data_6062 ####################### # Entry information # ####################### save_entry_information _Saveframe_category entry_information _Entry_title ; Assignments for the Negative Regulator of Splicing from Rous Sarcoma Virus residues 907 to 929 ; _BMRB_accession_number 6062 _BMRB_flat_file_name bmr6062.str _Entry_type original _Submission_date 2004-01-06 _Accession_date 2004-01-07 _Entry_origination author _NMR_STAR_version 2.1.1 _Experimental_method NMR _Details . loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Cabello-Villegas Javier . . 2 Guiles Keith . . 3 Soto Ana M. . 4 Yu Ping . . 5 Beemon Karen L. . 6 Wang Yun-Xing . . stop_ loop_ _Saveframe_category_type _Saveframe_category_type_count assigned_chemical_shifts 1 stop_ loop_ _Data_type _Data_type_count "1H chemical shifts" 198 "13C chemical shifts" 153 "15N chemical shifts" 15 "31P chemical shifts" 17 stop_ loop_ _Revision_date _Revision_keyword _Revision_author _Revision_detail 2015-03-18 update author "update C5' assignments" 2004-10-29 original author 'original release' stop_ save_ ############################# # Citation for this entry # ############################# save_entry_citation _Saveframe_category entry_citation _Citation_full . _Citation_title ; Solution structure of the pseudo-5' splice site of a retroviral splicing suppressor ; _Citation_status published _Citation_type journal _CAS_abstract_code . _MEDLINE_UI_code . _PubMed_ID 15317975 loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Cabello-Villegas Javier . . 2 Giles Keith E. . 3 Soto Ana M. . 4 Yu Ping . . 5 Mougin A. . . 6 Beemon Karen L. . 7 Wang Yun-Xing . . stop_ _Journal_abbreviation RNA _Journal_volume 10 _Journal_issue 9 _Journal_CSD . _Book_chapter_title . _Book_volume . _Book_series . _Book_ISBN . _Conference_state_province . _Conference_abstract_number . _Page_first 1388 _Page_last 1398 _Year 2004 _Details . loop_ _Keyword 'NMR structrue' NRS 'U1 snRNP binding site' stop_ save_ ################################## # Molecular system description # ################################## save_system_NRS _Saveframe_category molecular_system _Mol_system_name NRS23 _Abbreviation_common NRS _Enzyme_commission_number . loop_ _Mol_system_component_name _Mol_label NRS23 $NRS23 stop_ _System_molecular_weight . _System_physical_state native _System_oligomer_state monomer _System_paramagnetic no _System_thiol_state 'not present' loop_ _Biological_function "pseudo-5' splice site part of a splicing suppressor of Rous Sarcoma virus" stop_ _Database_query_date . _Details . save_ ######################## # Monomeric polymers # ######################## save_NRS23 _Saveframe_category monomeric_polymer _Mol_type polymer _Mol_polymer_class RNA _Name_common 'RNA