data_18975 ####################### # Entry information # ####################### save_entry_information _Saveframe_category entry_information _Entry_title ; Unmodified Helix 69 ; _BMRB_accession_number 18975 _BMRB_flat_file_name bmr18975.str _Entry_type original _Submission_date 2013-01-25 _Accession_date 2013-01-25 _Entry_origination author _NMR_STAR_version 2.1.1 _Experimental_method NMR _Details . loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 JIANG JUN . . 2 ADURI RAVIPRASAD . . 3 CHOW CHRISTINE S. . 4 SANTALUCIA JOHN . Jr. stop_ loop_ _Saveframe_category_type _Saveframe_category_type_count assigned_chemical_shifts 1 stop_ loop_ _Data_type _Data_type_count "1H chemical shifts" 160 "13C chemical shifts" 128 stop_ loop_ _Revision_date _Revision_keyword _Revision_author _Revision_detail 2014-02-17 update BMRB 'update entry citation' 2014-01-02 original author 'original release' stop_ save_ ############################# # Citation for this entry # ############################# save_entry_citation _Saveframe_category entry_citation _Citation_full . _Citation_title 'Structure modulation of helix 69 from Escherichia coli 23S ribosomal RNA by pseudouridylations.' _Citation_status published _Citation_type journal _CAS_abstract_code . _MEDLINE_UI_code . _PubMed_ID 24371282 loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Jiang Jun . . 2 Aduri Raviprasad . . 3 Chow Christine S. . 4 Santalucia John . Jr. stop_ _Journal_abbreviation 'Nucleic Acids Res.' _Journal_name_full 'Nucleic acids research' _Journal_volume . _Journal_issue . _Journal_CSD . _Book_chapter_title . _Book_volume . _Book_series . _Book_ISBN . _Conference_state_province . _Conference_abstract_number . _Page_first . _Page_last . _Year 2013 _Details . save_ ################################## # Molecular system description # ################################## save_assembly _Saveframe_category molecular_system _Mol_system_name 'Unmodified Helix 69' _Enzyme_commission_number . loop_ _Mol_system_component_name _Mol_label RNA $RNA stop_ _System_molecular_weight . _System_physical_state native _System_oligomer_state ? _System_paramagnetic no _System_thiol_state . _Database_query_date . _Details . save_ ######################## # Monomeric polymers # ######################## save_RNA _Saveframe_category monomeric_polymer _Mol_type polymer _Mol_polymer_class RNA _Name_common RNA _Molecular_mass 6077.715 _Mol_thiol_state 'Not present' _Details . ############################## # Polymer residue sequence # ############################## _Residue_count 19 _Mol_residue_sequence GGCCGUAACUAUAACGGUC loop_ _Residue_seq_code _Residue_author_seq_code _Residue_label 1 1 G 2 2 G 3 3 C 4 4 C 5 5 G 6 6 U 7 7 A 8 8 A 9 9 C 10 10 U 11 11 A 12 12 U 13 13 A 14 14 A 15 15 C 16 16 G 17 17 G 18 18 U 19 19 C stop_ _Sequence_homology_query_date . _Sequence_homology_query_revised_last_date . save_ #################### # Natural source # #################### save_natural_source _Saveframe_category natural_source loop_ _Mol_label _Organism_name_common _NCBI_taxonomy_ID _Superkingdom _Kingdom _Genus _Species $RNA 'E. coli' 562 Bacteria . Escherichia coli stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Saveframe_category experimental_source loop_ _Mol_label _Production_method _Host_organism_name_common _Genus _Species _Strain _Vector_name $RNA 'enzymatic semisynthesis' . . . . . stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $RNA 1.0 mM 'natural abundance' 'Potassium Phosphate' 10 mM 'natural abundance' 'Potassium Chloride' 50 mM 'natural abundance' EDTA 0.1 mM 'natural abundance' D20 100 % 'natural abundance' stop_ save_ save_sample_2 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $RNA 1.0 mM 'natural abundance' 'Potassium Phosphate' 10 mM 'natural abundance' 'Potassium Chloride' 50 mM 'natural abundance' EDTA 0.1 mM 'natural abundance' D20 90 % 'natural abundance' H2O 10 % 'natural abundance' stop_ save_ save_sample_3 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $RNA 1.0 mM '[U-100% 13C; U-100% 15N]' 'Potassium Phosphate' 10 mM 'natural abundance' 'Potassium Chloride' 50 mM 'natural abundance' EDTA 0.1 mM 'natural abundance' D20 100 % 'natural abundance' stop_ save_ ############################ # Computer software used # ############################ save_SPARKY _Saveframe_category software _Name SPARKY _Version . loop_ _Vendor _Address _Electronic_address Goddard . . stop_ loop_ _Task 'chemical shift assignment' 'data analysis' stop_ _Details . save_ save_CNS _Saveframe_category software _Name CNS _Version 1.2 loop_ _Vendor _Address _Electronic_address 'Brunger, Adams, Clore, Gros, Nilges and Read' . . stop_ loop_ _Task refinement 'structure solution' stop_ _Details . save_ save_TOPSPIN _Saveframe_category software _Name TOPSPIN _Version . loop_ _Vendor _Address _Electronic_address 'Bruker Biospin' . . stop_ loop_ _Task collection processing stop_ _Details . save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_spectrometer_1 _Saveframe_category NMR_spectrometer _Manufacturer Bruker _Model Avance _Field_strength 700 _Details . save_ save_spectrometer_2 _Saveframe_category NMR_spectrometer _Manufacturer Varian _Model Mercury _Field_strength 400 _Details . save_ ############################# # NMR applied experiments # ############################# save_2D_1H-13C_NATURAL_ABUNDANCE_HMQC_1 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-13C NATURAL ABUNDANCE HMQC' _Sample_label $sample_1 save_ save_2D_1H-1H_NOESY_2 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-1H NOESY' _Sample_label $sample_1 save_ save_2D_DQF-COSY_3 _Saveframe_category NMR_applied_experiment _Experiment_name '2D DQF-COSY' _Sample_label $sample_1 save_ save_3D_1H-1H-1H_TOCSY-NOESY_4 _Saveframe_category NMR_applied_experiment _Experiment_name '3D 1H-1H-1H TOCSY-NOESY' _Sample_label $sample_1 save_ save_2D_1H-31P_HETCOR_5 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-31P HETCOR' _Sample_label $sample_1 save_ save_1D_31P_6 _Saveframe_category NMR_applied_experiment _Experiment_name '1D 31P' _Sample_label $sample_1 save_ save_2D_1H-1H_NOESY_7 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-1H NOESY' _Sample_label $sample_2 save_ save_2D_1H-13C_HSQC_8 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-13C HSQC' _Sample_label $sample_3 save_ save_3D_1H-13C-1H_HCCH-COSY_9 _Saveframe_category NMR_applied_experiment _Experiment_name '3D 1H-13C-1H HCCH-COSY' _Sample_label $sample_3 save_ save_3D_1H-13C-1H_HCCH-TOCSY_10 _Saveframe_category NMR_applied_experiment _Experiment_name '3D 1H-13C-1H HCCH-TOCSY' _Sample_label $sample_3 save_ save_3D_1H-13C-13C_HCCH-TOCSY_11 _Saveframe_category NMR_applied_experiment _Experiment_name '3D 1H-13C-13C HCCH-TOCSY' _Sample_label $sample_3 save_ save_3D_1H-1H-13C_NOESY-HMQC_12 _Saveframe_category NMR_applied_experiment _Experiment_name '3D 1H-1H-13C NOESY-HMQC' _Sample_label $sample_3 save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Saveframe_category sample_conditions _Details . loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units 'ionic strength' 70 . mM pH 7.3 . pH pressure 1 . atm temperature 298.2 . K stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference_1 _Saveframe_category chemical_shift_reference _Details . loop_ _Mol_common_name _Atom_type _Atom_isotope_number _Atom_group _Chem_shift_units _Chem_shift_value _Reference_method _Reference_type _External_reference_sample_geometry _External_reference_location _External_reference_axis _Indirect_shift_ratio TSP H 1 'methyl protons' ppm 0 internal direct . . . 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_1 _Saveframe_category assigned_chemical_shifts _Details . loop_ _Experiment_label '2D 1H-13C NATURAL ABUNDANCE HMQC' '2D 1H-1H NOESY' '2D DQF-COSY' '3D 1H-1H-1H TOCSY-NOESY' '2D 1H-13C HSQC' '3D 1H-13C-1H HCCH-COSY' '3D 1H-13C-1H HCCH-TOCSY' '3D 1H-13C-13C HCCH-TOCSY' '3D 1H-1H-13C NOESY-HMQC' stop_ loop_ _Sample_label $sample_1 $sample_2 $sample_3 stop_ _Sample_conditions_label $sample_conditions_1 _Chem_shift_reference_set_label $chemical_shift_reference_1 _Mol_system_component_name RNA _Text_data_format . _Text_data . loop_ _Atom_shift_assign_ID _Residue_author_seq_code _Residue_seq_code _Residue_label _Atom_name _Atom_type _Chem_shift_value _Chem_shift_value_error _Chem_shift_ambiguity_code 1 1 1 G H1' H 5.829 0.003 1 2 1 1 G H2' H 4.835 0.002 1 3 1 1 G H3' H 4.744 0.003 1 