 1 1 67 67 MET N N 15 122.0 . . . . . . . . . . . 5858 10 120 . 1 1 67 67 MET H H 1 8.18 . . . . . . . . . . . 5858 10 121 . 1 1 68 68 SER N N 15 114.2 . . . . . . . . . . . 5858 10 122 . 1 1 68 68 SER H H 1 8.41 . . . . . . . . . . . 5858 10 123 . 1 1 70 70 GLY N N 15 112.7 . . . . . . . . . . . 5858 10 124 . 1 1 70 70 GLY H H 1 8.97 . . . . . . . . . . . 5858 10 125 . 1 1 71 71 GLN N N 15 119.8 . . . . . . . . . . . 5858 10 126 . 1 1 71 71 GLN H H 1 7.51 . . . . . . . . . . . 5858 10 127 . 1 1 72 72 SER N N 15 115.7 . . . . . . . . . . . 5858 10 128 . 1 1 72 72 SER H H 1 8.70 . . . . . . . . . . . 5858 10 129 . 1 1 73 73 THR N N 15 115.6 . . . . . . . . . . . 5858 10 130 . 1 1 73 73 THR H H 1 8.73 . . . . . . . . . . . 5858 10 131 . 1 1 74 74 SER N N 15 118.4 . . . . . . . . . . . 5858 10 132 . 1 1 74 74 SER H H 1 8.16 . . . . . . . . . . . 5858 10 133 . 1 1 75 75 THR N N 15 120.9 . . . . . . . . . . . 5858 10 134 . 1 1 75 75 THR H H 1 9.50 . . . . . . . . . . . 5858 10 135 . 1 1 76 76 THR N N 15 127.2 . . . . . . . . . . . 5858 10 136 . 1 1 76 76 THR H H 1 9.13 . . . . . . . . . . . 5858 10 137 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 10 138 . 1 1 77 77 PHE H H 1 9.16 . . . . . . . . . . . 5858 10 139 . 1 1 79 79 ALA N N 15 123.2 . . . . . . . . . . . 5858 10 140 . 1 1 79 79 ALA H H 1 8.82 . . . . . . . . . . . 5858 10 141 . 1 1 80 80 ASP N N 15 112.8 . . . . . . . . . . . 5858 10 142 . 1 1 80 80 ASP H H 1 7.94 . . . . . . . . . . . 5858 10 143 . 1 1 81 81 ALA N N 15 124.7 . . . . . . . . . . . 5858 10 144 . 1 1 81 81 ALA H H 1 7.60 . . . . . . . . . . . 5858 10 145 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 10 146 . 1 1 83 83 ALA H H 1 8.39 . . . . . . . . . . . 5858 10 147 . 1 1 84 84 GLY N N 15 107.3 . . . . . . . . . . . 5858 10 148 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 10 149 . 1 1 85 85 GLU N N 15 119.7 . . . . . . . . . . . 5858 10 150 . 1 1 85 85 GLU H H 1 8.49 . . . . . . . . . . . 5858 10 151 . 1 1 86 86 TYR N N 15 125.4 . . . . . . . . . . . 5858 10 152 . 1 1 86 86 TYR H H 1 10.16 . . . . . . . . . . . 5858 10 153 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 10 154 . 1 1 87 87 THR H H 1 8.64 . . . . . . . . . . . 5858 10 155 . 1 1 88 88 PHE N N 15 125.9 . . . . . . . . . . . 5858 10 156 . 1 1 88 88 PHE H H 1 8.57 . . . . . . . . . . . 5858 10 157 . 1 1 89 89 TYR N N 15 115.2 . . . . . . . . . . . 5858 10 158 . 1 1 89 89 TYR H H 1 9.06 . . . . . . . . . . . 5858 10 159 . 1 1 90 90 CYS N N 15 124.3 . . . . . . . . . . . 5858 10 160 . 1 1 90 90 CYS H H 1 7.77 . . . . . . . . . . . 5858 10 161 . 1 1 91 91 GLU N N 15 125.9 . . . . . . . . . . . 5858 10 162 . 1 1 91 91 GLU H H 1 10.04 . . . . . . . . . . . 5858 10 163 . 1 1 93 93 HIS N N 15 112.6 . . . . . . . . . . . 5858 10 164 . 1 1 93 93 HIS H H 1 8.21 . . . . . . . . . . . 5858 10 165 . 1 1 94 94 ARG N N 15 128.4 . . . . . . . . . . . 5858 10 166 . 1 1 94 94 ARG H H 1 8.22 . . . . . . . . . . . 5858 10 167 . 1 1 95 95 GLY N N 15 108.0 . . . . . . . . . . . 5858 10 168 . 1 1 95 95 GLY H H 1 9.06 . . . . . . . . . . . 5858 10 169 . 1 1 96 96 ALA N N 15 121.1 . . . . . . . . . . . 5858 10 170 . 1 1 96 96 ALA H H 1 7.42 . . . . . . . . . . . 5858 10 171 . 1 1 97 97 GLY N N 15 106.1 . . . . . . . . . . . 5858 10 172 . 1 1 97 97 GLY H H 1 8.15 . . . . . . . . . . . 5858 10 173 . 1 1 98 98 MET N N 15 122.4 . . . . . . . . . . . 5858 10 174 . 1 1 98 98 MET H H 1 7.46 . . . . . . . . . . . 5858 10 175 . 1 1 99 99 VAL N N 15 126.5 . . . . . . . . . . . 5858 10 176 . 1 1 99 99 VAL H H 1 7.99 . . . . . . . . . . . 5858 10 177 . 1 1 100 100 GLY N N 15 117.7 . . . . . . . . . . . 5858 10 178 . 1 1 100 100 GLY H H 1 8.92 . . . . . . . . . . . 5858 10 179 . 1 1 101 101 LYS N N 15 117.7 . . . . . . . . . . . 5858 10 180 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 10 181 . 1 1 102 102 ILE N N 15 127.3 . . . . . . . . . . . 5858 10 182 . 1 1 102 102 ILE H H 1 9.46 . . . . . . . . . . . 5858 10 183 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 10 184 . 1 1 103 103 THR H H 1 9.26 . . . . . . . . . . . 5858 10 185 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 10 186 . 1 1 104 104 VAL H H 1 9.33 . . . . . . . . . . . 5858 10 187 . 1 1 105 105 ALA N N 15 133.6 . . . . . . . . . . . 5858 10 188 . 1 1 105 105 ALA H H 1 9.24 . . . . . . . . . . . 5858 10 189 . 1 1 106 106 GLY N N 15 113.1 . . . . . . . . . . . 5858 10 190 . 1 1 106 106 GLY H H 1 7.89 . . . . . . . . . . . 5858 10 stop_ save_ save_shift_set_11 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_11 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 11 _Assigned_chem_shift_list.Sample_condition_list_ID 11 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_11 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 11 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 124.9 . . . . . . . . . . . 5858 11 2 . 1 1 3 3 THR H H 1 8.74 . . . . . . . . . . . 5858 11 3 . 1 1 4 4 TYR N N 15 127.1 . . . . . . . . . . . 5858 11 4 . 1 1 4 4 TYR H H 1 8.87 . . . . . . . . . . . 5858 11 5 . 1 1 5 5 THR N N 15 117.8 . . . . . . . . . . . 5858 11 6 . 1 1 5 5 THR H H 1 8.65 . . . . . . . . . . . 5858 11 7 . 1 1 6 6 VAL N N 15 129.2 . . . . . . . . . . . 5858 11 8 . 1 1 6 6 VAL H H 1 9.26 . . . . . . . . . . . 5858 11 9 . 1 1 7 7 LYS N N 15 126.7 . . . . . . . . . . . 5858 11 10 . 1 1 7 7 LYS H H 1 9.12 . . . . . . . . . . . 5858 11 11 . 1 1 8 8 LEU N N 15 121.2 . . . . . . . . . . . 5858 11 12 . 1 1 8 8 LEU H H 1 8.86 . . . . . . . . . . . 5858 11 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 11 14 . 1 1 9 9 GLY H H 1 7.50 . . . . . . . . . . . 5858 11 15 . 1 1 10 10 SER N N 15 119.9 . . . . . . . . . . . 5858 11 16 . 1 1 10 10 SER H H 1 8.77 . . . . . . . . . . . 5858 11 17 . 1 1 11 11 ASP N N 15 120.6 . . . . . . . . . . . 5858 11 18 . 1 1 11 11 ASP H H 1 9.22 . . . . . . . . . . . 5858 11 19 . 1 1 12 12 LYS N N 15 115.9 . . . . . . . . . . . 5858 11 20 . 1 1 12 12 LYS H H 1 7.50 . . . . . . . . . . . 5858 11 21 . 1 1 13 13 GLY N N 15 108.6 . . . . . . . . . . . 5858 11 22 . 1 1 13 13 GLY H H 1 8.27 . . . . . . . . . . . 5858 11 23 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 11 24 . 1 1 14 14 LEU H H 1 7.50 . . . . . . . . . . . 5858 11 25 . 1 1 15 15 LEU N N 15 125.6 . . . . . . . . . . . 5858 11 26 . 1 1 15 15 LEU H H 1 8.67 . . . . . . . . . . . 5858 11 27 . 1 1 16 16 VAL N N 15 112.7 . . . . . . . . . . . 5858 11 28 . 1 1 16 16 VAL H H 1 7.62 . . . . . . . . . . . 5858 11 29 . 1 1 17 17 PHE N N 15 121.5 . . . . . . . . . . . 5858 11 30 . 1 1 17 17 PHE H H 1 8.88 . . . . . . . . . . . 5858 11 31 . 1 1 18 18 GLU N N 15 122.5 . . . . . . . . . . . 5858 11 32 . 1 1 18 18 GLU H H 1 9.00 . . . . . . . . . . . 5858 11 33 . 1 1 20 20 ALA N N 15 116.4 . . . . . . . . . . . 5858 11 34 . 1 1 20 20 ALA H H 1 7.98 . . . . . . . . . . . 5858 11 35 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 11 36 . 1 1 21 21 LYS H H 1 7.39 . . . . . . . . . . . 5858 11 37 . 1 1 22 22 LEU N N 15 121.5 . . . . . . . . . . . 5858 11 38 . 1 1 22 22 LEU H H 1 7.73 . . . . . . . . . . . 5858 11 39 . 1 1 23 23 THR N N 15 121.2 . . . . . . . . . . . 5858 11 40 . 1 1 23 23 THR H H 1 8.23 . . . . . . . . . . . 5858 11 41 . 1 1 24 24 ILE N N 15 120.7 . . . . . . . . . . . 5858 11 42 . 1 1 24 24 ILE H H 1 8.93 . . . . . . . . . . . 5858 11 43 . 1 1 25 25 LYS N N 15 119.4 . . . . . . . . . . . 5858 11 44 . 1 1 25 25 LYS H H 1 8.86 . . . . . . . . . . . 5858 11 45 . 1 1 27 27 GLY N N 15 114.5 . . . . . . . . . . . 5858 11 46 . 1 1 27 27 GLY H H 1 7.14 . . . . . . . . . . . 5858 11 47 . 1 1 28 28 ASP N N 15 119.7 . . . . . . . . . . . 5858 11 48 . 1 1 28 28 ASP H H 1 7.91 . . . . . . . . . . . 5858 11 49 . 1 1 29 29 THR N N 15 114.8 . . . . . . . . . . . 5858 11 50 . 1 1 29 29 THR H H 1 8.59 . . . . . . . . . . . 5858 11 51 . 1 1 30 30 VAL N N 15 126.4 . . . . . . . . . . . 5858 11 52 . 1 1 30 30 VAL H H 1 9.18 . . . . . . . . . . . 5858 11 53 . 1 1 31 31 GLU N N 15 128.2 . . . . . . . . . . . 5858 11 54 . 1 1 31 31 GLU H H 1 9.26 . . . . . . . . . . . 5858 11 55 . 1 1 32 32 PHE N N 15 126.4 . . . . . . . . . . . 5858 11 56 . 1 1 32 32 PHE H H 1 9.23 . . . . . . . . . . . 5858 11 57 . 1 1 33 33 LEU N N 15 125.2 . . . . . . . . . . . 5858 11 58 . 1 1 33 33 LEU H H 1 8.93 . . . . . . . . . . . 5858 11 59 . 1 1 34 34 ASN N N 15 127.2 . . . . . . . . . . . 5858 11 60 . 1 1 34 34 ASN H H 1 9.38 . . . . . . . . . . . 5858 11 61 . 1 1 35 35 ASN N N 15 129.5 . . . . . . . . . . . 5858 11 62 . 1 1 35 35 ASN H H 1 8.60 . . . . . . . . . . . 5858 11 63 . 1 1 36 36 LYS N N 15 116.8 . . . . . . . . . . . 5858 11 64 . 1 1 36 36 LYS H H 1 8.13 . . . . . . . . . . . 5858 11 65 . 1 1 37 37 VAL N N 15 116.8 . . . . . . . . . . . 5858 11 66 . 1 1 37 37 VAL H H 1 9.11 . . . . . . . . . . . 5858 11 67 . 1 1 40 40 HIS N N 15 111.1 . . . . . . . . . . . 5858 11 68 . 1 1 40 40 HIS H H 1 7.42 . . . . . . . . . . . 5858 11 69 . 1 1 41 41 ASN N N 15 122.1 . . . . . . . . . . . 5858 11 70 . 1 1 41 41 ASN H H 1 9.50 . . . . . . . . . . . 5858 11 71 . 1 1 42 42 VAL N N 15 109.5 . . . . . . . . . . . 5858 11 72 . 1 1 42 42 VAL H H 1 6.97 . . . . . . . . . . . 5858 11 73 . 1 1 43 43 VAL N N 15 128.5 . . . . . . . . . . . 5858 11 74 . 1 1 43 43 VAL H H 1 9.35 . . . . . . . . . . . 5858 11 75 . 1 1 44 44 PHE N N 15 125.8 . . . . . . . . . . . 5858 11 76 . 1 1 44 44 PHE H H 1 8.79 . . . . . . . . . . . 5858 11 77 . 1 1 45 45 ASP N N 15 124.1 . . . . . . . . . . . 5858 11 78 . 1 1 45 45 ASP H H 1 8.41 . . . . . . . . . . . 5858 11 79 . 1 1 46 46 ALA N N 15 128.4 . . . . . . . . . . . 5858 11 80 . 1 1 46 46 ALA H H 1 8.62 . . . . . . . . . . . 5858 11 81 . 1 1 47 47 ALA N N 15 117.5 . . . . . . . . . . . 5858 11 82 . 1 1 47 47 ALA H H 1 8.46 . . . . . . . . . . . 5858 11 83 . 1 1 48 48 LEU N N 15 123.0 . . . . . . . . . . . 5858 11 84 . 1 1 48 48 LEU H H 1 8.62 . . . . . . . . . . . 5858 11 85 . 1 1 49 49 ASN N N 15 114.6 . . . . . . . . . . . 5858 11 86 . 1 1 49 49 ASN H H 1 8.05 . . . . . . . . . . . 5858 11 87 . 1 1 51 51 ALA N N 15 115.5 . . . . . . . . . . . 5858 11 88 . 1 1 51 51 ALA H H 1 7.00 . . . . . . . . . . . 5858 11 89 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 11 90 . 1 1 52 52 LYS H H 1 7.96 . . . . . . . . . . . 5858 11 91 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 11 92 . 1 1 53 53 SER H H 1 8.22 . . . . . . . . . . . 5858 11 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 11 94 . 1 1 54 54 ALA H H 1 9.19 . . . . . . . . . . . 5858 11 95 . 1 1 55 55 ASP N N 15 119.9 . . . . . . . . . . . 5858 11 96 . 1 1 55 55 ASP H H 1 8.46 . . . . . . . . . . . 5858 11 97 . 1 1 56 56 LEU N N 15 123.8 . . . . . . . . . . . 5858 11 98 . 1 1 56 56 LEU H H 1 8.15 . . . . . . . . . . . 5858 11 99 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 11 100 . 1 1 57 57 ALA H H 1 7.58 . . . . . . . . . . . 5858 11 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 11 102 . 1 1 58 58 LYS H H 1 8.55 . . . . . . . . . . . 5858 11 103 . 1 1 59 59 SER N N 15 115.3 . . . . . . . . . . . 5858 11 104 . 1 1 59 59 SER H H 1 7.75 . . . . . . . . . . . 5858 11 105 . 1 1 60 60 LEU N N 15 120.5 . . . . . . . . . . . 5858 11 106 . 1 1 60 60 LEU H H 1 6.90 . . . . . . . . . . . 5858 11 107 . 1 1 61 61 SER N N 15 111.3 . . . . . . . . . . . 5858 11 108 . 1 1 61 61 SER H H 1 6.98 . . . . . . . . . . . 5858 11 109 . 1 1 62 62 HIS N N 15 120.1 . . . . . . . . . . . 5858 11 110 . 1 1 62 62 HIS H H 1 9.56 . . . . . . . . . . . 5858 11 111 . 1 1 63 63 LYS N N 15 123.8 . . . . . . . . . . . 5858 11 112 . 1 1 63 63 LYS H H 1 8.89 . . . . . . . . . . . 5858 11 113 . 1 1 64 64 GLN N N 15 120.8 . . . . . . . . . . . 5858 11 114 . 1 1 64 64 GLN H H 1 8.48 . . . . . . . . . . . 5858 11 115 . 1 1 65 65 LEU N N 15 121.7 . . . . . . . . . . . 5858 11 116 . 1 1 65 65 LEU H H 1 8.29 . . . . . . . . . . . 5858 11 117 . 1 1 66 66 LEU N N 15 124.5 . . . . . . . . . . . 5858 11 118 . 1 1 66 66 LEU H H 1 9.34 . . . . . . . . . . . 5858 11 119 . 1 1 67 67 MET N N 15 122.0 . . . . . . . . . . . 5858 11 120 . 1 1 67 67 MET H H 1 8.20 . . . . . . . . . . . 5858 11 121 . 1 1 68 68 SER N N 15 114.2 . . . . . . . . . . . 5858 11 122 . 1 1 68 68 SER H H 1 8.42 . . . . . . . . . . . 5858 11 123 . 1 1 70 70 GLY N N 15 112.6 . . . . . . . . . . . 5858 11 124 . 1 1 70 70 GLY H H 1 8.96 . . . . . . . . . . . 5858 11 125 . 1 1 71 71 GLN N N 15 119.8 . . . . . . . . . . . 5858 11 126 . 1 1 71 71 GLN H H 1 7.51 . . . . . . . . . . . 5858 11 127 . 1 1 72 72 SER N N 15 115.4 . . . . . . . . . . . 5858 11 128 . 1 1 72 72 SER H H 1 8.73 . . . . . . . . . . . 5858 11 129 . 1 1 73 73 THR N N 15 115.7 . . . . . . . . . . . 5858 11 130 . 1 1 73 73 THR H H 1 8.71 . . . . . . . . . . . 5858 11 131 . 1 1 74 74 SER N N 15 118.4 . . . . . . . . . . . 5858 11 132 . 1 1 74 74 SER H H 1 8.17 . . . . . . . . . . . 5858 11 133 . 1 1 75 75 THR N N 15 120.9 . . . . . . . . . . . 5858 11 134 . 1 1 75 75 THR H H 1 9.48 . . . . . . . . . . . 5858 11 135 . 1 1 76 76 THR N N 15 127.3 . . . . . . . . . . . 5858 11 136 . 1 1 76 76 THR H H 1 9.13 . . . . . . . . . . . 5858 11 137 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 11 138 . 1 1 77 77 PHE H H 1 9.15 . . . . . . . . . . . 5858 11 139 . 1 1 79 79 ALA N N 15 123.2 . . . . . . . . . . . 5858 11 140 . 1 1 79 79 ALA H H 1 8.81 . . . . . . . . . . . 5858 11 141 . 1 1 80 80 ASP N N 15 112.5 . . . . . . . . . . . 5858 11 142 . 1 1 80 80 ASP H H 1 7.90 . . . . . . . . . . . 5858 11 143 . 1 1 81 81 ALA N N 15 124.8 . . . . . . . . . . . 5858 11 144 . 1 1 81 81 ALA H H 1 7.62 . . . . . . . . . . . 5858 11 145 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 11 146 . 1 1 83 83 ALA H H 1 8.39 . . . . . . . . . . . 5858 11 147 . 1 1 84 84 GLY N N 15 107.3 . . . . . . . . . . . 5858 11 148 . 1 1 84 84 GLY H H 1 8.86 . . . . . . . . . . . 5858 11 149 . 1 1 85 85 GLU N N 15 119.7 . . . . . . . . . . . 5858 11 150 . 1 1 85 85 GLU H H 1 8.50 . . . . . . . . . . . 5858 11 151 . 1 1 86 86 TYR N N 15 125.3 . . . . . . . . . . . 5858 11 152 . 1 1 86 86 TYR H H 1 10.16 . . . . . . . . . . . 5858 11 153 . 1 1 87 87 THR N N 15 121.6 . . . . . . . . . . . 5858 11 154 . 1 1 87 87 THR H H 1 8.64 . . . . . . . . . . . 5858 11 155 . 1 1 88 88 PHE N N 15 125.9 . . . . . . . . . . . 5858 11 156 . 1 1 88 88 PHE H H 1 8.56 . . . . . . . . . . . 5858 11 157 . 1 1 89 89 TYR N N 15 115.1 . . . . . . . . . . . 5858 11 158 . 1 1 89 89 TYR H H 1 9.07 . . . . . . . . . . . 5858 11 159 . 1 1 90 90 CYS N N 15 124.1 . . . . . . . . . . . 5858 11 160 . 1 1 90 90 CYS H H 1 7.78 . . . . . . . . . . . 5858 11 161 . 1 1 91 91 GLU N N 15 126.0 . . . . . . . . . . . 5858 11 162 . 1 1 91 91 GLU H H 1 10.04 . . . . . . . . . . . 5858 11 163 . 1 1 93 93 HIS N N 15 112.1 . . . . . . . . . . . 5858 11 164 . 1 1 93 93 HIS H H 1 8.13 . . . . . . . . . . . 5858 11 165 . 1 1 94 94 ARG N N 15 128.2 . . . . . . . . . . . 5858 11 166 . 1 1 94 94 ARG H H 1 8.17 . . . . . . . . . . . 5858 11 167 . 1 1 95 95 GLY N N 15 108.0 . . . . . . . . . . . 5858 11 168 . 1 1 95 95 GLY H H 1 9.06 . . . . . . . . . . . 5858 11 169 . 1 1 96 96 ALA N N 15 121.0 . . . . . . . . . . . 5858 11 170 . 1 1 96 96 ALA H H 1 7.39 . . . . . . . . . . . 5858 11 171 . 1 1 97 97 GLY N N 15 106.0 . . . . . . . . . . . 5858 11 172 . 1 1 97 97 GLY H H 1 8.16 . . . . . . . . . . . 5858 11 173 . 1 1 98 98 MET N N 15 122.1 . . . . . . . . . . . 5858 11 174 . 1 1 98 98 MET H H 1 7.43 . . . . . . . . . . . 5858 11 175 . 1 1 99 99 VAL N N 15 126.6 . . . . . . . . . . . 5858 11 176 . 1 1 99 99 VAL H H 1 7.99 . . . . . . . . . . . 5858 11 177 . 1 1 100 100 GLY N N 15 117.6 . . . . . . . . . . . 5858 11 178 . 1 1 100 100 GLY H H 1 8.91 . . . . . . . . . . . 5858 11 179 . 1 1 101 101 LYS N N 15 117.7 . . . . . . . . . . . 5858 11 180 . 1 1 101 101 LYS H H 1 8.27 . . . . . . . . . . . 5858 11 181 . 1 1 102 102 ILE N N 15 127.3 . . . . . . . . . . . 5858 11 182 . 1 1 102 102 ILE H H 1 9.46 . . . . . . . . . . . 5858 11 183 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 11 184 . 1 1 103 103 THR H H 1 9.26 . . . . . . . . . . . 5858 11 185 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 11 186 . 1 1 104 104 VAL H H 1 9.33 . . . . . . . . . . . 5858 11 187 . 1 1 105 105 ALA N N 15 133.6 . . . . . . . . . . . 5858 11 188 . 1 1 105 105 ALA H H 1 9.24 . . . . . . . . . . . 5858 11 189 . 1 1 106 106 GLY N N 15 112.6 . . . . . . . . . . . 5858 11 190 . 1 1 106 106 GLY H H 1 7.94 . . . . . . . . . . . 