stem-loop' _Abbreviation_common NRS23 _Molecular_mass . _Mol_thiol_state 'not present' _Details . ############################## # Polymer residue sequence # ############################## _Residue_count 23 _Mol_residue_sequence ; GGGGAGUGGUUUGUAUCCUU CCC ; loop_ _Residue_seq_code _Residue_author_seq_code _Residue_label 1 907 G 2 908 G 3 909 G 4 910 G 5 911 A 6 912 G 7 913 U 8 914 G 9 915 G 10 916 U 11 917 U 12 918 U 13 919 G 14 920 U 15 921 A 16 922 U 17 923 C 18 924 C 19 925 U 20 926 U 21 927 C 22 928 C 23 929 C stop_ _Sequence_homology_query_date . _Sequence_homology_query_revised_last_date . save_ #################### # Natural source # #################### save_natural_source _Saveframe_category natural_source loop_ _Mol_label _Organism_name_common _NCBI_taxonomy_ID _Superkingdom _Kingdom _Genus _Species _Details $NRS23 'Rous sarcoma virus' 11886 Viruses . alpharetrovirus 'Rous sarcoma virus' 'The family is Retroviridae' stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Saveframe_category experimental_source loop_ _Mol_label _Production_method _Host_organism_name_common _Genus _Species _Strain _Vector_name _Details $NRS23 'enzymatic semisynthesis' . . . . . 'In vitro transcription' stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_Sample_1 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $NRS23 1.2 mM '[U-13C; U-15N]' 'sodium phosphate buffer' 10 mM . NaCl 25 mM . stop_ save_ ############################ # Computer software used # ############################ save_nmrDraw _Saveframe_category software _Name NMRDraw _Version . loop_ _Task 'Spectra analysis' stop_ _Details ; F. Delaglio, S. Grzesiek, G. Vuister, G. Zhu, J. Pfeifer,and A. Bax. J. Biomol. NMR, 6 (1995) 277-293. ; save_ save_nmrView _Saveframe_category software _Name NMRView _Version . loop_ _Task 'Spectra analysis' stop_ _Details ; Johnson, B.A. and Blevins, R.A. NMR View- a computer program for the visualization and analysis of NMR data. J. Biomol. NMR 4 (1994): 603-614. ; save_ save_nmrPipe _Saveframe_category software _Name NMRPipe _Version . loop_ _Task 'Spectra processing' stop_ _Details ; F. Delaglio, S. Grzesiek, G. Vuister, G. Zhu, J. Pfeifer,and A. Bax. J. Biomol. NMR, 6 (1995) 277-293. ; save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _Saveframe_category NMR_spectrometer _Manufacturer Varian _Model INOVA _Field_strength 800 _Details . save_ save_NMR_spectrometer_2 _Saveframe_category NMR_spectrometer _Manufacturer Varian _Model INOVA _Field_strength 600 _Details . save_ save_NMR_spectrometer_3 _Saveframe_category NMR_spectrometer _Manufacturer Varian _Model INOVA _Field_strength 500 _Details . save_ save_NMR_spectrometer_4 _Saveframe_category NMR_spectrometer _Manufacturer Bruker _Model DRX _Field_strength 500 _Details . save_ ############################# # NMR applied experiments # ############################# save_1H-13C_NOESY-HSQC_1 _Saveframe_category NMR_applied_experiment _Experiment_name '1H-13C NOESY-HSQC' _Sample_label . save_ save_2D_NOESY_2 _Saveframe_category NMR_applied_experiment _Experiment_name '2D NOESY' _Sample_label . save_ save_15N/1H_HMQC_3 _Saveframe_category NMR_applied_experiment _Experiment_name '15N/1H HMQC' _Sample_label . save_ save_HCCH-TOCSY_4 _Saveframe_category NMR_applied_experiment _Experiment_name HCCH-TOCSY _Sample_label . save_ save_HCCH-COSY_5 _Saveframe_category NMR_applied_experiment _Experiment_name HCCH-COSY _Sample_label . save_ save_HNCCCH_6 _Saveframe_category NMR_applied_experiment _Experiment_name HNCCCH _Sample_label . save_ save_HCP_7 _Saveframe_category NMR_applied_experiment _Experiment_name HCP _Sample_label . save_ ####################### # Sample conditions # ####################### save_condition_1 _Saveframe_category sample_conditions _Details . loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units pH 6.5 0.2 n/a temperature 298 1 K stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference _Saveframe_category chemical_shift_reference _Details . loop_ _Mol_common_name _Atom_type _Atom_isotope_number _Atom_group _Chem_shift_units _Chem_shift_value _Reference_method _Reference_type _External_reference_sample_geometry _External_reference_location _External_reference_axis _Indirect_shift_ratio DSS C 13 'methyl protons' ppm 0.0 . indirect . . . 0.251449530 DSS H 1 'methyl protons' ppm 0.0 internal direct . . . 1.0 DSS N 15 'methyl protons' ppm 0.0 . indirect . . . 0.101329118 DSS P 31 'methyl protons' ppm 0.0 . indirect . . . 0.404808636 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_chemical_shift_1 _Saveframe_category assigned_chemical_shifts _Details ; The chemical shifts of the exchangeable protons and their attached nitrogens were measured at 15 deg C. ; loop_ _Sample_label $Sample_1 stop_ _Sample_conditions_label $condition_1 _Chem_shift_reference_set_label $chemical_shift_reference _Mol_system_component_name NRS23 _Text_data_format . _Text_data . loop_ _Atom_shift_assign_ID _Residue_author_seq_code _Residue_seq_code _Residue_label _Atom_name _Atom_type _Chem_shift_value _Chem_shift_value_error _Chem_shift_ambiguity_code 1 . 1 G H8 H 8.140 0.01 1 2 . 1 G C8 C 139.166 0.01 1 3 . 1 G H1' H 5.841 0.01 1 4 . 1 G H2' H 4.921 0.01 1 5 . 1 G H3' H 4.728 0.01 9 6 . 1 G H4' H 4.569 0.01 1 7 . 1 G H5' H 4.456 0.01 2 8 . 1 G H5'' H 4.284 0.01 2 9 . 1 G C1' C 91.685 0.01 1 10 . 1 G C2' C 75.143 0.01 1 11 . 1 G C3' C 74.562 0.01 9 12 . 1 G C4' C 83.365 0.01 1 13 . 1 G C5' C 67.089 0.01 1 14 . 2 G H1 H 12.783 0.01 1 15 . 