data_25534 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 25534 _Entry.Title ; RNA structure determination by solid-state NMR spectroscopy ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2015-03-12 _Entry.Accession_date 2015-03-12 _Entry.Last_release_date 2015-05-08 _Entry.Original_release_date 2015-05-08 _Entry.Origination author _Entry.NMR_STAR_version 3.1.2.6 _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype SOLID-STATE _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Alexander Marchanka . . . . 25534 2 Bernd Simon . . . . 25534 3 Gerhard Althoff-Ospelt . . . . 25534 4 Teresa Carlomagno . . . . 25534 stop_ loop_ _SG_project.SG_project_ID _SG_project.Project_name _SG_project.Full_name_of_center _SG_project.Initial_of_center _SG_project.Entry_ID 1 'not applicable' 'not applicable' . 25534 stop_ loop_ _Struct_keywords.Keywords _Struct_keywords.Text _Struct_keywords.Entry_ID RNA . 25534 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 25534 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '13C chemical shifts' 173 25534 '15N chemical shifts' 49 25534 '31P chemical shifts' 9 25534 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2016-08-29 2015-03-12 update BMRB 'update entry citation' 25534 1 . . 2015-05-08 2015-03-12 original author 'original release' 25534 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID PDB 2N0R 'BMRB Entry Tracking System' 25534 stop_ save_ ############### # Citations # ############### save_citations _Citation.Sf_category citations _Citation.Sf_framecode citations _Citation.Entry_ID 25534 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 25960310 _Citation.Full_citation . _Citation.Title ; RNA structure determination by solid-state NMR spectroscopy ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'Nat. Commun.' _Citation.Journal_name_full . _Citation.Journal_volume 6 _Citation.Journal_issue . _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 7024 _Citation.Page_last 7024 _Citation.Year 2015 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Alexander Marchanka . . . . 25534 1 2 Bernd Simon . . . . 25534 1 3 Gerhard Althoff-Ospelt . . . . 25534 1 4 Teresa Carlomagno . . . . 25534 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 25534 _Assembly.ID 1 _Assembly.Name "26mer Box C/D RNA (5'-R(P*CP*UP*GP*AP*GP*CP*UP*CP*GP*AP*AP*AP*GP*AP*GP*CP*AP*AP*UP*GP*AP*UP*G)-3')" _Assembly.BMRB_code . _Assembly.Number_of_components 1 _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 entity 1 $entity A . yes native no no . . . 