data_4346 ####################### # Entry information # ####################### save_entry_information _Saveframe_category entry_information _Entry_title ; 1H, 13C, and 15N Chemical Shift Assignments for the Regulatory mRNA of the Yeast Ribosomal Protein L30 ; _BMRB_accession_number 4346 _BMRB_flat_file_name bmr4346.str _Entry_type original _Submission_date 1999-05-07 _Accession_date 1999-05-10 _Entry_origination author _NMR_STAR_version 2.1.1 _Experimental_method NMR _Details . loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Mao Hongyuan . . 2 White Susan A. . 3 Williamson james R. . stop_ loop_ _Saveframe_category_type _Saveframe_category_type_count assigned_chemical_shifts 1 stop_ loop_ _Data_type _Data_type_count "1H chemical shifts" 255 "13C chemical shifts" 193 "15N chemical shifts" 24 stop_ loop_ _Revision_date _Revision_keyword _Revision_author _Revision_detail 2000-03-08 original author . stop_ loop_ _Related_BMRB_accession_number _Relationship 4345 . stop_ _Original_release_date 2000-03-08 save_ ############################# # Citation for this entry # ############################# save_entry_citation _Saveframe_category entry_citation _Citation_full ; Mao, H. N., White, S. A., and Williamson, J. R., "A Novel Loop-loop Recognition Motif in the Yeast Ribosomal Protein L30 Autoregulatory RNA Complex," Nat. Struct. Biol. 6, 1139-1147 (1999). ; _Citation_title ; A Novel Loop-loop Recognition Motif in the Yeast Ribosomal Protein L30 Autoregulatory RNA Complex ; _Citation_status published _Citation_type journal _CAS_abstract_code . _MEDLINE_UI_code 20051011 _PubMed_ID ? loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Mao Hongyuan . . 2 White Susan A. . 3 Williamson james R. . stop_ _Journal_abbreviation 'Nat. Struct. Biol.' _Journal_name_full 'Nature Structural Biology' _Journal_volume 6 _Journal_issue 12 _Journal_CSD . _Book_chapter_title . _Book_volume . _Book_series . _Book_ISBN . _Conference_state_province . _Conference_abstract_number . _Page_first 1139 _Page_last 1147 _Year 1999 _Details . loop_ _Keyword 'AUTO-REGULATION OF PRE-MRNA SPLICING AND MRNA TRANSLATION' 'PROTEIN-RNA COMPLEX' 'RIBOSOMAL PROTEIN' stop_ save_ ################################## # Molecular system description # ################################## save_SYSTEM_L30_MRNA _Saveframe_category molecular_system _Mol_system_name 'L30 MRNA' _Abbreviation_common 'L30 MRNA' _Enzyme_commission_number . loop_ _Mol_system_component_name _Mol_label L30RNA $L30_MRNA stop_ _System_molecular_weight . _System_physical_state native _System_oligomer_state MONOMER _System_paramagnetic no _System_thiol_state 'not present' loop_ _Biological_function 'THE AUTOREGULATORY BINDING SITE FOR THE YEAST RIBOSOMAL PROTEIN L30.' stop_ _Database_query_date . _Details 'THE RNA USED IN THE NMR STUDIES IS ONLY A SMALL FRACTION OF THE PRE-MRNA. DETAILED DESCRIPTION CAN BE FOUND IN THE REFERENCE PAPER.' save_ ######################## # Monomeric polymers # ######################## save_L30_MRNA _Saveframe_category monomeric_polymer _Mol_type polymer _Mol_polymer_class RNA _Name_common 'L30 MRNA' _Abbreviation_common 'L30 MRNA' _Molecular_mass . _Mol_thiol_state . _Details . ############################## # Polymer residue sequence # ############################## _Residue_count 33 _Mol_residue_sequence ; GGACCGGAGUGUCGCAAGAC GCAGAGAUGGUCC ; loop_ _Residue_seq_code _Residue_author_seq_code _Residue_label 1 5 G 2 6 G 3 7 A 4 8 C 5 9 C 6 10 G 7 11 G 8 12 A 9 13 G 10 14 U 11 15 G 12 16 U 13 17 C 14 18 G 15 19 C 16 20 A 17 21 A 18 50 G 19 51 A 20 52 C 21 53 G 22 54 C 23 55 A 24 56 G 25 57 A 26 58 G 27 59 A 28 60 U 29 61 G 30 62 G 31 63 U 32 64 C 33 65 C stop_ _Sequence_homology_query_date . _Sequence_homology_query_revised_last_date . save_ #################### # Natural source # #################### save_natural_source _Saveframe_category natural_source loop_ _Mol_label _Organism_name_common _NCBI_taxonomy_ID _Superkingdom _Kingdom _Genus _Species _Fraction _Gene_mnemonic _Details $L30_MRNA 'BAKER'S YEAST' 4932 Eukaryota FUNGI SACCHAROMYCES CEREVISIAE NUCLEUS 'L30 PRE-MRNA' 'IN VITRO T7 RNA POLYMERASE TRANSCRIPTION' stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Saveframe_category experimental_source loop_ _Mol_label _Production_method _Host_organism_name_common _Genus _Species _Strain _Vector_name _Details $L30_MRNA 'enzymatic semisynthesis' . . . . . 'IN VITRO T7 RNA POLYMERASE TRANSCRIPTION' stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_SAMPLE_1 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Concentration_min_value _Concentration_max_value _Isotopic_labeling $L30_MRNA 1.8 mM 0.7 1.8 N/A stop_ save_ save_SAMPLE_2 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $L30_MRNA 0.9 mM '[U-99% 13C; U-99% 15N]' stop_ save_ save_SAMPLE_3 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $L30_MRNA 0.5 mM '[U-95% 13C; U-99% 15N]-G' stop_ save_ ############################ # Computer software used # ############################ save_NMRPIPE _Saveframe_category software _Name NMRPipe _Version . _Details . save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer1 _Saveframe_category NMR_spectrometer _Manufacturer VARIAN _Model INOVA _Field_strength 600 _Details . save_ save_NMR_spectrometer2 _Saveframe_category NMR_spectrometer _Manufacturer FBML _Model FBML _Field_strength 500 _Details . save_ ####################### # Sample conditions # ####################### save_Ex-cond_1 _Saveframe_category sample_conditions _Details . loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units 'ionic strength' 0.1 0.02 M pH 6.0 0.2 n/a temperature 288 1 K stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference _Saveframe_category chemical_shift_reference _Details . loop_ _Mol_common_name _Atom_type _Atom_isotope_number _Atom_group _Chem_shift_units _Chem_shift_value _Reference_method _Reference_type _External_reference_sample_geometry _External_reference_location _External_reference_axis TSP C 13 'methyl protons' ppm 0.00 internal direct spherical internal parallel_to_Bo TSP H 1 'methyl protons' ppm 0.00 internal direct spherical internal parallel_to_Bo 'ammonium chloride NH4Cl' N 15 'ammonium nitrogen' ppm 0.00 internal direct spherical internal parallel_to_Bo stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_shift_set_1 _Saveframe_category assigned_chemical_shifts _Details . loop_ _Sample_label $SAMPLE_1 $SAMPLE_2 $SAMPLE_3 stop_ _Sample_conditions_label $Ex-cond_1 _Chem_shift_reference_set_label $chemical_shift_reference _Mol_system_component_name L30RNA _Text_data_format . _Text_data . loop_ _Atom_shift_assign_ID _Residue_author_seq_code _Residue_seq_code _Residue_label _Atom_name _Atom_type _Chem_shift_value _Chem_shift_value_error _Chem_shift_ambiguity_code 1 . 1 G H8 H 8.18 0.02 1 2 . 1 G C8 C 139.4 0.2 1 3 . 1 G H1' H 5.85 0.02 1 4 . 1 G H2' H 4.97 0.02 1 5 . 1 G H3' H 4.75 0.02 1 6 . 1 G H4' H 4.58 0.02 1 7 . 1 G H5' H 4.42 0.02 2 8 . 1 G H5'' H 4.33 0.02 2 9 . 1 G C1' C 90.8 0.2 1 10 . 1 G C2' C 75.5 0.2 1 11 . 1 G C3' C 75.4 0.2 1 12 . 1 G C4' C 84.2 0.2 1 13 . 1 G C5' C 67.8 0.2 1 14 . 2 G H1 H 12.50 0.02 1 15 . 2 G H8 H 7.67 0.02 1 16 . 2 G C8 C 137.6 0.2 1 17 . 2 G N1 N 146.8 0.2 1 18 . 2 G H1' H 5.92 0.02 1 19 . 2 G H2' H 4.69 0.02 1 20 . 2 G H3' H 4.65 0.02 1 21 . 2 G H4' H 4.61 0.02 1 22 . 2 G H5' H 4.37 0.02 2 23 . 2 G H5'' H 4.51 0.02 2 24 . 2 G C1' C 93.1 0.2 1 25 . 2 G C2' C 75.9 0.2 1 26 . 2 G C3' C 74.0 0.2 1 27 . 2 G C4' C 83.2 0.2 1 28 . 