5858 11 stop_ save_ save_shift_set_12 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_12 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 12 _Assigned_chem_shift_list.Sample_condition_list_ID 12 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_12 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 12 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.5 . . . . . . . . . . . 5858 12 2 . 1 1 3 3 THR H H 1 8.74 . . . . . . . . . . . 5858 12 3 . 1 1 4 4 TYR N N 15 127.1 . . . . . . . . . . . 5858 12 4 . 1 1 4 4 TYR H H 1 8.81 . . . . . . . . . . . 5858 12 5 . 1 1 5 5 THR N N 15 118.4 . . . . . . . . . . . 5858 12 6 . 1 1 5 5 THR H H 1 8.60 . . . . . . . . . . . 5858 12 7 . 1 1 6 6 VAL N N 15 129.7 . . . . . . . . . . . 5858 12 8 . 1 1 6 6 VAL H H 1 9.28 . . . . . . . . . . . 5858 12 9 . 1 1 7 7 LYS N N 15 126.6 . . . . . . . . . . . 5858 12 10 . 1 1 7 7 LYS H H 1 9.04 . . . . . . . . . . . 5858 12 11 . 1 1 8 8 LEU N N 15 121.8 . . . . . . . . . . . 5858 12 12 . 1 1 8 8 LEU H H 1 8.82 . . . . . . . . . . . 5858 12 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 12 14 . 1 1 9 9 GLY H H 1 7.61 . . . . . . . . . . . 5858 12 15 . 1 1 10 10 SER N N 15 119.7 . . . . . . . . . . . 5858 12 16 . 1 1 10 10 SER H H 1 8.65 . . . . . . . . . . . 5858 12 17 . 1 1 11 11 ASP N N 15 120.9 . . . . . . . . . . . 5858 12 18 . 1 1 11 11 ASP H H 1 9.45 . . . . . . . . . . . 5858 12 19 . 1 1 12 12 LYS N N 15 115.9 . . . . . . . . . . . 5858 12 20 . 1 1 12 12 LYS H H 1 7.46 . . . . . . . . . . . 5858 12 21 . 1 1 13 13 GLY N N 15 108.9 . . . . . . . . . . . 5858 12 22 . 1 1 13 13 GLY H H 1 8.28 . . . . . . . . . . . 5858 12 23 . 1 1 14 14 LEU N N 15 117.4 . . . . . . . . . . . 5858 12 24 . 1 1 14 14 LEU H H 1 7.44 . . . . . . . . . . . 5858 12 25 . 1 1 15 15 LEU N N 15 125.0 . . . . . . . . . . . 5858 12 26 . 1 1 15 15 LEU H H 1 8.41 . . . . . . . . . . . 5858 12 27 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 12 28 . 1 1 16 16 VAL H H 1 7.46 . . . . . . . . . . . 5858 12 29 . 1 1 17 17 PHE N N 15 120.2 . . . . . . . . . . . 5858 12 30 . 1 1 17 17 PHE H H 1 8.67 . . . . . . . . . . . 5858 12 31 . 1 1 18 18 GLU N N 15 122.1 . . . . . . . . . . . 5858 12 32 . 1 1 18 18 GLU H H 1 8.97 . . . . . . . . . . . 5858 12 33 . 1 1 20 20 ALA N N 15 116.8 . . . . . . . . . . . 5858 12 34 . 1 1 20 20 ALA H H 1 8.06 . . . . . . . . . . . 5858 12 35 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 12 36 . 1 1 21 21 LYS H H 1 7.35 . . . . . . . . . . . 5858 12 37 . 1 1 22 22 LEU N N 15 121.4 . . . . . . . . . . . 5858 12 38 . 1 1 22 22 LEU H H 1 7.71 . . . . . . . . . . . 5858 12 39 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 12 40 . 1 1 23 23 THR H H 1 8.21 . . . . . . . . . . . 5858 12 41 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 12 42 . 1 1 24 24 ILE H H 1 8.89 . . . . . . . . . . . 5858 12 43 . 1 1 25 25 LYS N N 15 119.5 . . . . . . . . . . . 5858 12 44 . 1 1 25 25 LYS H H 1 8.93 . . . . . . . . . . . 5858 12 45 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 12 46 . 1 1 27 27 GLY H H 1 7.05 . . . . . . . . . . . 5858 12 47 . 1 1 28 28 ASP N N 15 119.8 . . . . . . . . . . . 5858 12 48 . 1 1 28 28 ASP H H 1 7.87 . . . . . . . . . . . 5858 12 49 . 1 1 29 29 THR N N 15 114.7 . . . . . . . . . . . 5858 12 50 . 1 1 29 29 THR H H 1 8.63 . . . . . . . . . . . 5858 12 51 . 1 1 30 30 VAL N N 15 126.4 . . . . . . . . . . . 5858 12 52 . 1 1 30 30 VAL H H 1 9.12 . . . . . . . . . . . 5858 12 53 . 1 1 31 31 GLU N N 15 128.7 . . . . . . . . . . . 5858 12 54 . 1 1 31 31 GLU H H 1 9.19 . . . . . . . . . . . 5858 12 55 . 1 1 32 32 PHE N N 15 126.0 . . . . . . . . . . . 5858 12 56 . 1 1 32 32 PHE H H 1 9.13 . . . . . . . . . . . 5858 12 57 . 1 1 33 33 LEU N N 15 125.3 . . . . . . . . . . . 5858 12 58 . 1 1 33 33 LEU H H 1 8.92 . . . . . . . . . . . 5858 12 59 . 1 1 34 34 ASN N N 15 127.3 . . . . . . . . . . . 5858 12 60 . 1 1 34 34 ASN H H 1 9.30 . . . . . . . . . . . 5858 12 61 . 1 1 35 35 ASN N N 15 129.7 . . . . . . . . . . . 5858 12 62 . 1 1 35 35 ASN H H 1 8.74 . . . . . . . . . . . 5858 12 63 . 1 1 36 36 LYS N N 15 116.8 . . . . . . . . . . . 5858 12 64 . 1 1 36 36 LYS H H 1 8.10 . . . . . . . . . . . 5858 12 65 . 1 1 37 37 VAL N N 15 115.5 . . . . . . . . . . . 5858 12 66 . 1 1 37 37 VAL H H 1 8.94 . . . . . . . . . . . 5858 12 67 . 1 1 40 40 HIS N N 15 112.3 . . . . . . . . . . . 5858 12 68 . 1 1 40 40 HIS H H 1 7.17 . . . . . . . . . . . 5858 12 69 . 1 1 41 41 ASN N N 15 122.8 . . . . . . . . . . . 5858 12 70 . 1 1 41 41 ASN H H 1 9.78 . . . . . . . . . . . 5858 12 71 . 1 1 42 42 VAL N N 15 108.9 . . . . . . . . . . . 5858 12 72 . 1 1 42 42 VAL H H 1 6.89 . . . . . . . . . . . 5858 12 73 . 1 1 43 43 VAL N N 15 128.5 . . . . . . . . . . . 5858 12 74 . 1 1 43 43 VAL H H 1 9.39 . . . . . . . . . . . 5858 12 75 . 1 1 44 44 PHE N N 15 125.5 . . . . . . . . . . . 5858 12 76 . 1 1 44 44 PHE H H 1 8.69 . . . . . . . . . . . 5858 12 77 . 1 1 45 45 ASP N N 15 124.0 . . . . . . . . . . . 5858 12 78 . 1 1 45 45 ASP H H 1 8.36 . . . . . . . . . . . 5858 12 79 . 1 1 46 46 ALA N N 15 128.2 . . . . . . . . . . . 5858 12 80 . 1 1 46 46 ALA H H 1 8.60 . . . . . . . . . . . 5858 12 81 . 1 1 47 47 ALA N N 15 117.6 . . . . . . . . . . . 5858 12 82 . 1 1 47 47 ALA H H 1 8.41 . . . . . . . . . . . 5858 12 83 . 1 1 48 48 LEU N N 15 123.2 . . . . . . . . . . . 5858 12 84 . 1 1 48 48 LEU H H 1 8.63 . . . . . . . . . . . 5858 12 85 . 1 1 49 49 ASN N N 15 114.5 . . . . . . . . . . . 5858 12 86 . 1 1 49 49 ASN H H 1 8.02 . . . . . . . . . . . 5858 12 87 . 1 1 51 51 ALA N N 15 115.4 . . . . . . . . . . . 5858 12 88 . 1 1 51 51 ALA H H 1 6.95 . . . . . . . . . . . 5858 12 89 . 1 1 52 52 LYS N N 15 120.6 . . . . . . . . . . . 5858 12 90 . 1 1 52 52 LYS H H 1 7.92 . . . . . . . . . . . 5858 12 91 . 1 1 53 53 SER N N 15 109.7 . . . . . . . . . . . 5858 12 92 . 1 1 53 53 SER H H 1 8.19 . . . . . . . . . . . 5858 12 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 12 94 . 1 1 54 54 ALA H H 1 9.16 . . . . . . . . . . . 5858 12 95 . 1 1 55 55 ASP N N 15 120.1 . . . . . . . . . . . 5858 12 96 . 1 1 55 55 ASP H H 1 8.41 . . . . . . . . . . . 5858 12 97 . 1 1 56 56 LEU N N 15 123.8 . . . . . . . . . . . 5858 12 98 . 1 1 56 56 LEU H H 1 8.12 . . . . . . . . . . . 5858 12 99 . 1 1 57 57 ALA N N 15 119.7 . . . . . . . . . . . 5858 12 100 . 1 1 57 57 ALA H H 1 7.54 . . . . . . . . . . . 5858 12 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 12 102 . 1 1 58 58 LYS H H 1 8.50 . . . . . . . . . . . 5858 12 103 . 1 1 59 59 SER N N 15 115.3 . . . . . . . . . . . 5858 12 104 . 1 1 59 59 SER H H 1 7.70 . . . . . . . . . . . 5858 12 105 . 1 1 60 60 LEU N N 15 120.6 . . . . . . . . . . . 5858 12 106 . 1 1 60 60 LEU H H 1 6.84 . . . . . . . . . . . 5858 12 107 . 1 1 61 61 SER N N 15 111.2 . . . . . . . . . . . 5858 12 108 . 1 1 61 61 SER H H 1 6.91 . . . . . . . . . . . 5858 12 109 . 1 1 62 62 HIS N N 15 120.5 . . . . . . . . . . . 5858 12 110 . 1 1 62 62 HIS H H 1 9.58 . . . . . . . . . . . 5858 12 111 . 1 1 63 63 LYS N N 15 123.3 . . . . . . . . . . . 5858 12 112 . 1 1 63 63 LYS H H 1 8.77 . . . . . . . . . . . 5858 12 113 . 1 1 64 64 GLN N N 15 120.4 . . . . . . . . . . . 5858 12 114 . 1 1 64 64 GLN H H 1 8.37 . . . . . . . . . . . 5858 12 115 . 1 1 65 65 LEU N N 15 121.9 . . . . . . . . . . . 5858 12 116 . 1 1 65 65 LEU H H 1 8.21 . . . . . . . . . . . 5858 12 117 . 1 1 66 66 LEU N N 15 124.9 . . . . . . . . . . . 5858 12 118 . 1 1 66 66 LEU H H 1 9.44 . . . . . . . . . . . 5858 12 119 . 1 1 67 67 MET N N 15 121.9 . . . . . . . . . . . 5858 12 120 . 1 1 67 67 MET H H 1 8.07 . . . . . . . . . . . 5858 12 121 . 1 1 68 68 SER N N 15 113.7 . . . . . . . . . . . 5858 12 122 . 1 1 68 68 SER H H 1 8.34 . . . . . . . . . . . 5858 12 123 . 1 1 70 70 GLY N N 15 112.8 . . . . . . . . . . . 5858 12 124 . 1 1 70 70 GLY H H 1 8.97 . . . . . . . . . . . 5858 12 125 . 1 1 71 71 GLN N N 15 119.8 . . . . . . . . . . . 5858 12 126 . 1 1 71 71 GLN H H 1 7.47 . . . . . . . . . . . 5858 12 127 . 1 1 72 72 SER N N 15 115.8 . . . . . . . . . . . 5858 12 128 . 1 1 72 72 SER H H 1 8.65 . . . . . . . . . . . 5858 12 129 . 1 1 73 73 THR N N 15 116.3 . . . . . . . . . . . 5858 12 130 . 1 1 73 73 THR H H 1 8.70 . . . . . . . . . . . 5858 12 131 . 1 1 74 74 SER N N 15 118.3 . . . . . . . . . . . 5858 12 132 . 1 1 74 74 SER H H 1 8.12 . . . . . . . . . . . 5858 12 133 . 1 1 75 75 THR N N 15 121.0 . . . . . . . . . . . 5858 12 134 . 1 1 75 75 THR H H 1 9.51 . . . . . . . . . . . 5858 12 135 . 1 1 76 76 THR N N 15 127.2 . . . . . . . . . . . 5858 12 136 . 1 1 76 76 THR H H 1 9.11 . . . . . . . . . . . 5858 12 137 . 1 1 77 77 PHE N N 15 131.7 . . . . . . . . . . . 5858 12 138 . 1 1 77 77 PHE H H 1 9.15 . . . . . . . . . . . 5858 12 139 . 1 1 79 79 ALA N N 15 123.1 . . . . . . . . . . . 5858 12 140 . 1 1 79 79 ALA H H 1 8.81 . . . . . . . . . . . 5858 12 141 . 1 1 80 80 ASP N N 15 113.1 . . . . . . . . . . . 5858 12 142 . 1 1 80 80 ASP H H 1 7.95 . . . . . . . . . . . 5858 12 143 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 12 144 . 1 1 81 81 ALA H H 1 7.54 . . . . . . . . . . . 5858 12 145 . 1 1 83 83 ALA N N 15 124.5 . . . . . . . . . . . 5858 12 146 . 1 1 83 83 ALA H H 1 8.36 . . . . . . . . . . . 5858 12 147 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 12 148 . 1 1 84 84 GLY H H 1 8.82 . . . . . . . . . . . 5858 12 149 . 1 1 85 85 GLU N N 15 119.7 . . . . . . . . . . . 5858 12 150 . 1 1 85 85 GLU H H 1 8.46 . . . . . . . . . . . 5858 12 151 . 1 1 86 86 TYR N N 15 125.4 . . . . . . . . . . . 5858 12 152 . 1 1 86 86 TYR H H 1 10.13 . . . . . . . . . . . 5858 12 153 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 12 154 . 1 1 87 87 THR H H 1 8.59 . . . . . . . . . . . 5858 12 155 . 1 1 88 88 PHE N N 15 126.2 . . . . . . . . . . . 5858 12 156 . 1 1 88 88 PHE H H 1 8.54 . . . . . . . . . . . 5858 12 157 . 1 1 89 89 TYR N N 15 115.2 . . . . . . . . . . . 5858 12 158 . 1 1 89 89 TYR H H 1 8.91 . . . . . . . . . . . 5858 12 159 . 1 1 90 90 CYS N N 15 125.0 . . . . . . . . . . . 5858 12 160 . 1 1 90 90 CYS H H 1 7.71 . . . . . . . . . . . 5858 12 161 . 1 1 91 91 GLU N N 15 125.5 . . . . . . . . . . . 5858 12 162 . 1 1 91 91 GLU H H 1 9.99 . . . . . . . . . . . 5858 12 163 . 1 1 93 93 HIS N N 15 115.1 . . . . . . . . . . . 5858 12 164 . 1 1 93 93 HIS H H 1 8.49 . . . . . . . . . . . 5858 12 165 . 1 1 94 94 ARG N N 15 129.2 . . . . . . . . . . . 5858 12 166 . 1 1 94 94 ARG H H 1 8.39 . . . . . . . . . . . 5858 12 167 . 1 1 95 95 GLY N N 15 107.7 . . . . . . . . . . . 5858 12 168 . 1 1 95 95 GLY H H 1 9.06 . . . . . . . . . . . 5858 12 169 . 1 1 96 96 ALA N N 15 121.5 . . . . . . . . . . . 5858 12 170 . 1 1 96 96 ALA H H 1 7.49 . . . . . . . . . . . 5858 12 171 . 1 1 97 97 GLY N N 15 106.4 . . . . . . . . . . . 5858 12 172 . 1 1 97 97 GLY H H 1 8.05 . . . . . . . . . . . 5858 12 173 . 1 1 98 98 MET N N 15 123.9 . . . . . . . . . . . 5858 12 174 . 1 1 98 98 MET H H 1 7.57 . . . . . . . . . . . 5858 12 175 . 1 1 99 99 VAL N N 15 125.9 . . . . . . . . . . . 5858 12 176 . 1 1 99 99 VAL H H 1 7.91 . . . . . . . . . . . 5858 12 177 . 1 1 100 100 GLY N N 15 118.1 . . . . . . . . . . . 5858 12 178 . 1 1 100 100 GLY H H 1 8.93 . . . . . . . . . . . 5858 12 179 . 1 1 101 101 LYS N N 15 117.5 . . . . . . . . . . . 5858 12 180 . 1 1 101 101 LYS H H 1 8.22 . . . . . . . . . . . 5858 12 181 . 1 1 102 102 ILE N N 15 127.6 . . . . . . . . . . . 5858 12 182 . 1 1 102 102 ILE H H 1 9.44 . . . . . . . . . . . 5858 12 183 . 1 1 103 103 THR N N 15 126.0 . . . . . . . . . . . 5858 12 184 . 1 1 103 103 THR H H 1 9.23 . . . . . . . . . . . 5858 12 185 . 1 1 104 104 VAL N N 15 128.6 . . . . . . . . . . . 5858 12 186 . 1 1 104 104 VAL H H 1 9.29 . . . . . . . . . . . 5858 12 187 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 12 188 . 1 1 105 105 ALA H H 1 9.22 . . . . . . . . . . . 5858 12 189 . 1 1 106 106 GLY N N 15 113.7 . . . . . . . . . . . 5858 12 190 . 1 1 106 106 GLY H H 1 7.80 . . . . . . . . . . . 5858 12 stop_ save_ save_shift_set_13 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_13 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 13 _Assigned_chem_shift_list.Sample_condition_list_ID 13 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_13 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 13 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.7 . . . . . . . . . . . 5858 13 2 . 1 1 3 3 THR H H 1 8.84 . . . . . . . . . . . 5858 13 3 . 1 1 4 4 TYR N N 15 127.0 . . . . . . . . . . . 5858 13 4 . 1 1 4 4 TYR H H 1 8.87 . . . . . . . . . . . 5858 13 5 . 1 1 5 5 THR N N 15 118.4 . . . . . . . . . . . 5858 13 6 . 1 1 5 5 THR H H 1 8.64 . . . . . . . . . . . 5858 13 7 . 1 1 6 6 VAL N N 15 129.7 . . . . . . . . . . . 5858 13 8 . 1 1 6 6 VAL H H 1 9.35 . . . . . . . . . . . 5858 13 9 . 1 1 7 7 LYS N N 15 126.7 . . . . . . . . . . . 5858 13 10 . 1 1 7 7 LYS H H 1 9.14 . . . . . . . . . . . 5858 13 11 . 1 1 8 8 LEU N N 15 122.0 . . . . . . . . . . . 5858 13 12 . 1 1 8 8 LEU H H 1 8.91 . . . . . . . . . . . 5858 13 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 13 14 . 1 1 9 9 GLY H H 1 7.71 . . . . . . . . . . . 5858 13 15 . 1 1 10 10 SER N N 15 119.7 . . . . . . . . . . . 5858 13 16 . 1 1 10 10 SER H H 1 8.73 . . . . . . . . . . . 5858 13 17 . 1 1 11 11 ASP N N 15 121.0 . . . . . . . . . . . 5858 13 18 . 1 1 11 11 ASP H H 1 9.49 . . . . . . . . . . . 5858 13 19 . 1 1 12 12 LYS N N 15 115.9 . . . . . . . . . . . 5858 13 20 . 1 1 12 12 LYS H H 1 7.56 . . . . . . . . . . . 5858 13 21 . 1 1 13 13 GLY N N 15 108.8 . . . . . . . . . . . 5858 13 22 . 1 1 13 13 GLY H H 1 8.37 . . . . . . . . . . . 5858 13 23 . 1 1 14 14 LEU N N 15 117.5 . . . . . . . . . . . 5858 13 24 . 1 1 14 14 LEU H H 1 7.48 . . . . . . . . . . . 5858 13 25 . 1 1 15 15 LEU N N 15 125.1 . . . . . . . . . . . 5858 13 26 . 1 1 15 15 LEU H H 1 8.47 . . . . . . . . . . . 5858 13 27 . 1 1 16 16 VAL N N 15 112.6 . . . . . . . . . . . 5858 13 28 . 1 1 16 16 VAL H H 1 7.54 . . . . . . . . . . . 5858 13 29 . 1 1 17 17 PHE N N 15 120.2 . . . . . . . . . . . 5858 13 30 . 1 1 17 17 PHE H H 1 8.70 . . . . . . . . . . . 5858 13 31 . 1 1 18 18 GLU N N 15 122.2 . . . . . . . . . . . 5858 13 32 . 1 1 18 18 GLU H H 1 9.04 . . . . . . . . . . . 5858 13 33 . 1 1 20 20 ALA N N 15 117.0 . . . . . . . . . . . 5858 13 34 . 1 1 20 20 ALA H H 1 8.14 . . . . . . . . . . . 5858 13 35 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 13 36 . 1 1 21 21 LYS H H 1 7.43 . . . . . . . . . . . 5858 13 37 . 1 1 22 22 LEU N N 15 121.6 . . . . . . . . . . . 5858 13 38 . 1 1 22 22 LEU H H 1 7.83 . . . . . . . . . . . 5858 13 39 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 13 40 . 1 1 23 23 THR H H 1 8.25 . . . . . . . . . . . 5858 13 41 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 13 42 . 1 1 24 24 ILE H H 1 8.97 . . . . . . . . . . . 5858 13 43 . 1 1 25 25 LYS N N 15 119.7 . . . . . . . . . . . 5858 13 44 . 1 1 25 25 LYS H H 1 9.02 . . . . . . . . . . . 5858 13 45 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 13 46 . 1 1 27 27 GLY H H 1 7.16 . . . . . . . . . . . 5858 13 47 . 1 1 28 28 ASP N N 15 119.9 . . . . . . . . . . . 5858 13 48 . 1 1 28 28 ASP H H 1 7.95 . . . . . . . . . . . 5858 13 49 . 1 1 29 29 THR N N 15 114.8 . . . . . . . . . . . 5858 13 50 . 1 1 29 29 THR H H 1 8.70 . . . . . . . . . . . 5858 13 51 . 1 1 30 30 VAL N N 15 126.5 . . . . . . . . . . . 5858 13 52 . 1 1 30 30 VAL H H 1 9.20 . . . . . . . . . . . 5858 13 53 . 1 1 31 31 GLU N N 15 128.8 . . . . . . . . . . . 5858 13 54 . 1 1 31 31 GLU H H 1 9.27 . . . . . . . . . . . 5858 13 55 . 1 1 32 32 PHE N N 15 125.9 . . . . . . . . . . . 5858 13 56 . 1 1 32 32 PHE H H 1 9.20 . . . . . . . . . . . 5858 13 57 . 1 1 33 33 LEU N N 15 125.3 . . . . . . . . . . . 5858 13 58 . 1 1 33 33 LEU H H 1 9.02 . . . . . . . . . . . 5858 13 59 . 1 1 34 34 ASN N N 15 127.4 . . . . . . . . . . . 5858 13 60 . 1 1 34 34 ASN H H 1 9.38 . . . . . . . . . . . 5858 13 61 . 1 1 35 35 ASN N N 15 129.7 . . . . . . . . . . . 5858 13 62 . 1 1 35 35 ASN H H 1 8.81 . . . . . . . . . . . 5858 13 63 . 1 1 36 36 LYS N N 15 116.8 . . . . . . . . . . . 5858 13 64 . 1 1 36 36 LYS H H 1 8.20 . . . . . . . . . . . 5858 13 65 . 1 1 37 37 VAL N N 15 115.8 . . . . . . . . . . . 5858 13 66 . 1 1 37 37 VAL H H 1 8.99 . . . . . . . . . . . 5858 13 67 . 1 1 40 40 HIS N N 15 112.3 . . . . . . . . . . . 5858 13 68 . 1 1 40 40 HIS H H 1 7.27 . . . . . . . . . . . 5858 13 69 . 1 1 41 41 ASN N N 15 122.9 . . . . . . . . . . . 5858 13 70 . 1 1 41 41 ASN H H 1 9.88 . . . . . . . . . . . 5858 13 71 . 1 1 42 42 VAL N N 15 109.0 . . . . . . . . . . . 5858 13 72 . 1 1 42 42 VAL H H 1 7.00 . . . . . . . . . . . 5858 13 73 . 1 1 43 43 VAL N N 15 128.5 . . . . . . . . . . . 5858 13 74 . 1 1 43 43 VAL H H 1 9.47 . . . . . . . . . . . 5858 13 75 . 1 1 44 44 PHE N N 15 125.5 . . . . . . . . . . . 