25534 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity _Entity.Sf_category entity _Entity.Sf_framecode entity _Entity.Entry_ID 25534 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name '26mer Box C/D RNA' _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polyribonucleotide _Entity.Polymer_type_details . _Entity.Polymer_strand_ID A _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; GCUGAGCUCGAAAGAGCAAU GAUGUC ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 26 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method syn _Entity.Parent_entity_ID . _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight 7450.573 _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . G . 25534 1 2 . C . 25534 1 3 . U . 25534 1 4 . G . 25534 1 5 . A . 25534 1 6 . G . 25534 1 7 . C . 25534 1 8 . U . 25534 1 9 . C . 25534 1 10 . G . 25534 1 11 . A . 25534 1 12 . A . 25534 1 13 . A . 25534 1 14 . G . 25534 1 15 . A . 25534 1 16 . G . 25534 1 17 . C . 25534 1 18 . A . 25534 1 19 . A . 25534 1 20 . U . 25534 1 21 . G . 25534 1 22 . A . 25534 1 23 . U . 25534 1 24 . G . 25534 1 25 . U . 25534 1 26 . C . 25534 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . G 1 1 25534 1 . C 2 2 25534 1 . U 3 3 25534 1 . G 4 4 25534 1 . A 5 5 25534 1 . G 6 6 25534 1 . C 7 7 25534 1 . U 8 8 25534 1 . C 9 9 25534 1 . G 10 10 25534 1 . A 11 11 25534 1 . A 12 12 25534 1 . A 13 13 25534 1 . G 14 14 25534 1 . A 15 15 25534 1 . G 16 16 25534 1 . C 17 17 25534 1 . A 18 18 25534 1 . A 19 19 25534 1 . U 20 20 25534 1 . G 21 21 25534 1 . A 22 22 25534 1 . U 23 23 25534 1 . G 24 24 25534 1 . U 25 25 25534 1 . C 26 26 25534 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 25534 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity . 562 organism . 'Escherichia coli' 'E. coli' . . Bacteria . Escherichia coli . . . . . . . . . . . . . 25534 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 25534 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity . 'enzymatic semisynthesis' . . . . . . . . . . . . . . . . 25534 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 25534 _Sample.ID 1 _Sample.Type microcrystalline _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system H2O _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 entity 'nucleotide-type-selective [U-99% 13C; U-99% 15N]' . . 1 $entity . . 20 . . mg/mL . . . . 25534 1 2 H2O 'natural abundance' . . . . . . 100 . . % . . . . 25534 1 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 25534 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 7.5 . pH 25534 1 temperature 260 . K 25534 1 stop_ save_ ############################ # Computer software used # ############################ save_CNS _Software.Sf_category software _Software.Sf_framecode CNS _Software.Entry_ID 25534 _Software.ID 1 _Software.Name CNS _Software.Version 1.2 _Software.Details . loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'data analysis' 