2 G H8 H 7.576 0.01 1 16 . 2 G C8 C 136.915 0.01 1 17 . 2 G N1 N 147.587 0.01 1 18 . 2 G H1' H 5.951 0.01 1 19 . 2 G H2' H 4.693 0.01 1 20 . 2 G H3' H 4.618 0.01 1 21 . 2 G H4' H 4.564 0.01 1 22 . 2 G H5' H 4.276 0.01 2 23 . 2 G H5'' H 4.527 0.01 2 24 . 2 G C1' C 92.798 0.01 1 25 . 2 G C2' C 75.623 0.01 1 26 . 2 G C3' C 72.925 0.01 1 27 . 2 G C4' C 82.309 0.01 1 28 . 2 G C5' C 65.916 0.01 1 29 . 3 G H1 H 12.531 0.01 1 30 . 3 G H8 H 7.311 0.01 1 31 . 3 G C8 C 136.213 0.01 1 32 . 3 G N1 N 147.927 0.01 1 33 . 3 G H1' H 5.860 0.01 1 34 . 3 G H2' H 4.605 0.01 1 35 . 3 G H3' H 4.525 0.01 1 36 . 3 G H4' H 4.489 0.01 1 37 . 3 G H5' H 4.536 0.01 2 38 . 3 G H5'' H 4.123 0.01 2 39 . 3 G C1' C 92.595 0.01 1 40 . 3 G C2' C 76.092 0.01 1 41 . 3 G C3' C 73.004 0.01 1 42 . 3 G C4' C 81.901 0.01 1 43 . 3 G C5' C 65.182 0.01 1 44 . 4 G H1 H 10.474 0.01 1 45 . 4 G H21 H 6.252 0.01 9 46 . 4 G H22 H 6.252 0.01 9 47 . 4 G H8 H 7.128 0.01 1 48 . 4 G C8 C 136.853 0.01 1 49 . 4 G N1 N 142.916 0.01 1 50 . 4 G N2 N 73.265 0.01 9 51 . 4 G H1' H 5.772 0.01 1 52 . 4 G H2' H 4.838 0.01 1 53 . 4 G H3' H 4.356 0.01 1 54 . 4 G H4' H 4.529 0.01 1 55 . 4 G H5' H 4.380 0.01 2 56 . 4 G H5'' H 4.047 0.01 2 57 . 4 G C1' C 93.533 0.01 1 58 . 4 G C2' C 75.260 0.01 1 59 . 4 G C3' C 73.708 0.01 1 60 . 4 G C4' C 82.426 0.01 1 61 . 4 G C5' C 66.972 0.01 1 62 . 4 G P P -3.67 0.01 1 63 . 5 A H2 H 7.579 0.01 1 64 . 5 A H8 H 7.591 0.01 1 65 . 5 A C2 C 153.577 0.01 1 66 . 5 A C8 C 139.119 0.01 1 67 . 5 A H1' H 5.923 0.01 1 68 . 5 A H2' H 4.543 0.01 1 69 . 5 A H3' H 4.634 0.01 1 70 . 5 A H4' H 4.500 0.01 1 71 . 5 A H5' H 4.506 0.01 2 72 . 5 A H5'' H 4.131 0.01 2 73 . 5 A C1' C 93.455 0.01 1 74 . 5 A C2' C 75.556 0.01 1 75 . 5 A C3' C 72.690 0.01 1 76 . 5 A C4' C 82.339 0.01 1 77 . 5 A C5' C 64.896 0.01 1 78 . 5 A P P -3.93 0.01 1 79 . 6 G H1 H 13.014 0.01 1 80 . 6 G H8 H 7.342 0.01 1 81 . 6 G C8 C 136.882 0.01 1 82 . 6 G N1 N 147.980 0.01 1 83 . 6 G H1' H 5.793 0.01 1 84 . 6 G H2' H 4.323 0.01 1 85 . 6 G H3' H 4.677 0.01 1 86 . 6 G H4' H 4.482 0.01 1 87 . 6 G H5' H 4.536 0.01 2 88 . 6 G H5'' H 4.147 0.01 2 89 . 6 G C1' C 90.800 0.01 1 90 . 6 G C2' C 77.734 0.01 1 91 . 6 G C3' C 75.506 0.01 1 92 . 6 G C4' C 84.186 0.01 1 93 . 6 G C5' C 66.066 0.01 1 94 . 6 G P P -4.02 0.01 1 95 . 7 U H5 H 5.820 0.01 1 96 . 7 U H6 H 7.856 0.01 1 97 . 7 U C5 C 104.943 0.01 1 98 . 7 U C6 C 143.730 0.01 1 99 . 7 U H1' H 5.911 0.01 1 100 . 7 U H2' H 4.364 0.01 1 101 . 7 U H3' H 4.708 0.01 1 102 . 7 U H4' H 4.441 0.01 1 103 . 7 U H5' H 4.288 0.01 2 104 . 7 U H5'' H 4.154 0.01 2 105 . 7 U C1' C 91.518 0.01 1 106 . 7 U C2' C 75.740 0.01 1 107 . 7 U C3' C 75.362 0.01 1 108 . 7 U C4' C 84.538 0.01 1 109 . 7 U C5' C 66.841 0.01 1 110 . 7 U P P -4.37 0.01 1 111 . 