5858 13 76 . 1 1 44 44 PHE H H 1 8.76 . . . . . . . . . . . 5858 13 77 . 1 1 45 45 ASP N N 15 124.1 . . . . . . . . . . . 5858 13 78 . 1 1 45 45 ASP H H 1 8.43 . . . . . . . . . . . 5858 13 79 . 1 1 46 46 ALA N N 15 128.3 . . . . . . . . . . . 5858 13 80 . 1 1 46 46 ALA H H 1 8.65 . . . . . . . . . . . 5858 13 81 . 1 1 47 47 ALA N N 15 117.6 . . . . . . . . . . . 5858 13 82 . 1 1 47 47 ALA H H 1 8.51 . . . . . . . . . . . 5858 13 83 . 1 1 48 48 LEU N N 15 123.1 . . . . . . . . . . . 5858 13 84 . 1 1 48 48 LEU H H 1 8.69 . . . . . . . . . . . 5858 13 85 . 1 1 49 49 ASN N N 15 114.6 . . . . . . . . . . . 5858 13 86 . 1 1 49 49 ASN H H 1 8.10 . . . . . . . . . . . 5858 13 87 . 1 1 51 51 ALA N N 15 115.6 . . . . . . . . . . . 5858 13 88 . 1 1 51 51 ALA H H 1 7.06 . . . . . . . . . . . 5858 13 89 . 1 1 52 52 LYS N N 15 120.5 . . . . . . . . . . . 5858 13 90 . 1 1 52 52 LYS H H 1 8.00 . . . . . . . . . . . 5858 13 91 . 1 1 53 53 SER N N 15 109.8 . . . . . . . . . . . 5858 13 92 . 1 1 53 53 SER H H 1 8.25 . . . . . . . . . . . 5858 13 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 13 94 . 1 1 54 54 ALA H H 1 9.22 . . . . . . . . . . . 5858 13 95 . 1 1 55 55 ASP N N 15 120.0 . . . . . . . . . . . 5858 13 96 . 1 1 55 55 ASP H H 1 8.43 . . . . . . . . . . . 5858 13 97 . 1 1 56 56 LEU N N 15 123.7 . . . . . . . . . . . 5858 13 98 . 1 1 56 56 LEU H H 1 8.17 . . . . . . . . . . . 5858 13 99 . 1 1 57 57 ALA N N 15 119.6 . . . . . . . . . . . 5858 13 100 . 1 1 57 57 ALA H H 1 7.61 . . . . . . . . . . . 5858 13 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 13 102 . 1 1 58 58 LYS H H 1 8.59 . . . . . . . . . . . 5858 13 103 . 1 1 59 59 SER N N 15 115.4 . . . . . . . . . . . 5858 13 104 . 1 1 59 59 SER H H 1 7.79 . . . . . . . . . . . 5858 13 105 . 1 1 60 60 LEU N N 15 120.4 . . . . . . . . . . . 5858 13 106 . 1 1 60 60 LEU H H 1 6.96 . . . . . . . . . . . 5858 13 107 . 1 1 61 61 SER N N 15 111.2 . . . . . . . . . . . 5858 13 108 . 1 1 61 61 SER H H 1 7.02 . . . . . . . . . . . 5858 13 109 . 1 1 62 62 HIS N N 15 120.7 . . . . . . . . . . . 5858 13 110 . 1 1 62 62 HIS H H 1 9.67 . . . . . . . . . . . 5858 13 111 . 1 1 63 63 LYS N N 15 123.3 . . . . . . . . . . . 5858 13 112 . 1 1 63 63 LYS H H 1 8.81 . . . . . . . . . . . 5858 13 113 . 1 1 64 64 GLN N N 15 120.3 . . . . . . . . . . . 5858 13 114 . 1 1 64 64 GLN H H 1 8.40 . . . . . . . . . . . 5858 13 115 . 1 1 65 65 LEU N N 15 121.8 . . . . . . . . . . . 5858 13 116 . 1 1 65 65 LEU H H 1 8.25 . . . . . . . . . . . 5858 13 117 . 1 1 66 66 LEU N N 15 124.9 . . . . . . . . . . . 5858 13 118 . 1 1 66 66 LEU H H 1 9.52 . . . . . . . . . . . 5858 13 119 . 1 1 67 67 MET N N 15 121.9 . . . . . . . . . . . 5858 13 120 . 1 1 67 67 MET H H 1 8.15 . . . . . . . . . . . 5858 13 121 . 1 1 68 68 SER N N 15 113.8 . . . . . . . . . . . 5858 13 122 . 1 1 68 68 SER H H 1 8.39 . . . . . . . . . . . 5858 13 123 . 1 1 70 70 GLY N N 15 112.8 . . . . . . . . . . . 5858 13 124 . 1 1 70 70 GLY H H 1 9.06 . . . . . . . . . . . 5858 13 125 . 1 1 71 71 GLN N N 15 119.9 . . . . . . . . . . . 5858 13 126 . 1 1 71 71 GLN H H 1 7.58 . . . . . . . . . . . 5858 13 127 . 1 1 72 72 SER N N 15 115.9 . . . . . . . . . . . 5858 13 128 . 1 1 72 72 SER H H 1 8.68 . . . . . . . . . . . 5858 13 129 . 1 1 73 73 THR N N 15 116.2 . . . . . . . . . . . 5858 13 130 . 1 1 73 73 THR H H 1 8.78 . . . . . . . . . . . 5858 13 131 . 1 1 74 74 SER N N 15 118.4 . . . . . . . . . . . 5858 13 132 . 1 1 74 74 SER H H 1 8.20 . . . . . . . . . . . 5858 13 133 . 1 1 75 75 THR N N 15 121.1 . . . . . . . . . . . 5858 13 134 . 1 1 75 75 THR H H 1 9.59 . . . . . . . . . . . 5858 13 135 . 1 1 76 76 THR N N 15 127.1 . . . . . . . . . . . 5858 13 136 . 1 1 76 76 THR H H 1 9.12 . . . . . . . . . . . 5858 13 137 . 1 1 77 77 PHE N N 15 131.6 . . . . . . . . . . . 5858 13 138 . 1 1 77 77 PHE H H 1 9.21 . . . . . . . . . . . 5858 13 139 . 1 1 79 79 ALA N N 15 123.1 . . . . . . . . . . . 5858 13 140 . 1 1 79 79 ALA H H 1 8.84 . . . . . . . . . . . 5858 13 141 . 1 1 80 80 ASP N N 15 113.2 . . . . . . . . . . . 5858 13 142 . 1 1 80 80 ASP H H 1 8.06 . . . . . . . . . . . 5858 13 143 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 13 144 . 1 1 81 81 ALA H H 1 7.62 . . . . . . . . . . . 5858 13 145 . 1 1 83 83 ALA N N 15 124.6 . . . . . . . . . . . 5858 13 146 . 1 1 83 83 ALA H H 1 8.40 . . . . . . . . . . . 5858 13 147 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 13 148 . 1 1 84 84 GLY H H 1 8.90 . . . . . . . . . . . 5858 13 149 . 1 1 85 85 GLU N N 15 119.8 . . . . . . . . . . . 5858 13 150 . 1 1 85 85 GLU H H 1 8.51 . . . . . . . . . . . 5858 13 151 . 1 1 86 86 TYR N N 15 125.6 . . . . . . . . . . . 5858 13 152 . 1 1 86 86 TYR H H 1 10.21 . . . . . . . . . . . 5858 13 153 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 13 154 . 1 1 87 87 THR H H 1 8.67 . . . . . . . . . . . 5858 13 155 . 1 1 88 88 PHE N N 15 126.3 . . . . . . . . . . . 5858 13 156 . 1 1 88 88 PHE H H 1 8.63 . . . . . . . . . . . 5858 13 157 . 1 1 89 89 TYR N N 15 115.3 . . . . . . . . . . . 5858 13 158 . 1 1 89 89 TYR H H 1 9.01 . . . . . . . . . . . 5858 13 159 . 1 1 90 90 CYS N N 15 125.1 . . . . . . . . . . . 5858 13 160 . 1 1 90 90 CYS H H 1 7.80 . . . . . . . . . . . 5858 13 161 . 1 1 91 91 GLU N N 15 125.7 . . . . . . . . . . . 5858 13 162 . 1 1 91 91 GLU H H 1 10.06 . . . . . . . . . . . 5858 13 163 . 1 1 93 93 HIS N N 15 115.2 . . . . . . . . . . . 5858 13 164 . 1 1 93 93 HIS H H 1 8.60 . . . . . . . . . . . 5858 13 165 . 1 1 94 94 ARG N N 15 129.1 . . . . . . . . . . . 5858 13 166 . 1 1 94 94 ARG H H 1 8.49 . . . . . . . . . . . 5858 13 167 . 1 1 95 95 GLY N N 15 107.6 . . . . . . . . . . . 5858 13 168 . 1 1 95 95 GLY H H 1 9.12 . . . . . . . . . . . 5858 13 169 . 1 1 96 96 ALA N N 15 121.6 . . . . . . . . . . . 5858 13 170 . 1 1 96 96 ALA H H 1 7.60 . . . . . . . . . . . 5858 13 171 . 1 1 97 97 GLY N N 15 106.3 . . . . . . . . . . . 5858 13 172 . 1 1 97 97 GLY H H 1 8.13 . . . . . . . . . . . 5858 13 173 . 1 1 98 98 MET N N 15 124.0 . . . . . . . . . . . 5858 13 174 . 1 1 98 98 MET H H 1 7.65 . . . . . . . . . . . 5858 13 175 . 1 1 99 99 VAL N N 15 126.0 . . . . . . . . . . . 5858 13 176 . 1 1 99 99 VAL H H 1 8.00 . . . . . . . . . . . 5858 13 177 . 1 1 100 100 GLY N N 15 118.0 . . . . . . . . . . . 5858 13 178 . 1 1 100 100 GLY H H 1 9.01 . . . . . . . . . . . 5858 13 179 . 1 1 101 101 LYS N N 15 117.6 . . . . . . . . . . . 5858 13 180 . 1 1 101 101 LYS H H 1 8.32 . . . . . . . . . . . 5858 13 181 . 1 1 102 102 ILE N N 15 127.3 . . . . . . . . . . . 5858 13 182 . 1 1 102 102 ILE H H 1 9.51 . . . . . . . . . . . 5858 13 183 . 1 1 103 103 THR N N 15 126.1 . . . . . . . . . . . 5858 13 184 . 1 1 103 103 THR H H 1 9.31 . . . . . . . . . . . 5858 13 185 . 1 1 104 104 VAL N N 15 128.7 . . . . . . . . . . . 5858 13 186 . 1 1 104 104 VAL H H 1 9.36 . . . . . . . . . . . 5858 13 187 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 13 188 . 1 1 105 105 ALA H H 1 9.28 . . . . . . . . . . . 5858 13 189 . 1 1 106 106 GLY N N 15 113.8 . . . . . . . . . . . 5858 13 190 . 1 1 106 106 GLY H H 1 7.82 . . . . . . . . . . . 5858 13 stop_ save_ save_shift_set_14 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode shift_set_14 _Assigned_chem_shift_list.Entry_ID 5858 _Assigned_chem_shift_list.ID 14 _Assigned_chem_shift_list.Sample_condition_list_ID 14 _Assigned_chem_shift_list.Sample_condition_list_label $Condition_14 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID . . 1 $sample_1 . 5858 14 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 3 3 THR N N 15 125.8 . . . . . . . . . . . 5858 14 2 . 1 1 3 3 THR H H 1 8.89 . . . . . . . . . . . 5858 14 3 . 1 1 4 4 TYR N N 15 126.9 . . . . . . . . . . . 5858 14 4 . 1 1 4 4 TYR H H 1 8.90 . . . . . . . . . . . 5858 14 5 . 1 1 5 5 THR N N 15 118.5 . . . . . . . . . . . 5858 14 6 . 1 1 5 5 THR H H 1 8.65 . . . . . . . . . . . 5858 14 7 . 1 1 6 6 VAL N N 15 129.6 . . . . . . . . . . . 5858 14 8 . 1 1 6 6 VAL H H 1 9.38 . . . . . . . . . . . 5858 14 9 . 1 1 7 7 LYS N N 15 126.7 . . . . . . . . . . . 5858 14 10 . 1 1 7 7 LYS H H 1 9.19 . . . . . . . . . . . 5858 14 11 . 1 1 8 8 LEU N N 15 122.1 . . . . . . . . . . . 5858 14 12 . 1 1 8 8 LEU H H 1 8.96 . . . . . . . . . . . 5858 14 13 . 1 1 9 9 GLY N N 15 114.9 . . . . . . . . . . . 5858 14 14 . 1 1 9 9 GLY H H 1 7.75 . . . . . . . . . . . 5858 14 15 . 1 1 10 10 SER N N 15 119.8 . . . . . . . . . . . 5858 14 16 . 1 1 10 10 SER H H 1 8.76 . . . . . . . . . . . 5858 14 17 . 1 1 11 11 ASP N N 15 121.1 . . . . . . . . . . . 5858 14 18 . 1 1 11 11 ASP H H 1 9.50 . . . . . . . . . . . 5858 14 19 . 1 1 12 12 LYS N N 15 116.0 . . . . . . . . . . . 5858 14 20 . 1 1 12 12 LYS H H 1 7.60 . . . . . . . . . . . 5858 14 21 . 1 1 13 13 GLY N N 15 108.8 . . . . . . . . . . . 5858 14 22 . 1 1 13 13 GLY H H 1 8.41 . . . . . . . . . . . 5858 14 23 . 1 1 14 14 LEU N N 15 117.5 . . . . . . . . . . . 5858 14 24 . 1 1 14 14 LEU H H 1 7.50 . . . . . . . . . . . 5858 14 25 . 1 1 15 15 LEU N N 15 125.2 . . . . . . . . . . . 5858 14 26 . 1 1 15 15 LEU H H 1 8.50 . . . . . . . . . . . 5858 14 27 . 1 1 16 16 VAL N N 15 112.7 . . . . . . . . . . . 5858 14 28 . 1 1 16 16 VAL H H 1 7.58 . . . . . . . . . . . 5858 14 29 . 1 1 17 17 PHE N N 15 120.2 . . . . . . . . . . . 5858 14 30 . 1 1 17 17 PHE H H 1 8.71 . . . . . . . . . . . 5858 14 31 . 1 1 18 18 GLU N N 15 122.2 . . . . . . . . . . . 5858 14 32 . 1 1 18 18 GLU H H 1 9.08 . . . . . . . . . . . 5858 14 33 . 1 1 20 20 ALA N N 15 117.1 . . . . . . . . . . . 5858 14 34 . 1 1 20 20 ALA H H 1 8.21 . . . . . . . . . . . 5858 14 35 . 1 1 21 21 LYS N N 15 115.9 . . . . . . . . . . . 5858 14 36 . 1 1 21 21 LYS H H 1 7.47 . . . . . . . . . . . 5858 14 37 . 1 1 22 22 LEU N N 15 121.7 . . . . . . . . . . . 5858 14 38 . 1 1 22 22 LEU H H 1 7.89 . . . . . . . . . . . 5858 14 39 . 1 1 23 23 THR N N 15 121.1 . . . . . . . . . . . 5858 14 40 . 1 1 23 23 THR H H 1 8.27 . . . . . . . . . . . 5858 14 41 . 1 1 24 24 ILE N N 15 120.8 . . . . . . . . . . . 5858 14 42 . 1 1 24 24 ILE H H 1 9.00 . . . . . . . . . . . 5858 14 43 . 1 1 25 25 LYS N N 15 119.8 . . . . . . . . . . . 5858 14 44 . 1 1 25 25 LYS H H 1 9.07 . . . . . . . . . . . 5858 14 45 . 1 1 27 27 GLY N N 15 114.6 . . . . . . . . . . . 5858 14 46 . 1 1 27 27 GLY H H 1 7.21 . . . . . . . . . . . 5858 14 47 . 1 1 28 28 ASP N N 15 119.9 . . . . . . . . . . . 5858 14 48 . 1 1 28 28 ASP H H 1 7.99 . . . . . . . . . . . 5858 14 49 . 1 1 29 29 THR N N 15 114.8 . . . . . . . . . . . 5858 14 50 . 1 1 29 29 THR H H 1 8.73 . . . . . . . . . . . 5858 14 51 . 1 1 30 30 VAL N N 15 126.5 . . . . . . . . . . . 5858 14 52 . 1 1 30 30 VAL H H 1 9.24 . . . . . . . . . . . 5858 14 53 . 1 1 31 31 GLU N N 15 128.8 . . . . . . . . . . . 5858 14 54 . 1 1 31 31 GLU H H 1 9.31 . . . . . . . . . . . 5858 14 55 . 1 1 32 32 PHE N N 15 125.9 . . . . . . . . . . . 5858 14 56 . 1 1 32 32 PHE H H 1 9.24 . . . . . . . . . . . 5858 14 57 . 1 1 33 33 LEU N N 15 125.4 . . . . . . . . . . . 5858 14 58 . 1 1 33 33 LEU H H 1 9.07 . . . . . . . . . . . 5858 14 59 . 1 1 34 34 ASN N N 15 127.4 . . . . . . . . . . . 5858 14 60 . 1 1 34 34 ASN H H 1 9.41 . . . . . . . . . . . 5858 14 61 . 1 1 35 35 ASN N N 15 129.8 . . . . . . . . . . . 5858 14 62 . 1 1 35 35 ASN H H 1 8.85 . . . . . . . . . . . 5858 14 63 . 1 1 36 36 LYS N N 15 116.8 . . . . . . . . . . . 5858 14 64 . 1 1 36 36 LYS H H 1 8.18 . . . . . . . . . . . 5858 14 65 . 1 1 37 37 VAL N N 15 115.9 . . . . . . . . . . . 5858 14 66 . 1 1 37 37 VAL H H 1 9.01 . . . . . . . . . . . 5858 14 67 . 1 1 40 40 HIS N N 15 112.3 . . . . . . . . . . . 5858 14 68 . 1 1 40 40 HIS H H 1 7.31 . . . . . . . . . . . 5858 14 69 . 1 1 41 41 ASN N N 15 123.0 . . . . . . . . . . . 5858 14 70 . 1 1 41 41 ASN H H 1 9.92 . . . . . . . . . . . 5858 14 71 . 1 1 42 42 VAL N N 15 109.1 . . . . . . . . . . . 5858 14 72 . 1 1 42 42 VAL H H 1 7.06 . . . . . . . . . . . 5858 14 73 . 1 1 43 43 VAL N N 15 128.5 . . . . . . . . . . . 5858 14 74 . 1 1 43 43 VAL H H 1 9.51 . . . . . . . . . . . 5858 14 75 . 1 1 44 44 PHE N N 15 125.6 . . . . . . . . . . . 5858 14 76 . 1 1 44 44 PHE H H 1 8.79 . . . . . . . . . . . 5858 14 77 . 1 1 45 45 ASP N N 15 124.1 . . . . . . . . . . . 5858 14 78 . 1 1 45 45 ASP H H 1 8.46 . . . . . . . . . . . 5858 14 79 . 1 1 46 46 ALA N N 15 128.3 . . . . . . . . . . . 5858 14 80 . 1 1 46 46 ALA H H 1 8.67 . . . . . . . . . . . 5858 14 81 . 1 1 47 47 ALA N N 15 117.6 . . . . . . . . . . . 5858 14 82 . 1 1 47 47 ALA H H 1 8.55 . . . . . . . . . . . 5858 14 83 . 1 1 48 48 LEU N N 15 123.0 . . . . . . . . . . . 5858 14 84 . 1 1 48 48 LEU H H 1 8.72 . . . . . . . . . . . 5858 14 85 . 1 1 49 49 ASN N N 15 114.7 . . . . . . . . . . . 5858 14 86 . 1 1 49 49 ASN H H 1 8.13 . . . . . . . . . . . 5858 14 87 . 1 1 51 51 ALA N N 15 115.7 . . . . . . . . . . . 5858 14 88 . 1 1 51 51 ALA H H 1 7.12 . . . . . . . . . . . 5858 14 89 . 1 1 52 52 LYS N N 15 120.4 . . . . . . . . . . . 5858 14 90 . 1 1 52 52 LYS H H 1 8.05 . . . . . . . . . . . 5858 14 91 . 1 1 53 53 SER N N 15 109.9 . . . . . . . . . . . 5858 14 92 . 1 1 53 53 SER H H 1 8.28 . . . . . . . . . . . 5858 14 93 . 1 1 54 54 ALA N N 15 134.0 . . . . . . . . . . . 5858 14 94 . 1 1 54 54 ALA H H 1 9.24 . . . . . . . . . . . 5858 14 95 . 1 1 55 55 ASP N N 15 119.9 . . . . . . . . . . . 5858 14 96 . 1 1 55 55 ASP H H 1 8.44 . . . . . . . . . . . 5858 14 97 . 1 1 56 56 LEU N N 15 123.6 . . . . . . . . . . . 5858 14 98 . 1 1 56 56 LEU H H 1 8.19 . . . . . . . . . . . 5858 14 99 . 1 1 57 57 ALA N N 15 119.6 . . . . . . . . . . . 5858 14 100 . 1 1 57 57 ALA H H 1 7.64 . . . . . . . . . . . 5858 14 101 . 1 1 58 58 LYS N N 15 120.9 . . . . . . . . . . . 5858 14 102 . 1 1 58 58 LYS H H 1 8.62 . . . . . . . . . . . 5858 14 103 . 1 1 59 59 SER N N 15 115.4 . . . . . . . . . . . 5858 14 104 . 1 1 59 59 SER H H 1 7.83 . . . . . . . . . . . 5858 14 105 . 1 1 60 60 LEU N N 15 120.4 . . . . . . . . . . . 5858 14 106 . 1 1 60 60 LEU H H 1 7.02 . . . . . . . . . . . 5858 14 107 . 1 1 61 61 SER N N 15 111.2 . . . . . . . . . . . 5858 14 108 . 1 1 61 61 SER H H 1 7.07 . . . . . . . . . . . 5858 14 109 . 1 1 62 62 HIS N N 15 120.8 . . . . . . . . . . . 5858 14 110 . 1 1 62 62 HIS H H 1 9.71 . . . . . . . . . . . 5858 14 111 . 1 1 63 63 LYS N N 15 123.3 . . . . . . . . . . . 5858 14 112 . 1 1 63 63 LYS H H 1 8.83 . . . . . . . . . . . 5858 14 113 . 1 1 64 64 GLN N N 15 120.3 . . . . . . . . . . . 5858 14 114 . 1 1 64 64 GLN H H 1 8.42 . . . . . . . . . . . 5858 14 115 . 1 1 65 65 LEU N N 15 121.8 . . . . . . . . . . . 5858 14 116 . 1 1 65 65 LEU H H 1 8.26 . . . . . . . . . . . 5858 14 117 . 1 1 66 66 LEU N N 15 124.9 . . . . . . . . . . . 5858 14 118 . 1 1 66 66 LEU H H 1 9.55 . . . . . . . . . . . 5858 14 119 . 1 1 67 67 MET N N 15 122.0 . . . . . . . . . . . 5858 14 120 . 1 1 67 67 MET H H 1 8.19 . . . . . . . . . . . 5858 14 121 . 1 1 68 68 SER N N 15 113.8 . . . . . . . . . . . 5858 14 122 . 1 1 68 68 SER H H 1 8.41 . . . . . . . . . . . 5858 14 123 . 1 1 70 70 GLY N N 15 112.8 . . . . . . . . . . . 5858 14 124 . 1 1 70 70 GLY H H 1 9.11 . . . . . . . . . . . 5858 14 125 . 1 1 71 71 GLN N N 15 119.9 . . . . . . . . . . . 5858 14 126 . 1 1 71 71 GLN H H 1 7.62 . . . . . . . . . . . 5858 14 127 . 1 1 72 72 SER N N 15 116.0 . . . . . . . . . . . 5858 14 128 . 1 1 72 72 SER H H 1 8.70 . . . . . . . . . . . 5858 14 129 . 1 1 73 73 THR N N 15 116.2 . . . . . . . . . . . 5858 14 130 . 1 1 73 73 THR H H 1 8.82 . . . . . . . . . . . 5858 14 131 . 1 1 74 74 SER N N 15 118.4 . . . . . . . . . . . 5858 14 132 . 1 1 74 74 SER H H 1 8.23 . . . . . . . . . . . 5858 14 133 . 1 1 75 75 THR N N 15 121.1 . . . . . . . . . . . 5858 14 134 . 1 1 75 75 THR H H 1 9.62 . . . . . . . . . . . 5858 14 135 . 1 1 76 76 THR N N 15 127.1 . . . . . . . . . . . 5858 14 136 . 1 1 76 76 THR H H 1 9.13 . . . . . . . . . . . 5858 14 137 . 1 1 77 77 PHE N N 15 131.5 . . . . . . . . . . . 5858 14 138 . 1 1 77 77 PHE H H 1 9.24 . . . . . . . . . . . 5858 14 139 . 1 1 79 79 ALA N N 15 123.2 . . . . . . . . . . . 5858 14 140 . 1 1 79 79 ALA H H 1 8.86 . . . . . . . . . . . 5858 14 141 . 1 1 80 80 ASP N N 15 113.2 . . . . . . . . . . . 5858 14 142 . 1 1 80 80 ASP H H 1 8.11 . . . . . . . . . . . 5858 14 143 . 1 1 81 81 ALA N N 15 124.6 . . . . . . . . . . . 5858 14 144 . 1 1 81 81 ALA H H 1 7.66 . . . . . . . . . . . 5858 14 145 . 1 1 83 83 ALA N N 15 124.7 . . . . . . . . . . . 5858 14 146 . 1 1 83 83 ALA H H 1 8.42 . . . . . . . . . . . 5858 14 147 . 1 1 84 84 GLY N N 15 107.4 . . . . . . . . . . . 5858 14 148 . 1 1 84 84 GLY H H 1 8.93 . . . . . . . . . . . 5858 14 149 . 1 1 85 85 GLU N N 15 119.9 . . . . . . . . . . . 