25534 1 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode spectrometer_1 _NMR_spectrometer.Entry_ID 25534 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 700 save_ save_spectrometer_2 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode spectrometer_2 _NMR_spectrometer.Entry_ID 25534 _NMR_spectrometer.ID 2 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_NMR_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode NMR_spectrometer_list _NMR_spectrometer_list.Entry_ID 25534 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 spectrometer_1 Bruker Avance . 700 . . . 25534 1 2 spectrometer_2 Bruker Avance . 600 . . . 25534 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 25534 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '(13C,15N-TEDOR)-13C,13C PDSD' no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 25534 1 2 '13C-31P TEDOR' no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 2 $spectrometer_2 . . . . . . . . . . . . . . . . 25534 1 3 CHHC no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 25534 1 4 NHHC no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 25534 1 5 CN-TEDOR no . . . . . . . . . . 1 $sample_1 solid . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 25534 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chemical_shift_reference_1 _Chem_shift_reference.Entry_ID 25534 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID C 13 adamantane 'methyl carbons' . . . . ppm 38.48 external direct 1 . . . . . 25534 1 N 15 adamantane 'methyl carbons' . . . . ppm 38.48 na indirect 0.402980 . . . . . 25534 1 P 31 adamantane 'methyl carbons' . . . . ppm 38.48 na indirect 1.609894 . . . . . 25534 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_1 _Assigned_chem_shift_list.Entry_ID 25534 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '(13C,15N-TEDOR)-13C,13C PDSD' . . . 25534 1 2 '13C-31P TEDOR' . . . 25534 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 2 2 C C2 C 13 158.1 0 . 1 . . . A 2 C C2 . 25534 1 2 . 1 1 3 3 U C1' C 13 93.7 0 . 1 . . . A 3 U C1' . 25534 1 3 . 1 1 3 3 U C2 C 13 154.1 0 . 1 . . . A 3 U C2 . 25534 1 4 . 1 1 3 3 U C2' C 13 75.6 0 . 1 . . . A 3 U C2' . 25534 1 5 . 1 1 3 3 U C3' C 13 71.9 0 . 1 . . . A 3 U C3' . 25534 1 6 . 1 1 3 3 U C4 C 13 165.7 0 . 1 . . . A 3 U C4 . 25534 1 7 . 1 1 3 3 U C4' C 13 82.9 0 . 1 . . . A 3 U C4' . 25534 1 8 . 1 1 3 3 U C5 C 13 104.7 0 . 1 . . . A 3 U C5 . 25534 1 9 . 1 1 3 3 U C5' C 13 64.0 0 . 1 . . . A 3 U C5' . 25534 1 10 . 1 1 3 3 U C6 C 13 139.3 0 . 1 . . . A 3 U C6 . 25534 1 11 . 1 1 3 3 U N1 N 15 145.5 0 . 1 . . . A 3 U N1 . 25534 1 12 . 1 1 3 3 U N3 N 15 157.1 0 . 1 . . . A 3 U N3 . 25534 1 13 . 1 1 4 4 G C1' C 13 90.1 0 . 1 . . . A 4 G C1' . 25534 1 14 . 