data_5841 ####################### # Entry information # ####################### save_entry_information _Saveframe_category entry_information _Entry_title ; 15N T1 and T2 relaxation rates, 1H{15N} NOE, and Hydrogen/Deuterium exchange data of kinase-interacting FHA domain of Arabidopsis kinase associasted protein phosphatase ; _BMRB_accession_number 5841 _BMRB_flat_file_name bmr5841.str _Entry_type original _Submission_date 2003-06-24 _Accession_date 2003-06-25 _Entry_origination author _NMR_STAR_version 2.1.1 _Experimental_method NMR _Details . loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Ding Zhaofeng . . 2 Lee Gui-in . . 3 Liang Xiangyang . . 4 Gallazzi Fabio . . 5 'Van Doren' Steven R. . stop_ loop_ _Saveframe_category_type _Saveframe_category_type_count S2_parameters 1 H_exch_rates 1 H_exchange_protection_factors 1 T1_relaxation 2 T2_relaxation 2 heteronucl_NOE 2 stop_ loop_ _Data_type _Data_type_count "T1 relaxation values" 215 "T2 relaxation values" 208 "order parameters" 104 "H exchange rates" 43 "H exchange protection factors" 44 stop_ loop_ _Revision_date _Revision_keyword _Revision_author _Revision_detail 2005-06-09 update author 'update the data tables' 2005-01-24 update author 'update the data tables' 2003-10-03 original author 'original release' stop_ loop_ _Related_BMRB_accession_number _Relationship 5564 'Chemical shift data of the protein' 6474 'relaxation data of CLV1 pT868 bound KI-FHA from KAPP' stop_ save_ ############################# # Citation for this entry # ############################# save_entry_citation _Saveframe_category entry_citation _Citation_full . _Citation_title ; 1H, (13)C and (15)N Resonance Assignments of the Kinase-interacting FHA Domain of Arabidopsis thaliana Kinase-associated Protein Phophatase ; _Citation_status published _Citation_type journal _CAS_abstract_code . _MEDLINE_UI_code 22538551 _PubMed_ID 12652139 loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Lee Gui-in . . 2 Li Jia . . 3 Walker John C. . 4 'Van Doren' Steven R. . stop_ _Journal_abbreviation 'J. Biomol. NMR' _Journal_volume 25 _Journal_issue 3 _Journal_CSD . _Book_chapter_title . _Book_volume . _Book_series . _Book_ISBN . _Conference_state_province . _Conference_abstract_number . _Page_first 253 _Page_last 254 _Year 2003 _Details . loop_ _Keyword 'phosphoprotein binding module' '15N relaxation' 'hydrogen exchange' stop_ save_ ################################## # Molecular system description # ################################## save_system_KAPP _Saveframe_category molecular_system _Mol_system_name 'kinase associated protein phosphatase, kinase interaction domain' _Abbreviation_common KAPP _Enzyme_commission_number 3.1.3.16 loop_ _Mol_system_component_name _Mol_label 'Kinase-interacting FHA domain of KAPP' $KAPP stop_ _System_molecular_weight . _System_physical_state native _System_oligomer_state monomer _System_paramagnetic no _System_thiol_state 'not present' loop_ _Biological_function 'phosphoprotein binding domain of KAPP' stop_ _Database_query_date . _Details . save_ ######################## # Monomeric polymers # ######################## save_KAPP _Saveframe_category monomeric_polymer _Mol_type polymer _Mol_polymer_class protein _Name_common 'kinase associated protein phosphatase' _Abbreviation_common KAPP _Molecular_mass . _Mol_thiol_state 'not present' _Details ; This molecule has five residue linker G-P-L-G-S, originated from Glutathione-S-transferase tag at N terminus. ; ############################## # Polymer residue sequence # ############################## _Residue_count 139 _Mol_residue_sequence ; GPLGSSWLFLEVIAGPAIGL QHAVNSTSSSKLPVKLGRVS PSDLALKDSEVSGKHAQITW NSTKFKWELVDMGSLNGTLV NSHSISHPDLGSRKWGNPVE LASDDIITLGTTTKVYVRIS SQNEFQIPFKIGVASDPMA ; loop_ _Residue_seq_code _Residue_author_seq_code _Residue_label 1 1 GLY 2 2 PRO 3 3 LEU 4 4 GLY 5 5 SER 6 180 SER 7 181 TRP 8 182 LEU 9 183 PHE 10 184 LEU 11 185 GLU 12 186 VAL 13 187 ILE 14 188 ALA 15 189 GLY 16 190 PRO 17 191 ALA 18 192 ILE 19 193 GLY 20 194 LEU 21 195 GLN 22 196 HIS 23 197 ALA 24 198 VAL 25 199 ASN 26 200 SER 27 201 THR 28 202 SER 29 203 SER 30 204 SER 31 205 LYS 32 206 LEU 33 207 PRO 34 208 VAL 35 209 LYS 36 210 LEU 37 211 GLY 38 212 ARG 39 213 VAL 40 214 SER 41 215 PRO 42 216 SER 43 217 ASP 44 218 LEU 45 219 ALA 46 220 LEU 47 221 LYS 48 222 ASP 49 223 SER 50 224 GLU 51 225 VAL 52 226 SER 53 227 GLY 54 228 LYS 55 229 HIS 56 230 ALA 57 231 GLN 58 232 ILE 59 233 THR 60 234 TRP 61 235 ASN 62 236 SER 63 237 THR 64 238 LYS 65 239 PHE 66 240 LYS 67 241 TRP 68 242 GLU 69 243 LEU 70 244 VAL 71 245 ASP 72 246 MET 73 247 GLY 74 248 SER 75 249 LEU 76 250 ASN 77 251 GLY 78 252 THR 79 253 LEU 80 254 