4 1 1 G H4' H 4.538 0.002 1 5 1 1 G H5' H 4.303 0.003 2 6 1 1 G H5'' H 4.132 0.002 2 7 1 1 G H8 H 8.216 0.002 1 8 1 1 G C1' C 89.302 0.000 1 9 1 1 G C2' C 72.544 0.000 1 10 1 1 G C3' C 72.110 0.000 1 11 1 1 G C4' C 80.878 0.000 1 12 1 1 G C5' C 64.593 0.000 1 13 1 1 G C8 C 136.526 0.006 1 14 2 2 G H1 H 11.601 0.002 1 15 2 2 G H1' H 5.948 0.003 1 16 2 2 G H2' H 4.730 0.003 1 17 2 2 G H3' H 4.580 0.003 1 18 2 2 G H4' H 4.586 0.004 1 19 2 2 G H5' H 4.572 0.002 2 20 2 2 G H5'' H 4.307 0.003 2 21 2 2 G H8 H 7.604 0.004 1 22 2 2 G C1' C 90.595 0.020 1 23 2 2 G C2' C 72.606 0.010 1 24 2 2 G C3' C 70.197 0.004 1 25 2 2 G C4' C 79.810 0.036 1 26 2 2 G C5' C 63.185 0.016 1 27 2 2 G C8 C 134.435 0.027 1 28 3 3 C H1' H 5.573 0.002 1 29 3 3 C H2' H 4.339 0.002 2 30 3 3 C H3' H 4.558 0.004 1 31 3 3 C H4' H 4.461 0.003 1 32 3 3 C H5 H 5.493 0.031 1 33 3 3 C H5' H 4.572 0.003 2 34 3 3 C H5'' H 4.138 0.002 2 35 3 3 C H6 H 7.802 0.016 1 36 3 3 C H41 H 8.398 0.003 1 37 3 3 C H42 H 6.919 0.004 1 38 3 3 C C1' C 91.135 0.025 1 39 3 3 C C2' C 73.044 0.014 1 40 3 3 C C3' C 69.227 0.036 1 41 3 3 C C4' C 79.206 0.015 1 42 3 3 C C5 C 94.663 0.020 1 43 3 3 C C5' C 61.397 0.024 1 44 3 3 C C6 C 137.828 0.007 1 45 4 4 C H1' H 5.557 0.003 1 46 4 4 C H2' H 4.617 0.002 1 47 4 4 C H3' H 4.561 0.003 1 48 4 4 C H4' H 4.442 0.003 1 49 4 4 C H5 H 5.528 0.034 1 50 4 4 C H5' H 4.551 0.002 2 51 4 4 C H5'' H 4.127 0.002 2 52 4 4 C H6 H 7.753 0.022 1 53 4 4 C H41 H 8.269 0.003 1 54 4 4 C H42 H 6.700 0.007 1 55 4 4 C C1' C 91.218 0.021 1 56 4 4 C C2' C 72.823 0.010 1 57 4 4 C C3' C 69.805 0.012 1 58 4 4 C C4' C 79.101 0.013 1 59 4 4 C C5 C 95.360 0.011 1 60 4 4 C C5' C 62.075 0.008 1 61 4 4 C C6 C 138.037 0.015 1 62 5 5 G H1 H 12.710 0.004 1 63 5 5 G H1' H 5.720 0.004 1 64 5 5 G H2' H 4.501 0.003 1 65 5 5 G H3' H 4.492 0.004 1 66 5 5 G H4' H 4.489 0.004 1 67 5 5 G H5' H 4.480 0.004 2 68 5 5 G H5'' H 4.124 0.001 2 69 5 5 G H8 H 7.523 0.003 1 70 5 5 G C1' C 90.414 0.020 1 71 5 5 G C2' C 72.683 0.031 1 72 5 5 G C3' C 70.536 0.011 1 73 5 5 G C4' C 79.449 0.009 1 74 5 5 G C5' C 63.309 0.010 1 75 5 5 G C8 C 133.533 0.014 1 76 6 6 U H1' H 5.577 0.003 1 77 6 6 U H2' H 4.561 0.001 1 78 6 6 U H3' H 4.483 0.003 1 79 6 6 U H4' H 4.444 0.005 1 80 6 6 U H5 H 4.952 0.020 1 81 6 6 U H5' H 4.543 0.003 2 82 6 6 U H5'' H 4.124 0.002 2 83 6 6 U H6 H 7.529 0.016 1 84 6 6 U C1' C 90.620 0.031 1 85 6 6 U C2' C 72.871 0.036 1 86 6 6 U C3' C 70.239 0.009 1 87 6 6 U C4' C 79.769 0.007 1 88 6 6 U C5 C 100.071 0.079 1 89 6 6 U C5' C 62.186 0.008 1 90 6 6 U C6 C 138.339 0.015 1 91 7 7 A H1' H 5.756 0.002 1 92 7 7 A H2 H 7.508 0.003 1 93 7 7 A H2' H 4.621 0.002 1 94 7 7 A H3' H 4.634 0.002 1 95 7 7 A H4' H 4.549 0.002 1 96 7 7 A H5' H 4.428 0.001 2 97 7 7 A H5'' H 4.204 0.001 2 98 7 7 A H8 H 8.118 0.002 1 99 7 7 A C1' C 89.992 