1 1 4 4 G C2 C 13 156.6 0 . 1 . . . A 4 G C2 . 25534 1 15 . 1 1 4 4 G C2' C 13 76.0 0 . 1 . . . A 4 G C2' . 25534 1 16 . 1 1 4 4 G C3' C 13 79.6 0 . 1 . . . A 4 G C3' . 25534 1 17 . 1 1 4 4 G C4 C 13 155.3 0 . 1 . . . A 4 G C4 . 25534 1 18 . 1 1 4 4 G C4' C 13 88.3 0 . 1 . . . A 4 G C4' . 25534 1 19 . 1 1 4 4 G C5 C 13 116.7 0 . 1 . . . A 4 G C5 . 25534 1 20 . 1 1 4 4 G C5' C 13 67.8 0 . 1 . . . A 4 G C5' . 25534 1 21 . 1 1 4 4 G C6 C 13 160.3 0 . 1 . . . A 4 G C6 . 25534 1 22 . 1 1 4 4 G C8 C 13 139.0 0 . 1 . . . A 4 G C8 . 25534 1 23 . 1 1 4 4 G N1 N 15 145.0 0 . 1 . . . A 4 G N1 . 25534 1 24 . 1 1 4 4 G N2 N 15 81.4 0 . 1 . . . A 4 G N2 . 25534 1 25 . 1 1 4 4 G N9 N 15 167.0 0 . 1 . . . A 4 G N9 . 25534 1 26 . 1 1 4 4 G P P 31 -3.8 0 . 1 . . . A 4 G P . 25534 1 27 . 1 1 5 5 A C1' C 13 88.1 0 . 1 . . . A 5 A C1' . 25534 1 28 . 1 1 5 5 A C2 C 13 156.0 0 . 1 . . . A 5 A C2 . 25534 1 29 . 1 1 5 5 A C2' C 13 78.4 0 . 1 . . . A 5 A C2' . 25534 1 30 . 1 1 5 5 A C3' C 13 80.0 0 . 1 . . . A 5 A C3' . 25534 1 31 . 1 1 5 5 A C4 C 13 150.9 0 . 1 . . . A 5 A C4 . 25534 1 32 . 1 1 5 5 A C4' C 13 83.4 0 . 1 . . . A 5 A C4' . 25534 1 33 . 1 1 5 5 A C5 C 13 118.8 0 . 1 . . . A 5 A C5 . 25534 1 34 . 1 1 5 5 A C5' C 13 70.3 0 . 1 . . . A 5 A C5' . 25534 1 35 . 1 1 5 5 A C6 C 13 156.6 0 . 1 . . . A 5 A C6 . 25534 1 36 . 1 1 5 5 A C8 C 13 139.8 0 . 1 . . . A 5 A C8 . 25534 1 37 . 1 1 5 5 A N6 N 15 81.4 0 . 1 . . . A 5 A N6 . 25534 1 38 . 1 1 5 5 A N9 N 15 166.9 0 . 1 . . . A 5 A N9 . 25534 1 39 . 1 1 5 5 A P P 31 -0.7 0 . 1 . . . A 5 A P . 25534 1 40 . 1 1 6 6 G C1' C 13 92.6 0 . 1 . . . A 6 G C1' . 25534 1 41 . 1 1 6 6 G C2 C 13 158.2 0 . 1 . . . A 6 G C2 . 25534 1 42 . 1 1 6 6 G C2' C 13 75.8 0 . 1 . . . A 6 G C2' . 25534 1 43 . 1 1 6 6 G C3' C 13 77.3 0 . 1 . . . A 6 G C3' . 25534 1 44 . 1 1 6 6 G C4 C 13 152.2 0 . 1 . . . A 6 G C4 . 25534 1 45 . 1 1 6 6 G C4' C 13 83.4 0 . 1 . . . A 6 G C4' . 25534 1 46 . 1 1 6 6 G C5 C 13 119.5 0 . 1 . . . A 6 G C5 . 25534 1 47 . 1 1 6 6 G C5' C 13 70.9 0 . 1 . . . A 6 G C5' . 25534 1 48 . 1 1 6 6 G C6 C 13 157.9 0 . 1 . . . A 6 G C6 . 25534 1 49 . 1 1 6 6 G C8 C 13 139.0 0 . 1 . . . A 6 G C8 . 25534 1 50 . 1 1 6 6 G N1 N 15 148.9 0 . 1 . . . A 6 G N1 . 25534 1 51 . 1 1 6 6 G N2 N 15 75.8 0 . 1 . . . A 6 G N2 . 25534 1 52 . 1 1 6 6 G N9 N 15 171.1 0 . 1 . . . A 6 G N9 . 25534 1 53 . 1 1 6 6 G P P 31 -3.8 0 . 1 . . . A 6 G P . 25534 1 54 . 1 1 7 7 C C1' C 13 93.9 0 . 1 . . . A 7 C C1' . 25534 1 55 . 1 1 7 7 C C2 C 13 159.3 0 . 1 . . . A 7 C C2 . 25534 1 56 . 1 1 7 7 C C2' C 13 75.4 0 . 1 . . . A 7 C C2' . 25534 1 57 . 1 1 7 7 C C3' C 13 72.1 0 . 1 . . . A 7 C C3' . 25534 1 58 . 1 1 7 7 C C4 C 13 168.1 0 . 1 . . . A 7 C C4 . 25534 1 59 . 1 1 7 7 C C4' C 13 82.0 0 . 