VAL 81 255 ASN 82 256 SER 83 257 HIS 84 258 SER 85 259 ILE 86 260 SER 87 261 HIS 88 262 PRO 89 263 ASP 90 264 LEU 91 265 GLY 92 266 SER 93 267 ARG 94 268 LYS 95 269 TRP 96 270 GLY 97 271 ASN 98 272 PRO 99 273 VAL 100 274 GLU 101 275 LEU 102 276 ALA 103 277 SER 104 278 ASP 105 279 ASP 106 280 ILE 107 281 ILE 108 282 THR 109 283 LEU 110 284 GLY 111 285 THR 112 286 THR 113 287 THR 114 288 LYS 115 289 VAL 116 290 TYR 117 291 VAL 118 292 ARG 119 293 ILE 120 294 SER 121 295 SER 122 296 GLN 123 297 ASN 124 298 GLU 125 299 PHE 126 300 GLN 127 301 ILE 128 302 PRO 129 303 PHE 130 304 LYS 131 305 ILE 132 306 GLY 133 307 VAL 134 308 ALA 135 309 SER 136 310 ASP 137 311 PRO 138 312 MET 139 313 ALA stop_ _Sequence_homology_query_date 2008-08-19 _Sequence_homology_query_revised_last_date 2008-08-19 loop_ _Database_name _Database_accession_code _Database_entry_mol_name _Sequence_query_to_submitted_percentage _Sequence_subject_length _Sequence_identity _Sequence_positive _Sequence_homology_expectation_value REF NP_197429 'KAPP (Kinase-associated protein phosphatase); protein serine/threonine phosphatase [Arabidopsis thaliana]' 96.40 581 100.00 100.00 1.10e-72 SWISS-PROT P46014 'Kinase-associated protein phosphatase' 96.40 581 100.00 100.00 1.10e-72 GenBank AAK76527 'putative kinase associated protein phosphatase [Arabidopsis thaliana]' 96.40 581 100.00 100.00 1.10e-72 GenBank AAM51227 'putative kinase associated protein phosphatase [Arabidopsis thaliana]' 96.40 581 100.00 100.00 1.10e-72 PDB 1MZK 'Nmr Structure Of Kinase-Interacting Fha Domain Of Kinase Associated Protein Phosphatase, Kapp In Arabidopsis' 100.00 139 100.00 100.00 4.02e-74 GenBank AAB38148 'kinase associated protein phosphatase' 96.40 581 100.00 100.00 1.10e-72 BMRB 5564 'kinase associated protein phosphatase' 100.00 139 100.00 100.00 4.02e-74 BMRB 6474 'Kinase Interacting FHA (KI-FHA) domain from KAPP' 100.00 139 100.00 100.00 4.02e-74 stop_ save_ #################### # Natural source # #################### save_natural_source _Saveframe_category natural_source loop_ _Mol_label _Organism_name_common _NCBI_taxonomy_ID _Superkingdom _Kingdom _Genus _Species _Plasmid $KAPP 'Thale cress' 3702 Eukaryota Viridiplantae Arabidopsis thaliana 'pGEX 6P-1' stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Saveframe_category experimental_source loop_ _Mol_label _Production_method _Host_organism_name_common _Genus _Species _Strain _Vector_type _Vector_name $KAPP 'recombinant technology' 'E. coli' Escherichia coli DH5a plasmid pGEX6P-1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_one _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $KAPP 0.6 mM '[U-99% 15N]' NaCl 120 mM . stop_ save_ ############################ # Computer software used # ############################ save_Sybyl_TRIAD _Saveframe_category software _Name 'Sybyl TRIAD' _Version 6.3 loop_ _Task 'data processing' stop_ _Details . save_ save_Kaleidograph_for_windows _Saveframe_category software _Name 'Kaleidograph for windows' _Version 3.08 loop_ _Task 'R1, R2, Hydrogen exchange data fitting' stop_ _Details . save_ save_Modelfree _Saveframe_category software _Name Modelfree _Version 4.1 loop_ _Task "for optimizing 'Lipari-Szabo model free' parameters to heteronuclear relaxation data" stop_ _Details 'Copyright 1998, Arthur G. Palmer, III' save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _Saveframe_category NMR_spectrometer _Manufacturer Bruker _Model DRX _Field_strength 500 _Details . save_ save_NMR_spectrometer_2 _Saveframe_category NMR_spectrometer _Manufacturer Varian _Model INOVA _Field_strength 600 _Details . save_ ############################# # NMR applied experiments # ############################# save_15N_T1_relaxation_1 _Saveframe_category NMR_applied_experiment _Experiment_name '15N T1 relaxation' _Sample_label $sample_one save_ save_15N_T2_relaxation_2 _Saveframe_category NMR_applied_experiment _Experiment_name '15N T2 relaxation' _Sample_label $sample_one save_ save_heteronuclear_1H-15N_NOE_3 _Saveframe_category NMR_applied_experiment _Experiment_name 'heteronuclear 1H-15N NOE' _Sample_label $sample_one save_ save_1H-15N_HSQC_4 _Saveframe_category NMR_applied_experiment _Experiment_name '1H-15N HSQC' _Sample_label $sample_one save_ save_NMR_spec_expt__0_1 _Saveframe_category NMR_applied_experiment _Experiment_name '15N T1 relaxation' _BMRB_pulse_sequence_accession_number . _Details . save_ save_NMR_spec_expt__0_2 _Saveframe_category NMR_applied_experiment _Experiment_name '15N T2 relaxation' _BMRB_pulse_sequence_accession_number . _Details . save_ save_NMR_spec_expt__0_3 _Saveframe_category NMR_applied_experiment _Experiment_name 'heteronuclear 1H-15N