2 G C5' C 67.4 0.2 1 29 . 3 A H2 H 7.86 0.02 1 30 . 3 A H8 H 7.94 0.02 1 31 . 3 A C2 C 154.4 0.2 1 32 . 3 A C8 C 140.5 0.2 1 33 . 3 A H1' H 6.05 0.02 1 34 . 3 A H2' H 4.63 0.02 1 35 . 3 A H3' H 4.63 0.02 1 36 . 3 A H4' H 4.55 0.02 1 37 . 3 A H5' H 4.20 0.02 2 38 . 3 A H5'' H 4.65 0.02 2 39 . 3 A C1' C 93.3 0.2 1 40 . 3 A C2' C 76.1 0.2 1 41 . 3 A C3' C 73.1 0.2 1 42 . 3 A C4' C 82.5 0.2 1 43 . 3 A C5' C 65.4 0.2 1 44 . 4 C H41 H 8.39 0.02 1 45 . 4 C H42 H 7.13 0.02 1 46 . 4 C H5 H 5.28 0.02 1 47 . 4 C H6 H 7.36 0.02 1 48 . 4 C C5 C 97.7 0.2 1 49 . 4 C C6 C 141.0 0.2 1 50 . 4 C N4 N 97.2 0.2 1 51 . 4 C H1' H 5.35 0.02 1 52 . 4 C H2' H 4.29 0.02 1 53 . 4 C H3' H 4.26 0.02 1 54 . 4 C H4' H 4.42 0.02 1 55 . 4 C H5' H 4.06 0.02 2 56 . 4 C H5'' H 4.47 0.02 2 57 . 4 C C1' C 94.2 0.2 1 58 . 4 C C2' C 76.0 0.2 1 59 . 4 C C3' C 73.0 0.2 1 60 . 4 C C4' C 82.3 0.2 1 61 . 4 C C5' C 65.6 0.2 1 62 . 5 C H41 H 8.35 0.02 1 63 . 5 C H42 H 6.67 0.02 1 64 . 5 C H5 H 5.34 0.02 1 65 . 5 C H6 H 7.44 0.02 1 66 . 5 C C5 C 98.2 0.2 1 67 . 5 C C6 C 141.2 0.2 1 68 . 5 C N4 N 97.1 0.2 1 69 . 5 C H1' H 5.42 0.02 1 70 . 5 C H2' H 4.55 0.02 1 71 . 5 C H3' H 4.29 0.02 1 72 . 5 C H4' H 4.35 0.02 1 73 . 5 C H5' H 4.07 0.02 2 74 . 5 C H5'' H 4.52 0.02 2 75 . 5 C C1' C 95.1 0.2 1 76 . 5 C C2' C 75.2 0.2 1 77 . 5 C C3' C 72.8 0.2 1 78 . 5 C C4' C 82.6 0.2 1 79 . 5 C C5' C 65.2 0.2 1 80 . 6 G H1 H 10.80 0.02 1 81 . 6 G H21 H 6.45 0.02 1 82 . 6 G H22 H 6.45 0.02 1 83 . 6 G H8 H 7.70 0.02 1 84 . 6 G C8 C 137.5 0.2 1 85 . 6 G N1 N 144.6 0.2 1 86 . 6 G N2 N 72.9 0.2 1 87 . 6 G H1' H 5.57 0.02 1 88 . 6 G H2' H 4.48 0.02 1 89 . 6 G H3' H 4.78 0.02 1 90 . 6 G H4' H 4.29 0.02 1 91 . 6 G C1' C 93.2 0.2 1 92 . 6 G C2' C 78.0 0.2 1 93 . 6 G C3' C 75.3 0.2 1 94 . 6 G C4' C 83.5 0.2 1 95 . 7 G H1 H 10.92 0.02 9 96 . 7 G H8 H 7.93 0.02 1 97 . 7 G C8 C 139.4 0.2 1 98 . 7 G N1 N 146.0 0.2 1 99 . 7 G H1' H 5.68 0.02 1 100 . 7 G H2' H 4.86 0.02 1 101 . 7 G H3' H 4.96 0.02 1 102 . 7 G H4' H 4.55 0.02 1 103 . 7 G H5' H 4.08 0.02 2 104 . 7 G C1' C 89.1 0.2 9 105 . 7 G C2' C 79.2 0.2 1 106 . 7 G C3' C 75.9 0.2 1 107 . 7 G C4' C 87.1 0.2 1 108 . 8 A H2 H 8.00 0.02 1 109 . 8 A H8 H 8.10 0.02 9 110 . 8 A C2 C 154.9 0.2 1 111 . 8 A C8 C 141.4 0.2 9 112 . 8 A H1' H 5.76 0.02 1 113 . 8 A H2' H 4.15 0.02 1 114 . 8 A H3' H 4.52 0.02 1 115 . 8 A H4' H 4.63 0.02 1 116 . 8 A C1' C 93.8 0.2 9 117 . 8 A C2' C 75.9 0.2 9 118 . 8 A C3' C 73.0 0.2 9 119 . 8 A C4' C 82.2 0.2 9 120 . 9 G H1 H 12.96 0.02 1 121 . 9 G H8 H 8.06 0.02 1 122 . 