8 G H1 H 12.678 0.01 1 112 . 8 G H8 H 7.586 0.01 1 113 . 8 G C8 C 137.363 0.01 1 114 . 8 G N1 N 148.490 0.01 1 115 . 8 G H1' H 5.817 0.01 1 116 . 8 G H2' H 4.803 0.01 1 117 . 8 G H3' H 4.432 0.01 1 118 . 8 G H4' H 4.570 0.01 1 119 . 8 G H5' H 4.329 0.01 2 120 . 8 G H5'' H 4.136 0.01 2 121 . 8 G C1' C 92.698 0.01 1 122 . 8 G C2' C 75.148 0.01 1 123 . 8 G C3' C 75.040 0.01 1 124 . 8 G C4' C 83.247 0.01 1 125 . 8 G C5' C 67.910 0.01 1 126 . 8 G P P -3.98 0.01 9 127 . 9 G H1 H 11.403 0.01 1 128 . 9 G H21 H 6.428 0.01 9 129 . 9 G H22 H 6.428 0.01 9 130 . 9 G H8 H 7.372 0.01 1 131 . 9 G C8 C 137.257 0.01 1 132 . 9 G N1 N 145.313 0.01 1 133 . 9 G N2 N 73.652 0.01 9 134 . 9 G H1' H 5.845 0.01 1 135 . 9 G H2' H 4.607 0.01 1 136 . 9 G H3' H 4.478 0.01 1 137 . 9 G H4' H 4.499 0.01 1 138 . 9 G H5' H 4.447 0.01 2 139 . 9 G H5'' H 4.138 0.01 2 140 . 9 G C1' C 92.928 0.01 1 141 . 9 G C2' C 75.506 0.01 1 142 . 9 G C3' C 73.370 0.01 1 143 . 9 G C4' C 82.778 0.01 1 144 . 9 G C5' C 65.799 0.01 1 145 . 9 G P P -3.98 0.01 1 146 . 10 U H5 H 5.317 0.01 1 147 . 10 U H6 H 7.585 0.01 1 148 . 10 U C5 C 103.848 0.01 1 149 . 10 U C6 C 141.486 0.01 1 150 . 10 U H1' H 5.777 0.01 1 151 . 10 U H2' H 4.432 0.01 1 152 . 10 U H3' H 4.555 0.01 1 153 . 10 U H4' H 4.417 0.01 1 154 . 10 U H5' H 4.443 0.01 2 155 . 10 U H5'' H 4.103 0.01 2 156 . 10 U C1' C 92.595 0.01 1 157 . 10 U C2' C 75.975 0.01 1 158 . 10 U C3' C 74.042 0.01 1 159 . 10 U C4' C 83.482 0.01 1 160 . 10 U C5' C 65.212 0.01 1 161 . 10 U P P -4.37 0.01 1 162 . 11 U H5 H 5.828 0.01 1 163 . 11 U H6 H 7.806 0.01 1 164 . 11 U C5 C 105.440 0.01 1 165 . 11 U C6 C 143.320 0.01 1 166 . 11 U H1' H 5.769 0.01 1 167 . 11 U H2' H 4.382 0.01 1 168 . 11 U H3' H 4.483 0.01 1 169 . 11 U H4' H 4.411 0.01 1 170 . 11 U H5' H 4.200 0.01 2 171 . 11 U H5'' H 4.062 0.01 2 172 . 11 U C1' C 91.110 0.01 1 173 . 11 U C2' C 75.506 0.01 1 174 . 11 U C3' C 76.549 0.01 1 175 . 11 U C4' C 85.124 0.01 1 176 . 11 U C5' C 67.206 0.01 1 177 . 11 U P P -3.96 0.01 1 178 . 12 U H5 H 5.840 0.01 1 179 . 12 U H6 H 7.705 0.01 1 180 . 12 U C5 C 105.585 0.01 1 181 . 12 U C6 C 143.595 0.01 1 182 . 12 U H1' H 5.713 0.01 1 183 . 12 U H2' H 4.258 0.01 1 184 . 12 U H3' H 4.496 0.01 1 185 . 12 U H4' H 4.060 0.01 1 186 . 12 U H5' H 3.909 0.01 2 187 . 12 U H5'' H 3.897 0.01 2 188 . 12 U C1' C 89.877 0.01 1 189 . 12 U C2' C 75.483 0.01 1 190 . 12 U C3' C 77.774 0.01 1 191 . 12 U C4' C 85.007 0.01 1 192 . 12 U C5' C 67.419 0.01 1 193 . 12 U P P -3.963 0.01 1 194 . 13 G H8 H 7.708 0.01 1 195 . 13 G C8 C 139.964 0.01 1 196 . 13 G H1' H 5.449 0.01 1 197 . 13 G H2' H 4.648 0.01 1 198 . 13 G H3' H 4.786 0.01 1 199 . 13 G H4' H 4.359 0.01 1 200 . 13 G H5' H 4.125 0.01 2 201 . 13 G H5'' H 4.025 0.01 2 202 . 13 G C1' C 90.624 0.01 1 203 . 