NOE' _BMRB_pulse_sequence_accession_number . _Details . save_ save_NMR_spec_expt__0_4 _Saveframe_category NMR_applied_experiment _Experiment_name '1H-15N HSQC' _BMRB_pulse_sequence_accession_number . _Details . save_ ####################### # Sample conditions # ####################### save_condition_one _Saveframe_category sample_conditions _Details . loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units pH 6.3 0.2 pH temperature 298 1 K 'ionic strength' 0.12 . M stop_ save_ save_condition_two _Saveframe_category sample_conditions _Details 'The sample was lyophilized and redissolved in the same volume of D2O.' loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units pH 6.3 0.2 pH temperature 293 1 K 'ionic strength' 0.12 . M stop_ save_ save_15N_T1_set_1 _Saveframe_category T1_relaxation _Details . loop_ _Sample_label $sample_one stop_ _Sample_conditions_label $condition_one _Spectrometer_frequency_1H 500 _T1_coherence_type Nz _T1_value_units s _Mol_system_component_name 'Kinase-interacting FHA domain of KAPP' _Text_data_format . _Text_data . loop_ _T1_ID _Residue_seq_code _Residue_label _Atom_name _T1_value _T1_value_error 1 3 LEU N 0.510 0.041 2 4 GLY N 0.472 0.027 3 5 SER N 0.441 0.025 4 6 SER N 0.442 0.038 5 7 TRP N 0.468 0.029 6 8 LEU N 0.496 0.017 7 9 PHE N 0.487 0.018 8 10 LEU N 0.523 0.026 9 11 GLU N 0.521 0.015 10 12 VAL N 0.526 0.025 11 14 ALA N 0.491 0.015 12 15 GLY N 0.491 0.028 13 17 ALA N 0.437 0.035 14 18 ILE N 0.565 0.018 15 19 GLY N 0.504 0.021 16 20 LEU N 0.545 0.020 17 21 GLN N 0.530 0.018 18 22 HIS N 0.538 0.018 19 23 ALA N 0.519 0.017 20 24 VAL N 0.439 0.023 21 25 ASN N 0.506 0.020 22 26 SER N 0.439 0.030 23 27 THR N 0.398 0.029 24 28 SER N 0.444 0.024 25 29 SER N 0.407 0.038 26 31 LYS N 0.496 0.021 27 32 LEU N 0.540 0.027 28 34 VAL N 0.516 0.011 29 35 LYS N 0.522 0.019 30 36 LEU N 0.519 0.018 31 37 GLY N 0.478 0.022 32 38 ARG N 0.490 0.025 33 39 VAL N 0.445 0.023 34 42 SER N 0.397 0.026 35 43 ASP N 0.501 0.017 36 44 LEU N 0.507 0.022 37 45 ALA N 0.554 0.018 38 46 LEU N 0.498 0.018 39 47 LYS N 0.488 0.019 40 48 ASP N 0.664 0.044 41 49 SER N 0.406 0.029 42 50 GLU N 0.381 0.034 43 51 VAL N 0.452 0.022 44 53 GLY N 0.659 0.247 45 54 LYS N 0.446 0.035 46 55 HIS N 0.524 0.026 47 56 ALA N 0.490 0.017 48 57 GLN N 0.508 0.014 49 58 ILE N 0.526 0.011 50 59 THR N 0.503 0.014 51 60 TRP N 0.503 0.016 52 61 ASN N 0.487 0.018 53 62 SER N 0.430 0.033 54 63 THR N 0.508 0.030 55 64 LYS N 0.518 0.017 56 65 PHE N 0.499 0.018 57 66 LYS N 0.527 0.023 58 67 TRP N 0.508 0.017 59 68 GLU N 0.506 0.018 60 69 LEU N 0.508 0.018 61 70 VAL N 0.494 0.015 62 71 ASP N 0.438 0.026 63 72 MET N 0.546 0.019 64 73 GLY N 0.478 0.019 65 74 SER N 0.431 0.033 66 75 LEU N 0.379 0.030 67 76 ASN N 0.393 0.030 68 77 GLY N 0.396 0.031 69 78 THR N 0.436 0.022 70 79 LEU N 0.460 0.021 71 80 VAL N 0.480 0.025 72 81 ASN N 0.416 0.030 73 82 SER N 0.504 0.055 74 83 HIS N 0.452 0.028 75 84 SER N 0.533 0.069 76 85 ILE N 0.441 0.019 77 86 SER N 0.429 0.028 78 87 HIS N 0.404 0.034 79 89 ASP N 0.500 0.030 80 90 LEU N 0.515 0.023 81 91 GLY N 0.490 0.027 82 92 SER N 0.414 0.034 83 93 ARG N 0.404 0.023 84 94 LYS N 0.466 0.025 85 95 TRP N 0.490 0.022 86 96 GLY N 0.441 0.021 87 97 ASN N 0.481 0.027 88 99 VAL N 0.519 0.016 89 100 GLU N 0.546 0.015 90 101 LEU N 0.515 0.016 91 102 ALA N 0.559 0.012 92 103 SER N 0.567 0.017 93 104 ASP N 0.446 0.030 94 105 ASP N 0.514 0.018 95 106 ILE N 0.516 0.021 96 107 ILE N 0.527 0.020 97 108 THR N 0.487 0.020 98 109 LEU N 0.465 0.030 99 110 GLY N 0.442 0.026 100 111 THR N 0.397 0.037 101 112 THR N 0.370 0.041 102 113 THR N 0.400 0.050 103 114 LYS N 0.472 0.029 104 115 VAL N 0.509 0.017 105 116 TYR N 0.491 0.028 106 117 VAL N 0.519 0.034 107 118 ARG N 0.467 0.018 108 119 ILE N 0.501 0.021 109 120 SER N 0.477 0.019 110 121 SER N 0.644 0.096 111 122 GLN N 0.392 0.027 112 123 ASN N 0.573 0.038 113 124 GLU N 0.641 0.016 stop_ save_ save_15N_T1_set_2 _Saveframe_category T1_relaxation _Details . loop_ _Sample_label $sample_one stop_ _Sample_conditions_label $condition_one _Spectrometer_frequency_1H 600 _T1_coherence_type Nz _T1_value_units s _Mol_system_component_name 'Kinase-interacting FHA domain of KAPP' _Text_data_format . _Text_data . loop_ _T1_ID _Residue_seq_code _Residue_label _Atom_name _T1_value _T1_value_error 1 3 LEU N 0.494 0.009 2 4 GLY N 0.436 0.007 3 5 SER N 0.445 0.011 4 6 SER N 0.461 0.010 5 7 TRP N 0.504 0.036 6 8 LEU N 0.531 0.032 7 9 PHE N 0.557 0.046 8 10 LEU N 0.575 0.028 9 11 GLU N 0.581 0.035 10 12 VAL N 0.621 0.023 11 14 ALA N 0.544 0.028 12 15 GLY N 0.533 0.024 13 17 ALA N 0.491 0.024 14 18 ILE N 0.573 0.035 15 19 GLY N 0.636 0.023 16 20 LEU N 0.625 0.070 17 21 