1 . . . A 7 C C4' . 25534 1 60 . 1 1 7 7 C C5 C 13 97.1 0 . 1 . . . A 7 C C5 . 25534 1 61 . 1 1 7 7 C C5' C 13 64.3 0 . 1 . . . A 7 C C5' . 25534 1 62 . 1 1 7 7 C C6 C 13 142.2 0 . 1 . . . A 7 C C6 . 25534 1 63 . 1 1 7 7 C N1 N 15 152.2 0 . 1 . . . A 7 C N1 . 25534 1 64 . 1 1 7 7 C N3 N 15 196.3 0 . 1 . . . A 7 C N3 . 25534 1 65 . 1 1 7 7 C N4 N 15 100.1 0 . 1 . . . A 7 C N4 . 25534 1 66 . 1 1 8 8 U C1' C 13 93.7 0 . 1 . . . A 8 U C1' . 25534 1 67 . 1 1 8 8 U C2 C 13 152.8 0 . 1 . . . A 8 U C2 . 25534 1 68 . 1 1 8 8 U C2' C 13 75.5 0 . 1 . . . A 8 U C2' . 25534 1 69 . 1 1 8 8 U C3' C 13 72.1 0 . 1 . . . A 8 U C3' . 25534 1 70 . 1 1 8 8 U C4 C 13 169.4 0 . 1 . . . A 8 U C4 . 25534 1 71 . 1 1 8 8 U C4' C 13 82.1 0 . 1 . . . A 8 U C4' . 25534 1 72 . 1 1 8 8 U C5 C 13 103.2 0 . 1 . . . A 8 U C5 . 25534 1 73 . 1 1 8 8 U C5' C 13 64.3 0 . 1 . . . A 8 U C5' . 25534 1 74 . 1 1 8 8 U C6 C 13 142.3 0 . 1 . . . A 8 U C6 . 25534 1 75 . 1 1 8 8 U N1 N 15 145.5 0 . 1 . . . A 8 U N1 . 25534 1 76 . 1 1 8 8 U N3 N 15 163.6 0 . 1 . . . A 8 U N3 . 25534 1 77 . 1 1 9 9 C C1' C 13 93.2 0 . 1 . . . A 9 C C1' . 25534 1 78 . 1 1 9 9 C C2 C 13 158.2 0 . 1 . . . A 9 C C2 . 25534 1 79 . 1 1 9 9 C C2' C 13 75.9 0 . 1 . . . A 9 C C2' . 25534 1 80 . 1 1 9 9 C C3' C 13 71.4 0 . 1 . . . A 9 C C3' . 25534 1 81 . 1 1 9 9 C C4 C 13 168.1 0 . 1 . . . A 9 C C4 . 25534 1 82 . 1 1 9 9 C C4' C 13 81.2 0 . 1 . . . A 9 C C4' . 25534 1 83 . 1 1 9 9 C C5 C 13 98.2 0 . 1 . . . A 9 C C5 . 25534 1 84 . 1 1 9 9 C C5' C 13 64.2 0 . 1 . . . A 9 C C5' . 25534 1 85 . 1 1 9 9 C C6 C 13 140.2 0 . 1 . . . A 9 C C6 . 25534 1 86 . 1 1 9 9 C N1 N 15 151.7 0 . 1 . . . A 9 C N1 . 25534 1 87 . 1 1 9 9 C N3 N 15 197.7 0 . 1 . . . A 9 C N3 . 25534 1 88 . 1 1 9 9 C N4 N 15 99.1 0 . 1 . . . A 9 C N4 . 25534 1 89 . 1 1 10 10 G C1' C 13 94.0 0 . 1 . . . A 10 G C1' . 25534 1 90 . 1 1 10 10 G C2' C 13 75.7 0 . 1 . . . A 10 G C2' . 25534 1 91 . 1 1 10 10 G C3' C 13 71.5 0 . 1 . . . A 10 G C3' . 25534 1 92 . 1 1 10 10 G C4 C 13 155.5 0 . 1 . . . A 10 G C4 . 25534 1 93 . 1 1 10 10 G C4' C 13 81.8 0 . 1 . . . A 10 G C4' . 25534 1 94 . 1 1 10 10 G C5' C 13 64.4 0 . 1 . . . A 10 G C5' . 25534 1 95 . 1 1 10 10 G C6 C 13 161.7 0 . 1 . . . A 10 G C6 . 25534 1 96 . 1 1 10 10 G C8 C 13 136.3 0 . 1 . . . A 10 G C8 . 25534 1 97 . 1 1 10 10 G N1 N 15 146.2 0 . 1 . . . A 10 G N1 . 25534 1 98 . 1 1 10 10 G N2 N 15 75.5 0 . 1 . . . A 10 G N2 . 25534 1 99 . 1 1 10 10 G N9 N 15 171.3 0 . 1 . . . A 10 G N9 . 25534 1 100 . 1 1 14 14 G C1' C 13 92.6 0 . 1 . . . A 14 G C1' . 25534 1 101 . 1 1 14 14 G C2 C 13 157.5 0 . 1 . . . A 14 G C2 . 25534 1 102 . 1 1 14 14 G C2' C 13 74.6 0 . 1 . . . A 14 G C2' . 25534 1 103 . 1 1 14 14 G C4 C 13 151.9 0 . 1 . . . A 14 G C4 . 25534 1 104 . 