9 G C8 C 138.3 0.2 1 123 . 9 G N1 N 147.4 0.2 1 124 . 9 G H1' H 5.99 0.02 1 125 . 9 G H2' H 4.90 0.02 1 126 . 9 G H3' H 4.32 0.02 1 127 . 9 G C1' C 92.3 0.2 1 128 . 9 G C2' C 75.5 0.2 1 129 . 9 G C3' C 70.5 0.2 1 130 . 10 U H3 H 11.93 0.02 1 131 . 10 U H6 H 7.89 0.02 1 132 . 10 U C5 C 104.5 0.2 1 133 . 10 U C6 C 141.4 0.2 1 134 . 10 U N3 N 158.5 0.2 1 135 . 10 U H1' H 5.49 0.02 1 136 . 10 U H2' H 4.46 0.02 1 137 . 10 U H3' H 4.42 0.02 1 138 . 10 U H4' H 4.39 0.02 1 139 . 10 U H5' H 4.26 0.02 2 140 . 10 U H5'' H 4.32 0.02 2 141 . 10 U C1' C 94.3 0.2 1 142 . 10 U C2' C 75.9 0.2 1 143 . 10 U C3' C 72.7 0.2 1 144 . 10 U C4' C 82.3 0.2 1 145 . 10 U C5' C 67.9 0.2 1 146 . 11 G H1 H 12.79 0.02 1 147 . 11 G H8 H 7.91 0.02 1 148 . 11 G C8 C 137.7 0.2 1 149 . 11 G N1 N 147.4 0.2 1 150 . 11 G H1' H 5.84 0.02 1 151 . 11 G H2' H 4.52 0.02 1 152 . 11 G H3' H 4.59 0.02 1 153 . 11 G H4' H 4.55 0.02 1 154 . 11 G H5' H 4.40 0.02 2 155 . 11 G H5'' H 4.08 0.02 2 156 . 11 G C1' C 93.3 0.2 1 157 . 11 G C2' C 75.7 0.2 1 158 . 11 G C3' C 73.6 0.2 1 159 . 11 G C4' C 82.7 0.2 1 160 . 11 G C5' C 67.4 0.2 1 161 . 12 U H3 H 14.36 0.02 1 162 . 12 U H5 H 5.15 0.02 1 163 . 12 U H6 H 7.80 0.02 1 164 . 12 U C5 C 103.0 0.2 1 165 . 12 U C6 C 142.3 0.2 1 166 . 12 U N3 N 162.4 0.2 1 167 . 12 U H1' H 5.58 0.02 1 168 . 12 U H2' H 4.51 0.02 1 169 . 12 U H3' H 4.43 0.02 1 170 . 12 U H4' H 4.44 0.02 1 171 . 12 U H5' H 4.15 0.02 2 172 . 12 U H5'' H 4.54 0.02 2 173 . 12 U C1' C 94.5 0.2 1 174 . 12 U C2' C 76.0 0.2 1 175 . 12 U C3' C 73.1 0.2 1 176 . 12 U C4' C 82.3 0.2 1 177 . 12 U C5' C 65.3 0.2 1 178 . 13 C H41 H 8.28 0.02 2 179 . 13 C H42 H 6.88 0.02 2 180 . 13 C H5 H 5.56 0.02 1 181 . 13 C H6 H 7.68 0.02 1 182 . 13 C C5 C 98.4 0.2 1 183 . 13 C C6 C 141.2 0.2 1 184 . 13 C N4 N 97.9 0.2 1 185 . 13 C H1' H 5.61 0.02 1 186 . 13 C H2' H 4.30 0.02 1 187 . 13 C H3' H 4.50 0.02 1 188 . 13 C H4' H 4.47 0.02 1 189 . 13 C H5' H 4.11 0.02 2 190 . 13 C H5'' H 4.57 0.02 2 191 . 13 C C1' C 94.7 0.2 1 192 . 13 C C2' C 76.0 0.2 1 193 . 13 C C3' C 72.6 0.2 1 194 . 13 C C4' C 82.4 0.2 1 195 . 13 C C5' C 64.9 0.2 1 196 . 14 G H1 H 10.74 0.02 1 197 . 14 G H8 H 7.70 0.02 1 198 . 14 G C8 C 137.0 0.2 1 199 . 14 G N1 N 146.0 0.2 1 200 . 14 G H1' H 5.62 0.02 1 201 . 14 G H2' H 4.56 0.02 1 202 . 14 G H3' H 4.68 0.02 1 203 . 14 G H4' H 4.43 0.02 1 204 . 14 G H5' H 4.43 0.02 2 205 . 14 G H5'' H 4.12 0.02 2 206 . 14 G C1' C 92.4 0.2 1 207 . 14 G C2' C 76.7 0.2 1 208 . 14 G C3' C 74.9 0.2 1 209 . 14 G C4' C 83.2 0.2 1 210 . 