GLN N 0.644 0.056 18 22 HIS N 0.598 0.039 19 23 ALA N 0.541 0.015 20 25 ASN N 0.560 0.036 21 27 THR N 0.425 0.018 22 28 SER N 0.493 0.038 23 29 SER N 0.427 0.014 24 31 LYS N 0.545 0.016 25 32 LEU N 0.599 0.025 26 34 VAL N 0.561 0.036 27 35 LYS N 0.589 0.014 28 37 GLY N 0.516 0.031 29 38 ARG N 0.520 0.022 30 39 VAL N 0.479 0.018 31 42 SER N 0.393 0.020 32 44 LEU N 0.580 0.035 33 45 ALA N 0.641 0.032 34 46 LEU N 0.570 0.024 35 47 LYS N 0.553 0.035 36 48 ASP N 0.681 0.019 37 51 VAL N 0.466 0.025 38 53 GLY N 0.402 0.033 39 54 LYS N 0.454 0.018 40 55 HIS N 0.586 0.016 41 56 ALA N 0.583 0.046 42 57 GLN N 0.579 0.034 43 58 ILE N 0.615 0.033 44 59 THR N 0.570 0.030 45 60 TRP N 0.551 0.015 46 61 ASN N 0.426 0.012 47 62 SER N 0.521 0.023 48 63 THR N 0.603 0.025 49 64 LYS N 0.561 0.030 50 65 PHE N 0.597 0.029 51 66 LYS N 0.559 0.050 52 67 TRP N 0.579 0.048 53 68 GLU N 0.566 0.019 54 69 LEU N 0.553 0.032 55 70 VAL N 0.474 0.022 56 71 ASP N 0.417 0.015 57 75 LEU N 0.439 0.015 58 76 ASN N 0.442 0.012 59 77 GLY N 0.490 0.033 60 78 THR N 0.503 0.022 61 79 LEU N 0.529 0.020 62 80 VAL N 0.468 0.012 63 81 ASN N 0.350 0.017 64 82 SER N 0.468 0.020 65 83 HIS N 0.373 0.030 66 84 SER N 0.475 0.016 67 85 ILE N 0.447 0.009 68 86 SER N 0.441 0.021 69 87 HIS N 0.589 0.077 70 89 ASP N 0.500 0.047 71 90 LEU N 0.524 0.018 72 91 GLY N 0.436 0.025 73 92 SER N 0.440 0.023 74 93 ARG N 0.496 0.018 75 94 LYS N 0.528 0.039 76 95 TRP N 0.471 0.021 77 96 GLY N 0.521 0.014 78 97 ASN N 0.573 0.018 79 99 VAL N 0.578 0.022 80 100 GLU N 0.574 0.028 81 101 LEU N 0.623 0.022 82 102 ALA N 0.628 0.022 83 103 SER N 0.462 0.031 84 104 ASP N 0.527 0.014 85 105 ASP N 0.580 0.029 86 106 ILE N 0.572 0.029 87 107 ILE N 0.543 0.048 88 108 THR N 0.509 0.015 89 110 GLY N 0.430 0.015 90 111 THR N 0.418 0.012 91 112 THR N 0.429 0.015 92 113 THR N 0.543 0.030 93 114 LYS N 0.593 0.044 94 115 VAL N 0.563 0.032 95 116 TYR N 0.511 0.015 96 117 VAL N 0.548 0.038 97 118 ARG N 0.531 0.031 98 120 SER N 0.392 0.055 99 121 SER N 0.400 0.011 100 122 GLN N 0.379 0.023 101 123 ASN N 0.600 0.027 102 124 GLU N 0.604 0.027 stop_ save_ save_15N_T2_set_1 _Saveframe_category T2_relaxation _Details . loop_ _Sample_label $sample_one stop_ _Sample_conditions_label $condition_one _Spectrometer_frequency_1H 500 _T2_coherence_type Ny _T2_value_units s _Mol_system_component_name 'Kinase-interacting FHA domain of KAPP' _Text_data_format . _Text_data . loop_ _T2_ID _Residue_seq_code _Residue_label _Atom_name _T2_value _T2_value_error _Rex_value _Rex_error 1 3 LEU N 0.1992 0.0031 . . 2 4 GLY N 0.1808 0.0041 . . 3 5 SER N 0.1808 0.0041 . . 4 6 SER N 0.0855 0.0039 . . 5 7 TRP N 0.0893 0.0057 . . 6 8 LEU N 0.0901 0.0052 . . 7 9 PHE N 0.0901 0.0059 . . 8 10 LEU N 0.0813 0.0078 . . 9 11 GLU N 0.0862 0.0058 . . 10 12 VAL N 0.0806 0.0072 . . 11 14 ALA N 0.0699 0.0030 . . 12 15 GLY N 0.0877 0.0059 . . 13 17 ALA N 0.0781 0.0042 . . 14 18 ILE N 0.0862 0.0028 . . 15 19 GLY N 0.0847 0.0090 . . 16 20 LEU N 0.0935 0.0073 . . 17 21 GLN N 0.0885 0.0081 . . 18 22 HIS N 0.0877 0.0044 . . 19 23 ALA N 0.0855 0.0079 . . 20 25 ASN N 0.0926 0.0059 . . 21 26 SER N 0.0840 0.0033 . . 22 27 THR N 0.0741 0.0026 . . 23 28 SER N 0.0794 0.0019 . . 24 29 SER N 0.0855 0.0021 . . 25 31 LYS N 0.0787 0.0022 . . 26 32 LEU N 0.0990 0.0029 . . 27 34 VAL N 0.1000 0.0040 . . 28 35 LYS N 0.1000 0.0061 . . 29 36 LEU N 0.0870 0.0033 . . 30 37 GLY N 0.0735 0.0026 . . 31 38 ARG N 0.0813 0.0036 . . 32 39 VAL N 0.0781 0.0032 . . 33 42 SER N 0.0813 0.0028 . . 34 43 ASP N 0.0885 0.0026 . . 35 44 LEU N 0.0735 0.0027 . . 36 45 ALA N 0.0840 0.0032 . . 37 46 LEU N 0.0901 0.0043 . . 38 47 LYS N 0.0847 0.0051 . . 39 48 ASP N 0.1160 0.0059 . . 40 50 GLU N 0.0813 0.0025 . . 41 51 VAL N 0.0758 0.0023 . . 42 53 GLY N 0.0658 0.0058 . . 43 54 LYS N 0.0769 0.0030 . . 44 55 HIS N 0.0885 0.0031 . . 45 56 ALA N 0.0826 0.0024 . . 46 57 GLN N 0.0980 0.0040 . . 47 58 ILE N 0.0909 0.0037 . . 48 59 THR N 0.0885 0.0036 . . 49 60 TRP N 0.0893 0.0039 . . 50 61 ASN N 0.0893 0.0031 . . 51 62 SER N 0.0820 0.0027 . . 52 63 THR N 0.0800 0.0025 . . 53 64 LYS N 0.0826 0.0031 . . 54 65 PHE N 0.0877 0.0034 . . 55 66 LYS N 0.0943 0.0041 . . 56 67 TRP N 0.0917 0.0037 . . 57 68 GLU N 0.0901 0.0038 . . 58 69 LEU N 0.1007 0.0052 . . 59 70 VAL N 0.0847 0.0030 . . 60 71 ASP N 0.0763 0.0033 . . 61 75 LEU N 0.0746 0.0038 . . 62 76 ASN N 0.0826 0.0042 . . 63 77 GLY N 0.0870 0.0027 . . 64 78 THR N 0.0775 0.0026 . . 65 79 LEU N 0.0763 0.0030 . . 66 80 VAL N 0.0820 0.0029 . . 67 81 ASN N 0.0826 0.0034 . . 68 82 SER N 0.0373 0.0047 . . 69 83 HIS N 0.0746 0.0021 . . 70 84 SER N 0.0709 0.0066 . . 71 85 ILE N 0.0813 0.0038 . . 72 86 SER N 0.0840 0.0024 . . 