5858 14 150 . 1 1 85 85 GLU H H 1 8.54 . . . . . . . . . . . 5858 14 151 . 1 1 86 86 TYR N N 15 125.6 . . . . . . . . . . . 5858 14 152 . 1 1 86 86 TYR H H 1 10.25 . . . . . . . . . . . 5858 14 153 . 1 1 87 87 THR N N 15 121.5 . . . . . . . . . . . 5858 14 154 . 1 1 87 87 THR H H 1 8.70 . . . . . . . . . . . 5858 14 155 . 1 1 88 88 PHE N N 15 126.3 . . . . . . . . . . . 5858 14 156 . 1 1 88 88 PHE H H 1 8.67 . . . . . . . . . . . 5858 14 157 . 1 1 89 89 TYR N N 15 115.3 . . . . . . . . . . . 5858 14 158 . 1 1 89 89 TYR H H 1 9.06 . . . . . . . . . . . 5858 14 159 . 1 1 90 90 CYS N N 15 125.2 . . . . . . . . . . . 5858 14 160 . 1 1 90 90 CYS H H 1 7.84 . . . . . . . . . . . 5858 14 161 . 1 1 91 91 GLU N N 15 125.8 . . . . . . . . . . . 5858 14 162 . 1 1 91 91 GLU H H 1 10.09 . . . . . . . . . . . 5858 14 163 . 1 1 93 93 HIS N N 15 115.2 . . . . . . . . . . . 5858 14 164 . 1 1 93 93 HIS H H 1 8.65 . . . . . . . . . . . 5858 14 165 . 1 1 94 94 ARG N N 15 129.1 . . . . . . . . . . . 5858 14 166 . 1 1 94 94 ARG H H 1 8.54 . . . . . . . . . . . 5858 14 167 . 1 1 95 95 GLY N N 15 107.6 . . . . . . . . . . . 5858 14 168 . 1 1 95 95 GLY H H 1 9.15 . . . . . . . . . . . 5858 14 169 . 1 1 96 96 ALA N N 15 121.7 . . . . . . . . . . . 5858 14 170 . 1 1 96 96 ALA H H 1 7.65 . . . . . . . . . . . 5858 14 171 . 1 1 97 97 GLY N N 15 106.2 . . . . . . . . . . . 5858 14 172 . 1 1 97 97 GLY H H 1 8.16 . . . . . . . . . . . 5858 14 173 . 1 1 98 98 MET N N 15 124.0 . . . . . . . . . . . 5858 14 174 . 1 1 98 98 MET H H 1 7.69 . . . . . . . . . . . 5858 14 175 . 1 1 99 99 VAL N N 15 126.0 . . . . . . . . . . . 5858 14 176 . 1 1 99 99 VAL H H 1 8.04 . . . . . . . . . . . 5858 14 177 . 1 1 100 100 GLY N N 15 118.0 . . . . . . . . . . . 5858 14 178 . 1 1 100 100 GLY H H 1 9.05 . . . . . . . . . . . 5858 14 179 . 1 1 101 101 LYS N N 15 117.7 . . . . . . . . . . . 5858 14 180 . 1 1 101 101 LYS H H 1 8.37 . . . . . . . . . . . 5858 14 181 . 1 1 102 102 ILE N N 15 127.1 . . . . . . . . . . . 5858 14 182 . 1 1 102 102 ILE H H 1 9.54 . . . . . . . . . . . 5858 14 183 . 1 1 103 103 THR N N 15 126.1 . . . . . . . . . . . 5858 14 184 . 1 1 103 103 THR H H 1 9.34 . . . . . . . . . . . 5858 14 185 . 1 1 104 104 VAL N N 15 128.8 . . . . . . . . . . . 5858 14 186 . 1 1 104 104 VAL H H 1 9.40 . . . . . . . . . . . 5858 14 187 . 1 1 105 105 ALA N N 15 133.7 . . . . . . . . . . . 5858 14 188 . 1 1 105 105 ALA H H 1 9.30 . . . . . . . . . . . 5858 14 189 . 1 1 106 106 GLY N N 15 113.8 . . . . . . . . . . . 5858 14 190 . 1 1 106 106 GLY H H 1 7.83 . . . . . . . . . . . 5858 14 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_relax_1_1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode relax_1_1 _Heteronucl_T1_list.Entry_ID 5858 _Heteronucl_T1_list.ID 1 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $Condition_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 800 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 5858 1 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 4 4 TYR N N 15 1.349 0.020 . . . . . 5858 1 2 . 1 1 5 5 THR N N 15 1.278 0.009 . . . . . 5858 1 3 . 1 1 6 6 VAL N N 15 1.344 0.021 . . . . . 5858 1 4 . 1 1 7 7 LYS N N 15 1.382 0.015 . . . . . 5858 1 5 . 1 1 8 8 LEU N N 15 1.373 0.017 . . . . . 5858 1 6 . 1 1 9 9 GLY N N 15 1.220 0.017 . . . . . 5858 1 7 . 1 1 10 10 SER N N 15 1.468 0.012 . . . . . 5858 1 8 . 1 1 13 13 GLY N N 15 1.445 0.018 . . . . . 5858 1 9 . 1 1 14 14 LEU N N 15 1.436 0.014 . . . . . 5858 1 10 . 1 1 15 15 LEU N N 15 1.346 0.006 . . . . . 5858 1 11 . 1 1 16 16 VAL N N 15 1.302 0.026 . . . . . 5858 1 12 . 1 1 17 17 PHE N N 15 1.400 0.008 . . . . . 5858 1 13 . 1 1 18 18 GLU N N 15 1.379 0.018 . . . . . 5858 1 14 . 1 1 20 20 ALA N N 15 1.171 0.012 . . . . . 5858 1 15 . 1 1 21 21 LYS N N 15 1.289 0.017 . . . . . 5858 1 16 . 1 1 22 22 LEU N N 15 1.325 0.008 . . . . . 5858 1 17 . 1 1 23 23 THR N N 15 1.317 0.021 . . . . . 5858 1 18 . 1 1 24 24 ILE N N 15 1.395 0.012 . . . . . 5858 1 19 . 1 1 25 25 LYS N N 15 1.359 0.015 . . . . . 5858 1 20 . 1 1 27 27 GLY N N 15 1.384 0.012 . . . . . 5858 1 21 . 1 1 28 28 ASP N N 15 1.483 0.014 . . . . . 5858 1 22 . 1 1 29 29 THR N N 15 1.349 0.017 . . . . . 5858 1 23 . 1 1 30 30 VAL N N 15 1.366 0.012 . . . . . 5858 1 24 . 1 1 31 31 GLU N N 15 1.400 0.015 . . . . . 5858 1 25 . 1 1 32 32 PHE N N 15 1.336 0.019 . . . . . 5858 1 26 . 1 1 33 33 LEU N N 15 1.369 0.008 . . . . . 5858 1 27 . 1 1 34 34 ASN N N 15 1.448 0.014 . . . . . 5858 1 28 . 1 1 35 35 ASN N N 15 1.385 0.020 . . . . . 5858 1 29 . 1 1 36 36 LYS N N 15 1.345 0.008 . . . . . 5858 1 30 . 1 1 37 37 VAL N N 15 1.349 0.016 . . . . . 5858 1 31 . 1 1 40 40 HIS N N 15 1.319 0.021 . . . . . 5858 1 32 . 1 1 41 41 ASN N N 15 1.384 0.010 . . . . . 5858 1 33 . 1 1 42 42 VAL N N 15 1.317 0.022 . . . . . 5858 1 34 . 1 1 43 43 VAL N N 15 1.323 0.021 . . . . . 5858 1 35 . 1 1 44 44 PHE N N 15 1.409 0.008 . . . . . 5858 1 36 . 1 1 45 45 ASP N N 15 1.467 0.009 . . . . . 5858 1 37 . 1 1 46 46 ALA N N 15 1.576 0.222 . . . . . 5858 1 38 . 1 1 47 47 ALA N N 15 1.318 0.009 . . . . . 5858 1 39 . 1 1 48 48 LEU N N 15 1.179 0.011 . . . . . 5858 1 40 . 1 1 49 49 ASN N N 15 1.326 0.007 . . . . . 5858 1 41 . 1 1 51 51 ALA N N 15 1.340 0.008 . . . . . 5858 1 42 . 1 1 52 52 LYS N N 15 1.503 0.007 . . . . . 5858 1 43 . 1 1 53 53 SER N N 15 1.451 0.007 . . . . . 5858 1 44 . 1 1 56 56 LEU N N 15 1.430 0.031 . . . . . 5858 1 45 . 1 1 57 57 ALA N N 15 1.372 0.016 . . . . . 5858 1 46 . 1 1 58 58 LYS N N 15 1.400 0.009 . . . . . 5858 1 47 . 1 1 59 59 SER N N 15 1.374 0.023 . . . . . 5858 1 48 . 1 1 60 60 LEU N N 15 1.482 0.009 . . . . . 5858 1 49 . 1 1 61 61 SER N N 15 1.280 0.020 . . . . . 5858 1 50 . 1 1 62 62 HIS N N 15 1.403 0.019 . . . . . 5858 1 51 . 1 1 63 63 LYS N N 15 1.091 0.142 . . . . . 5858 1 52 . 1 1 64 64 GLN N N 15 1.413 0.029 . . . . . 5858 1 53 . 1 1 65 65 LEU N N 15 1.349 0.014 . . . . . 5858 1 54 . 1 1 66 66 LEU N N 15 1.370 0.013 . . . . . 5858 1 55 . 1 1 67 67 MET N N 15 1.322 0.024 . . . . . 5858 1 56 . 1 1 68 68 SER N N 15 1.229 0.032 . . . . . 5858 1 57 . 1 1 70 70 GLY N N 15 1.317 0.020 . . . . . 5858 1 58 . 1 1 71 71 GLN N N 15 1.368 0.011 . . . . . 5858 1 59 . 1 1 72 72 SER N N 15 1.431 0.014 . . . . . 5858 1 60 . 1 1 73 73 THR N N 15 1.408 0.013 . . . . . 5858 1 61 . 1 1 75 75 THR N N 15 1.338 0.011 . . . . . 5858 1 62 . 1 1 76 76 THR N N 15 1.349 0.027 . . . . . 5858 1 63 . 1 1 77 77 PHE N N 15 1.389 0.015 . . . . . 5858 1 64 . 1 1 79 79 ALA N N 15 1.651 0.135 . . . . . 5858 1 65 . 1 1 80 80 ASP N N 15 1.422 0.016 . . . . . 5858 1 66 . 1 1 81 81 ALA N N 15 1.414 0.015 . . . . . 5858 1 67 . 1 1 83 83 ALA N N 15 1.304 0.008 . . . . . 5858 1 68 . 1 1 84 84 GLY N N 15 1.369 0.019 . . . . . 5858 1 69 . 1 1 85 85 GLU N N 15 1.360 0.009 . . . . . 5858 1 70 . 1 1 86 86 TYR N N 15 1.351 0.009 . . . . . 5858 1 71 . 1 1 87 87 THR N N 15 1.285 0.011 . . . . . 5858 1 72 . 1 1 88 88 PHE N N 15 1.506 0.015 . . . . . 5858 1 73 . 1 1 89 89 TYR N N 15 1.383 0.012 . . . . . 5858 1 74 . 1 1 90 90 CYS N N 15 1.471 0.035 . . . . . 5858 1 75 . 1 1 91 91 GLU N N 15 1.468 0.014 . . . . . 5858 1 76 . 1 1 93 93 HIS N N 15 1.307 0.017 . . . . . 5858 1 77 . 1 1 94 94 ARG N N 15 1.478 0.020 . . . . . 5858 1 78 . 1 1 96 96 ALA N N 15 1.416 0.010 . . . . . 5858 1 79 . 1 1 97 97 GLY N N 15 1.455 0.023 . . . . . 5858 1 80 . 1 1 98 98 MET N N 15 1.412 0.017 . . . . . 5858 1 81 . 1 1 99 99 VAL N N 15 1.314 0.011 . . . . . 5858 1 82 . 1 1 100 100 GLY N N 15 1.420 0.020 . . . . . 5858 1 83 . 1 1 101 101 LYS N N 15 1.368 0.011 . . . . . 5858 1 84 . 1 1 102 102 ILE N N 15 1.365 0.011 . . . . . 5858 1 85 . 1 1 103 103 THR N N 15 1.317 0.018 . . . . . 5858 1 86 . 1 1 104 104 VAL N N 15 1.358 0.019 . . . . . 5858 1 87 . 1 1 105 105 ALA N N 15 1.398 0.013 . . . . . 5858 1 88 . 1 1 106 106 GLY N N 15 0.810 0.007 . . . . . 5858 1 stop_ save_ save_relax_1_2 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode relax_1_2 _Heteronucl_T1_list.Entry_ID 5858 _Heteronucl_T1_list.ID 2 _Heteronucl_T1_list.Sample_condition_list_ID 2 _Heteronucl_T1_list.Sample_condition_list_label $Condition_2 _Heteronucl_T1_list.Spectrometer_frequency_1H 800 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 5858 2 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 4 4 TYR N N 15 1.352 0.011 . . . . . 5858 2 2 . 1 1 5 5 THR N N 15 1.276 0.009 . . . . . 5858 2 3 . 1 1 6 6 VAL N N 15 1.371 0.013 . . . . . 5858 2 4 . 1 1 7 7 LYS N N 15 1.399 0.012 . . . . . 5858 2 5 . 1 1 8 8 LEU N N 15 1.396 0.008 . . . . . 5858 2 6 . 1 1 9 9 GLY N N 15 1.249 0.010 . . . . . 5858 2 7 . 1 1 10 10 SER N N 15 1.493 0.009 . . . . . 5858 2 8 . 1 1 11 11 ASP N N 15 1.412 0.077 . . . . . 5858 2 9 . 1 1 13 13 GLY N N 15 1.437 0.006 . . . . . 5858 2 10 . 1 1 14 14 LEU N N 15 1.434 0.015 . . . . . 5858 2 11 . 1 1 15 15 LEU N N 15 1.335 0.007 . . . . . 5858 2 12 . 1 1 16 16 VAL N N 15 1.339 0.019 . . . . . 5858 2 13 . 1 1 17 17 PHE N N 15 1.432 0.009 . . . . . 5858 2 14 . 1 1 18 18 GLU N N 15 1.395 0.010 . . . . . 5858 2 15 . 1 1 20 20 ALA N N 15 1.177 0.009 . . . . . 5858 2 16 . 1 1 21 21 LYS N N 15 1.300 0.012 . . . . . 5858 2 17 . 1 1 22 22 LEU N N 15 1.329 0.016 . . . . . 5858 2 18 . 1 1 23 23 THR N N 15 1.326 0.023 . . . . . 5858 2 19 . 1 1 24 24 ILE N N 15 1.420 0.011 . . . . . 5858 2 20 . 1 1 25 25 LYS N N 15 1.389 0.013 . . . . . 5858 2 21 . 1 1 27 27 GLY N N 15 1.399 0.013 . . . . . 5858 2 22 . 1 1 28 28 ASP N N 15 1.486 0.012 . . . . . 5858 2 23 . 1 1 29 29 THR N N 15 1.382 0.011 . . . . . 5858 2 24 . 1 1 30 30 VAL N N 15 1.379 0.012 . . . . . 5858 2 25 . 1 1 31 31 GLU N N 15 1.404 0.016 . . . . . 5858 2 26 . 1 1 32 32 PHE N N 15 1.347 0.013 . . . . . 5858 2 27 . 1 1 33 33 LEU N N 15 1.383 0.013 . . . . . 5858 2 28 . 1 1 34 34 ASN N N 15 1.459 0.010 . . . . . 5858 2 29 . 1 1 35 35 ASN N N 15 1.420 0.011 . . . . . 5858 2 30 . 1 1 36 36 LYS N N 15 1.337 0.007 . . . . . 5858 2 31 . 1 1 37 37 VAL N N 15 1.376 0.010 . . . . . 5858 2 32 . 1 1 40 40 HIS N N 15 1.328 0.014 . . . . . 5858 2 33 . 1 1 41 41 ASN N N 15 1.409 0.010 . . . . . 5858 2 34 . 1 1 42 42 VAL N N 15 1.346 0.017 . . . . . 5858 2 35 . 1 1 43 43 VAL N N 15 1.354 0.013 . . . . . 5858 2 36 . 1 1 44 44 PHE N N 15 1.424 0.011 . . . . . 5858 2 37 . 1 1 45 45 ASP N N 15 1.493 0.009 . . . . . 5858 2 38 . 1 1 46 46 ALA N N 15 1.324 0.022 . . . . . 5858 2 39 . 1 1 47 47 ALA N N 15 1.328 0.006 . . . . . 5858 2 40 . 1 1 48 48 LEU N N 15 1.184 0.006 . . . . . 5858 2 41 . 1 1 49 49 ASN N N 15 1.343 0.012 . . . . . 5858 2 42 . 1 1 51 51 ALA N N 15 1.349 0.013 . . . . . 5858 2 43 . 1 1 52 52 LYS N N 15 1.513 0.011 . . . . . 5858 2 44 . 1 1 53 53 SER N N 15 1.444 0.011 . . . . . 5858 2 45 . 1 1 56 56 LEU N N 15 1.505 0.016 . . . . . 5858 2 46 . 1 1 57 57 ALA N N 15 1.393 0.011 . . . . . 5858 2 47 . 1 1 58 58 LYS N N 15 1.424 0.010 . . . . . 5858 2 48 . 1 1 59 59 SER N N 15 1.404 0.013 . . . . . 5858 2 49 . 1 1 60 60 LEU N N 15 1.494 0.009 . . . . . 5858 2 50 . 1 1 61 61 SER N N 15 1.325 0.009 . . . . . 5858 2 51 . 1 1 62 62 HIS N N 15 1.392 0.020 . . . . . 5858 2 52 . 1 1 63 63 LYS N N 15 1.263 0.070 . . . . . 5858 2 53 . 1 1 64 64 GLN N N 15 1.435 0.021 . . . . . 5858 2 54 . 1 1 65 65 LEU N N 15 1.381 0.008 . . . . . 5858 2 55 . 1 1 66 66 LEU N N 15 1.387 0.007 . . . . . 5858 2 56 . 1 1 67 67 MET N N 15 1.331 0.007 . . . . . 5858 2 57 . 1 1 68 68 SER N N 15 1.263 0.015 . . . . . 5858 2 58 . 1 1 70 70 GLY N N 15 1.379 0.014 . . . . . 5858 2 59 . 1 1 71 71 GLN N N 15 1.358 0.013 . . . . . 5858 2 60 . 1 1 72 72 SER N N 15 1.429 0.009 . . . . . 5858 2 61 . 1 1 73 73 THR N N 15 1.449 0.009 . . . . . 5858 2 62 . 1 1 74 74 SER N N 15 1.298 0.021 . . . . . 5858 2 63 . 1 1 75 75 THR N N 15 1.351 0.015 . . . . . 5858 2 64 . 1 1 76 76 THR N N 15 1.360 0.014 . . . . . 5858 2 65 . 1 1 77 77 PHE N N 15 1.428 0.011 . . . . . 5858 2 66 . 1 1 79 79 ALA N N 15 1.375 0.021 . . . . . 5858 2 67 . 1 1 80 80 ASP N N 15 1.442 0.010 . . . . . 5858 2 68 . 1 1 81 81 ALA N N 15 1.407 0.016 . . . . . 5858 2 69 . 1 1 83 83 ALA N N 15 1.303 0.010 . . . . . 5858 2 70 . 1 1 84 84 GLY N N 15 1.380 0.013 . . . . . 5858 2 71 . 1 1 85 85 GLU N N 15 1.350 0.007 . . . . . 5858 2 72 . 1 1 86 86 TYR N N 15 1.374 0.009 . . . . . 5858 2 73 . 1 1 87 87 THR N N 15 1.286 0.012 . . . . . 5858 2 74 . 1 1 88 88 PHE N N 15 1.541 0.011 . . . . . 5858 2 75 . 1 1 89 89 TYR N N 15 1.379 0.011 . . . . . 5858 2 76 . 1 1 90 90 CYS N N 15 1.407 0.059 . . . . . 5858 2 77 . 1 1 91 91 GLU N N 15 1.490 0.013 . . . . . 5858 2 78 . 1 1 93 93 HIS N N 15 1.307 0.013 . . . . . 5858 2 79 . 1 1 94 94 ARG N N 15 1.533 0.010 . . . . . 5858 2 80 . 1 1 96 96 ALA N N 15 1.414 0.008 . . . . . 5858 2 81 . 1 1 97 97 GLY N N 15 1.477 0.014 . . . . . 5858 2 82 . 1 1 98 98 MET N N 15 1.429 0.013 . . . . . 5858 2 83 . 1 1 99 99 VAL N N 15 1.333 0.007 . . . . . 5858 2 84 . 1 1 100 100 GLY N N 15 1.446 0.014 . . . . . 5858 2 85 . 1 1 101 101 LYS N N 15 1.389 0.008 . . . . . 5858 2 86 . 1 1 102 102 ILE N N 15 1.369 0.007 . . . . . 5858 2 87 . 1 1 103 103 THR N N 15 1.326 0.011 . . . . . 5858 2 88 . 1 1 104 104 VAL N N 15 1.381 0.022 . . . . . 5858 2 89 . 1 1 105 105 ALA N N 15 1.408 0.007 . . . . . 5858 2 90 . 1 1 106 106 GLY N N 15 0.799 0.007 . . . . . 5858 2 stop_ save_ save_relax_1_3 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode relax_1_3 _Heteronucl_T1_list.Entry_ID 5858 _Heteronucl_T1_list.ID 3 _Heteronucl_T1_list.Sample_condition_list_ID 3 _Heteronucl_T1_list.Sample_condition_list_label $Condition_3 _Heteronucl_T1_list.Spectrometer_frequency_1H 800 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 5858 3 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 THR N N 15 1.291 0.064 . . . . . 5858 3 2 . 1 1 4 4 TYR N N 15 1.347 0.014 . . . . . 5858 3 3 . 1 1 5 5 THR N N 15 1.269 0.014 . . . . . 5858 3 4 . 1 1 6 6 VAL N N 15 1.371 0.022 . . . . . 5858 3 5 . 1 1 7 7 LYS N N 15 1.387 0.018 . . . . . 5858 3 6 . 1 1 8 8 LEU N N 15 1.399 0.019 . . . . . 5858 3 7 . 1 1 9 9 GLY N N 15 1.242 0.017 . . . . . 5858 3 8 . 1 1 10 10 SER N N 15 1.478 0.010 . . . . . 5858 3 9 . 1 1 11 11 ASP N N 15 1.387 0.036 . . . . . 5858 3 10 . 1 1 13 13 GLY N N 15 1.406 0.009 . . . . . 5858 3 11 . 1 1 14 14 LEU N N 15 1.443 0.017 . . . . . 5858 3 12 . 1 1 15 15 LEU N N 15 1.334 0.012 . . . . . 5858 3 13 . 1 1 16 16 VAL N N 15 1.325 0.020 . . . . . 5858 3 14 . 1 1 17 17 PHE N N 15 1.427 0.012 . . . . . 5858 3 15 . 1 1 18 18 GLU N N 15 1.404 0.019 . . . . . 5858 3 16 . 1 1 20 20 ALA N N 15 1.180 0.012 . . . . . 5858 3 17 . 1 1 21 21 LYS N N 15 1.291 0.023 . . . . . 5858 3 18 . 1 1 22 22 LEU N N 15 1.317 0.018 . . . . . 5858 3 19 . 1 1 23 23 THR N N 15 1.334 0.010 . . . . . 5858 3 20 . 1 1 24 24 ILE N N 15 1.418 0.018 . . . . . 5858 3 21 . 1 1 25 25 LYS N N 15 1.374 0.018 . . . . . 5858 3 22 . 1 1 27 27 GLY N N 15 1.410 0.018 . . . . . 5858 3 23 . 1 1 28 28 ASP N N 15 1.508 0.013 . . . . . 5858 3 24 . 1 1 29 29 THR N N 15 1.378 0.010 . . . . . 5858 3 25 . 1 1 30 30 VAL N N 15 1.376 0.014 . . . . . 5858 3 26 . 1 1 31 31 GLU N N 15 1.405 0.022 . . . . . 5858 3 27 . 1 1 32 32 PHE N N 15 1.363 0.018 . . . . . 5858 3 28 . 1 1 33 33 LEU N N 15 1.377 0.012 . . . . . 5858 3 29 . 1 1 34 34 ASN N N 15 1.470 0.012 . . . . . 5858 3 30 . 1 1 35 35 ASN N N 15 1.408 0.013 . . . . . 5858 3 31 . 1 1 36 36 LYS N N 15 1.327 0.013 . . . . . 5858 3 32 . 1 1 37 37 VAL N N 15 1.380 0.014 . . . . . 5858 3 33 . 1 1 40 40 HIS N N 15 1.328 0.018 . . . . . 5858 3 34 . 1 1 41 41 ASN N N 15 1.420 0.014 . . . . . 5858 3 35 . 1 1 42 42 VAL N N 15 1.349 0.024 . . . . . 5858 3 36 . 1 1 43 43 VAL N N 15 1.370 0.018 . . . . . 5858 3 37 . 1 1 44 44 PHE N N 15 1.433 0.013 . . . . . 5858 3 38 . 1 1 45 45 ASP N N 15 1.480 0.009 . . . . . 5858 3 39 . 1 1 46 46 ALA N N 15 1.347 0.022 . . . . . 5858 3 40 . 1 1 47 47 ALA N N 15 1.328 0.007 . . . . . 5858 3 41 . 1 1 48 48 LEU N N 15 1.181 0.010 . . . . . 5858 3 42 . 1 1 49 49 ASN N N 15 1.338 0.012 . . . . . 5858 3 43 . 1 1 51 51 ALA N N 15 1.339 0.015 . . . . . 5858 3 44 . 1 1 52 52 LYS N N 15 1.509 0.014 . . . . . 5858 3 45 . 1 1 53 53 SER N N 15 1.435 0.009 . . . . . 5858 3 46 . 1 1 56 56 LEU N N 15 1.521 0.015 . . . . . 5858 3 47 . 1 1 57 57 ALA N N 15 1.383 0.014 . . . . . 5858 3 48 . 1 1 58 58 LYS N N 15 1.410 0.012 . . . . . 5858 3 49 . 1 1 59 59 SER N N 15 1.406 0.012 . . . . . 5858 3 50 . 1 1 60 60 LEU N N 15 1.486 0.014 . . . . . 5858 3 51 . 1 1 61 61 SER N N 15 1.313 0.012 . . . . . 5858 3 52 . 1 1 62 62 HIS N N 15 1.393 0.021 . . . . . 5858 3 53 . 1 1 63 63 LYS N N 15 1.344 0.055 . . . . . 5858 3 54 . 1 1 64 64 GLN N N 15 1.427 0.016 . . . . . 5858 3 55 . 1 1 65 65 LEU N N 15 1.384 0.009 . . . . . 5858 3 56 . 1 1 66 66 LEU N N 15 1.404 0.009 . . . . . 