14 G C5' C 65.9 0.2 1 211 . 15 C H41 H 7.21 0.02 1 212 . 15 C H5 H 5.75 0.02 1 213 . 15 C H6 H 7.82 0.02 1 214 . 15 C C5 C 98.6 0.2 1 215 . 15 C C6 C 144.5 0.2 1 216 . 15 C N4 N 97.1 0.2 1 217 . 15 C H1' H 5.70 0.02 1 218 . 15 C H2' H 4.40 0.02 1 219 . 15 C H3' H 4.30 0.02 1 220 . 15 C H4' H 4.15 0.02 1 221 . 15 C H5' H 4.15 0.02 2 222 . 15 C H5'' H 3.98 0.02 2 223 . 15 C C1' C 92.0 0.2 1 224 . 15 C C2' C 76.4 0.2 1 225 . 15 C C3' C 76.0 0.2 1 226 . 15 C C4' C 84.2 0.2 1 227 . 15 C C5' C 66.6 0.2 1 228 . 16 A H2 H 7.90 0.02 1 229 . 16 A H8 H 8.02 0.02 1 230 . 16 A C2 C 155.0 0.2 1 231 . 16 A C8 C 141.1 0.2 1 232 . 16 A H1' H 5.63 0.02 1 233 . 16 A H2' H 4.37 0.02 1 234 . 16 A H3' H 4.57 0.02 1 235 . 16 A H4' H 4.22 0.02 1 236 . 16 A H5' H 3.77 0.02 2 237 . 16 A H5'' H 3.88 0.02 2 238 . 16 A C1' C 91.7 0.2 1 239 . 16 A C2' C 77.5 0.2 1 240 . 16 A C3' C 76.6 0.2 1 241 . 16 A C4' C 84.4 0.2 1 242 . 16 A C5' C 66.9 0.2 1 243 . 17 A H2 H 8.10 0.02 1 244 . 17 A H8 H 8.28 0.02 1 245 . 17 A C2 C 155.3 0.2 1 246 . 17 A C8 C 142.9 0.2 1 247 . 17 A H1' H 6.10 0.02 1 248 . 17 A H2' H 4.73 0.02 1 249 . 17 A H3' H 5.41 0.02 1 250 . 17 A H4' H 4.54 0.02 1 251 . 17 A H5' H 4.44 0.02 2 252 . 17 A H5'' H 4.53 0.02 2 253 . 17 A C1' C 92.8 0.2 1 254 . 17 A C2' C 77.4 0.2 1 255 . 17 A C3' C 75.5 0.2 1 256 . 17 A C4' C 83.6 0.2 1 257 . 17 A C5' C 67.4 0.2 1 258 . 18 G H1 H 12.35 0.02 1 259 . 18 G H8 H 7.82 0.02 1 260 . 18 G C8 C 137.9 0.2 1 261 . 18 G N1 N 146.6 0.2 1 262 . 18 G H1' H 4.00 0.02 1 263 . 18 G H2' H 4.42 0.02 1 264 . 18 G H3' H 4.30 0.02 1 265 . 18 G H4' H 4.40 0.02 1 266 . 18 G H5' H 4.41 0.02 2 267 . 18 G H5'' H 4.31 0.02 2 268 . 18 G C1' C 92.9 0.2 1 269 . 18 G C2' C 75.4 0.2 1 270 . 18 G C3' C 74.8 0.2 1 271 . 18 G C4' C 83.3 0.2 1 272 . 18 G C5' C 70.1 0.2 1 273 . 19 A H2 H 7.78 0.02 1 274 . 19 A H8 H 7.81 0.02 1 275 . 19 A C2 C 154.2 0.2 1 276 . 19 A C8 C 139.9 0.2 1 277 . 19 A H1' H 6.02 0.02 1 278 . 19 A H2' H 4.47 0.02 1 279 . 19 A H3' H 4.64 0.02 1 280 . 19 A H4' H 4.47 0.02 1 281 . 19 A H5' H 4.13 0.02 2 282 . 19 A H5'' H 4.56 0.02 2 283 . 19 A C1' C 93.3 0.2 1 284 . 19 A C2' C 76.1 0.2 1 285 . 19 A C3' C 72.7 0.2 1 286 . 19 A C4' C 82.6 0.2 1 287 . 19 A C5' C 64.9 0.2 1 288 . 20 C H41 H 8.45 0.02 2 289 . 20 C H42 H 6.95 0.02 2 290 . 20 C H5 H 5.22 0.02 1 291 . 20 C H6 H 7.40 0.02 1 292 . 20 C C5 C 97.8 0.2 1 293 . 20 C C6 C 141.0 0.2 1 294 . 20 C N4 N 98.3 0.2 1 295 . 20 C H1' H 5.51 0.02 1 296 . 20 C H2' H 4.41 0.02 1 297 . 20 C H3' H 4.40 0.02 1 298 . 