73 87 HIS N 0.0775 0.0025 . . 74 89 ASP N 0.0833 0.0027 . . 75 90 LEU N 0.0926 0.0035 . . 76 91 GLY N 0.0962 0.0026 . . 77 92 SER N 0.0980 0.0020 . . 78 93 ARG N 0.0735 0.0020 . . 79 94 LYS N 0.0943 0.0023 . . 80 95 TRP N 0.0870 0.0029 . . 81 96 GLY N 0.0847 0.0037 . . 82 97 ASN N 0.0971 0.0027 . . 83 99 VAL N 0.0980 0.0037 . . 84 100 GLU N 0.0909 0.0023 . . 85 101 LEU N 0.0909 0.0044 . . 86 102 ALA N 0.0980 0.0052 . . 87 103 SER N 0.0885 0.0028 . . 88 104 ASP N 0.1027 0.0099 . . 89 105 ASP N 0.0787 0.0027 . . 90 106 ILE N 0.0926 0.0045 . . 91 107 ILE N 0.0877 0.0066 . . 92 108 THR N 0.0847 0.0037 . . 93 109 LEU N 0.0962 0.0042 . . 94 110 GLY N 0.0877 0.0037 . . 95 111 THR N 0.0806 0.0042 . . 96 112 THR N 0.0746 0.0040 . . 97 113 THR N 0.0781 0.0039 . . 98 114 LYS N 0.0943 0.0056 . . 99 115 VAL N 0.0893 0.0071 . . 100 116 TYR N 0.0943 0.0085 . . 101 117 VAL N 0.0971 0.0119 . . 102 118 ARG N 0.0885 0.0065 . . 103 120 SER N 0.0800 0.0053 . . 104 121 SER N 0.0917 0.0059 . . 105 122 GLN N 0.1106 0.0052 . . 106 123 ASN N 0.1202 0.0047 . . 107 124 GLU N 0.2762 0.0053 . . stop_ save_ save_15N_T2_set_2 _Saveframe_category T2_relaxation _Details . loop_ _Sample_label $sample_one stop_ _Sample_conditions_label $condition_one _Spectrometer_frequency_1H 600 _T2_coherence_type Ny _T2_value_units s _Mol_system_component_name 'Kinase-interacting FHA domain of KAPP' _Text_data_format . _Text_data . loop_ _T2_ID _Residue_seq_code _Residue_label _Atom_name _T2_value _T2_value_error _Rex_value _Rex_error 1 3 LEU N 0.1983 0.0025 . . 2 4 GLY N 0.1757 0.0027 . . 3 5 SER N 0.1160 0.0013 . . 4 6 SER N 0.0829 0.0018 . . 5 7 TRP N 0.0780 0.0023 . . 6 8 LEU N 0.0837 0.0021 . . 7 9 PHE N 0.0822 0.0028 . . 8 10 LEU N 0.0676 0.0042 . . 9 11 GLU N 0.0724 0.0018 . . 10 12 VAL N 0.0611 0.0031 . . 11 14 ALA N 0.0780 0.0014 . . 12 15 GLY N 0.0798 0.0017 . . 13 17 ALA N 0.0791 0.0024 . . 14 18 ILE N 0.0720 0.0010 . . 15 19 GLY N 0.0769 0.0032 . . 16 20 LEU N 0.0684 0.0033 . . 17 21 GLN N 0.0729 0.0020 . . 18 22 HIS N 0.0806 0.0024 . . 19 23 ALA N 0.0708 0.0021 . . 20 25 ASN N 0.0803 0.0022 . . 21 27 THR N 0.0766 0.0013 . . 22 28 SER N 0.0813 0.0011 . . 23 29 SER N 0.0794 0.000904 . . 24 31 LYS N 0.0776 0.0010 . . 25 32 LEU N 0.0856 0.0012 . . 26 34 VAL N 0.0796 0.0016 . . 27 35 LYS N 0.0848 0.0028 . . 28 37 GLY N 0.0800 0.0018 . . 29 38 ARG N 0.0817 0.0014 . . 30 39 VAL N 0.0702 0.0017 . . 31 42 SER N 0.0775 0.0014 . . 32 44 LEU N 0.0676 0.0012 . . 33 45 ALA N 0.0758 0.0017 . . 34 46 LEU N 0.0858 0.0009746 . . 35 47 LYS N 0.0762 0.0030 . . 36 48 ASP N 0.1129 0.0040 . . 37 51 VAL N 0.0781 0.0011 . . 38 53 GLY N 0.0633 0.0046 . . 39 54 LYS N 0.0774 0.0012 . . 40 55 HIS N 0.0844 0.0016 . . 41 56 ALA N 0.0821 0.0014 . . 42 57 GLN N 0.0779 0.0012 . . 43 58 ILE N 0.0854 0.0017 . . 44 59 THR N 0.0780 0.0014 . . 45 60 TRP N 0.0883 0.0026 . . 46 62 SER N 0.0791 0.0013 . . 47 63 THR N 0.0797 0.0009801 . . 48 64 LYS N 0.0828 0.0022 . . 49 65 PHE N 0.0817 0.0015 . . 50 66 LYS N 0.0853 0.0015 . . 51 67 TRP N 0.0835 0.0018 . . 52 68 GLU N 0.0813 0.0019 . . 53 69 LEU N 0.0821 0.0018 . . 54 70 VAL N 0.0771 0.0017 . . 55 71 ASP N 0.0735 0.0023 . . 56 75 LEU N 0.0776 0.0017 . . 57 76 ASN N 0.0805 0.0020 . . 58 77 GLY N 0.0793 0.0012 . . 59 78 THR N 0.0745 0.0017 . . 60 79 LEU N 0.0758 0.0022 . . 61 80 VAL N 0.0808 0.0012 . . 62 81 ASN N 0.0703 0.0015 . . 63 82 SER N 0.0366 0.0027 . . 64 83 HIS N 0.0734 0.00087184 . . 65 84 SER N 0.0701 0.0066 . . 66 85 ILE N 0.0752 0.0014 . . 67 86 SER N 0.0749 0.0011 . . 68 87 HIS N 0.0820 0.0016 . . 69 89 ASP N 0.0837 0.0016 . . 70 90 LEU N 0.0832 0.0014 . . 71 91 GLY N 0.0944 0.0019 . . 72 92 SER N 0.0858 0.000824 . . 73 93 ARG N 0.0784 0.0013 . . 74 94 LYS N 0.0859 0.0015 . . 75 95 TRP N 0.0807 0.0014 . . 76 96 GLY N 0.0777 0.0017 . . 77 97 ASN N 0.0855 0.0016 . . 78 99 VAL N 0.0823 0.0013 . . 79 100 GLU N 0.0857 0.0012 . . 80 101 LEU N 0.0860 0.0020 . . 81 102 ALA N 0.0762 0.0031 . . 82 103 SER N 0.0807 0.0017 . . 83 104 ASP N 0.0719 0.0043 . . 84 105 ASP N 0.0712 0.0012 . . 85 106 ILE N 0.0852 0.0020 . . 86 107 ILE N 0.0709 0.0022 . . 87 108 THR N 0.0815 0.0017 . . 88 110 GLY N 0.0841 0.0015 . . 89 111 THR N 0.0818 0.0021 . . 90 112 THR N 0.0732 0.0027 . . 91 113 THR N 0.0786 0.0017 . . 92 114 LYS N 0.0851 0.0021 . . 93 115 VAL N 0.0776 0.0028 . . 94 116 TYR N 0.0782 0.0029 . . 95 117 VAL N 0.0633 0.0026 . . 96 118 ARG N 0.0818 0.0038 . . 97 120 SER N 0.0769 0.0027 . . 98 121 SER N 0.0809 0.0031 . . 99 122 GLN N 0.0994 0.0019 . . 100 123 ASN N 0.1197 0.0026 . . 