5858 3 57 . 1 1 67 67 MET N N 15 1.313 0.008 . . . . . 5858 3 58 . 1 1 68 68 SER N N 15 1.289 0.019 . . . . . 5858 3 59 . 1 1 70 70 GLY N N 15 1.376 0.011 . . . . . 5858 3 60 . 1 1 71 71 GLN N N 15 1.362 0.018 . . . . . 5858 3 61 . 1 1 72 72 SER N N 15 1.431 0.012 . . . . . 5858 3 62 . 1 1 73 73 THR N N 15 1.460 0.012 . . . . . 5858 3 63 . 1 1 74 74 SER N N 15 1.360 0.025 . . . . . 5858 3 64 . 1 1 75 75 THR N N 15 1.358 0.014 . . . . . 5858 3 65 . 1 1 76 76 THR N N 15 1.361 0.015 . . . . . 5858 3 66 . 1 1 77 77 PHE N N 15 1.419 0.010 . . . . . 5858 3 67 . 1 1 79 79 ALA N N 15 1.363 0.030 . . . . . 5858 3 68 . 1 1 80 80 ASP N N 15 1.423 0.011 . . . . . 5858 3 69 . 1 1 81 81 ALA N N 15 1.406 0.023 . . . . . 5858 3 70 . 1 1 83 83 ALA N N 15 1.309 0.011 . . . . . 5858 3 71 . 1 1 84 84 GLY N N 15 1.371 0.018 . . . . . 5858 3 72 . 1 1 85 85 GLU N N 15 1.366 0.010 . . . . . 5858 3 73 . 1 1 86 86 TYR N N 15 1.358 0.011 . . . . . 5858 3 74 . 1 1 87 87 THR N N 15 1.287 0.014 . . . . . 5858 3 75 . 1 1 88 88 PHE N N 15 1.542 0.014 . . . . . 5858 3 76 . 1 1 89 89 TYR N N 15 1.382 0.016 . . . . . 5858 3 77 . 1 1 90 90 CYS N N 15 1.406 0.046 . . . . . 5858 3 78 . 1 1 91 91 GLU N N 15 1.486 0.016 . . . . . 5858 3 79 . 1 1 93 93 HIS N N 15 1.319 0.020 . . . . . 5858 3 80 . 1 1 94 94 ARG N N 15 1.513 0.014 . . . . . 5858 3 81 . 1 1 96 96 ALA N N 15 1.404 0.014 . . . . . 5858 3 82 . 1 1 97 97 GLY N N 15 1.482 0.011 . . . . . 5858 3 83 . 1 1 98 98 MET N N 15 1.432 0.017 . . . . . 5858 3 84 . 1 1 99 99 VAL N N 15 1.312 0.011 . . . . . 5858 3 85 . 1 1 100 100 GLY N N 15 1.440 0.020 . . . . . 5858 3 86 . 1 1 101 101 LYS N N 15 1.388 0.009 . . . . . 5858 3 87 . 1 1 102 102 ILE N N 15 1.364 0.015 . . . . . 5858 3 88 . 1 1 103 103 THR N N 15 1.341 0.017 . . . . . 5858 3 89 . 1 1 104 104 VAL N N 15 1.358 0.021 . . . . . 5858 3 90 . 1 1 105 105 ALA N N 15 1.408 0.016 . . . . . 5858 3 91 . 1 1 106 106 GLY N N 15 0.794 0.010 . . . . . 5858 3 stop_ save_ save_relax_1_4 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode relax_1_4 _Heteronucl_T1_list.Entry_ID 5858 _Heteronucl_T1_list.ID 4 _Heteronucl_T1_list.Sample_condition_list_ID 4 _Heteronucl_T1_list.Sample_condition_list_label $Condition_4 _Heteronucl_T1_list.Spectrometer_frequency_1H 800 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 5858 4 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 THR N N 15 1.378 0.027 . . . . . 5858 4 2 . 1 1 4 4 TYR N N 15 1.370 0.013 . . . . . 5858 4 3 . 1 1 5 5 THR N N 15 1.251 0.014 . . . . . 5858 4 4 . 1 1 6 6 VAL N N 15 1.402 0.014 . . . . . 5858 4 5 . 1 1 7 7 LYS N N 15 1.417 0.014 . . . . . 5858 4 6 . 1 1 8 8 LEU N N 15 1.418 0.011 . . . . . 5858 4 7 . 1 1 9 9 GLY N N 15 1.251 0.013 . . . . . 5858 4 8 . 1 1 10 10 SER N N 15 1.494 0.014 . . . . . 5858 4 9 . 1 1 11 11 ASP N N 15 1.398 0.026 . . . . . 5858 4 10 . 1 1 13 13 GLY N N 15 1.439 0.007 . . . . . 5858 4 11 . 1 1 14 14 LEU N N 15 1.445 0.013 . . . . . 5858 4 12 . 1 1 15 15 LEU N N 15 1.338 0.011 . . . . . 5858 4 13 . 1 1 16 16 VAL N N 15 1.362 0.012 . . . . . 5858 4 14 . 1 1 17 17 PHE N N 15 1.438 0.010 . . . . . 5858 4 15 . 1 1 18 18 GLU N N 15 1.432 0.015 . . . . . 5858 4 16 . 1 1 20 20 ALA N N 15 1.199 0.011 . . . . . 5858 4 17 . 1 1 21 21 LYS N N 15 1.334 0.018 . . . . . 5858 4 18 . 1 1 22 22 LEU N N 15 1.338 0.021 . . . . . 5858 4 19 . 1 1 23 23 THR N N 15 1.330 0.006 . . . . . 5858 4 20 . 1 1 24 24 ILE N N 15 1.436 0.010 . . . . . 5858 4 21 . 1 1 25 25 LYS N N 15 1.397 0.013 . . . . . 5858 4 22 . 1 1 27 27 GLY N N 15 1.409 0.009 . . . . . 5858 4 23 . 1 1 28 28 ASP N N 15 1.513 0.019 . . . . . 5858 4 24 . 1 1 29 29 THR N N 15 1.411 0.010 . . . . . 5858 4 25 . 1 1 30 30 VAL N N 15 1.388 0.013 . . . . . 5858 4 26 . 1 1 31 31 GLU N N 15 1.419 0.022 . . . . . 5858 4 27 . 1 1 32 32 PHE N N 15 1.357 0.019 . . . . . 5858 4 28 . 1 1 33 33 LEU N N 15 1.394 0.015 . . . . . 5858 4 29 . 1 1 34 34 ASN N N 15 1.481 0.011 . . . . . 5858 4 30 . 1 1 35 35 ASN N N 15 1.426 0.008 . . . . . 5858 4 31 . 1 1 36 36 LYS N N 15 1.327 0.012 . . . . . 5858 4 32 . 1 1 37 37 VAL N N 15 1.406 0.011 . . . . . 5858 4 33 . 1 1 40 40 HIS N N 15 1.355 0.017 . . . . . 5858 4 34 . 1 1 41 41 ASN N N 15 1.436 0.011 . . . . . 5858 4 35 . 1 1 42 42 VAL N N 15 1.358 0.012 . . . . . 5858 4 36 . 1 1 43 43 VAL N N 15 1.373 0.014 . . . . . 5858 4 37 . 1 1 44 44 PHE N N 15 1.451 0.017 . . . . . 5858 4 38 . 1 1 45 45 ASP N N 15 1.511 0.009 . . . . . 5858 4 39 . 1 1 46 46 ALA N N 15 1.385 0.016 . . . . . 5858 4 40 . 1 1 47 47 ALA N N 15 1.343 0.009 . . . . . 5858 4 41 . 1 1 48 48 LEU N N 15 1.205 0.008 . . . . . 5858 4 42 . 1 1 49 49 ASN N N 15 1.363 0.007 . . . . . 5858 4 43 . 1 1 51 51 ALA N N 15 1.352 0.009 . . . . . 5858 4 44 . 1 1 52 52 LYS N N 15 1.502 0.009 . . . . . 5858 4 45 . 1 1 53 53 SER N N 15 1.468 0.019 . . . . . 5858 4 46 . 1 1 54 54 ALA N N 15 1.377 0.052 . . . . . 5858 4 47 . 1 1 55 55 ASP N N 15 1.387 0.029 . . . . . 5858 4 48 . 1 1 56 56 LEU N N 15 1.516 0.015 . . . . . 5858 4 49 . 1 1 57 57 ALA N N 15 1.425 0.021 . . . . . 5858 4 50 . 1 1 58 58 LYS N N 15 1.441 0.006 . . . . . 5858 4 51 . 1 1 59 59 SER N N 15 1.422 0.009 . . . . . 5858 4 52 . 1 1 60 60 LEU N N 15 1.512 0.009 . . . . . 5858 4 53 . 1 1 61 61 SER N N 15 1.326 0.009 . . . . . 5858 4 54 . 1 1 62 62 HIS N N 15 1.407 0.024 . . . . . 5858 4 55 . 1 1 63 63 LYS N N 15 1.302 0.068 . . . . . 5858 4 56 . 1 1 64 64 GLN N N 15 1.444 0.012 . . . . . 5858 4 57 . 1 1 65 65 LEU N N 15 1.386 0.008 . . . . . 5858 4 58 . 1 1 66 66 LEU N N 15 1.431 0.008 . . . . . 5858 4 59 . 1 1 67 67 MET N N 15 1.303 0.013 . . . . . 5858 4 60 . 1 1 68 68 SER N N 15 1.298 0.008 . . . . . 5858 4 61 . 1 1 70 70 GLY N N 15 1.369 0.013 . . . . . 5858 4 62 . 1 1 71 71 GLN N N 15 1.376 0.017 . . . . . 5858 4 63 . 1 1 72 72 SER N N 15 1.404 0.025 . . . . . 5858 4 64 . 1 1 73 73 THR N N 15 1.438 0.014 . . . . . 5858 4 65 . 1 1 74 74 SER N N 15 1.420 0.025 . . . . . 5858 4 66 . 1 1 75 75 THR N N 15 1.374 0.013 . . . . . 5858 4 67 . 1 1 76 76 THR N N 15 1.385 0.017 . . . . . 5858 4 68 . 1 1 77 77 PHE N N 15 1.463 0.011 . . . . . 5858 4 69 . 1 1 79 79 ALA N N 15 1.408 0.029 . . . . . 5858 4 70 . 1 1 80 80 ASP N N 15 1.418 0.018 . . . . . 5858 4 71 . 1 1 81 81 ALA N N 15 1.419 0.027 . . . . . 5858 4 72 . 1 1 83 83 ALA N N 15 1.293 0.015 . . . . . 5858 4 73 . 1 1 84 84 GLY N N 15 1.394 0.018 . . . . . 5858 4 74 . 1 1 85 85 GLU N N 15 1.348 0.011 . . . . . 5858 4 75 . 1 1 86 86 TYR N N 15 1.381 0.009 . . . . . 5858 4 76 . 1 1 87 87 THR N N 15 1.330 0.016 . . . . . 5858 4 77 . 1 1 88 88 PHE N N 15 1.551 0.010 . . . . . 5858 4 78 . 1 1 89 89 TYR N N 15 1.389 0.010 . . . . . 5858 4 79 . 1 1 90 90 CYS N N 15 1.518 0.041 . . . . . 5858 4 80 . 1 1 91 91 GLU N N 15 1.506 0.016 . . . . . 5858 4 81 . 1 1 93 93 HIS N N 15 1.342 0.025 . . . . . 5858 4 82 . 1 1 94 94 ARG N N 15 1.526 0.012 . . . . . 5858 4 83 . 1 1 95 95 GLY N N 15 1.545 0.079 . . . . . 5858 4 84 . 1 1 96 96 ALA N N 15 1.415 0.011 . . . . . 5858 4 85 . 1 1 97 97 GLY N N 15 1.489 0.008 . . . . . 5858 4 86 . 1 1 98 98 MET N N 15 1.455 0.012 . . . . . 5858 4 87 . 1 1 99 99 VAL N N 15 1.336 0.010 . . . . . 5858 4 88 . 1 1 100 100 GLY N N 15 1.447 0.018 . . . . . 5858 4 89 . 1 1 101 101 LYS N N 15 1.392 0.007 . . . . . 5858 4 90 . 1 1 102 102 ILE N N 15 1.376 0.011 . . . . . 5858 4 91 . 1 1 103 103 THR N N 15 1.367 0.016 . . . . . 5858 4 92 . 1 1 104 104 VAL N N 15 1.396 0.013 . . . . . 5858 4 93 . 1 1 105 105 ALA N N 15 1.442 0.016 . . . . . 5858 4 94 . 1 1 106 106 GLY N N 15 0.791 0.006 . . . . . 5858 4 stop_ save_ save_relax_1_5 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode relax_1_5 _Heteronucl_T1_list.Entry_ID 5858 _Heteronucl_T1_list.ID 5 _Heteronucl_T1_list.Sample_condition_list_ID 5 _Heteronucl_T1_list.Sample_condition_list_label $Condition_5 _Heteronucl_T1_list.Spectrometer_frequency_1H 800 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 5858 5 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 THR N N 15 1.382 0.014 . . . . . 5858 5 2 . 1 1 4 4 TYR N N 15 1.354 0.010 . . . . . 5858 5 3 . 1 1 5 5 THR N N 15 1.263 0.011 . . . . . 5858 5 4 . 1 1 6 6 VAL N N 15 1.419 0.013 . . . . . 5858 5 5 . 1 1 7 7 LYS N N 15 1.412 0.022 . . . . . 5858 5 6 . 1 1 8 8 LEU N N 15 1.424 0.014 . . . . . 5858 5 7 . 1 1 9 9 GLY N N 15 1.270 0.014 . . . . . 5858 5 8 . 1 1 10 10 SER N N 15 1.489 0.011 . . . . . 5858 5 9 . 1 1 11 11 ASP N N 15 1.438 0.040 . . . . . 5858 5 10 . 1 1 12 12 LYS N N 15 1.308 0.157 . . . . . 5858 5 11 . 1 1 13 13 GLY N N 15 1.408 0.010 . . . . . 5858 5 12 . 1 1 14 14 LEU N N 15 1.455 0.018 . . . . . 5858 5 13 . 1 1 15 15 LEU N N 15 1.337 0.012 . . . . . 5858 5 14 . 1 1 16 16 VAL N N 15 1.361 0.019 . . . . . 5858 5 15 . 1 1 17 17 PHE N N 15 1.422 0.016 . . . . . 5858 5 16 . 1 1 18 18 GLU N N 15 1.410 0.018 . . . . . 5858 5 17 . 1 1 20 20 ALA N N 15 1.185 0.009 . . . . . 5858 5 18 . 1 1 21 21 LYS N N 15 1.299 0.014 . . . . . 5858 5 19 . 1 1 22 22 LEU N N 15 1.350 0.015 . . . . . 5858 5 20 . 1 1 23 23 THR N N 15 1.305 0.006 . . . . . 5858 5 21 . 1 1 24 24 ILE N N 15 1.435 0.013 . . . . . 5858 5 22 . 1 1 25 25 LYS N N 15 1.384 0.020 . . . . . 5858 5 23 . 1 1 27 27 GLY N N 15 1.402 0.017 . . . . . 5858 5 24 . 1 1 28 28 ASP N N 15 1.516 0.010 . . . . . 5858 5 25 . 1 1 29 29 THR N N 15 1.384 0.015 . . . . . 5858 5 26 . 1 1 30 30 VAL N N 15 1.405 0.015 . . . . . 5858 5 27 . 1 1 31 31 GLU N N 15 1.419 0.020 . . . . . 5858 5 28 . 1 1 32 32 PHE N N 15 1.371 0.022 . . . . . 5858 5 29 . 1 1 33 33 LEU N N 15 1.401 0.016 . . . . . 5858 5 30 . 1 1 34 34 ASN N N 15 1.483 0.012 . . . . . 5858 5 31 . 1 1 35 35 ASN N N 15 1.428 0.010 . . . . . 5858 5 32 . 1 1 36 36 LYS N N 15 1.327 0.014 . . . . . 5858 5 33 . 1 1 37 37 VAL N N 15 1.349 0.013 . . . . . 5858 5 34 . 1 1 40 40 HIS N N 15 1.360 0.019 . . . . . 5858 5 35 . 1 1 41 41 ASN N N 15 1.425 0.014 . . . . . 5858 5 36 . 1 1 42 42 VAL N N 15 1.364 0.019 . . . . . 5858 5 37 . 1 1 43 43 VAL N N 15 1.404 0.011 . . . . . 5858 5 38 . 1 1 44 44 PHE N N 15 1.463 0.017 . . . . . 5858 5 39 . 1 1 45 45 ASP N N 15 1.509 0.010 . . . . . 5858 5 40 . 1 1 46 46 ALA N N 15 1.407 0.011 . . . . . 5858 5 41 . 1 1 47 47 ALA N N 15 1.339 0.008 . . . . . 5858 5 42 . 1 1 48 48 LEU N N 15 1.187 0.017 . . . . . 5858 5 43 . 1 1 49 49 ASN N N 15 1.320 0.017 . . . . . 5858 5 44 . 1 1 51 51 ALA N N 15 1.338 0.012 . . . . . 5858 5 45 . 1 1 52 52 LYS N N 15 1.487 0.015 . . . . . 5858 5 46 . 1 1 53 53 SER N N 15 1.457 0.014 . . . . . 5858 5 47 . 1 1 54 54 ALA N N 15 1.468 0.027 . . . . . 5858 5 48 . 1 1 55 55 ASP N N 15 1.403 0.026 . . . . . 5858 5 49 . 1 1 56 56 LEU N N 15 1.487 0.009 . . . . . 5858 5 50 . 1 1 57 57 ALA N N 15 1.395 0.020 . . . . . 5858 5 51 . 1 1 58 58 LYS N N 15 1.436 0.010 . . . . . 5858 5 52 . 1 1 59 59 SER N N 15 1.367 0.022 . . . . . 5858 5 53 . 1 1 60 60 LEU N N 15 1.497 0.015 . . . . . 5858 5 54 . 1 1 61 61 SER N N 15 1.322 0.007 . . . . . 5858 5 55 . 1 1 62 62 HIS N N 15 1.438 0.014 . . . . . 5858 5 56 . 1 1 63 63 LYS N N 15 1.369 0.028 . . . . . 5858 5 57 . 1 1 64 64 GLN N N 15 1.401 0.008 . . . . . 5858 5 58 . 1 1 65 65 LEU N N 15 1.364 0.019 . . . . . 5858 5 59 . 1 1 66 66 LEU N N 15 1.421 0.010 . . . . . 5858 5 60 . 1 1 67 67 MET N N 15 1.307 0.008 . . . . . 5858 5 61 . 1 1 68 68 SER N N 15 1.292 0.009 . . . . . 5858 5 62 . 1 1 70 70 GLY N N 15 1.365 0.018 . . . . . 5858 5 63 . 1 1 71 71 GLN N N 15 1.382 0.017 . . . . . 5858 5 64 . 1 1 72 72 SER N N 15 1.409 0.015 . . . . . 5858 5 65 . 1 1 73 73 THR N N 15 1.464 0.009 . . . . . 5858 5 66 . 1 1 74 74 SER N N 15 1.356 0.013 . . . . . 5858 5 67 . 1 1 75 75 THR N N 15 1.365 0.008 . . . . . 5858 5 68 . 1 1 76 76 THR N N 15 1.341 0.014 . . . . . 5858 5 69 . 1 1 77 77 PHE N N 15 1.454 0.013 . . . . . 5858 5 70 . 1 1 79 79 ALA N N 15 1.404 0.008 . . . . . 5858 5 71 . 1 1 80 80 ASP N N 15 1.416 0.008 . . . . . 5858 5 72 . 1 1 81 81 ALA N N 15 1.441 0.017 . . . . . 5858 5 73 . 1 1 83 83 ALA N N 15 1.291 0.014 . . . . . 5858 5 74 . 1 1 84 84 GLY N N 15 1.392 0.015 . . . . . 5858 5 75 . 1 1 85 85 GLU N N 15 1.344 0.009 . . . . . 5858 5 76 . 1 1 86 86 TYR N N 15 1.378 0.012 . . . . . 5858 5 77 . 1 1 87 87 THR N N 15 1.300 0.010 . . . . . 5858 5 78 . 1 1 88 88 PHE N N 15 1.552 0.009 . . . . . 5858 5 79 . 1 1 89 89 TYR N N 15 1.430 0.010 . . . . . 5858 5 80 . 1 1 90 90 CYS N N 15 1.458 0.043 . . . . . 5858 5 81 . 1 1 91 91 GLU N N 15 1.520 0.014 . . . . . 5858 5 82 . 1 1 93 93 HIS N N 15 1.338 0.021 . . . . . 5858 5 83 . 1 1 94 94 ARG N N 15 1.565 0.012 . . . . . 5858 5 84 . 1 1 95 95 GLY N N 15 1.498 0.029 . . . . . 5858 5 85 . 1 1 96 96 ALA N N 15 1.386 0.020 . . . . . 5858 5 86 . 1 1 97 97 GLY N N 15 1.427 0.014 . . . . . 5858 5 87 . 1 1 98 98 MET N N 15 1.468 0.021 . . . . . 5858 5 88 . 1 1 99 99 VAL N N 15 1.348 0.009 . . . . . 5858 5 89 . 1 1 100 100 GLY N N 15 1.457 0.028 . . . . . 5858 5 90 . 1 1 101 101 LYS N N 15 1.394 0.009 . . . . . 5858 5 91 . 1 1 102 102 ILE N N 15 1.404 0.009 . . . . . 5858 5 92 . 1 1 103 103 THR N N 15 1.377 0.021 . . . . . 5858 5 93 . 1 1 104 104 VAL N N 15 1.398 0.018 . . . . . 5858 5 94 . 1 1 105 105 ALA N N 15 1.426 0.019 . . . . . 5858 5 95 . 1 1 106 106 GLY N N 15 0.780 0.019 . . . . . 5858 5 stop_ save_ save_relax_1_6 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode relax_1_6 _Heteronucl_T1_list.Entry_ID 5858 _Heteronucl_T1_list.ID 6 _Heteronucl_T1_list.Sample_condition_list_ID 6 _Heteronucl_T1_list.Sample_condition_list_label $Condition_6 _Heteronucl_T1_list.Spectrometer_frequency_1H 800 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 5858 6 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 THR N N 15 1.400 0.010 . . . . . 5858 6 2 . 1 1 4 4 TYR N N 15 1.374 0.011 . . . . . 5858 6 3 . 1 1 5 5 THR N N 15 1.259 0.017 . . . . . 5858 6 4 . 1 1 6 6 VAL N N 15 1.392 0.022 . . . . . 5858 6 5 . 1 1 7 7 LYS N N 15 1.436 0.011 . . . . . 5858 6 6 . 1 1 8 8 LEU N N 15 1.444 0.013 . . . . . 5858 6 7 . 1 1 9 9 GLY N N 15 1.247 0.018 . . . . . 5858 6 8 . 1 1 10 10 SER N N 15 1.529 0.016 . . . . . 5858 6 9 . 1 1 11 11 ASP N N 15 1.387 0.010 . . . . . 5858 6 10 . 1 1 12 12 LYS N N 15 1.308 0.023 . . . . . 5858 6 11 . 1 1 13 13 GLY N N 15 1.412 0.014 . . . . . 5858 6 12 . 1 1 14 14 LEU N N 15 1.475 0.019 . . . . . 5858 6 13 . 1 1 15 15 LEU N N 15 1.305 0.009 . . . . . 5858 6 14 . 1 1 16 16 VAL N N 15 1.346 0.022 . . . . . 5858 6 15 . 1 1 17 17 PHE N N 15 1.469 0.021 . . . . . 5858 6 16 . 1 1 18 18 GLU N N 15 1.454 0.012 . . . . . 5858 6 17 . 1 1 20 20 ALA N N 15 1.172 0.016 . . . . . 5858 6 18 . 1 1 21 21 LYS N N 15 1.316 0.021 . . . . . 5858 6 19 . 1 1 22 22 LEU N N 15 1.361 0.011 . . . . . 5858 6 20 . 1 1 23 23 THR N N 15 1.287 0.009 . . . . . 5858 6 21 . 1 1 24 24 ILE N N 15 1.439 0.014 . . . . . 5858 6 22 . 1 1 25 25 LYS N N 15 1.419 0.028 . . . . . 5858 6 23 . 1 1 27 27 GLY N N 15 1.429 0.014 . . . . . 5858 6 24 . 1 1 28 28 ASP N N 15 1.527 0.012 . . . . . 5858 6 25 . 1 1 29 29 THR N N 15 1.399 0.018 . . . . . 5858 6 26 . 1 1 30 30 VAL N N 15 1.393 0.014 . . . . . 5858 6 27 . 1 1 31 31 GLU N N 15 1.454 0.013 . . . . . 5858 6 28 . 1 1 32 32 PHE N N 15 1.368 0.020 . . . . . 5858 6 29 . 1 1 33 33 LEU N N 15 1.408 0.027 . . . . . 5858 6 30 . 1 1 34 34 ASN N N 15 1.512 0.012 . . . . . 5858 6 31 . 1 1 35 35 ASN N N 15 1.446 0.013 . . . . . 5858 6 32 . 1 1 36 36 LYS N N 15 1.323 0.011 . . . . . 5858 6 33 . 1 1 37 37 VAL N N 15 1.332 0.022 . . . . . 5858 6 34 . 1 1 40 40 HIS N N 15 1.382 0.020 . . . . . 5858 6 35 . 1 1 41 41 ASN N N 15 1.478 0.026 . . . . . 5858 6 36 . 1 1 42 42 VAL N N 15 1.371 0.022 . . . . . 5858 6 37 . 1 1 43 43 VAL N N 15 1.400 0.011 . . . . . 5858 6 38 . 1 1 44 44 PHE N N 15 1.443 0.014 . . . . . 5858 6 39 . 1 1 45 45 ASP N N 15 1.477 0.013 . . . . . 5858 6 40 . 1 1 46 46 ALA N N 15 1.383 0.015 . . . . . 5858 6 41 . 1 1 47 47 ALA N N 15 1.337 0.011 . . . . . 5858 6 42 . 1 1 48 48 LEU N N 15 1.217 0.019 . . . . . 5858 6 43 . 1 1 49 49 ASN N N 15 1.342 0.009 . . . . . 5858 6 44 . 1 1 51 51 ALA N N 15 1.346 0.031 . . . . . 5858 6 45 . 1 1 52 52 LYS N N 15 1.474 0.017 . . . . . 5858 6 46 . 1 1 53 53 SER N N 15 1.440 0.015 . . . . . 5858 6 47 . 1 1 54 54 ALA N N 15 1.487 0.029 . . . . . 5858 6 48 . 1 1 55 55 ASP N N 15 1.476 0.023 . . . . . 5858 6 49 . 1 1 56 56 LEU N N 15 1.472 0.009 . . . . . 5858 6 50 . 1 1 57 57 ALA N N 15 1.413 0.025 . . . . . 5858 6 51 . 1 1 58 58 LYS N N 15 1.446 0.011 . . . . . 5858 6 52 . 1 1 59 59 SER N N 15 1.394 0.036 . . . . . 5858 6 53 . 1 1 60 60 LEU N N 15 1.517 0.015 . . . . . 5858 6 54 . 1 1 61 61 SER N N 15 1.307 0.021 . . . . . 5858 6 55 . 1 1 62 62 HIS N N 15 1.411 0.013 . . . . . 5858 6 56 . 1 1 63 63 LYS N N 15 1.341 0.023 . . . . . 5858 6 57 . 