1 1 14 14 G C5 C 13 119.2 0 . 1 . . . A 14 G C5 . 25534 1 105 . 1 1 14 14 G C5' C 13 69.5 0 . 1 . . . A 14 G C5' . 25534 1 106 . 1 1 14 14 G C8 C 13 137.4 0 . 1 . . . A 14 G C8 . 25534 1 107 . 1 1 14 14 G N1 N 15 148.2 0 . 1 . . . A 14 G N1 . 25534 1 108 . 1 1 14 14 G N2 N 15 75.4 0 . 1 . . . A 14 G N2 . 25534 1 109 . 1 1 14 14 G N9 N 15 170.1 0 . 1 . . . A 14 G N9 . 25534 1 110 . 1 1 15 15 A C1' C 13 92.9 0 . 1 . . . A 15 A C1' . 25534 1 111 . 1 1 15 15 A C2 C 13 153.0 0 . 1 . . . A 15 A C2 . 25534 1 112 . 1 1 15 15 A C2' C 13 75.5 0 . 1 . . . A 15 A C2' . 25534 1 113 . 1 1 15 15 A C3' C 13 72.3 0 . 1 . . . A 15 A C3' . 25534 1 114 . 1 1 15 15 A C4 C 13 148.6 0 . 1 . . . A 15 A C4 . 25534 1 115 . 1 1 15 15 A C4' C 13 81.8 0 . 1 . . . A 15 A C4' . 25534 1 116 . 1 1 15 15 A C5 C 13 120.6 0 . 1 . . . A 15 A C5 . 25534 1 117 . 1 1 15 15 A C5' C 13 65.2 0 . 1 . . . A 15 A C5' . 25534 1 118 . 1 1 15 15 A C6 C 13 157.6 0 . 1 . . . A 15 A C6 . 25534 1 119 . 1 1 15 15 A C8 C 13 139.5 0 . 1 . . . A 15 A C8 . 25534 1 120 . 1 1 15 15 A N1 N 15 222.1 0 . 1 . . . A 15 A N1 . 25534 1 121 . 1 1 15 15 A N9 N 15 171.5 0 . 1 . . . A 15 A N9 . 25534 1 122 . 1 1 16 16 G C1' C 13 92.5 0 . 1 . . . A 16 G C1' . 25534 1 123 . 1 1 16 16 G C2 C 13 157.0 0 . 1 . . . A 16 G C2 . 25534 1 124 . 1 1 16 16 G C2' C 13 75.8 0 . 1 . . . A 16 G C2' . 25534 1 125 . 1 1 16 16 G C3' C 13 72.0 0 . 1 . . . A 16 G C3' . 25534 1 126 . 1 1 16 16 G C4 C 13 151.6 0 . 1 . . . A 16 G C4 . 25534 1 127 . 1 1 16 16 G C4' C 13 81.7 0 . 1 . . . A 16 G C4' . 25534 1 128 . 1 1 16 16 G C5 C 13 119.0 0 . 1 . . . A 16 G C5 . 25534 1 129 . 1 1 16 16 G C5' C 13 64.3 0 . 1 . . . A 16 G C5' . 25534 1 130 . 1 1 16 16 G C6 C 13 160.9 0 . 1 . . . A 16 G C6 . 25534 1 131 . 1 1 16 16 G C8 C 13 135.6 0 . 1 . . . A 16 G C8 . 25534 1 132 . 1 1 16 16 G N1 N 15 148.0 0 . 1 . . . A 16 G N1 . 25534 1 133 . 1 1 16 16 G N2 N 15 74.6 0 . 1 . . . A 16 G N2 . 25534 1 134 . 1 1 16 16 G N9 N 15 170.9 0 . 1 . . . A 16 G N9 . 25534 1 135 . 1 1 17 17 C C1' C 13 93.6 0 . 1 . . . A 17 C C1' . 25534 1 136 . 1 1 17 17 C C2 C 13 158.5 0 . 1 . . . A 17 C C2 . 25534 1 137 . 1 1 17 17 C C2' C 13 75.7 0 . 1 . . . A 17 C C2' . 25534 1 138 . 1 1 17 17 C C3' C 13 71.7 0 . 1 . . . A 17 C C3' . 25534 1 139 . 1 1 17 17 C C4 C 13 167.6 0 . 1 . . . A 17 C C4 . 25534 1 140 . 1 1 17 17 C C4' C 13 81.6 0 . 1 . . . A 17 C C4' . 25534 1 141 . 1 1 17 17 C C5 C 13 97.9 0 . 1 . . . A 17 C C5 . 25534 1 142 . 1 1 17 17 C C5' C 13 64.1 0 . 1 . . . A 17 C C5' . 25534 1 143 . 1 1 17 17 C C6 C 13 139.0 0 . 1 . . . A 17 C C6 . 25534 1 144 . 1 1 17 17 C N1 N 15 150.5 0 . 1 . . . A 17 C N1 . 25534 1 145 . 1 1 17 17 C N3 N 15 195.9 0 . 1 . . . A 17 C N3 . 25534 1 146 . 1 1 17 17 C N4 N 15 99.0 0 . 1 . . . A 17 C N4 . 