101 124 GLU N 0.2445 0.0032 . . stop_ save_ save_heteronuclear_NOE_set_1 _Saveframe_category heteronuclear_NOE _Details . loop_ _Sample_label $sample_one stop_ _Sample_conditions_label $condition_one _Spectrometer_frequency_1H 500 _Mol_system_component_name 'Kinase-interacting FHA domain of KAPP' _Atom_one_atom_name N _Atom_two_atom_name H _Heteronuclear_NOE_value_type 'relative intensities' _NOE_reference_value 1 _NOE_reference_description 'internal reference' _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Heteronuclear_NOE_value _Heteronuclear_NOE_value_error 3 LEU -0.318 0.002 4 GLY -0.115 0.005 5 SER 0.376 0.005 6 SER 0.725 0.050 7 TRP 0.820 0.121 8 LEU 0.718 0.021 9 PHE 0.792 0.037 10 LEU 0.748 0.040 11 GLU 0.533 0.043 12 VAL 0.811 0.075 14 ALA 0.797 0.004 15 GLY 0.816 0.013 17 ALA 0.825 0.041 18 ILE 0.775 0.018 19 GLY 0.730 0.0003527 20 LEU 0.749 0.004 21 GLN 0.719 0.018 22 HIS 0.753 0.032 23 ALA 0.821 0.121 24 VAL 0.757 0.010 25 ASN 0.690 0.0006985 26 SER 0.774 0.003 27 THR 0.806 0.039 28 SER 0.759 0.023 29 SER 0.558 0.021 31 LYS 0.731 0.062 32 LEU 0.710 0.011 34 VAL 0.762 0.033 35 LYS 0.721 0.011 36 LEU 0.762 0.012 37 GLY 0.739 0.009 38 ARG 0.725 0.007 39 VAL 0.703 0.006 42 SER 0.650 0.013 43 ASP 0.794 0.009 44 LEU 0.778 0.035 45 ALA 0.780 0.029 46 LEU 0.700 0.037 47 LYS 0.747 0.054 48 ASP 0.190 0.046 49 SER 0.773 0.021 50 GLU 0.643 0.023 51 VAL 0.786 0.025 53 GLY 0.813 0.118 54 LYS 0.455 0.027 55 HIS 0.749 0.025 56 ALA 0.767 0.035 57 GLN 0.790 0.015 58 ILE 0.723 0.008 59 THR 0.782 0.027 60 TRP 0.728 0.013 61 ASN 0.783 0.011 62 SER 0.752 0.002 63 THR 0.720 0.040 64 LYS 0.751 0.070 65 PHE 0.790 0.036 66 LYS 0.758 0.036 67 TRP 0.755 0.040 68 GLU 0.794 0.055 70 VAL 0.675 0.010 71 ASP 0.779 0.007 72 MET 0.795 0.014 73 GLY 0.786 0.021 74 SER 0.802 0.034 75 LEU 0.801 0.067 76 ASN 0.822 0.021 77 GLY 0.769 0.047 78 THR 0.816 0.021 79 LEU 0.770 0.022 80 VAL 0.771 0.012 81 ASN 0.787 0.008 82 SER 0.809 0.081 83 HIS 0.768 0.050 84 SER 0.764 0.080 85 ILE 0.739 0.019 86 SER 0.581 0.051 87 HIS 0.775 0.0006151 89 ASP 0.699 0.015 90 LEU 0.610 0.011 91 GLY 0.469 0.018 92 SER 0.554 0.031 93 ARG 0.650 0.0005741 94 LYS 0.648 0.017 95 TRP 0.741 0.038 96 GLY 0.741 0.069 97 ASN 0.739 0.014 99 VAL 0.800 0.003 100 GLU 0.670 0.024 101 LEU 0.721 0.023 102 ALA 0.747 0.022 103 SER 0.769 0.025 104 ASP 0.766 0.042 105 ASP 0.812 0.045 106 ILE 0.813 0.021 107 ILE 0.769 0.007 108 THR 0.828 0.055 109 LEU 0.798 0.010 110 GLY 0.731 0.030 111 THR 0.720 0.015 112 THR 0.747 0.036 113 THR 0.752 0.057 114 LYS 0.818 0.039 115 VAL 0.759 0.020 116 TYR 0.772 0.003 117 VAL 0.788 0.058 118 ARG 0.784 0.027 120 SER 0.736 0.022 121 SER 0.630 0.005 122 GLN 0.496 0.005 123 ASN 0.266 0.059 124 GLU -0.276 0.012 stop_ save_ save_heteronuclear_NOE_set_2 _Saveframe_category heteronuclear_NOE _Details . loop_ _Sample_label $sample_one stop_ _Sample_conditions_label $condition_one _Spectrometer_frequency_1H 600 _Mol_system_component_name 'Kinase-interacting FHA domain of KAPP' _Atom_one_atom_name N _Atom_two_atom_name H _Heteronuclear_NOE_value_type 'relative intensities' _NOE_reference_value 1 _NOE_reference_description 'internal reference' _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Heteronuclear_NOE_value _Heteronuclear_NOE_value_error 5 SER 0.499 0.004 6 SER 0.764 0.008 7 TRP 0.881 0.013 8 LEU 0.806 0.027 9 PHE 0.852 0.006 10 LEU 0.791 0.042 11 GLU 0.777 0.038 12 VAL 0.796 0.011 14 ALA 0.750 0.005 15 GLY 0.789 0.015 17 ALA 0.805 0.028 18 ILE 0.751 0.015 19 GLY 0.778 0.041 20 LEU 0.780 0.038 21 GLN 0.730 0.032 22 HIS 0.831 0.010 23 ALA 0.838 0.025 25 ASN 0.744 0.006 27 THR 0.804 0.034 28 SER 0.795 0.018 29 SER 0.616 0.025 31 LYS 0.800 0.003 32 LEU 0.782 0.019 34 VAL 0.782 0.022 35 LYS 0.723 0.008 37 GLY 0.840 0.045 38 ARG 0.720 0.024 39 VAL 0.768 0.021 42 SER 0.570 0.037 44 LEU 0.758 0.023 45 ALA 0.808 0.008 46 LEU 0.803 0.031 47 LYS 0.809 0.025 48 ASP 0.277 0.007 51 VAL 0.703 0.024 53 GLY 0.826 0.056 54 LYS 0.648 0.041 55 HIS 0.832 0.018 56 ALA 0.851 0.016 57 GLN 0.849 0.024 58 ILE 0.810 0.018 59 THR 0.800 0.013 60 TRP 0.743 0.013 62 SER 0.729 0.010 63 THR 0.691 0.014 64 LYS 0.748 0.018 65 PHE 0.849 0.019 66 LYS 0.776 0.020 67 TRP 0.794 0.009 68 GLU 0.827 0.016 69 LEU 0.781 0.018 70 VAL 0.772 0.013 71 ASP 0.825 0.065 75 LEU 0.789 0.031 76 ASN 0.795 0.041 77 GLY 0.856 0.008 78 THR 0.735 0.023 79 LEU 0.802 0.016 80 VAL 0.800 0.023 81 ASN 0.792 0.006 82 SER 0.854 0.026 83 HIS 0.586 0.170 84 SER 0.788 0.116 85 ILE 0.778 0.017 86 SER 0.766 0.002 87 HIS 0.814 0.018 89 ASP 0.695 0.013 90 LEU 0.694 0.066 91 GLY 0.523 0.045 92 SER 0.769 0.006 93 ARG 0.781 0.064 94 LYS 0.749 0.011 95 TRP 0.757 0.013 96 GLY 0.812 0.025 97 ASN 0.789 0.015 99 VAL 0.808 0.018 100 GLU 0.725 0.007 101 LEU 0.783 0.013 102 ALA 0.805 0.009 103 SER 0.739 0.011 104 ASP 0.775 0.051 105 ASP 0.765 0.013 