1 1 64 64 GLN N N 15 1.391 0.009 . . . . . 5858 6 58 . 1 1 65 65 LEU N N 15 1.418 0.020 . . . . . 5858 6 59 . 1 1 66 66 LEU N N 15 1.403 0.021 . . . . . 5858 6 60 . 1 1 67 67 MET N N 15 1.281 0.010 . . . . . 5858 6 61 . 1 1 68 68 SER N N 15 1.261 0.015 . . . . . 5858 6 62 . 1 1 70 70 GLY N N 15 1.350 0.013 . . . . . 5858 6 63 . 1 1 71 71 GLN N N 15 1.377 0.020 . . . . . 5858 6 64 . 1 1 72 72 SER N N 15 1.417 0.011 . . . . . 5858 6 65 . 1 1 73 73 THR N N 15 1.497 0.034 . . . . . 5858 6 66 . 1 1 74 74 SER N N 15 1.347 0.014 . . . . . 5858 6 67 . 1 1 75 75 THR N N 15 1.381 0.011 . . . . . 5858 6 68 . 1 1 76 76 THR N N 15 1.341 0.012 . . . . . 5858 6 69 . 1 1 77 77 PHE N N 15 1.504 0.025 . . . . . 5858 6 70 . 1 1 79 79 ALA N N 15 1.369 0.022 . . . . . 5858 6 71 . 1 1 80 80 ASP N N 15 1.388 0.016 . . . . . 5858 6 72 . 1 1 81 81 ALA N N 15 1.431 0.020 . . . . . 5858 6 73 . 1 1 83 83 ALA N N 15 1.318 0.010 . . . . . 5858 6 74 . 1 1 84 84 GLY N N 15 1.405 0.023 . . . . . 5858 6 75 . 1 1 85 85 GLU N N 15 1.334 0.008 . . . . . 5858 6 76 . 1 1 86 86 TYR N N 15 1.394 0.012 . . . . . 5858 6 77 . 1 1 87 87 THR N N 15 1.321 0.013 . . . . . 5858 6 78 . 1 1 88 88 PHE N N 15 1.559 0.010 . . . . . 5858 6 79 . 1 1 89 89 TYR N N 15 1.465 0.023 . . . . . 5858 6 80 . 1 1 90 90 CYS N N 15 1.521 0.024 . . . . . 5858 6 81 . 1 1 91 91 GLU N N 15 1.529 0.014 . . . . . 5858 6 82 . 1 1 93 93 HIS N N 15 1.397 0.055 . . . . . 5858 6 83 . 1 1 94 94 ARG N N 15 1.516 0.016 . . . . . 5858 6 84 . 1 1 95 95 GLY N N 15 1.549 0.047 . . . . . 5858 6 85 . 1 1 96 96 ALA N N 15 1.388 0.018 . . . . . 5858 6 86 . 1 1 97 97 GLY N N 15 1.474 0.012 . . . . . 5858 6 87 . 1 1 98 98 MET N N 15 1.458 0.019 . . . . . 5858 6 88 . 1 1 99 99 VAL N N 15 1.320 0.015 . . . . . 5858 6 89 . 1 1 100 100 GLY N N 15 1.460 0.020 . . . . . 5858 6 90 . 1 1 101 101 LYS N N 15 1.385 0.010 . . . . . 5858 6 91 . 1 1 102 102 ILE N N 15 1.396 0.012 . . . . . 5858 6 92 . 1 1 103 103 THR N N 15 1.361 0.015 . . . . . 5858 6 93 . 1 1 104 104 VAL N N 15 1.399 0.019 . . . . . 5858 6 94 . 1 1 105 105 ALA N N 15 1.441 0.014 . . . . . 5858 6 95 . 1 1 106 106 GLY N N 15 0.792 0.006 . . . . . 5858 6 stop_ save_ save_relax_1_7 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode relax_1_7 _Heteronucl_T1_list.Entry_ID 5858 _Heteronucl_T1_list.ID 7 _Heteronucl_T1_list.Sample_condition_list_ID 7 _Heteronucl_T1_list.Sample_condition_list_label $Condition_7 _Heteronucl_T1_list.Spectrometer_frequency_1H 800 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 5858 7 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 THR N N 15 1.389 0.010 . . . . . 5858 7 2 . 1 1 4 4 TYR N N 15 1.371 0.012 . . . . . 5858 7 3 . 1 1 5 5 THR N N 15 1.269 0.014 . . . . . 5858 7 4 . 1 1 6 6 VAL N N 15 1.398 0.020 . . . . . 5858 7 5 . 1 1 7 7 LYS N N 15 1.422 0.029 . . . . . 5858 7 6 . 1 1 8 8 LEU N N 15 1.433 0.011 . . . . . 5858 7 7 . 1 1 9 9 GLY N N 15 1.262 0.009 . . . . . 5858 7 8 . 1 1 10 10 SER N N 15 1.512 0.009 . . . . . 5858 7 9 . 1 1 11 11 ASP N N 15 1.353 0.024 . . . . . 5858 7 10 . 1 1 12 12 LYS N N 15 1.260 0.016 . . . . . 5858 7 11 . 1 1 13 13 GLY N N 15 1.411 0.006 . . . . . 5858 7 12 . 1 1 14 14 LEU N N 15 1.461 0.013 . . . . . 5858 7 13 . 1 1 15 15 LEU N N 15 1.337 0.022 . . . . . 5858 7 14 . 1 1 16 16 VAL N N 15 1.352 0.026 . . . . . 5858 7 15 . 1 1 17 17 PHE N N 15 1.439 0.014 . . . . . 5858 7 16 . 1 1 18 18 GLU N N 15 1.422 0.007 . . . . . 5858 7 17 . 1 1 20 20 ALA N N 15 1.199 0.019 . . . . . 5858 7 18 . 1 1 21 21 LYS N N 15 1.323 0.014 . . . . . 5858 7 19 . 1 1 22 22 LEU N N 15 1.326 0.034 . . . . . 5858 7 20 . 1 1 23 23 THR N N 15 1.298 0.014 . . . . . 5858 7 21 . 1 1 24 24 ILE N N 15 1.440 0.012 . . . . . 5858 7 22 . 1 1 25 25 LYS N N 15 1.382 0.016 . . . . . 5858 7 23 . 1 1 27 27 GLY N N 15 1.434 0.016 . . . . . 5858 7 24 . 1 1 28 28 ASP N N 15 1.518 0.012 . . . . . 5858 7 25 . 1 1 29 29 THR N N 15 1.398 0.028 . . . . . 5858 7 26 . 1 1 30 30 VAL N N 15 1.387 0.020 . . . . . 5858 7 27 . 1 1 31 31 GLU N N 15 1.427 0.020 . . . . . 5858 7 28 . 1 1 32 32 PHE N N 15 1.385 0.012 . . . . . 5858 7 29 . 1 1 33 33 LEU N N 15 1.394 0.015 . . . . . 5858 7 30 . 1 1 34 34 ASN N N 15 1.475 0.017 . . . . . 5858 7 31 . 1 1 35 35 ASN N N 15 1.448 0.012 . . . . . 5858 7 32 . 1 1 36 36 LYS N N 15 1.322 0.036 . . . . . 5858 7 33 . 1 1 37 37 VAL N N 15 1.326 0.018 . . . . . 5858 7 34 . 1 1 40 40 HIS N N 15 1.346 0.012 . . . . . 5858 7 35 . 1 1 41 41 ASN N N 15 1.389 0.023 . . . . . 5858 7 36 . 1 1 42 42 VAL N N 15 1.377 0.007 . . . . . 5858 7 37 . 1 1 43 43 VAL N N 15 1.402 0.015 . . . . . 5858 7 38 . 1 1 44 44 PHE N N 15 1.446 0.014 . . . . . 5858 7 39 . 1 1 45 45 ASP N N 15 1.494 0.015 . . . . . 5858 7 40 . 1 1 46 46 ALA N N 15 1.366 0.012 . . . . . 5858 7 41 . 1 1 47 47 ALA N N 15 1.336 0.015 . . . . . 5858 7 42 . 1 1 48 48 LEU N N 15 1.193 0.005 . . . . . 5858 7 43 . 1 1 49 49 ASN N N 15 1.365 0.005 . . . . . 5858 7 44 . 1 1 51 51 ALA N N 15 1.340 0.007 . . . . . 5858 7 45 . 1 1 52 52 LYS N N 15 1.512 0.007 . . . . . 5858 7 46 . 1 1 53 53 SER N N 15 1.426 0.010 . . . . . 5858 7 47 . 1 1 54 54 ALA N N 15 1.469 0.013 . . . . . 5858 7 48 . 1 1 55 55 ASP N N 15 1.448 0.014 . . . . . 5858 7 49 . 1 1 56 56 LEU N N 15 1.455 0.011 . . . . . 5858 7 50 . 1 1 57 57 ALA N N 15 1.414 0.035 . . . . . 5858 7 51 . 1 1 58 58 LYS N N 15 1.432 0.009 . . . . . 5858 7 52 . 1 1 59 59 SER N N 15 1.404 0.012 . . . . . 5858 7 53 . 1 1 60 60 LEU N N 15 1.517 0.008 . . . . . 5858 7 54 . 1 1 61 61 SER N N 15 1.337 0.007 . . . . . 5858 7 55 . 1 1 62 62 HIS N N 15 1.424 0.010 . . . . . 5858 7 56 . 1 1 63 63 LYS N N 15 1.340 0.011 . . . . . 5858 7 57 . 1 1 64 64 GLN N N 15 1.405 0.011 . . . . . 5858 7 58 . 1 1 65 65 LEU N N 15 1.403 0.007 . . . . . 5858 7 59 . 1 1 66 66 LEU N N 15 1.407 0.010 . . . . . 5858 7 60 . 1 1 67 67 MET N N 15 1.302 0.011 . . . . . 5858 7 61 . 1 1 68 68 SER N N 15 1.267 0.010 . . . . . 5858 7 62 . 1 1 70 70 GLY N N 15 1.345 0.014 . . . . . 5858 7 63 . 1 1 71 71 GLN N N 15 1.382 0.010 . . . . . 5858 7 64 . 1 1 72 72 SER N N 15 1.405 0.019 . . . . . 5858 7 65 . 1 1 73 73 THR N N 15 1.449 0.045 . . . . . 5858 7 66 . 1 1 74 74 SER N N 15 1.323 0.009 . . . . . 5858 7 67 . 1 1 75 75 THR N N 15 1.382 0.008 . . . . . 5858 7 68 . 1 1 76 76 THR N N 15 1.334 0.014 . . . . . 5858 7 69 . 1 1 77 77 PHE N N 15 1.445 0.009 . . . . . 5858 7 70 . 1 1 79 79 ALA N N 15 1.349 0.033 . . . . . 5858 7 71 . 1 1 80 80 ASP N N 15 1.406 0.005 . . . . . 5858 7 72 . 1 1 81 81 ALA N N 15 1.408 0.038 . . . . . 5858 7 73 . 1 1 83 83 ALA N N 15 1.304 0.008 . . . . . 5858 7 74 . 1 1 84 84 GLY N N 15 1.392 0.017 . . . . . 5858 7 75 . 1 1 85 85 GLU N N 15 1.345 0.013 . . . . . 5858 7 76 . 1 1 86 86 TYR N N 15 1.376 0.010 . . . . . 5858 7 77 . 1 1 87 87 THR N N 15 1.310 0.010 . . . . . 5858 7 78 . 1 1 88 88 PHE N N 15 1.561 0.018 . . . . . 5858 7 79 . 1 1 89 89 TYR N N 15 1.466 0.018 . . . . . 5858 7 80 . 1 1 90 90 CYS N N 15 1.486 0.010 . . . . . 5858 7 81 . 1 1 91 91 GLU N N 15 1.539 0.011 . . . . . 5858 7 82 . 1 1 93 93 HIS N N 15 1.322 0.074 . . . . . 5858 7 83 . 1 1 94 94 ARG N N 15 1.552 0.013 . . . . . 5858 7 84 . 1 1 95 95 GLY N N 15 1.552 0.020 . . . . . 5858 7 85 . 1 1 96 96 ALA N N 15 1.390 0.017 . . . . . 5858 7 86 . 1 1 97 97 GLY N N 15 1.440 0.012 . . . . . 5858 7 87 . 1 1 98 98 MET N N 15 1.460 0.015 . . . . . 5858 7 88 . 1 1 99 99 VAL N N 15 1.352 0.019 . . . . . 5858 7 89 . 1 1 100 100 GLY N N 15 1.465 0.023 . . . . . 5858 7 90 . 1 1 101 101 LYS N N 15 1.394 0.013 . . . . . 5858 7 91 . 1 1 102 102 ILE N N 15 1.381 0.020 . . . . . 5858 7 92 . 1 1 103 103 THR N N 15 1.353 0.017 . . . . . 5858 7 93 . 1 1 104 104 VAL N N 15 1.381 0.017 . . . . . 5858 7 94 . 1 1 105 105 ALA N N 15 1.429 0.019 . . . . . 5858 7 95 . 1 1 106 106 GLY N N 15 0.788 0.018 . . . . . 5858 7 stop_ save_ save_relax_1_8 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode relax_1_8 _Heteronucl_T1_list.Entry_ID 5858 _Heteronucl_T1_list.ID 8 _Heteronucl_T1_list.Sample_condition_list_ID 8 _Heteronucl_T1_list.Sample_condition_list_label $Condition_8 _Heteronucl_T1_list.Spectrometer_frequency_1H 800 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID . . 1 $sample_1 . 5858 8 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 THR N N 15 1.358 0.019 . . . . . 5858 8 2 . 1 1 4 4 TYR N N 15 1.369 0.019 . . . . . 5858 8 3 . 1 1 5 5 THR N N 15 1.275 0.012 . . . . . 5858 8 4 . 1 1 6 6 VAL N N 15 1.389 0.018 . . . . . 5858 8 5 . 1 1 7 7 LYS N N 15 1.419 0.013 . . . . . 5858 8 6 . 1 1 8 8 LEU N N 15 1.441 0.014 . . . . . 5858 8 7 . 1 1 9 9 GLY N N 15 1.261 0.022 . . . . . 5858 8 8 . 1 1 10 10 SER N N 15 1.512 0.014 . . . . . 5858 8 9 . 1 1 11 11 ASP N N 15 1.385 0.013 . . . . . 5858 8 10 . 1 1 12 12 LYS N N 15 1.286 0.011 . . . . . 5858 8 11 . 1 1 13 13 GLY N N 15 1.406 0.016 . . . . . 5858 8 12 . 1 1 14 14 LEU N N 15 1.450 0.018 . . . . . 5858 8 13 . 1 1 15 15 LEU N N 15 1.282 0.014 . . . . . 5858 8 14 . 1 1 16 16 VAL N N 15 1.360 0.022 . . . . . 5858 8 15 . 1 1 17 17 PHE N N 15 1.442 0.025 . . . . . 5858 8 16 . 1 1 18 18 GLU N N 15 1.411 0.016 . . . . . 5858 8 17 . 1 1 20 20 ALA N N 15 1.165 0.016 . . . . . 5858 8 18 . 1 1 21 21 LYS N N 15 1.334 0.021 . . . . . 5858 8 19 . 1 1 22 22 LEU N N 15 1.338 0.020 . . . . . 5858 8 20 . 1 1 23 23 THR N N 15 1.266 0.011 . . . . . 5858 8 21 . 1 1 24 24 ILE N N 15 1.448 0.013 . . . . . 5858 8 22 . 1 1 25 25 LYS N N 15 1.411 0.018 . . . . . 5858 8 23 . 1 1 27 27 GLY N N 15 1.417 0.023 . . . . . 5858 8 24 . 1 1 28 28 ASP N N 15 1.525 0.014 . . . . . 5858 8 25 . 1 1 29 29 THR N N 15 1.404 0.012 . . . . . 5858 8 26 . 1 1 30 30 VAL N N 15 1.392 0.017 . . . . . 5858 8 27 . 1 1 31 31 GLU N N 15 1.422 0.026 . . . . . 5858 8 28 . 1 1 32 32 PHE N N 15 1.394 0.016 . . . . . 5858 8 29 . 1 1 33 33 LEU N N 15 1.416 0.011 . . . . . 5858 8 30 . 1 1 34 34 ASN N N 15 1.484 0.021 . . . . . 5858 8 31 . 1 1 35 35 ASN N N 15 1.503 0.018 . . . . . 5858 8 32 . 1 1 36 36 LYS N N 15 1.326 0.007 . . . . . 5858 8 33 . 1 1 37 37 VAL N N 15 1.313 0.019 . . . . . 5858 8 34 . 1 1 40 40 HIS N N 15 1.375 0.022 . . . . . 5858 8 35 . 1 1 41 41 ASN N N 15 1.492 0.058 . . . . . 5858 8 36 . 1 1 42 42 VAL N N 15 1.402 0.011 . . . . . 5858 8 37 . 1 1 43 43 VAL N N 15 1.370 0.016 . . . . . 5858 8 38 . 1 1 44 44 PHE N N 15 1.425 0.022 . . . . . 5858 8 39 . 1 1 45 45 ASP N N 15 1.475 0.011 . . . . . 5858 8 40 . 1 1 46 46 ALA N N 15 1.359 0.012 . . . . . 5858 8 41 . 1 1 47 47 ALA N N 15 1.350 0.009 . . . . . 5858 8 42 . 1 1 48 48 LEU N N 15 1.199 0.010 . . . . . 5858 8 43 . 1 1 49 49 ASN N N 15 1.259 0.013 . . . . . 5858 8 44 . 1 1 51 51 ALA N N 15 1.340 0.012 . . . . . 5858 8 45 . 1 1 52 52 LYS N N 15 1.394 0.008 . . . . . 5858 8 46 . 1 1 53 53 SER N N 15 1.485 0.029 . . . . . 5858 8 47 . 1 1 54 54 ALA N N 15 1.452 0.014 . . . . . 5858 8 48 . 1 1 55 55 ASP N N 15 1.422 0.012 . . . . . 5858 8 49 . 1 1 56 56 LEU N N 15 1.471 0.009 . . . . . 5858 8 50 . 1 1 57 57 ALA N N 15 1.409 0.026 . . . . . 5858 8 51 . 1 1 58 58 LYS N N 15 1.438 0.007 . . . . . 5858 8 52 . 1 1 59 59 SER N N 15 1.428 0.012 . . . . . 5858 8 53 . 1 1 60 60 LEU N N 15 1.497 0.023 . . . . . 5858 8 54 . 1 1 61 61 SER N N 15 1.326 0.010 . . . . . 5858 8 55 . 1 1 62 62 HIS N N 15 1.392 0.012 . . . . . 5858 8 56 . 1 1 63 63 LYS N N 15 1.324 0.014 . . . . . 5858 8 57 . 1 1 64 64 GLN N N 15 1.360 0.008 . . . . . 5858 8 58 . 1 1 65 65 LEU N N 15 1.392 0.009 . . . . . 5858 8 59 . 1 1 66 66 LEU N N 15 1.416 0.017 . . . . . 5858 8 60 . 1 1 67 67 MET N N 15 1.262 0.009 . . . . . 5858 8 61 . 1 1 68 68 SER N N 15 1.253 0.015 . . . . . 5858 8 62 . 1 1 70 70 GLY N N 15 1.346 0.019 . . . . . 5858 8 63 . 1 1 71 71 GLN N N 15 1.408 0.016 . . . . . 5858 8 64 . 1 1 72 72 SER N N 15 1.430 0.014 . . . . . 5858 8 65 . 1 1 73 73 THR N N 15 1.452 0.015 . . . . . 5858 8 66 . 1 1 74 74 SER N N 15 1.331 0.012 . . . . . 5858 8 67 . 1 1 75 75 THR N N 15 1.383 0.010 . . . . . 5858 8 68 . 1 1 76 76 THR N N 15 1.357 0.013 . . . . . 5858 8 69 . 1 1 77 77 PHE N N 15 1.470 0.016 . . . . . 5858 8 70 . 1 1 79 79 ALA N N 15 1.367 0.012 . . . . . 5858 8 71 . 1 1 80 80 ASP N N 15 1.400 0.010 . . . . . 5858 8 72 . 1 1 81 81 ALA N N 15 1.424 0.022 . . . . . 5858 8 73 . 1 1 83 83 ALA N N 15 1.288 0.010 . . . . . 5858 8 74 . 1 1 84 84 GLY N N 15 1.395 0.020 . . . . . 5858 8 75 . 1 1 85 85 GLU N N 15 1.348 0.012 . . . . . 5858 8 76 . 1 1 86 86 TYR N N 15 1.390 0.011 . . . . . 5858 8 77 . 1 1 87 87 THR N N 15 1.336 0.011 . . . . . 5858 8 78 . 1 1 88 88 PHE N N 15 1.563 0.010 . . . . . 5858 8 79 . 1 1 89 89 TYR N N 15 1.467 0.022 . . . . . 5858 8 80 . 1 1 90 90 CYS N N 15 1.455 0.017 . . . . . 5858 8 81 . 1 1 91 91 GLU N N 15 1.528 0.015 . . . . . 5858 8 82 . 1 1 94 94 ARG N N 15 1.524 0.027 . . . . . 5858 8 83 . 1 1 95 95 GLY N N 15 1.539 0.014 . . . . . 5858 8 84 . 1 1 96 96 ALA N N 15 1.399 0.015 . . . . . 5858 8 85 . 1 1 97 97 GLY N N 15 1.428 0.020 . . . . . 5858 8 86 . 1 1 98 98 MET N N 15 1.464 0.043 . . . . . 5858 8 87 . 1 1 99 99 VAL N N 15 1.350 0.011 . . . . . 5858 8 88 . 1 1 100 100 GLY N N 15 1.474 0.020 . . . . . 5858 8 89 . 1 1 101 101 LYS N N 15 1.397 0.011 . . . . . 5858 8 90 . 1 1 102 102 ILE N N 15 1.396 0.017 . . . . . 5858 8 91 . 1 1 103 103 THR N N 15 1.382 0.013 . . . . . 5858 8 92 . 1 1 104 104 VAL N N 15 1.382 0.017 . . . . . 5858 8 93 . 1 1 105 105 ALA N N 15 1.415 0.018 . . . . . 5858 8 94 . 1 1 106 106 GLY N N 15 0.799 0.011 . . . . . 5858 8 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_relax_2_9 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode relax_2_9 _Heteronucl_T2_list.Entry_ID 5858 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 9 _Heteronucl_T2_list.Sample_condition_list_label $Condition_9 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 800 _Heteronucl_T2_list.T2_coherence_type Ny _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $sample_1 . 5858 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 THR N N 15 7.509 0.378 . . . . . . . 5858 1 2 . 1 1 4 4 TYR N N 15 7.613 0.077 . . . . . . . 5858 1 3 . 1 1 5 5 THR N N 15 7.141 0.053 . . . . . . . 5858 1 4 . 1 1 6 6 VAL N N 15 7.802 0.060 . . . . . . . 5858 1 5 . 1 1 7 7 LYS N N 15 7.680 0.072 . . . . . . . 5858 1 6 . 1 1 8 8 LEU N N 15 8.698 0.121 . . . . . . . 5858 1 7 . 1 1 9 9 GLY N N 15 7.836 0.121 . . . . . . . 5858 1 8 . 1 1 10 10 SER N N 15 8.828 0.089 . . . . . . . 5858 1 9 . 1 1 11 11 ASP N N 15 8.525 0.051 . . . . . . . 5858 1 10 . 1 1 12 12 LYS N N 15 8.944 0.110 . . . . . . . 5858 1 11 . 1 1 13 13 GLY N N 15 8.893 0.111 . . . . . . . 5858 1 12 . 1 1 14 14 LEU N N 15 8.439 0.104 . . . . . . . 5858 1 13 . 1 1 15 15 LEU N N 15 8.673 0.140 . . . . . . . 5858 1 14 . 1 1 16 16 VAL N N 15 7.640 0.192 . . . . . . . 5858 1 15 . 1 1 17 17 PHE N N 15 12.974 0.129 . . . . . . . 5858 1 16 . 1 1 18 18 GLU N N 15 8.531 0.111 . . . . . . . 5858 1 17 . 1 1 20 20 ALA N N 15 8.756 0.264 . . . . . . . 5858 1 18 . 1 1 21 21 LYS N N 15 7.879 0.204 . . . . . . . 5858 1 19 . 1 1 22 22 LEU N N 15 7.831 0.273 . . . . . . . 5858 1 20 . 1 1 23 23 THR N N 15 7.015 0.047 . . . . . . . 5858 1 21 . 1 1 24 24 ILE N N 15 8.091 0.098 . . . . . . . 5858 1 22 . 1 1 25 25 LYS N N 15 8.226 0.059 . . . . . . . 5858 1 23 . 1 1 27 27 GLY N N 15 7.371 0.065 . . . . . . . 5858 1 24 . 1 1 28 28 ASP N N 15 8.716 0.127 . . . . . . . 5858 1 25 . 1 1 29 29 THR N N 15 7.648 0.087 . . . . . . . 5858 1 26 . 1 1 30 30 VAL N N 15 7.901 0.095 . . . . . . . 5858 1 27 . 1 1 31 31 GLU N N 15 8.241 0.187 . . . . . . . 5858 1 28 . 1 1 32 32 PHE N N 15 7.866 0.136 . . . . . . . 5858 1 29 . 1 1 33 33 LEU N N 15 7.744 0.091 . . . . . . . 5858 1 30 . 1 1 34 34 ASN N N 15 8.468 0.080 . . . . . . . 5858 1 31 . 1 1 35 35 ASN N N 15 8.533 0.076 . . . . . . . 5858 1 32 . 1 1 36 36 LYS N N 15 7.138 0.113 . . . . . . . 5858 1 33 . 1 1 37 37 VAL N N 15 16.085 0.172 . . . . . . . 5858 1 34 . 1 1 40 40 HIS N N 15 14.535 0.198 . . . . . . . 5858 1 35 . 1 1 41 41 ASN N N 15 10.942 0.262 . . . . . . . 5858 1 36 . 1 1 42 42 VAL N N 15 9.826 0.133 . . . . . . . 5858 1 37 . 1 1 43 43 VAL N N 15 8.301 0.058 . . . . . . . 5858 1 38 . 1 1 44 44 PHE N N 15 8.214 0.124 . . . . . . . 5858 1 39 . 1 1 45 45 ASP N N 15 7.904 0.184 . . . . . . . 5858 1 40 . 1 1 46 46 ALA N N 15 8.343 0.073 . . . . . . . 5858 1 41 . 1 1 47 47 ALA N N 15 8.538 0.058 . . . . . . . 5858 1 42 . 1 1 48 48 LEU N N 15 6.888 0.066 . . . . . . . 5858 1 43 . 1 1 49 49 ASN N N 15 7.221 0.080 . . . . . . . 5858 1 44 . 1 1 51 51 ALA N N 15 8.269 0.102 . . . . . . . 5858 1 45 . 1 1 52 52 LYS N N 15 8.370 0.109 . . . . . . . 5858 1 46 . 1 1 53 53 SER N N 15 7.996 0.175 . . . . . . . 5858 1 47 . 1 1 54 54 ALA N N 15 8.524 0.067 . . . . . . . 5858 1 48 . 