20 C H4' H 4.41 0.02 1 299 . 20 C H5' H 4.07 0.02 2 300 . 20 C H5'' H 4.51 0.02 2 301 . 20 C C1' C 93.6 0.2 1 302 . 20 C C2' C 76.4 0.2 1 303 . 20 C C3' C 73.1 0.2 1 304 . 20 C C4' C 82.1 0.2 1 305 . 20 C C5' C 65.3 0.2 1 306 . 21 G H1 H 11.14 0.02 1 307 . 21 G H21 H 6.43 0.02 1 308 . 21 G H22 H 6.43 0.02 1 309 . 21 G H8 H 7.54 0.02 1 310 . 21 G C8 C 137.6 0.2 1 311 . 21 G N1 N 143.9 0.2 1 312 . 21 G N2 N 72.9 0.2 1 313 . 21 G H1' H 5.73 0.02 1 314 . 21 G H2' H 4.65 0.02 1 315 . 21 G H3' H 4.28 0.02 1 316 . 21 G H4' H 4.52 0.02 1 317 . 21 G H5' H 4.08 0.02 2 318 . 21 G H5'' H 4.41 0.02 2 319 . 21 G C1' C 94.0 0.2 1 320 . 21 G C2' C 75.6 0.2 1 321 . 21 G C3' C 74.1 0.2 1 322 . 21 G C4' C 83.1 0.2 1 323 . 21 G C5' C 64.8 0.2 1 324 . 22 C H41 H 8.10 0.02 2 325 . 22 C H42 H 7.13 0.02 2 326 . 22 C H5 H 5.25 0.02 1 327 . 22 C H6 H 7.54 0.02 1 328 . 22 C C5 C 97.7 0.2 1 329 . 22 C C6 C 140.5 0.2 1 330 . 22 C N4 N 98.8 0.2 1 331 . 22 C H1' H 5.57 0.02 1 332 . 22 C H2' H 4.47 0.02 1 333 . 22 C H3' H 4.52 0.02 1 334 . 22 C H4' H 4.47 0.02 1 335 . 22 C H5' H 4.11 0.02 2 336 . 22 C H5'' H 4.52 0.02 2 337 . 22 C C1' C 94.2 0.2 1 338 . 22 C C2' C 75.7 0.2 1 339 . 22 C C3' C 72.0 0.2 1 340 . 22 C C4' C 82.5 0.2 1 341 . 22 C C5' C 64.8 0.2 1 342 . 23 A H8 H 7.91 0.02 1 343 . 23 A C8 C 139.7 0.2 1 344 . 23 A H1' H 5.94 0.02 1 345 . 23 A H2' H 4.78 0.02 1 346 . 23 A C1' C 93.8 0.2 1 347 . 23 A C2' C 76.3 0.2 1 348 . 24 G H1 H 10.99 0.02 9 349 . 24 G H8 H 7.24 0.02 1 350 . 24 G C8 C 140.8 0.2 1 351 . 24 G N1 N 144.0 0.2 1 352 . 24 G H1' H 4.89 0.02 1 353 . 24 G H2' H 4.50 0.02 1 354 . 24 G H3' H 4.68 0.02 1 355 . 24 G H4' H 4.15 0.02 1 356 . 24 G H5' H 4.08 0.02 2 357 . 24 G H5'' H 4.49 0.02 2 358 . 24 G C1' C 90.8 0.2 1 359 . 24 G C2' C 77.8 0.2 1 360 . 24 G C3' C 75.8 0.2 1 361 . 24 G C5' C 68.0 0.2 1 362 . 25 A H8 H 8.35 0.02 9 363 . 25 A C8 C 143.1 0.2 9 364 . 25 A H1' H 6.04 0.02 1 365 . 25 A H2' H 4.91 0.02 1 366 . 25 A H3' H 4.70 0.02 1 367 . 25 A H4' H 4.58 0.02 9 368 . 25 A H5' H 4.31 0.02 9 369 . 25 A C1' C 89.3 0.2 1 370 . 26 G H8 H 8.15 0.02 1 371 . 26 G C8 C 139.6 0.2 1 372 . 26 G H1' H 5.99 0.02 1 373 . 26 G H2' H 5.04 0.02 1 374 . 26 G H3' H 5.01 0.02 1 375 . 26 G H4' H 4.31 0.02 9 376 . 26 G C1' C 87.5 0.2 1 377 . 26 G C2' C 76.8 0.2 1 378 . 26 G C3' C 75.0 0.2 1 379 . 27 A H8 H 8.17 0.02 9 380 . 27 A C8 C 141.6 0.2 9 381 . 27 A H1' H 5.77 0.02 9 382 . 27 A H2' H 4.49 0.02 9 383 . 27 A H3' H 4.73 0.02 9 384 . 27 A C1' C 93.9 0.2 9 385 . 