106 ILE 0.804 0.014 107 ILE 0.857 0.027 108 THR 0.830 0.036 110 GLY 0.826 0.024 111 THR 0.743 0.005 112 THR 0.763 0.037 113 THR 0.769 0.010 114 LYS 0.804 0.024 115 VAL 0.780 0.023 116 TYR 0.708 0.015 117 VAL 0.779 0.012 118 ARG 0.788 0.011 120 SER 0.768 0.030 121 SER 0.675 0.046 122 GLN 0.541 0.014 123 ASN 0.336 0.026 stop_ save_ save_S2_parameters_label _Saveframe_category S2_parameters _Details . loop_ _Sample_label $sample_one stop_ _Sample_conditions_label $condition_one _Mol_system_component_name 'Kinase-interacting FHA domain of KAPP' _Tau_e_value_units ns _Tau_s_value_units . _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Atom_name _Model_fit _S2_value _S2_value_fit_error _Tau_e_value _Tau_e_value_fit_error _S2f_value _S2f_value_fit_error _S2s_value _S2s_value_fit_error _Tau_s_value _Tau_s_value_fit_error _S2H_value _S2H_value_fit_error _S2N_value _S2N_value_fit_error 3 LEU N . 0.26 . 0.97 0.03 . . . . . . . . . . 4 GLY N . 0.33 . 0.99 0.05 . . . . . . . . . . 5 SER N . 0.59 . 1.37 0.13 . . . . . . . . . . 6 SER N . 0.91 . 1.61 0.56 . . . . . . . . . . 7 TRP N . 0.99 . . . . . . . . . . . . . 8 LEU N . 0.95 . 0.18 0.31 . . . . . . . . . . 9 PHE N . 0.94 . 0.02 0.09 . . . . . . . . . . 10 LEU N . 0.88 . 0.03 0.02 . . . . . . . . . . 11 GLU N . 0.88 . 0.11 0.09 . . . . . . . . . . 12 VAL N . 0.85 . . . . . . . . . . . . . 14 ALA N . 0.91 . 0.03 0.06 . . . . . . . . . . 15 GLY N . 0.98 . . . . . . . . . . . . . 17 ALA N . 0.98 . . . . . . . . . . . . . 18 ILE N . 0.85 . 0.02 0.01 . . . . . . . . . . 19 GLY N . 0.86 . 0.03 0.02 . . . . . . . . . . 20 LEU N . 0.83 . 0.02 0.01 . . . . . . . . . . 21 GLN N . 0.82 . 0.03 0.01 . . . . . . . . . . 22 HIS N . 0.85 . 0.01 0.01 . . . . . . . . . . 23 ALA N . 0.98 . 0.07 0.24 . . . . . . . . . . 25 ASN N . 0.9 . 0.09 0.09 . . . . . . . . . . 26 SER N . 0.96 . 0.9 0.9 . . . . . . . . . . 27 THR N . 0.93 . 1.46 0.71 . . . . . . . . . . 28 SER N . 0.99 . 0.29 0.66 . . . . . . . . . . 29 SER N . 0.59 . 1.92 0.12 . . . . . . . . . . 31 LYS N . 0.97 . 0.33 0.28 . . . . . . . . . . 32 LEU N . 0.82 . 0.02 0.01 . . . . . . . . . . 34 VAL N . 0.95 . 0.09 0.19 . . . . . . . . . . 35 LYS N . 0.9 . 0.07 0.07 . . . . . . . . . . 37 GLY N . 0.99 . 0.31 0.68 . . . . . . . . . . 38 ARG N . 0.95 . 0.63 0.54 . . . . . . . . . . 39 VAL N . 0.86 . 1.78 0.35 . . . . . . . . . . 42 SER N . 0.61 . 1.91 0.14 . . . . . . . . . . 44 LEU N . 0.9 . 0.04 0.03 . . . . . . . . . . 45 ALA N . 0.83 . . . . . . . . . . . . . 46 LEU N . 0.92 . 0.05 0.09 . . . . . . . . . . 47 LYS N . 0.96 . . . . . . . . . . . . . 48 ASP N . 0.65 . 0.11 0.01 . . . . . . . . . . 49 SER N . 0.95 . 0.81 0.93 . . . . . . . . . . 50 GLU N . 0.69 . 1.86 0.23 . . . . . . . . . . 51 VAL N . 0.94 . 1.45 0.74 . . . . . . . . . . 53 GLY N . 0.98 . . . . . . . . . . . . . 54 LYS N . 0.57 . 1.82 0.15 . . . . . . . . . . 55 HIS N . 0.92 . 0.02 0.07 . . . . . . . . . . 56 ALA N . 0.95 . . . . . . . . . . . . . 57 GLN N . 0.92 . . . . . . . . . . . . . 58 ILE N . 0.89 . 0.02 0.02 . . . . . . . . . . 59 THR N . 0.96 . 0.04 0.14 . . . . . . . . . . 60 TRP N . 0.92 . 0.13 0.2 . . . . . . . . . . 61 ASN N . 0.95 . . . . . . . . . . . . . 62 SER N . 0.93 . 1.5 0.71 . . . . . . . . . . 63 THR N . 0.94 . 0.57 0.34 . . . . . . . . . . 64 LYS N . 0.91 . 0.07 0.14 . . . . . . . . . . 65 PHE N . 0.89 . . . . . . . . . . . . . 66 LYS N . 0.83 . 0.02 0.01 . . . . . . . . . . 67 TRP N . 0.97 . 0.15 0.27 . . . . . . . . . . 68 GLU N . 0.93 . 0.01 0.04 . . . . . . . . . . 69 LEU N . 0.94 . . . . . . . . . . . . . 70 VAL N . 0.95 . 0.49 0.27 . . . . . . . . . . 71 ASP N . 0.98 . 0.36 0.72 . . . . . . . . . . 75 LEU N . 0.96 . 0.98 0.88 . . . . . . . . . . 76 ASN N . 0.96 . 1.1 0.89 . . . . . . . . . . 77 GLY N . 0.99 . 0.02 0.1 . . . . . . . . . . 78 THR N . 0.99 . 0.28 0.64 . . . . . . . . . . 79 LEU N . 0.99 . . . . . . . . . . . . . 80 VAL N . 0.99 . 0.26 0.63 . . . . . . . . . . 81 ASN N . 0.99 . 0.04 0.17 . . . . . . . . . . 82 SER N . 0.94 . 1.32 0.79 . . . . . . . . . . 83 HIS N . 0.93 . 0.46 0.32 . . . . . . . . . . 84 SER N . 0.88 . 1.6 0.57 . . . . . . . . . . 85 ILE N . 0.89 . 1.68 0.48 . . . . . . . . . . 86 SER N . 0.75 . 1.87 0.19 . . . . . . . . . . 87 HIS N . 0.96 . 1.03 0.91 . . . . . . . . . . 89 ASP N . 0.92 . 0.17 0.16 . . . . . . . . . . 90 LEU N . 0.89 . 0.71 0.29 . . . . . . . . . . 91 GLY N . 0.83 . 0.51 0.19 . . . . . . . . . . 92 SER N . 0.71 . 1.87 0.2 . . . . . . . . . . 93 ARG N . 0.82 . 1.8 0.32 . . . . . . . . . . 94 LYS N . 0.9 . 1.2 0.56 . . . . . . . . . . 95 TRP N . 0.95 . 0.42 0.57 . . . . . . . . . . 96 GLY N . 0.96 . 1.24 0.84 . . . . . . . . . . 97 ASN N . 0.96 . 