13 G C2' C 75.856 0.01 1 204 . 13 G C3' C 77.969 0.01 1 205 . 13 G C4' C 85.594 0.01 1 206 . 13 G C5' C 67.786 0.01 1 207 . 13 G P P -3.905 0.01 1 208 . 14 U H5 H 5.906 0.01 1 209 . 14 U H6 H 7.876 0.01 1 210 . 14 U C5 C 105.513 0.01 1 211 . 14 U C6 C 144.037 0.01 1 212 . 14 U H1' H 6.037 0.01 1 213 . 14 U H2' H 4.489 0.01 1 214 . 14 U H3' H 4.681 0.01 1 215 . 14 U H4' H 4.581 0.01 1 216 . 14 U H5' H 4.219 0.01 2 217 . 14 U H5'' H 4.174 0.01 2 218 . 14 U C1' C 90.250 0.01 1 219 . 14 U C2' C 75.435 0.01 1 220 . 14 U C3' C 77.088 0.01 1 221 . 14 U C4' C 85.359 0.01 1 222 . 14 U C5' C 68.027 0.01 1 223 . 14 U P P -4.01 0.01 1 224 . 15 A H2 H 7.986 0.01 1 225 . 15 A H8 H 8.257 0.01 1 226 . 15 A C2 C 154.384 0.01 1 227 . 15 A C8 C 141.120 0.01 1 228 . 15 A H1' H 5.842 0.01 1 229 . 15 A H2' H 4.728 0.01 1 230 . 15 A H3' H 4.531 0.01 1 231 . 15 A H4' H 4.534 0.01 1 232 . 15 A H5' H 4.397 0.01 2 233 . 15 A H5'' H 4.242 0.01 2 234 . 15 A C1' C 92.666 0.01 1 235 . 15 A C2' C 75.623 0.01 1 236 . 15 A C3' C 74.503 0.01 1 237 . 15 A C4' C 83.365 0.01 1 238 . 15 A C5' C 67.120 0.01 1 239 . 15 A P P -3.94 0.01 1 240 . 16 U H5 H 5.475 0.01 1 241 . 16 U H6 H 7.730 0.01 1 242 . 16 U C5 C 104.174 0.01 1 243 . 16 U C6 C 141.527 0.01 1 244 . 16 U H1' H 5.538 0.01 1 245 . 16 U H2' H 4.254 0.01 1 246 . 16 U H3' H 4.535 0.01 1 247 . 16 U H4' H 4.488 0.01 9 248 . 16 U H5' H 4.476 0.01 9 249 . 16 U H5'' H 4.148 0.01 9 250 . 16 U C1' C 92.536 0.01 1 251 . 16 U C2' C 75.740 0.01 1 252 . 16 U C3' C 73.629 0.01 1 253 . 16 U C4' C 83.130 0.01 9 254 . 16 U C5' C 65.330 0.01 9 255 . 17 C H41 H 8.569 0.01 2 256 . 17 C H42 H 7.011 0.01 2 257 . 17 C H5 H 5.740 0.01 1 258 . 17 C H6 H 7.888 0.01 1 259 . 17 C C5 C 97.894 0.01 1 260 . 17 C C6 C 142.181 0.01 1 261 . 17 C N4 N 99.13 0.01 1 262 . 17 C H1' H 5.640 0.01 1 263 . 17 C H2' H 4.500 0.01 1 264 . 17 C H3' H 4.423 0.01 1 265 . 17 C H4' H 4.458 0.01 1 266 . 17 C H5' H 4.515 0.01 2 267 . 17 C H5'' H 4.153 0.01 2 268 . 17 C C1' C 94.068 0.01 1 269 . 17 C C2' C 75.506 0.01 1 270 . 17 C C3' C 72.617 0.01 1 271 . 17 C C4' C 82.074 0.01 1 272 . 17 C C5' C 65.330 0.01 1 273 . 17 C P P -4.33 0.01 1 274 . 18 C H41 H 8.587 0.01 2 275 . 18 C H42 H 7.095 0.01 2 276 . 18 C H5 H 5.658 0.01 1 277 . 18 C H6 H 7.843 0.01 1 278 . 18 C C5 C 98.054 0.01 1 279 . 18 C C6 C 141.211 0.01 1 280 . 18 C N4 N 99.11 0.01 1 281 . 18 C H1' H 5.492 0.01 1 282 . 18 C H2' H 4.382 0.01 1 283 . 18 C H3' H 4.517 0.01 9 284 . 18 C H4' H 4.424 0.01 1 285 . 18 C H5' H 4.554 0.01 2 286 . 18 C H5'' H 4.112 0.01 2 287 . 18 C C1' C 94.243 0.01 1 288 . 18 C C2' C 75.271 0.01 1 289 . 18 C C3' C 72.020 0.01 9 290 . 18 C C4' C 82.074 0.01 1 291 . 18 C C5' C 64.391 0.01 1 292 . 18 C P P -4.56 0.01 1 293 . 