27 A C2' C 76.5 0.2 9 386 . 27 A C3' C 73.3 0.2 9 387 . 28 U H3 H 11.79 0.02 1 388 . 28 U H5 H 4.90 0.02 9 389 . 28 U H6 H 7.50 0.02 9 390 . 28 U C6 C 141.8 0.2 9 391 . 28 U N3 N 158.4 0.2 1 392 . 28 U H1' H 5.69 0.02 1 393 . 28 U C1' C 93.0 0.2 9 394 . 29 G H1 H 12.69 0.02 1 395 . 29 G H8 H 7.82 0.02 1 396 . 29 G C8 C 137.9 0.2 1 397 . 29 G N1 N 146.7 0.2 1 398 . 29 G H1' H 5.57 0.02 1 399 . 29 G H2' H 4.76 0.02 1 400 . 29 G H3' H 4.55 0.02 1 401 . 29 G H4' H 4.50 0.02 1 402 . 29 G H5' H 4.30 0.02 2 403 . 29 G C1' C 94.2 0.2 1 404 . 29 G C2' C 75.3 0.2 1 405 . 29 G C3' C 74.0 0.2 1 406 . 29 G C4' C 83.0 0.2 1 407 . 29 G C5' C 68.6 0.2 1 408 . 30 G H1 H 13.34 0.02 1 409 . 30 G H8 H 7.31 0.02 1 410 . 30 G C8 C 136.7 0.2 1 411 . 30 G N1 N 148.2 0.2 1 412 . 30 G H1' H 5.81 0.02 1 413 . 30 G H2' H 4.53 0.02 1 414 . 30 G H3' H 4.56 0.02 1 415 . 30 G H4' H 4.51 0.02 1 416 . 30 G H5' H 4.54 0.02 2 417 . 30 G H5'' H 4.11 0.02 2 418 . 30 G C1' C 93.6 0.2 1 419 . 30 G C2' C 75.8 0.2 1 420 . 30 G C3' C 72.9 0.2 1 421 . 30 G C4' C 82.6 0.2 1 422 . 30 G C5' C 65.1 0.2 1 423 . 31 U H3 H 14.47 0.02 1 424 . 31 U H5 H 5.12 0.02 1 425 . 31 U H6 H 7.78 0.02 1 426 . 31 U C5 C 102.9 0.2 1 427 . 31 U C6 C 142.3 0.2 1 428 . 31 U N3 N 162.5 0.2 1 429 . 31 U H1' H 5.62 0.02 1 430 . 31 U H2' H 4.57 0.02 1 431 . 31 U H3' H 4.51 0.02 1 432 . 31 U H4' H 4.46 0.02 1 433 . 31 U H5' H 4.13 0.02 2 434 . 31 U H5'' H 4.44 0.02 2 435 . 31 U C1' C 94.3 0.2 1 436 . 31 U C2' C 75.6 0.2 1 437 . 31 U C3' C 72.7 0.2 1 438 . 31 U C4' C 82.2 0.2 1 439 . 31 U C5' C 65.3 0.2 1 440 . 32 C H41 H 8.64 0.02 2 441 . 32 C H42 H 7.13 0.02 2 442 . 32 C H5 H 5.72 0.02 1 443 . 32 C H6 H 7.92 0.02 1 444 . 32 C C5 C 98.1 0.2 1 445 . 32 C C6 C 142.3 0.2 1 446 . 32 C N4 N 98.2 0.2 1 447 . 32 C H1' H 5.64 0.02 1 448 . 32 C H2' H 4.40 0.02 1 449 . 32 C H3' H 4.68 0.02 1 450 . 32 C H4' H 4.48 0.02 1 451 . 32 C H5' H 4.15 0.02 2 452 . 32 C H5'' H 4.52 0.02 2 453 . 32 C C1' C 94.3 0.2 1 454 . 32 C C2' C 76.8 0.2 1 455 . 32 C C3' C 74.5 0.2 1 456 . 32 C C4' C 83.0 0.2 1 457 . 32 C C5' C 64.6 0.2 1 458 . 33 C H5 H 5.60 0.02 1 459 . 33 C H6 H 7.72 0.02 1 460 . 33 C C5 C 98.7 0.2 1 461 . 33 C C6 C 142.3 0.2 1 462 . 33 C H1' H 5.78 0.02 1 463 . 33 C H2' H 4.03 0.02 1 464 . 33 C H3' H 4.20 0.02 1 465 . 33 C H4' H 4.20 0.02 1 466 . 33 C H5' H 4.06 0.02 2 467 . 33 C H5'' H 4.54 0.02 2 468 . 33 C C1' C 93.1 0.2 1 469 . 33 C C2' C 77.9 0.2 1 470 . 33 C C3' C 70.2 0.2 1 471 . 33 C C4' C 83.8 0.2 1 472 . 33 C C5' C 65.6 0.2 1 stop_ save_