0.19 0.29 . . . . . . . . . . 99 VAL N . 0.94 . 0.02 0.07 . . . . . . . . . . 100 GLU N . 0.89 . 0.09 0.11 . . . . . . . . . . 101 LEU N . 0.86 . 0.03 0.01 . . . . . . . . . . 102 ALA N . 0.83 . . . . . . . . . . . . . 103 SER N . 0.82 . 0.02 0.01 . . . . . . . . . . 104 ASP N . 0.91 . 1.64 0.54 . . . . . . . . . . 105 ASP N . 0.9 . 0.02 0.02 . . . . . . . . . . 106 ILE N . 0.92 . 0.01 0.01 . . . . . . . . . . 107 ILE N . 0.91 . . . . . . . . . . . . . 108 THR N . 0.99 . . . . . . . . . . . . . 109 LEU N . 0.94 . . . . . . . . . . . . . 110 GLY N . 0.99 . . . . . . . . . . . . . 111 THR N . 0.88 . 1.7 0.45 . . . . . . . . . . 112 THR N . 0.87 . 1.7 0.49 . . . . . . . . . . 114 LYS N . 0.97 . 0.02 0.07 . . . . . . . . . . 115 VAL N . 0.89 . 0.03 0.02 . . . . . . . . . . 116 TYR N . 0.93 . 0.15 0.18 . . . . . . . . . . 117 VAL N . 0.95 . 0.13 0.27 . . . . . . . . . . 118 ARG N . 0.95 . 0.04 0.08 . . . . . . . . . . 120 SER N . 0.95 . 0.19 0.23 . . . . . . . . . . 121 SER N . 0.7 . 1.87 0.2 . . . . . . . . . . 122 GLN N . 0.45 . 1.93 0.1 . . . . . . . . . . 123 ASN N . 0.41 . 1.36 0.12 . . . . . . . . . . stop_ save_ save_H_exch_rate_set_1 _Saveframe_category H_exchange_rates _Details ; The hyrogen exchange rates of the following residues are uncertain due to the spectral overlaps: 49 SER, 61 ASN, 72 MET, 73 GLY, and 90 LEU. ; loop_ _Sample_label $sample_one stop_ _Sample_conditions_label $condition_one _H_exchange_rate_units min-1 _Mol_system_component_name 'Kinase-interacting FHA domain of KAPP' _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Atom_name _H_exchange_rate_value _H_exchange_rate_min_value _H_exchange_rate_max_value _H_exchange_rate_value_error 8 LEU H 0.00623 . . 0.00024 9 PHE H 0.00652 . . 0.00023 10 LEU H 0.00537 . . 0.00021 11 GLU H 0.00698 . . 0.00017 12 VAL H 0.01150 . . 0.00077 18 ILE H 0.54500 . . 0.01482 20 LEU H 0.07411 . . 0.00481 22 HIS H 0.23170 . . 0.00652 34 VAL H 0.02290 . . 0.00083 46 LEU H 0.20290 . . 0.00861 49 SER H 0.03331 . . 0.000893 56 ALA H 0.04199 . . 0.00122 57 GLN H 0.01319 . . 0.00030 58 ILE H 0.00860 . . 0.00023 59 THR H 0.01194 . . 0.00020 61 ASN H 0.01739 . . 0.00051 65 PHE H 0.26760 . . 0.00629 66 LYS H 0.00805 . . 0.00017 69 LEU H 0.00652 . . 0.00086 70 VAL H 0.06297 . . 0.00377 71 ASP H 0.06084 . . 0.00135 72 MET H 0.24570 . . 0.00656 73 GLY H 0.11480 . . 0.00382 77 GLY H 0.36410 . . 0.00976 78 THR H 0.77850 . . 0.01826 79 LEU H 0.07048 . . 0.00118 80 VAL H 0.14390 . . 0.00255 90 LEU H 0.2016 . . 0.00668 99 VAL H 0.02199 . . 0.00062 101 LEU H 0.00858 . . 0.00022 102 ALA H 0.01745 . . 0.00046 104 ASP H 0.00847 . . 0.00028 105 ASP H 0.00866 . . 0.00019 106 ILE H 0.00851 . . 0.00018 107 ILE H 0.00600 . . 0.00029 108 THR H 0.01352 . . 0.00048 110 GLY H 0.08406 . . 0.00201 113 THR H 0.10940 . . 0.00205 114 LYS H 0.01311 . . 0.00044 115 VAL H 0.00639 . . 0.00050 116 TYR H 0.00657 . . 0.00028 117 VAL H 0.00646 . . 0.00025 118 ARG H 0.01082 . . 0.00026 stop_ save_ save_H_exchange_protection_factor_1 _Saveframe_category H_exchange_protection_factors _Details ; The hyrogen exchange protection factors of the following residues are uncertain due to the spectral overlaps: 49 SER, 61 ASN, 72 MET, 73 GLY, and 90 LEU. ; _Sample_label $condition_one _Sample_conditions_label $condition_one _Standard_values_source_citation_label $entry_citation _Mol_system_component_name 'Kinase-interacting FHA domain of KAPP' _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Atom_name _H_exchange_protection_factor_value _H_exchange_protection_factor_value_error 8 LEU H 18.703 3003.527 9 PHE H 34.358 5271.220 10 LEU H 28.883 5374.573 11 GLU H 108.178 15504.920 12 VAL H 48.309 4200.759 14 ALA H 58.526 3069.007 18 ILE H 16.825 30.871 20 LEU H 37.901 511.412 22 HIS H 127.425 549.957 34 VAL H 9.309 406.506 46 LEU H 24.835 122.402 49 SER H 954.462 28653.935 56 ALA H 139.894 3331.597 57 GLN H 116.050 8798.314 58 ILE H 28.170 3275.525 59 THR H 49.486 4144.568 61 ASN H 244.350 14051.230 65 PHE H 76.005 284.024 66 LYS H 105.672 13123.688 69 LEU H 64.379 9871.107 70 VAL H 10.179 161.652 71 ASP H 362.128 5952.138 72 MET H 397.197 1616.594 73 GLY H 244.350 2128.492 77 GLY H 397.197 1090.901 78 THR H 127.425 163.680 79 LEU H 40.778 578.575 80 VAL H 10.179 70.738 90 LEU H 105.671 524.166 99 VAL H 9.309 423.328 101 LEU H 64.379 7507.797 102 ALA H 61.386 3517.808 104 ASP H 999.490 118031.413 105 ASP H 1995.052 230269.196 106 ILE H 74.228 8723.441 107 ILE H 8.760 1459.788 108 THR H 49.486 3660.217 110 GLY H 116.050 1380.559 113 THR H 136.668 1249.254 114 LYS H 146.571 11180.079 115 VAL H 415.979 65139.271 116 TYR H 37.901 5773.148 117 VAL H 20.759 3213.418 118 ARG H 87.565 8092.892 stop_ save_