25534 1 147 . 1 1 18 18 A C1' C 13 94.1 0 . 1 . . . A 18 A C1' . 25534 1 148 . 1 1 18 18 A C2 C 13 156.0 0 . 1 . . . A 18 A C2 . 25534 1 149 . 1 1 18 18 A C2' C 13 76.6 0 . 1 . . . A 18 A C2' . 25534 1 150 . 1 1 18 18 A C3' C 13 72.5 0 . 1 . . . A 18 A C3' . 25534 1 151 . 1 1 18 18 A C4 C 13 150.6 0 . 1 . . . A 18 A C4 . 25534 1 152 . 1 1 18 18 A C4' C 13 81.6 0 . 1 . . . A 18 A C4' . 25534 1 153 . 1 1 18 18 A C5 C 13 121.6 0 . 1 . . . A 18 A C5 . 25534 1 154 . 1 1 18 18 A C5' C 13 64.6 0 . 1 . . . A 18 A C5' . 25534 1 155 . 1 1 18 18 A C6 C 13 157.7 0 . 1 . . . A 18 A C6 . 25534 1 156 . 1 1 18 18 A C8 C 13 138.6 0 . 1 . . . A 18 A C8 . 25534 1 157 . 1 1 18 18 A N6 N 15 80.7 0 . 1 . . . A 18 A N6 . 25534 1 158 . 1 1 18 18 A N7 N 15 230.9 0 . 1 . . . A 18 A N7 . 25534 1 159 . 1 1 18 18 A N9 N 15 173.2 0 . 1 . . . A 18 A N9 . 25534 1 160 . 1 1 18 18 A P P 31 -4.2 0 . 1 . . . A 18 A P . 25534 1 161 . 1 1 19 19 A C1' C 13 89.7 0 . 1 . . . A 19 A C1' . 25534 1 162 . 1 1 19 19 A C2 C 13 154.5 0 . 1 . . . A 19 A C2 . 25534 1 163 . 1 1 19 19 A C2' C 13 72.2 0 . 1 . . . A 19 A C2' . 25534 1 164 . 1 1 19 19 A C3' C 13 78.5 0 . 1 . . . A 19 A C3' . 25534 1 165 . 1 1 19 19 A C4 C 13 150.5 0 . 1 . . . A 19 A C4 . 25534 1 166 . 1 1 19 19 A C4' C 13 85.1 0 . 1 . . . A 19 A C4' . 25534 1 167 . 1 1 19 19 A C5 C 13 121.8 0 . 1 . . . A 19 A C5 . 25534 1 168 . 1 1 19 19 A C5' C 13 67.4 0 . 1 . . . A 19 A C5' . 25534 1 169 . 1 1 19 19 A C6 C 13 156.4 0 . 1 . . . A 19 A C6 . 25534 1 170 . 1 1 19 19 A C8 C 13 145.8 0 . 1 . . . A 19 A C8 . 25534 1 171 . 1 1 19 19 A N6 N 15 76.3 0 . 1 . . . A 19 A N6 . 25534 1 172 . 1 1 19 19 A N7 N 15 228.2 0 . 1 . . . A 19 A N7 . 25534 1 173 . 1 1 19 19 A N9 N 15 164.7 0 . 1 . . . A 19 A N9 . 25534 1 174 . 1 1 19 19 A P P 31 -1.8 0 . 1 . . . A 19 A P . 25534 1 175 . 1 1 20 20 U C1' C 13 89.4 0 . 1 . . . A 20 U C1' . 25534 1 176 . 1 1 20 20 U C2 C 13 154.2 0 . 1 . . . A 20 U C2 . 25534 1 177 . 1 1 20 20 U C2' C 13 75.4 0 . 1 . . . A 20 U C2' . 25534 1 178 . 1 1 20 20 U C3' C 13 80.5 0 . 1 . . . A 20 U C3' . 25534 1 179 . 1 1 20 20 U C4 C 13 167.9 0 . 1 . . . A 20 U C4 . 25534 1 180 . 1 1 20 20 U C4' C 13 84.2 0 . 1 . . . A 20 U C4' . 25534 1 181 . 1 1 20 20 U C5 C 13 105.7 0 . 1 . . . A 20 U C5 . 25534 1 182 . 1 1 20 20 U C5' C 13 69.5 0 . 1 . . . A 20 U C5' . 25534 1 183 . 1 1 20 20 U C6 C 13 146.8 0 . 1 . . . A 20 U C6 . 25534 1 184 . 1 1 20 20 U N1 N 15 147.4 0 . 1 . . . A 20 U N1 . 25534 1 185 . 1 1 20 20 U N3 N 15 158.5 0 . 1 . . . A 20 U N3 . 25534 1 186 . 1 1 20 20 U P P 31 -5.3 0 . 1 . . . A 20 U P . 25534 1 187 . 1 1 21 21 G C1' C 13 87.5 0 . 1 . . . A 21 G C1' . 25534 1 188 . 1 1 21 21 G C2' C 13 77.5 0 . 1 . . . A 21 G C2' . 25534 1 189 . 1 1 21 21 G C3' C 13 80.0 0 . 