1 1 55 55 ASP N N 15 8.396 0.088 . . . . . . . 5858 1 49 . 1 1 56 56 LEU N N 15 7.950 0.082 . . . . . . . 5858 1 50 . 1 1 57 57 ALA N N 15 8.650 0.162 . . . . . . . 5858 1 51 . 1 1 58 58 LYS N N 15 8.630 0.243 . . . . . . . 5858 1 52 . 1 1 59 59 SER N N 15 7.959 0.135 . . . . . . . 5858 1 53 . 1 1 60 60 LEU N N 15 8.360 0.125 . . . . . . . 5858 1 54 . 1 1 61 61 SER N N 15 7.937 0.103 . . . . . . . 5858 1 55 . 1 1 62 62 HIS N N 15 8.584 0.075 . . . . . . . 5858 1 56 . 1 1 63 63 LYS N N 15 8.388 0.082 . . . . . . . 5858 1 57 . 1 1 64 64 GLN N N 15 8.978 0.067 . . . . . . . 5858 1 58 . 1 1 65 65 LEU N N 15 7.588 0.065 . . . . . . . 5858 1 59 . 1 1 66 66 LEU N N 15 7.388 0.176 . . . . . . . 5858 1 60 . 1 1 67 67 MET N N 15 7.064 0.080 . . . . . . . 5858 1 61 . 1 1 68 68 SER N N 15 8.701 0.307 . . . . . . . 5858 1 62 . 1 1 70 70 GLY N N 15 6.573 0.271 . . . . . . . 5858 1 63 . 1 1 71 71 GLN N N 15 8.390 0.203 . . . . . . . 5858 1 64 . 1 1 72 72 SER N N 15 7.420 0.114 . . . . . . . 5858 1 65 . 1 1 73 73 THR N N 15 7.923 0.088 . . . . . . . 5858 1 66 . 1 1 74 74 SER N N 15 7.966 0.080 . . . . . . . 5858 1 67 . 1 1 75 75 THR N N 15 8.226 0.164 . . . . . . . 5858 1 68 . 1 1 76 76 THR N N 15 7.345 0.122 . . . . . . . 5858 1 69 . 1 1 77 77 PHE N N 15 8.226 0.169 . . . . . . . 5858 1 70 . 1 1 79 79 ALA N N 15 6.603 0.117 . . . . . . . 5858 1 71 . 1 1 80 80 ASP N N 15 7.041 0.121 . . . . . . . 5858 1 72 . 1 1 81 81 ALA N N 15 7.652 0.105 . . . . . . . 5858 1 73 . 1 1 83 83 ALA N N 15 7.581 0.054 . . . . . . . 5858 1 74 . 1 1 84 84 GLY N N 15 7.717 0.037 . . . . . . . 5858 1 75 . 1 1 85 85 GLU N N 15 7.461 0.057 . . . . . . . 5858 1 76 . 1 1 86 86 TYR N N 15 7.249 0.108 . . . . . . . 5858 1 77 . 1 1 87 87 THR N N 15 8.398 0.093 . . . . . . . 5858 1 78 . 1 1 88 88 PHE N N 15 8.731 0.162 . . . . . . . 5858 1 79 . 1 1 89 89 TYR N N 15 8.258 0.133 . . . . . . . 5858 1 80 . 1 1 90 90 CYS N N 15 12.956 0.090 . . . . . . . 5858 1 81 . 1 1 91 91 GLU N N 15 8.401 0.147 . . . . . . . 5858 1 82 . 1 1 93 93 HIS N N 15 48.208 12.734 . . . . . . . 5858 1 83 . 1 1 94 94 ARG N N 15 12.978 0.232 . . . . . . . 5858 1 84 . 1 1 95 95 GLY N N 15 9.791 0.070 . . . . . . . 5858 1 85 . 1 1 96 96 ALA N N 15 9.371 0.074 . . . . . . . 5858 1 86 . 1 1 97 97 GLY N N 15 8.277 0.154 . . . . . . . 5858 1 87 . 1 1 98 98 MET N N 15 24.395 0.354 . . . . . . . 5858 1 88 . 1 1 99 99 VAL N N 15 10.281 0.138 . . . . . . . 5858 1 89 . 1 1 100 100 GLY N N 15 9.485 0.072 . . . . . . . 5858 1 90 . 1 1 101 101 LYS N N 15 8.211 0.065 . . . . . . . 5858 1 91 . 1 1 102 102 ILE N N 15 7.952 0.159 . . . . . . . 5858 1 92 . 1 1 103 103 THR N N 15 8.073 0.270 . . . . . . . 5858 1 93 . 1 1 104 104 VAL N N 15 7.955 0.039 . . . . . . . 5858 1 94 . 1 1 105 105 ALA N N 15 7.723 0.056 . . . . . . . 5858 1 95 . 1 1 106 106 GLY N N 15 2.446 0.081 . . . . . . . 5858 1 stop_ save_ save_relax_2_10 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode relax_2_10 _Heteronucl_T2_list.Entry_ID 5858 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Sample_condition_list_ID 10 _Heteronucl_T2_list.Sample_condition_list_label $Condition_10 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 800 _Heteronucl_T2_list.T2_coherence_type Ny _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $sample_1 . 5858 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 THR N N 15 6.887 0.071 . . . . . . . 5858 2 2 . 1 1 4 4 TYR N N 15 7.682 0.082 . . . . . . . 5858 2 3 . 1 1 5 5 THR N N 15 7.170 0.083 . . . . . . . 5858 2 4 . 1 1 6 6 VAL N N 15 7.574 0.056 . . . . . . . 5858 2 5 . 1 1 7 7 LYS N N 15 7.722 0.064 . . . . . . . 5858 2 6 . 1 1 8 8 LEU N N 15 8.242 0.072 . . . . . . . 5858 2 7 . 1 1 9 9 GLY N N 15 7.662 0.093 . . . . . . . 5858 2 8 . 1 1 10 10 SER N N 15 8.750 0.127 . . . . . . . 5858 2 9 . 1 1 11 11 ASP N N 15 8.511 0.070 . . . . . . . 5858 2 10 . 1 1 12 12 LYS N N 15 8.276 0.082 . . . . . . . 5858 2 11 . 1 1 13 13 GLY N N 15 8.413 0.098 . . . . . . . 5858 2 12 . 1 1 14 14 LEU N N 15 8.469 0.053 . . . . . . . 5858 2 13 . 1 1 15 15 LEU N N 15 7.919 0.114 . . . . . . . 5858 2 14 . 1 1 16 16 VAL N N 15 7.716 0.128 . . . . . . . 5858 2 15 . 1 1 17 17 PHE N N 15 11.705 0.140 . . . . . . . 5858 2 16 . 1 1 18 18 GLU N N 15 7.945 0.060 . . . . . . . 5858 2 17 . 1 1 20 20 ALA N N 15 8.119 0.111 . . . . . . . 5858 2 18 . 1 1 21 21 LYS N N 15 7.662 0.069 . . . . . . . 5858 2 19 . 1 1 22 22 LEU N N 15 7.685 0.045 . . . . . . . 5858 2 20 . 1 1 23 23 THR N N 15 7.164 0.048 . . . . . . . 5858 2 21 . 1 1 24 24 ILE N N 15 7.915 0.086 . . . . . . . 5858 2 22 . 1 1 25 25 LYS N N 15 8.291 0.065 . . . . . . . 5858 2 23 . 1 1 27 27 GLY N N 15 7.359 0.070 . . . . . . . 5858 2 24 . 1 1 28 28 ASP N N 15 8.618 0.092 . . . . . . . 5858 2 25 . 1 1 29 29 THR N N 15 7.622 0.048 . . . . . . . 5858 2 26 . 1 1 30 30 VAL N N 15 7.783 0.164 . . . . . . . 5858 2 27 . 1 1 31 31 GLU N N 15 8.127 0.059 . . . . . . . 5858 2 28 . 1 1 32 32 PHE N N 15 7.722 0.130 . . . . . . . 5858 2 29 . 1 1 33 33 LEU N N 15 7.565 0.113 . . . . . . . 5858 2 30 . 1 1 34 34 ASN N N 15 8.259 0.098 . . . . . . . 5858 2 31 . 1 1 35 35 ASN N N 15 8.396 0.110 . . . . . . . 5858 2 32 . 1 1 36 36 LYS N N 15 7.217 0.065 . . . . . . . 5858 2 33 . 1 1 37 37 VAL N N 15 13.276 0.146 . . . . . . . 5858 2 34 . 1 1 40 40 HIS N N 15 11.864 0.176 . . . . . . . 5858 2 35 . 1 1 41 41 ASN N N 15 9.738 0.172 . . . . . . . 5858 2 36 . 1 1 42 42 VAL N N 15 8.879 0.107 . . . . . . . 5858 2 37 . 1 1 43 43 VAL N N 15 8.240 0.069 . . . . . . . 5858 2 38 . 1 1 44 44 PHE N N 15 7.822 0.174 . . . . . . . 5858 2 39 . 1 1 45 45 ASP N N 15 7.892 0.090 . . . . . . . 5858 2 40 . 1 1 46 46 ALA N N 15 8.415 0.131 . . . . . . . 5858 2 41 . 1 1 47 47 ALA N N 15 8.513 0.055 . . . . . . . 5858 2 42 . 1 1 48 48 LEU N N 15 6.926 0.086 . . . . . . . 5858 2 43 . 1 1 49 49 ASN N N 15 7.558 0.081 . . . . . . . 5858 2 44 . 1 1 51 51 ALA N N 15 7.966 0.094 . . . . . . . 5858 2 45 . 1 1 52 52 LYS N N 15 8.312 0.061 . . . . . . . 5858 2 46 . 1 1 53 53 SER N N 15 7.912 0.095 . . . . . . . 5858 2 47 . 1 1 54 54 ALA N N 15 8.318 0.098 . . . . . . . 5858 2 48 . 1 1 55 55 ASP N N 15 8.479 0.065 . . . . . . . 5858 2 49 . 1 1 56 56 LEU N N 15 7.915 0.065 . . . . . . . 5858 2 50 . 1 1 57 57 ALA N N 15 8.697 0.098 . . . . . . . 5858 2 51 . 1 1 58 58 LYS N N 15 8.448 0.155 . . . . . . . 5858 2 52 . 1 1 59 59 SER N N 15 8.386 0.119 . . . . . . . 5858 2 53 . 1 1 60 60 LEU N N 15 8.166 0.075 . . . . . . . 5858 2 54 . 1 1 61 61 SER N N 15 7.828 0.045 . . . . . . . 5858 2 55 . 1 1 62 62 HIS N N 15 8.369 0.131 . . . . . . . 5858 2 56 . 1 1 63 63 LYS N N 15 7.974 0.094 . . . . . . . 5858 2 57 . 1 1 64 64 GLN N N 15 8.661 0.060 . . . . . . . 5858 2 58 . 1 1 65 65 LEU N N 15 7.463 0.054 . . . . . . . 5858 2 59 . 1 1 66 66 LEU N N 15 7.154 0.110 . . . . . . . 5858 2 60 . 1 1 67 67 MET N N 15 7.029 0.054 . . . . . . . 5858 2 61 . 1 1 68 68 SER N N 15 8.480 0.070 . . . . . . . 5858 2 62 . 1 1 70 70 GLY N N 15 6.371 0.133 . . . . . . . 5858 2 63 . 1 1 71 71 GLN N N 15 8.314 0.104 . . . . . . . 5858 2 64 . 1 1 72 72 SER N N 15 7.545 0.052 . . . . . . . 5858 2 65 . 1 1 73 73 THR N N 15 7.955 0.045 . . . . . . . 5858 2 66 . 1 1 74 74 SER N N 15 7.773 0.108 . . . . . . . 5858 2 67 . 1 1 75 75 THR N N 15 8.026 0.053 . . . . . . . 5858 2 68 . 1 1 76 76 THR N N 15 7.423 0.071 . . . . . . . 5858 2 69 . 1 1 77 77 PHE N N 15 8.365 0.124 . . . . . . . 5858 2 70 . 1 1 79 79 ALA N N 15 6.610 0.068 . . . . . . . 5858 2 71 . 1 1 80 80 ASP N N 15 7.142 0.089 . . . . . . . 5858 2 72 . 1 1 81 81 ALA N N 15 7.666 0.153 . . . . . . . 5858 2 73 . 1 1 83 83 ALA N N 15 7.719 0.068 . . . . . . . 5858 2 74 . 1 1 84 84 GLY N N 15 7.703 0.056 . . . . . . . 5858 2 75 . 1 1 85 85 GLU N N 15 7.434 0.091 . . . . . . . 5858 2 76 . 1 1 86 86 TYR N N 15 7.426 0.069 . . . . . . . 5858 2 77 . 1 1 87 87 THR N N 15 8.410 0.067 . . . . . . . 5858 2 78 . 1 1 88 88 PHE N N 15 8.119 0.093 . . . . . . . 5858 2 79 . 1 1 89 89 TYR N N 15 8.250 0.169 . . . . . . . 5858 2 80 . 1 1 90 90 CYS N N 15 11.229 0.084 . . . . . . . 5858 2 81 . 1 1 91 91 GLU N N 15 8.275 0.111 . . . . . . . 5858 2 82 . 1 1 93 93 HIS N N 15 36.230 1.710 . . . . . . . 5858 2 83 . 1 1 94 94 ARG N N 15 11.293 0.120 . . . . . . . 5858 2 84 . 1 1 95 95 GLY N N 15 9.073 0.100 . . . . . . . 5858 2 85 . 1 1 96 96 ALA N N 15 8.600 0.216 . . . . . . . 5858 2 86 . 1 1 97 97 GLY N N 15 8.168 0.235 . . . . . . . 5858 2 87 . 1 1 98 98 MET N N 15 18.744 0.219 . . . . . . . 5858 2 88 . 1 1 99 99 VAL N N 15 9.639 0.123 . . . . . . . 5858 2 89 . 1 1 100 100 GLY N N 15 9.019 0.081 . . . . . . . 5858 2 90 . 1 1 101 101 LYS N N 15 8.060 0.068 . . . . . . . 5858 2 91 . 1 1 102 102 ILE N N 15 7.793 0.055 . . . . . . . 5858 2 92 . 1 1 103 103 THR N N 15 7.843 0.129 . . . . . . . 5858 2 93 . 1 1 104 104 VAL N N 15 7.921 0.064 . . . . . . . 5858 2 94 . 1 1 105 105 ALA N N 15 7.816 0.073 . . . . . . . 5858 2 95 . 1 1 106 106 GLY N N 15 2.693 0.054 . . . . . . . 5858 2 stop_ save_ save_relax_2_11 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode relax_2_11 _Heteronucl_T2_list.Entry_ID 5858 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Sample_condition_list_ID 11 _Heteronucl_T2_list.Sample_condition_list_label $Condition_11 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 800 _Heteronucl_T2_list.T2_coherence_type Ny _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $sample_1 . 5858 3 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 THR N N 15 6.781 0.046 . . . . . . . 5858 3 2 . 1 1 4 4 TYR N N 15 7.434 0.121 . . . . . . . 5858 3 3 . 1 1 5 5 THR N N 15 7.060 0.080 . . . . . . . 5858 3 4 . 1 1 6 6 VAL N N 15 7.696 0.073 . . . . . . . 5858 3 5 . 1 1 7 7 LYS N N 15 7.673 0.090 . . . . . . . 5858 3 6 . 1 1 8 8 LEU N N 15 9.911 0.180 . . . . . . . 5858 3 7 . 1 1 9 9 GLY N N 15 7.753 0.108 . . . . . . . 5858 3 8 . 1 1 10 10 SER N N 15 8.883 0.137 . . . . . . . 5858 3 9 . 1 1 11 11 ASP N N 15 8.823 0.111 . . . . . . . 5858 3 10 . 1 1 12 12 LYS N N 15 8.143 0.159 . . . . . . . 5858 3 11 . 1 1 13 13 GLY N N 15 8.084 0.118 . . . . . . . 5858 3 12 . 1 1 14 14 LEU N N 15 8.259 0.095 . . . . . . . 5858 3 13 . 1 1 15 15 LEU N N 15 7.605 0.101 . . . . . . . 5858 3 14 . 1 1 16 16 VAL N N 15 6.193 2.414 . . . . . . . 5858 3 15 . 1 1 17 17 PHE N N 15 7.717 0.152 . . . . . . . 5858 3 16 . 1 1 18 18 GLU N N 15 7.786 0.101 . . . . . . . 5858 3 17 . 1 1 20 20 ALA N N 15 7.904 0.132 . . . . . . . 5858 3 18 . 1 1 21 21 LYS N N 15 7.646 0.046 . . . . . . . 5858 3 19 . 1 1 22 22 LEU N N 15 7.523 0.192 . . . . . . . 5858 3 20 . 1 1 23 23 THR N N 15 6.519 0.062 . . . . . . . 5858 3 21 . 1 1 24 24 ILE N N 15 7.883 0.137 . . . . . . . 5858 3 22 . 1 1 25 25 LYS N N 15 8.256 0.101 . . . . . . . 5858 3 23 . 1 1 27 27 GLY N N 15 7.342 0.148 . . . . . . . 5858 3 24 . 1 1 28 28 ASP N N 15 8.334 0.081 . . . . . . . 5858 3 25 . 1 1 29 29 THR N N 15 7.523 0.104 . . . . . . . 5858 3 26 . 1 1 30 30 VAL N N 15 7.533 0.290 . . . . . . . 5858 3 27 . 1 1 31 31 GLU N N 15 8.085 0.131 . . . . . . . 5858 3 28 . 1 1 32 32 PHE N N 15 7.790 0.109 . . . . . . . 5858 3 29 . 1 1 33 33 LEU N N 15 7.420 0.084 . . . . . . . 5858 3 30 . 1 1 34 34 ASN N N 15 8.146 0.116 . . . . . . . 5858 3 31 . 1 1 35 35 ASN N N 15 8.624 0.136 . . . . . . . 5858 3 32 . 1 1 36 36 LYS N N 15 6.963 0.071 . . . . . . . 5858 3 33 . 1 1 37 37 VAL N N 15 10.768 0.170 . . . . . . . 5858 3 34 . 1 1 40 40 HIS N N 15 9.604 0.131 . . . . . . . 5858 3 35 . 1 1 41 41 ASN N N 15 8.669 0.177 . . . . . . . 5858 3 36 . 1 1 42 42 VAL N N 15 8.432 0.089 . . . . . . . 5858 3 37 . 1 1 43 43 VAL N N 15 8.357 0.089 . . . . . . . 5858 3 38 . 1 1 44 44 PHE N N 15 7.668 0.211 . . . . . . . 5858 3 39 . 1 1 45 45 ASP N N 15 7.337 0.124 . . . . . . . 5858 3 40 . 1 1 46 46 ALA N N 15 8.187 0.079 . . . . . . . 5858 3 41 . 1 1 47 47 ALA N N 15 8.389 0.096 . . . . . . . 5858 3 42 . 1 1 48 48 LEU N N 15 7.124 0.091 . . . . . . . 5858 3 43 . 1 1 49 49 ASN N N 15 7.291 0.079 . . . . . . . 5858 3 44 . 1 1 51 51 ALA N N 15 8.089 0.157 . . . . . . . 5858 3 45 . 1 1 52 52 LYS N N 15 8.410 0.103 . . . . . . . 5858 3 46 . 1 1 53 53 SER N N 15 7.618 0.072 . . . . . . . 5858 3 47 . 1 1 54 54 ALA N N 15 8.211 0.119 . . . . . . . 5858 3 48 . 1 1 55 55 ASP N N 15 7.988 0.110 . . . . . . . 5858 3 49 . 1 1 56 56 LEU N N 15 7.836 0.074 . . . . . . . 5858 3 50 . 1 1 57 57 ALA N N 15 8.565 0.076 . . . . . . . 5858 3 51 . 1 1 58 58 LYS N N 15 8.664 0.119 . . . . . . . 5858 3 52 . 1 1 59 59 SER N N 15 8.409 0.188 . . . . . . . 5858 3 53 . 1 1 60 60 LEU N N 15 8.425 0.104 . . . . . . . 5858 3 54 . 1 1 61 61 SER N N 15 7.941 0.109 . . . . . . . 5858 3 55 . 1 1 62 62 HIS N N 15 7.974 0.116 . . . . . . . 5858 3 56 . 1 1 63 63 LYS N N 15 7.901 0.099 . . . . . . . 5858 3 57 . 1 1 64 64 GLN N N 15 8.171 0.099 . . . . . . . 5858 3 58 . 1 1 65 65 LEU N N 15 6.900 0.115 . . . . . . . 5858 3 59 . 1 1 66 66 LEU N N 15 7.165 0.151 . . . . . . . 5858 3 60 . 1 1 67 67 MET N N 15 7.109 0.095 . . . . . . . 5858 3 61 . 1 1 68 68 SER N N 15 7.961 0.110 . . . . . . . 5858 3 62 . 1 1 70 70 GLY N N 15 6.489 0.087 . . . . . . . 5858 3 63 . 1 1 71 71 GLN N N 15 8.393 0.102 . . . . . . . 5858 3 64 . 1 1 72 72 SER N N 15 7.883 0.109 . . . . . . . 5858 3 65 . 1 1 73 73 THR N N 15 7.143 0.143 . . . . . . . 5858 3 66 . 1 1 74 74 SER N N 15 7.636 0.081 . . . . . . . 5858 3 67 . 1 1 75 75 THR N N 15 8.129 0.107 . . . . . . . 5858 3 68 . 1 1 76 76 THR N N 15 7.345 0.078 . . . . . . . 5858 3 69 . 1 1 77 77 PHE N N 15 8.335 0.091 . . . . . . . 5858 3 70 . 1 1 79 79 ALA N N 15 6.518 0.080 . . . . . . . 5858 3 71 . 1 1 80 80 ASP N N 15 6.860 0.110 . . . . . . . 5858 3 72 . 1 1 81 81 ALA N N 15 7.544 0.091 . . . . . . . 5858 3 73 . 1 1 83 83 ALA N N 15 7.367 0.073 . . . . . . . 5858 3 74 . 1 1 84 84 GLY N N 15 7.788 0.082 . . . . . . . 5858 3 75 . 1 1 85 85 GLU N N 15 7.145 0.084 . . . . . . . 5858 3 76 . 1 1 86 86 TYR N N 15 7.500 0.086 . . . . . . . 5858 3 77 . 1 1 87 87 THR N N 15 8.316 0.125 . . . . . . . 5858 3 78 . 1 1 88 88 PHE N N 15 7.868 0.101 . . . . . . . 5858 3 79 . 1 1 89 89 TYR N N 15 8.429 0.121 . . . . . . . 5858 3 80 . 1 1 90 90 CYS N N 15 9.794 0.137 . . . . . . . 5858 3 81 . 1 1 91 91 GLU N N 15 8.442 0.135 . . . . . . . 5858 3 82 . 1 1 93 93 HIS N N 15 21.722 0.900 . . . . . . . 5858 3 83 . 1 1 94 94 ARG N N 15 9.578 0.165 . . . . . . . 5858 3 84 . 1 1 95 95 GLY N N 15 8.630 0.110 . . . . . . . 5858 3 85 . 1 1 96 96 ALA N N 15 8.109 0.074 . . . . . . . 5858 3 86 . 1 1 97 97 GLY N N 15 7.962 0.218 . . . . . . . 5858 3 87 . 1 1 98 98 MET N N 15 13.994 0.175 . . . . . . . 5858 3 88 . 1 1 99 99 VAL N N 15 8.429 0.116 . . . . . . . 5858 3 89 . 1 1 100 100 GLY N N 15 8.892 0.137 . . . . . . . 5858 3 90 . 1 1 101 101 LYS N N 15 7.890 0.088 . . . . . . . 5858 3 91 . 1 1 102 102 ILE N N 15 7.998 0.137 . . . . . . . 5858 3 92 . 1 1 103 103 THR N N 15 7.802 0.104 . . . . . . . 5858 3 93 . 1 1 104 104 VAL N N 15 7.805 0.075 . . . . . . . 5858 3 94 . 1 1 105 105 ALA N N 15 7.828 0.117 . . . . . . . 5858 3 95 . 1 1 106 106 GLY N N 15 2.942 0.053 . . . . . . . 5858 3 stop_ save_ save_relax_2_12 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode relax_2_12 _Heteronucl_T2_list.Entry_ID 5858 _Heteronucl_T2_list.ID 4 _Heteronucl_T2_list.Sample_condition_list_ID 12 _Heteronucl_T2_list.Sample_condition_list_label $Condition_12 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 800 _Heteronucl_T2_list.T2_coherence_type Ny _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $sample_1 . 5858 4 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 THR N N 15 8.253 0.254 . . . . . . . 5858 4 2 . 1 1 4 4 TYR N N 15 8.613 0.093 . . . . . . . 5858 4 3 . 1 1 5 5 THR N N 15 8.174 0.060 . . . . . . . 5858 4 4 . 1 1 6 6 VAL N N 15 8.605 0.054 . . . . . . . 5858 4 5 . 1 1 7 7 LYS N N 15 8.721 0.047 . . . . . . . 5858 4 6 . 1 1 8 8 LEU N N 15 9.368 0.075 . . . . . . . 5858 4 7 . 1 1 9 9 GLY N N 15 8.892 0.075 . . . . . . . 5858 4 8 . 1 1 10 10 SER N N 15 9.880 0.098 . . . . . . . 5858 4 9 . 1 1 11 11 ASP N N 15 9.727 0.134 . . . . . . . 5858 4 10 . 1 1 12 12 LYS N N 15 10.123 0.089 . . . . . . . 5858 4 11 . 1 1 13 13 GLY N N 15 9.874 0.075 . . . . . . . 5858 4 12 . 1 1 14 14 LEU N N 15 9.584 0.075 . . . . . . . 5858 4 13 . 1 1 15 15 LEU N N 15 9.611 0.088 . . . . . . . 5858 4 14 . 1 1 16 16 VAL N N 15 9.062 0.095 . . . . . . . 5858 4 15 . 1 1 17 17 PHE N N 15 15.046 0.181 . . . . . . . 5858 4 16 . 1 1 18 18 GLU N N 15 9.406 0.092 . . . . . . . 5858 4 17 . 1 1 20 20 ALA N N 15 9.373 0.064 . . . . . . . 5858 4 18 . 1 1 21 21 LYS N N 15 8.836 0.057 . . . . . . . 5858 4 19 . 1 1 22 22 LEU N N 15 8.722 0.193 . . . . . . . 5858 4 20 . 1 1 23 23 THR N N 15 8.282 0.083 . . . . . . . 