19 U H3 H 14.305 0.01 1 294 . 19 U H5 H 5.521 0.01 1 295 . 19 U H6 H 7.933 0.01 1 296 . 19 U C5 C 103.385 0.01 1 297 . 19 U C6 C 141.895 0.01 1 298 . 19 U N3 N 161.914 0.01 1 299 . 19 U H1' H 5.523 0.01 1 300 . 19 U H2' H 4.620 0.01 1 301 . 19 U H3' H 4.481 0.01 1 302 . 19 U H4' H 4.438 0.01 9 303 . 19 U H5' H 4.328 0.01 2 304 . 19 U H5'' H 4.328 0.01 2 305 . 19 U C1' C 93.772 0.01 1 306 . 19 U C2' C 75.271 0.01 1 307 . 19 U C3' C 71.869 0.01 1 308 . 19 U C4' C 82.074 0.01 9 309 . 19 U C5' C 64.039 0.01 1 310 . 20 U H3 H 11.789 0.01 1 311 . 20 U H5 H 5.877 0.01 1 312 . 20 U H6 H 8.026 0.01 1 313 . 20 U C5 C 104.820 0.01 1 314 . 20 U C6 C 141.484 0.01 1 315 . 20 U N3 N 158.058 0.01 1 316 . 20 U H1' H 5.533 0.01 1 317 . 20 U H2' H 4.140 0.01 1 318 . 20 U H3' H 4.596 0.01 1 319 . 20 U H4' H 4.447 0.01 1 320 . 20 U H5' H 4.539 0.01 2 321 . 20 U H5'' H 4.116 0.01 2 322 . 20 U C1' C 93.846 0.01 1 323 . 20 U C2' C 75.766 0.01 1 324 . 20 U C3' C 72.428 0.01 1 325 . 20 U C4' C 82.426 0.01 1 326 . 20 U C5' C 64.329 0.01 1 327 . 21 C H41 H 8.475 0.01 2 328 . 21 C H42 H 6.906 0.01 2 329 . 21 C H5 H 5.685 0.01 1 330 . 21 C H6 H 8.000 0.01 1 331 . 21 C C5 C 97.237 0.01 1 332 . 21 C C6 C 142.599 0.01 1 333 . 21 C N4 N 98.31 0.01 1 334 . 21 C H1' H 5.506 0.01 1 335 . 21 C H2' H 4.337 0.01 1 336 . 21 C H3' H 4.490 0.01 1 337 . 21 C H4' H 4.398 0.01 1 338 . 21 C H5' H 4.556 0.01 2 339 . 21 C H5'' H 4.090 0.01 2 340 . 21 C C1' C 93.741 0.01 1 341 . 21 C C2' C 75.425 0.01 1 342 . 21 C C3' C 72.214 0.01 1 343 . 21 C C4' C 81.723 0.01 1 344 . 21 C C5' C 64.677 0.01 1 345 . 21 C P P -4.86 0.01 1 346 . 22 C H41 H 8.525 0.01 2 347 . 22 C H42 H 6.941 0.01 2 348 . 22 C H5 H 5.502 0.01 1 349 . 22 C H6 H 7.808 0.01 1 350 . 22 C C5 C 97.454 0.01 1 351 . 22 C C6 C 141.632 0.01 1 352 . 22 C N4 N 98.32 0.01 1 353 . 22 C H1' H 5.476 0.01 1 354 . 22 C H2' H 4.259 0.01 1 355 . 22 C H3' H 4.488 0.01 1 356 . 22 C H4' H 4.383 0.01 1 357 . 22 C H5' H 4.055 0.01 2 358 . 22 C H5'' H 4.055 0.01 2 359 . 22 C C1' C 94.314 0.01 1 360 . 22 C C2' C 75.553 0.01 1 361 . 22 C C3' C 72.042 0.01 1 362 . 22 C C4' C 82.005 0.01 1 363 . 22 C C5' C 64.475 0.01 1 364 . 22 C P P -4.57 0.01 1 365 . 23 C H41 H 8.264 0.01 2 366 . 23 C H42 H 7.012 0.01 2 367 . 23 C H5 H 5.504 0.01 1 368 . 23 C H6 H 7.698 0.01 1 369 . 23 C C5 C 97.953 0.01 1 370 . 23 C C6 C 141.883 0.01 1 371 . 23 C N4 N 97.04 0.01 1 372 . 23 C H1' H 5.754 0.01 1 373 . 23 C H2' H 4.002 0.01 1 374 . 23 C H3' H 4.191 0.01 1 375 . 23 C H4' H 4.175 0.01 1 376 . 23 C H5' H 4.490 0.01 2 377 . 23 C H5'' H 4.032 0.01 2 378 . 23 C C1' C 92.873 0.01 1 379 . 23 C C2' C 77.515 0.01 1 380 . 23 C C3' C 99.623 0.01 1 381 . 23 C C4' C 83.460 0.01 1 382 . 23 C C5' C 65.095 0.01 1 383 . 23 C P P -4.41 0.01 1 stop_ save_