1 . . . A 21 G C3' . 25534 1 190 . 1 1 21 21 G C4 C 13 155.7 0 . 1 . . . A 21 G C4 . 25534 1 191 . 1 1 21 21 G C4' C 13 87.5 0 . 1 . . . A 21 G C4' . 25534 1 192 . 1 1 21 21 G C5 C 13 117.6 0 . 1 . . . A 21 G C5 . 25534 1 193 . 1 1 21 21 G C5' C 13 68.3 0 . 1 . . . A 21 G C5' . 25534 1 194 . 1 1 21 21 G C6 C 13 160.3 0 . 1 . . . A 21 G C6 . 25534 1 195 . 1 1 21 21 G C8 C 13 139.1 0 . 1 . . . A 21 G C8 . 25534 1 196 . 1 1 21 21 G N1 N 15 145.6 0 . 1 . . . A 21 G N1 . 25534 1 197 . 1 1 21 21 G N2 N 15 81.0 0 . 1 . . . A 21 G N2 . 25534 1 198 . 1 1 21 21 G N9 N 15 168.8 0 . 1 . . . A 21 G N9 . 25534 1 199 . 1 1 21 21 G P P 31 -6.0 0 . 1 . . . A 21 G P . 25534 1 200 . 1 1 22 22 A C1' C 13 92.4 0 . 1 . . . A 22 A C1' . 25534 1 201 . 1 1 22 22 A C2 C 13 156.0 0 . 1 . . . A 22 A C2 . 25534 1 202 . 1 1 22 22 A C2' C 13 75.7 0 . 1 . . . A 22 A C2' . 25534 1 203 . 1 1 22 22 A C3' C 13 72.4 0 . 1 . . . A 22 A C3' . 25534 1 204 . 1 1 22 22 A C4 C 13 147.5 0 . 1 . . . A 22 A C4 . 25534 1 205 . 1 1 22 22 A C4' C 13 82.9 0 . 1 . . . A 22 A C4' . 25534 1 206 . 1 1 22 22 A C5 C 13 120.8 0 . 1 . . . A 22 A C5 . 25534 1 207 . 1 1 22 22 A C5' C 13 65.8 0 . 1 . . . A 22 A C5' . 25534 1 208 . 1 1 22 22 A C6 C 13 157.1 0 . 1 . . . A 22 A C6 . 25534 1 209 . 1 1 22 22 A C8 C 13 140.0 0 . 1 . . . A 22 A C8 . 25534 1 210 . 1 1 22 22 A N6 N 15 81.2 0 . 1 . . . A 22 A N6 . 25534 1 211 . 1 1 22 22 A N9 N 15 170.2 0 . 1 . . . A 22 A N9 . 25534 1 212 . 1 1 22 22 A P P 31 -0.1 0 . 1 . . . A 22 A P . 25534 1 213 . 1 1 23 23 U C1' C 13 93.0 0 . 1 . . . A 23 U C1' . 25534 1 214 . 1 1 23 23 U C2 C 13 151.0 0 . 1 . . . A 23 U C2 . 25534 1 215 . 1 1 23 23 U C2' C 13 74.6 0 . 1 . . . A 23 U C2' . 25534 1 216 . 1 1 23 23 U C3' C 13 72.1 0 . 1 . . . A 23 U C3' . 25534 1 217 . 1 1 23 23 U C4 C 13 167.6 0 . 1 . . . A 23 U C4 . 25534 1 218 . 1 1 23 23 U C4' C 13 82.3 0 . 1 . . . A 23 U C4' . 25534 1 219 . 1 1 23 23 U C5 C 13 103.8 0 . 1 . . . A 23 U C5 . 25534 1 220 . 1 1 23 23 U C5' C 13 63.1 0 . 1 . . . A 23 U C5' . 25534 1 221 . 1 1 23 23 U C6 C 13 140.0 0 . 1 . . . A 23 U C6 . 25534 1 222 . 1 1 23 23 U N1 N 15 144.7 0 . 1 . . . A 23 U N1 . 25534 1 223 . 1 1 23 23 U N3 N 15 155.7 0 . 1 . . . A 23 U N3 . 25534 1 224 . 1 1 23 23 U P P 31 -4.2 0 . 1 . . . A 23 U P . 25534 1 225 . 1 1 24 24 G C1' C 13 92.6 0 . 1 . . . A 24 G C1' . 25534 1 226 . 1 1 24 24 G C2 C 13 157.4 0 . 1 . . . A 24 G C2 . 25534 1 227 . 1 1 24 24 G C4 C 13 152.9 0 . 1 . . . A 24 G C4 . 25534 1 228 . 1 1 24 24 G C5 C 13 118.1 0 . 1 . . . A 24 G C5 . 25534 1 229 . 1 1 24 24 G C8 C 13 136.2 0 . 1 . . . A 24 G C8 . 25534 1 230 . 1 1 24 24 G N2 N 15 76.5 0 . 1 . . . A 24 G N2 . 25534 1 231 . 1 1 24 24 G N9 N 15 172.4 0 . 1 . . . A 24 G N9 . 25534 1 stop_ save_