5858 4 21 . 1 1 24 24 ILE N N 15 9.126 0.100 . . . . . . . 5858 4 22 . 1 1 25 25 LYS N N 15 9.503 0.062 . . . . . . . 5858 4 23 . 1 1 27 27 GLY N N 15 8.405 0.093 . . . . . . . 5858 4 24 . 1 1 28 28 ASP N N 15 9.811 0.059 . . . . . . . 5858 4 25 . 1 1 29 29 THR N N 15 8.585 0.046 . . . . . . . 5858 4 26 . 1 1 30 30 VAL N N 15 8.900 0.042 . . . . . . . 5858 4 27 . 1 1 31 31 GLU N N 15 9.229 0.048 . . . . . . . 5858 4 28 . 1 1 32 32 PHE N N 15 8.801 0.081 . . . . . . . 5858 4 29 . 1 1 33 33 LEU N N 15 8.737 0.165 . . . . . . . 5858 4 30 . 1 1 34 34 ASN N N 15 9.417 0.071 . . . . . . . 5858 4 31 . 1 1 35 35 ASN N N 15 9.405 0.148 . . . . . . . 5858 4 32 . 1 1 36 36 LYS N N 15 8.266 0.044 . . . . . . . 5858 4 33 . 1 1 37 37 VAL N N 15 16.694 0.349 . . . . . . . 5858 4 34 . 1 1 40 40 HIS N N 15 16.458 0.167 . . . . . . . 5858 4 35 . 1 1 41 41 ASN N N 15 12.094 0.295 . . . . . . . 5858 4 36 . 1 1 42 42 VAL N N 15 10.689 0.055 . . . . . . . 5858 4 37 . 1 1 43 43 VAL N N 15 9.508 0.053 . . . . . . . 5858 4 38 . 1 1 44 44 PHE N N 15 8.847 0.164 . . . . . . . 5858 4 39 . 1 1 45 45 ASP N N 15 9.080 0.104 . . . . . . . 5858 4 40 . 1 1 46 46 ALA N N 15 9.554 0.060 . . . . . . . 5858 4 41 . 1 1 47 47 ALA N N 15 9.984 0.076 . . . . . . . 5858 4 42 . 1 1 48 48 LEU N N 15 8.075 0.073 . . . . . . . 5858 4 43 . 1 1 49 49 ASN N N 15 8.607 0.087 . . . . . . . 5858 4 44 . 1 1 51 51 ALA N N 15 9.128 0.054 . . . . . . . 5858 4 45 . 1 1 52 52 LYS N N 15 9.597 0.101 . . . . . . . 5858 4 46 . 1 1 53 53 SER N N 15 8.875 0.070 . . . . . . . 5858 4 47 . 1 1 54 54 ALA N N 15 9.794 0.129 . . . . . . . 5858 4 48 . 1 1 55 55 ASP N N 15 9.656 0.091 . . . . . . . 5858 4 49 . 1 1 56 56 LEU N N 15 9.382 0.113 . . . . . . . 5858 4 50 . 1 1 57 57 ALA N N 15 9.878 0.081 . . . . . . . 5858 4 51 . 1 1 58 58 LYS N N 15 9.776 0.066 . . . . . . . 5858 4 52 . 1 1 59 59 SER N N 15 9.308 0.177 . . . . . . . 5858 4 53 . 1 1 60 60 LEU N N 15 9.520 0.054 . . . . . . . 5858 4 54 . 1 1 61 61 SER N N 15 9.112 0.160 . . . . . . . 5858 4 55 . 1 1 62 62 HIS N N 15 11.025 0.075 . . . . . . . 5858 4 56 . 1 1 63 63 LYS N N 15 9.822 0.089 . . . . . . . 5858 4 57 . 1 1 64 64 GLN N N 15 10.354 0.081 . . . . . . . 5858 4 58 . 1 1 65 65 LEU N N 15 9.163 0.076 . . . . . . . 5858 4 59 . 1 1 66 66 LEU N N 15 8.347 0.108 . . . . . . . 5858 4 60 . 1 1 67 67 MET N N 15 8.225 0.144 . . . . . . . 5858 4 61 . 1 1 68 68 SER N N 15 10.667 0.102 . . . . . . . 5858 4 62 . 1 1 70 70 GLY N N 15 7.411 0.070 . . . . . . . 5858 4 63 . 1 1 71 71 GLN N N 15 9.654 0.080 . . . . . . . 5858 4 64 . 1 1 72 72 SER N N 15 8.558 0.059 . . . . . . . 5858 4 65 . 1 1 73 73 THR N N 15 9.210 0.079 . . . . . . . 5858 4 66 . 1 1 74 74 SER N N 15 9.719 0.093 . . . . . . . 5858 4 67 . 1 1 75 75 THR N N 15 9.592 0.054 . . . . . . . 5858 4 68 . 1 1 76 76 THR N N 15 8.309 0.067 . . . . . . . 5858 4 69 . 1 1 77 77 PHE N N 15 9.644 0.158 . . . . . . . 5858 4 70 . 1 1 79 79 ALA N N 15 7.854 0.080 . . . . . . . 5858 4 71 . 1 1 80 80 ASP N N 15 8.312 0.145 . . . . . . . 5858 4 72 . 1 1 81 81 ALA N N 15 8.738 0.121 . . . . . . . 5858 4 73 . 1 1 83 83 ALA N N 15 8.920 0.114 . . . . . . . 5858 4 74 . 1 1 84 84 GLY N N 15 8.667 0.102 . . . . . . . 5858 4 75 . 1 1 85 85 GLU N N 15 8.746 0.052 . . . . . . . 5858 4 76 . 1 1 86 86 TYR N N 15 8.409 0.069 . . . . . . . 5858 4 77 . 1 1 87 87 THR N N 15 9.434 0.067 . . . . . . . 5858 4 78 . 1 1 88 88 PHE N N 15 10.209 0.089 . . . . . . . 5858 4 79 . 1 1 89 89 TYR N N 15 9.662 0.185 . . . . . . . 5858 4 80 . 1 1 90 90 CYS N N 15 14.011 0.104 . . . . . . . 5858 4 81 . 1 1 91 91 GLU N N 15 9.433 0.136 . . . . . . . 5858 4 82 . 1 1 93 93 HIS N N 15 54.000 6.823 . . . . . . . 5858 4 83 . 1 1 94 94 ARG N N 15 13.878 0.166 . . . . . . . 5858 4 84 . 1 1 95 95 GLY N N 15 11.016 0.092 . . . . . . . 5858 4 85 . 1 1 96 96 ALA N N 15 10.586 0.097 . . . . . . . 5858 4 86 . 1 1 97 97 GLY N N 15 9.651 0.178 . . . . . . . 5858 4 87 . 1 1 98 98 MET N N 15 26.981 0.679 . . . . . . . 5858 4 88 . 1 1 99 99 VAL N N 15 11.258 0.083 . . . . . . . 5858 4 89 . 1 1 100 100 GLY N N 15 10.708 0.084 . . . . . . . 5858 4 90 . 1 1 101 101 LYS N N 15 9.357 0.087 . . . . . . . 5858 4 91 . 1 1 102 102 ILE N N 15 8.901 0.058 . . . . . . . 5858 4 92 . 1 1 103 103 THR N N 15 8.956 0.059 . . . . . . . 5858 4 93 . 1 1 104 104 VAL N N 15 9.002 0.079 . . . . . . . 5858 4 94 . 1 1 105 105 ALA N N 15 8.901 0.071 . . . . . . . 5858 4 95 . 1 1 106 106 GLY N N 15 2.819 0.035 . . . . . . . 5858 4 stop_ save_ save_relax_2_13 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode relax_2_13 _Heteronucl_T2_list.Entry_ID 5858 _Heteronucl_T2_list.ID 5 _Heteronucl_T2_list.Sample_condition_list_ID 13 _Heteronucl_T2_list.Sample_condition_list_label $Condition_13 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 800 _Heteronucl_T2_list.T2_coherence_type Ny _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $sample_1 . 5858 5 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 THR N N 15 7.221 0.078 . . . . . . . 5858 5 2 . 1 1 4 4 TYR N N 15 6.690 0.068 . . . . . . . 5858 5 3 . 1 1 5 5 THR N N 15 6.381 0.054 . . . . . . . 5858 5 4 . 1 1 6 6 VAL N N 15 6.927 0.046 . . . . . . . 5858 5 5 . 1 1 7 7 LYS N N 15 6.837 0.039 . . . . . . . 5858 5 6 . 1 1 8 8 LEU N N 15 7.129 0.047 . . . . . . . 5858 5 7 . 1 1 9 9 GLY N N 15 6.986 0.091 . . . . . . . 5858 5 8 . 1 1 10 10 SER N N 15 7.751 0.076 . . . . . . . 5858 5 9 . 1 1 11 11 ASP N N 15 8.054 0.102 . . . . . . . 5858 5 10 . 1 1 12 12 LYS N N 15 9.103 0.133 . . . . . . . 5858 5 11 . 1 1 13 13 GLY N N 15 7.709 0.143 . . . . . . . 5858 5 12 . 1 1 14 14 LEU N N 15 7.546 0.089 . . . . . . . 5858 5 13 . 1 1 15 15 LEU N N 15 7.155 0.101 . . . . . . . 5858 5 14 . 1 1 16 16 VAL N N 15 6.980 0.068 . . . . . . . 5858 5 15 . 1 1 17 17 PHE N N 15 10.107 0.081 . . . . . . . 5858 5 16 . 1 1 18 18 GLU N N 15 7.221 0.064 . . . . . . . 5858 5 17 . 1 1 20 20 ALA N N 15 6.505 0.226 . . . . . . . 5858 5 18 . 1 1 21 21 LYS N N 15 6.921 0.093 . . . . . . . 5858 5 19 . 1 1 22 22 LEU N N 15 6.875 0.062 . . . . . . . 5858 5 20 . 1 1 23 23 THR N N 15 6.618 0.049 . . . . . . . 5858 5 21 . 1 1 24 24 ILE N N 15 7.109 0.052 . . . . . . . 5858 5 22 . 1 1 25 25 LYS N N 15 7.398 0.090 . . . . . . . 5858 5 23 . 1 1 27 27 GLY N N 15 6.584 0.039 . . . . . . . 5858 5 24 . 1 1 28 28 ASP N N 15 7.791 0.068 . . . . . . . 5858 5 25 . 1 1 29 29 THR N N 15 6.807 0.041 . . . . . . . 5858 5 26 . 1 1 30 30 VAL N N 15 7.002 0.071 . . . . . . . 5858 5 27 . 1 1 31 31 GLU N N 15 7.387 0.089 . . . . . . . 5858 5 28 . 1 1 32 32 PHE N N 15 6.899 0.083 . . . . . . . 5858 5 29 . 1 1 33 33 LEU N N 15 6.634 0.054 . . . . . . . 5858 5 30 . 1 1 34 34 ASN N N 15 7.446 0.061 . . . . . . . 5858 5 31 . 1 1 35 35 ASN N N 15 7.570 0.092 . . . . . . . 5858 5 32 . 1 1 36 36 LYS N N 15 7.328 0.094 . . . . . . . 5858 5 33 . 1 1 37 37 VAL N N 15 11.303 0.133 . . . . . . . 5858 5 34 . 1 1 40 40 HIS N N 15 9.756 0.086 . . . . . . . 5858 5 35 . 1 1 41 41 ASN N N 15 8.494 0.112 . . . . . . . 5858 5 36 . 1 1 42 42 VAL N N 15 8.296 0.090 . . . . . . . 5858 5 37 . 1 1 43 43 VAL N N 15 7.525 0.079 . . . . . . . 5858 5 38 . 1 1 44 44 PHE N N 15 6.957 0.121 . . . . . . . 5858 5 39 . 1 1 45 45 ASP N N 15 7.251 0.066 . . . . . . . 5858 5 40 . 1 1 46 46 ALA N N 15 7.853 0.066 . . . . . . . 5858 5 41 . 1 1 47 47 ALA N N 15 7.693 0.069 . . . . . . . 5858 5 42 . 1 1 48 48 LEU N N 15 6.233 0.066 . . . . . . . 5858 5 43 . 1 1 49 49 ASN N N 15 6.724 0.081 . . . . . . . 5858 5 44 . 1 1 51 51 ALA N N 15 7.285 0.050 . . . . . . . 5858 5 45 . 1 1 52 52 LYS N N 15 7.578 0.046 . . . . . . . 5858 5 46 . 1 1 53 53 SER N N 15 7.209 0.036 . . . . . . . 5858 5 47 . 1 1 54 54 ALA N N 15 8.357 0.095 . . . . . . . 5858 5 48 . 1 1 55 55 ASP N N 15 8.358 0.089 . . . . . . . 5858 5 49 . 1 1 56 56 LEU N N 15 7.456 0.068 . . . . . . . 5858 5 50 . 1 1 57 57 ALA N N 15 7.968 0.070 . . . . . . . 5858 5 51 . 1 1 58 58 LYS N N 15 7.853 0.185 . . . . . . . 5858 5 52 . 1 1 59 59 SER N N 15 6.491 0.480 . . . . . . . 5858 5 53 . 1 1 60 60 LEU N N 15 7.620 0.037 . . . . . . . 5858 5 54 . 1 1 61 61 SER N N 15 7.197 0.039 . . . . . . . 5858 5 55 . 1 1 62 62 HIS N N 15 8.864 0.087 . . . . . . . 5858 5 56 . 1 1 63 63 LYS N N 15 8.031 0.102 . . . . . . . 5858 5 57 . 1 1 64 64 GLN N N 15 7.974 0.087 . . . . . . . 5858 5 58 . 1 1 65 65 LEU N N 15 7.034 0.036 . . . . . . . 5858 5 59 . 1 1 66 66 LEU N N 15 6.581 0.069 . . . . . . . 5858 5 60 . 1 1 67 67 MET N N 15 6.305 0.052 . . . . . . . 5858 5 61 . 1 1 68 68 SER N N 15 7.705 0.058 . . . . . . . 5858 5 62 . 1 1 70 70 GLY N N 15 5.795 0.048 . . . . . . . 5858 5 63 . 1 1 71 71 GLN N N 15 7.405 0.079 . . . . . . . 5858 5 64 . 1 1 72 72 SER N N 15 6.535 0.069 . . . . . . . 5858 5 65 . 1 1 73 73 THR N N 15 7.090 0.080 . . . . . . . 5858 5 66 . 1 1 74 74 SER N N 15 7.916 0.112 . . . . . . . 5858 5 67 . 1 1 75 75 THR N N 15 7.282 0.085 . . . . . . . 5858 5 68 . 1 1 76 76 THR N N 15 6.858 0.071 . . . . . . . 5858 5 69 . 1 1 77 77 PHE N N 15 7.368 0.075 . . . . . . . 5858 5 70 . 1 1 79 79 ALA N N 15 6.367 0.103 . . . . . . . 5858 5 71 . 1 1 80 80 ASP N N 15 6.351 0.098 . . . . . . . 5858 5 72 . 1 1 81 81 ALA N N 15 6.968 0.111 . . . . . . . 5858 5 73 . 1 1 83 83 ALA N N 15 6.902 0.080 . . . . . . . 5858 5 74 . 1 1 84 84 GLY N N 15 6.718 0.061 . . . . . . . 5858 5 75 . 1 1 85 85 GLU N N 15 6.749 0.051 . . . . . . . 5858 5 76 . 1 1 86 86 TYR N N 15 6.723 0.074 . . . . . . . 5858 5 77 . 1 1 87 87 THR N N 15 7.394 0.071 . . . . . . . 5858 5 78 . 1 1 88 88 PHE N N 15 7.713 0.100 . . . . . . . 5858 5 79 . 1 1 89 89 TYR N N 15 7.523 0.046 . . . . . . . 5858 5 80 . 1 1 90 90 CYS N N 15 9.951 0.097 . . . . . . . 5858 5 81 . 1 1 91 91 GLU N N 15 7.340 0.089 . . . . . . . 5858 5 82 . 1 1 93 93 HIS N N 15 28.540 1.228 . . . . . . . 5858 5 83 . 1 1 94 94 ARG N N 15 10.505 0.124 . . . . . . . 5858 5 84 . 1 1 95 95 GLY N N 15 9.551 0.127 . . . . . . . 5858 5 85 . 1 1 96 96 ALA N N 15 8.232 0.147 . . . . . . . 5858 5 86 . 1 1 97 97 GLY N N 15 7.622 0.159 . . . . . . . 5858 5 87 . 1 1 98 98 MET N N 15 16.517 0.171 . . . . . . . 5858 5 88 . 1 1 99 99 VAL N N 15 8.474 0.101 . . . . . . . 5858 5 89 . 1 1 100 100 GLY N N 15 7.973 0.078 . . . . . . . 5858 5 90 . 1 1 101 101 LYS N N 15 7.171 0.050 . . . . . . . 5858 5 91 . 1 1 102 102 ILE N N 15 7.096 0.086 . . . . . . . 5858 5 92 . 1 1 103 103 THR N N 15 7.114 0.033 . . . . . . . 5858 5 93 . 1 1 104 104 VAL N N 15 7.084 0.051 . . . . . . . 5858 5 94 . 1 1 105 105 ALA N N 15 6.905 0.062 . . . . . . . 5858 5 95 . 1 1 106 106 GLY N N 15 2.026 0.055 . . . . . . . 5858 5 stop_ save_ save_relax_2_14 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode relax_2_14 _Heteronucl_T2_list.Entry_ID 5858 _Heteronucl_T2_list.ID 6 _Heteronucl_T2_list.Sample_condition_list_ID 14 _Heteronucl_T2_list.Sample_condition_list_label $Condition_14 _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 800 _Heteronucl_T2_list.T2_coherence_type Ny _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID . . 1 $sample_1 . 5858 6 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 THR N N 15 7.156 0.161 . . . . . . . 5858 6 2 . 1 1 4 4 TYR N N 15 6.126 0.039 . . . . . . . 5858 6 3 . 1 1 5 5 THR N N 15 5.799 0.045 . . . . . . . 5858 6 4 . 1 1 6 6 VAL N N 15 6.271 0.042 . . . . . . . 5858 6 5 . 1 1 7 7 LYS N N 15 6.251 0.068 . . . . . . . 5858 6 6 . 1 1 8 8 LEU N N 15 6.226 0.097 . . . . . . . 5858 6 7 . 1 1 9 9 GLY N N 15 6.052 0.061 . . . . . . . 5858 6 8 . 1 1 10 10 SER N N 15 7.080 0.044 . . . . . . . 5858 6 9 . 1 1 11 11 ASP N N 15 7.751 0.111 . . . . . . . 5858 6 10 . 1 1 12 12 LYS N N 15 8.866 0.356 . . . . . . . 5858 6 11 . 1 1 13 13 GLY N N 15 7.439 0.116 . . . . . . . 5858 6 12 . 1 1 14 14 LEU N N 15 6.924 0.067 . . . . . . . 5858 6 13 . 1 1 15 15 LEU N N 15 6.255 0.113 . . . . . . . 5858 6 14 . 1 1 16 16 VAL N N 15 6.195 0.062 . . . . . . . 5858 6 15 . 1 1 17 17 PHE N N 15 8.619 0.079 . . . . . . . 5858 6 16 . 1 1 18 18 GLU N N 15 6.323 0.035 . . . . . . . 5858 6 17 . 1 1 20 20 ALA N N 15 6.467 0.043 . . . . . . . 5858 6 18 . 1 1 21 21 LYS N N 15 6.052 0.088 . . . . . . . 5858 6 19 . 1 1 22 22 LEU N N 15 6.097 0.032 . . . . . . . 5858 6 20 . 1 1 23 23 THR N N 15 5.922 0.070 . . . . . . . 5858 6 21 . 1 1 24 24 ILE N N 15 6.334 0.075 . . . . . . . 5858 6 22 . 1 1 25 25 LYS N N 15 6.712 0.041 . . . . . . . 5858 6 23 . 1 1 27 27 GLY N N 15 5.970 0.063 . . . . . . . 5858 6 24 . 1 1 28 28 ASP N N 15 6.880 0.130 . . . . . . . 5858 6 25 . 1 1 29 29 THR N N 15 6.220 0.038 . . . . . . . 5858 6 26 . 1 1 30 30 VAL N N 15 6.465 0.042 . . . . . . . 5858 6 27 . 1 1 31 31 GLU N N 15 6.687 0.041 . . . . . . . 5858 6 28 . 1 1 32 32 PHE N N 15 6.096 0.074 . . . . . . . 5858 6 29 . 1 1 33 33 LEU N N 15 6.033 0.116 . . . . . . . 5858 6 30 . 1 1 34 34 ASN N N 15 6.809 0.068 . . . . . . . 5858 6 31 . 1 1 35 35 ASN N N 15 6.593 0.078 . . . . . . . 5858 6 32 . 1 1 36 36 LYS N N 15 5.796 0.095 . . . . . . . 5858 6 33 . 1 1 37 37 VAL N N 15 9.329 0.110 . . . . . . . 5858 6 34 . 1 1 40 40 HIS N N 15 8.008 0.117 . . . . . . . 5858 6 35 . 1 1 41 41 ASN N N 15 7.242 0.094 . . . . . . . 5858 6 36 . 1 1 42 42 VAL N N 15 7.346 0.068 . . . . . . . 5858 6 37 . 1 1 43 43 VAL N N 15 6.866 0.047 . . . . . . . 5858 6 38 . 1 1 44 44 PHE N N 15 6.361 0.083 . . . . . . . 5858 6 39 . 1 1 45 45 ASP N N 15 6.453 0.060 . . . . . . . 5858 6 40 . 1 1 46 46 ALA N N 15 7.505 0.063 . . . . . . . 5858 6 41 . 1 1 47 47 ALA N N 15 7.037 0.055 . . . . . . . 5858 6 42 . 1 1 48 48 LEU N N 15 5.645 0.050 . . . . . . . 5858 6 43 . 1 1 49 49 ASN N N 15 6.017 0.028 . . . . . . . 5858 6 44 . 1 1 51 51 ALA N N 15 6.658 0.056 . . . . . . . 5858 6 45 . 1 1 52 52 LYS N N 15 6.745 0.092 . . . . . . . 5858 6 46 . 1 1 53 53 SER N N 15 6.656 0.065 . . . . . . . 5858 6 47 . 1 1 54 54 ALA N N 15 8.271 0.200 . . . . . . . 5858 6 48 . 1 1 55 55 ASP N N 15 8.013 0.159 . . . . . . . 5858 6 49 . 1 1 56 56 LEU N N 15 6.761 0.132 . . . . . . . 5858 6 50 . 1 1 57 57 ALA N N 15 7.227 0.055 . . . . . . . 5858 6 51 . 1 1 58 58 LYS N N 15 6.720 0.066 . . . . . . . 5858 6 52 . 1 1 59 59 SER N N 15 6.434 0.130 . . . . . . . 5858 6 53 . 1 1 60 60 LEU N N 15 6.845 0.103 . . . . . . . 5858 6 54 . 1 1 61 61 SER N N 15 6.419 0.047 . . . . . . . 5858 6 55 . 1 1 62 62 HIS N N 15 8.112 0.094 . . . . . . . 5858 6 56 . 1 1 63 63 LYS N N 15 7.771 0.147 . . . . . . . 5858 6 57 . 1 1 64 64 GLN N N 15 7.427 0.066 . . . . . . . 5858 6 58 . 1 1 65 65 LEU N N 15 6.404 0.042 . . . . . . . 5858 6 59 . 1 1 66 66 LEU N N 15 5.637 0.191 . . . . . . . 5858 6 60 . 1 1 67 67 MET N N 15 5.923 0.105 . . . . . . . 5858 6 61 . 1 1 68 68 SER N N 15 6.845 0.043 . . . . . . . 5858 6 62 . 1 1 70 70 GLY N N 15 5.437 0.103 . . . . . . . 5858 6 63 . 1 1 71 71 GLN N N 15 6.699 0.090 . . . . . . . 5858 6 64 . 1 1 72 72 SER N N 15 5.971 0.070 . . . . . . . 5858 6 65 . 1 1 73 73 THR N N 15 6.518 0.055 . . . . . . . 5858 6 66 . 1 1 74 74 SER N N 15 7.455 0.115 . . . . . . . 5858 6 67 . 1 1 75 75 THR N N 15 6.690 0.062 . . . . . . . 5858 6 68 . 1 1 76 76 THR N N 15 6.321 0.106 . . . . . . . 5858 6 69 . 1 1 77 77 PHE N N 15 6.662 0.075 . . . . . . . 5858 6 70 . 1 1 79 79 ALA N N 15 6.230 0.087 . . . . . . . 5858 6 71 . 1 1 80 80 ASP N N 15 5.887 0.044 . . . . . . . 5858 6 72 . 1 1 81 81 ALA N N 15 6.208 0.139 . . . . . . . 5858 6 73 . 1 1 83 83 ALA N N 15 6.116 0.086 . . . . . . . 5858 6 74 . 1 1 84 84 GLY N N 15 6.238 0.064 . . . . . . . 5858 6 75 . 1 1 85 85 GLU N N 15 6.220 0.047 . . . . . . . 5858 6 76 . 1 1 86 86 TYR N N 15 6.026 0.058 . . . . . . . 5858 6 77 . 1 1 87 87 THR N N 15 6.886 0.076 . . . . . . . 5858 6 78 . 1 1 88 88 PHE N N 15 6.973 0.151 . . . . . . . 5858 6 79 . 1 1 89 89 TYR N N 15 6.859 0.129 . . . . . . . 5858 6 80 . 1 1 90 90 CYS N N 15 8.303 0.087 . . . . . . . 5858 6 81 . 1 1 91 91 GLU N N 15 6.565 0.098 . . . . . . . 5858 6 82 . 1 1 93 93 HIS N N 15 21.832 0.481 . . . . . . . 5858 6 83 . 1 1 94 94 ARG N N 15 9.083 0.069 . . . . . . . 5858 6 84 . 1 1 95 95 GLY N N 15 9.087 0.218 . . . . . . . 5858 6 85 . 1 1 96 96 ALA N N 15 7.301 0.064 . . . . . . . 5858 6 86 . 1 1 97 97 GLY N N 15 7.038 0.165 . . . . . . . 5858 6 87 . 1 1 98 98 MET N N 15 13.023 0.140 . . . . . . . 5858 6 88 . 1 1 99 99 VAL N N 15 7.605 0.113 . . . . . . . 5858 6 89 . 1 1 100 100 GLY N N 15 7.056 0.053 . . . . . . . 5858 6 90 . 1 1 101 101 LYS N N 15 6.560 0.059 . . . . . . . 5858 6 91 . 1 1 102 102 ILE N N 15 6.324 0.045 . . . . . . . 5858 6 92 . 1 1 103 103 THR N N 15 6.383 0.064 . . . . . . . 5858 6 93 . 1 1 104 104 VAL N N 15 6.579 0.062 . . . . . . . 5858 6 94 . 1 1 105 105 ALA N N 15 6.303 0.053 . . . . . . . 5858 6 95 . 1 1 106 106 GLY N N 15 1.912 0.023 . . . . . . . 5858 6 stop_ save_