0.052 1 100 7 7 A C2 C 151.572 0.009 1 101 7 7 A C2' C 72.566 0.015 1 102 7 7 A C3' C 71.698 0.006 1 103 7 7 A C4' C 80.647 0.011 1 104 7 7 A C5' C 63.773 0.009 1 105 7 7 A C8 C 137.365 0.008 1 106 8 8 A H1' H 5.558 0.002 1 107 8 8 A H2 H 7.909 0.002 1 108 8 8 A H2' H 4.298 0.002 1 109 8 8 A H3' H 4.574 0.003 1 110 8 8 A H4' H 4.258 0.003 1 111 8 8 A H5' H 4.428 0.002 2 112 8 8 A H5'' H 4.098 0.001 2 113 8 8 A H8 H 7.920 0.002 1 114 8 8 A C1' C 89.194 0.028 1 115 8 8 A C2 C 152.395 0.006 1 116 8 8 A C2' C 73.131 0.008 1 117 8 8 A C3' C 70.798 0.010 1 118 8 8 A C4' C 80.285 0.011 1 119 8 8 A C5' C 62.684 0.003 1 120 8 8 A C8 C 137.113 0.004 1 121 9 9 C H1' H 5.530 0.004 1 122 9 9 C H2' H 4.044 0.003 1 123 9 9 C H3' H 4.416 0.002 1 124 9 9 C H4' H 4.008 0.002 1 125 9 9 C H5 H 5.412 0.016 1 126 9 9 C H5' H 4.184 0.002 2 127 9 9 C H5'' H 3.941 0.002 2 128 9 9 C H6 H 7.389 0.014 1 129 9 9 C C1' C 88.113 0.032 1 130 9 9 C C2' C 73.525 0.004 1 131 9 9 C C3' C 73.931 0.051 1 132 9 9 C C4' C 81.562 0.010 1 133 9 9 C C5 C 95.421 0.006 1 134 9 9 C C5' C 64.058 0.004 1 135 9 9 C C6 C 139.443 0.005 1 136 10 10 U H1' H 5.785 0.003 1 137 10 10 U H2' H 4.204 0.002 1 138 10 10 U H3' H 4.459 0.002 1 139 10 10 U H4' H 4.304 0.003 1 140 10 10 U H5 H 5.783 0.020 1 141 10 10 U H5' H 3.916 0.001 2 142 10 10 U H5'' H 3.846 0.002 2 143 10 10 U H6 H 7.616 0.015 1 144 10 10 U C1' C 87.100 0.026 1 145 10 10 U C2' C 72.902 0.003 1 146 10 10 U C3' C 74.813 0.037 1 147 10 10 U C4' C 82.002 0.008 1 148 10 10 U C5 C 102.801 0.026 1 149 10 10 U C5' C 65.065 0.009 1 150 10 10 U C6 C 140.614 0.003 1 151 11 11 A H1' H 5.910 0.002 1 152 11 11 A H2 H 7.906 0.002 1 153 11 11 A H2' H 4.824 0.002 1 154 11 11 A H3' H 4.807 0.002 1 155 11 11 A H4' H 4.488 0.002 1 156 11 11 A H5' H 4.248 0.002 2 157 11 11 A H5'' H 4.123 0.003 2 158 11 11 A H8 H 8.281 0.002 1 159 11 11 A C1' C 87.700 0.045 1 160 11 11 A C2 C 152.250 0.017 1 161 11 11 A C2' C 72.996 0.004 1 162 11 11 A C3' C 73.505 0.008 1 163 11 11 A C4' C 81.897 0.016 1 164 11 11 A C5' C 64.847 0.003 1 165 11 11 A C8 C 139.152 0.005 1 166 12 12 U H1' H 5.954 0.008 1 167 12 12 U H2' H 4.418 0.002 1 168 12 12 U H3' H 4.729 0.002 1 169 12 12 U H4' H 4.553 0.001 1 170 12 12 U H5 H 5.738 0.023 1 171 12 12 U H5' H 4.305 0.002 2 172 12 12 U H5'' H 4.249 0.001 2 173 12 12 U H6 H 7.770 0.015 1 174 12 12 U C1' C 87.974 0.105 1 175 12 12 U C2' C 73.021 0.007 1 176 12 12 U C3' C 74.102 0.018 1 177 12 12 U C4' C 82.408 0.006 1 178 12 12 U C5 C 102.466 0.030 1 179 12 12 U C5' C 65.027 0.010 1 180 12 12 U C6 C 140.696 0.007 1 181 13 13 A H1' H 5.950 0.003 1 182 13 13 A H2 H 7.912 0.002 1 183 13 13 A H2' H 4.813 0.003 1 184 13 13 A H3' H 4.669 0.002 1 185 13 13 A H4' H 4.636 0.003 1 186 13 13 A H5' H 4.404 0.001 2 187 13 13 A H5'' H 4.293 0.002 2 188 13 13 A H8 H 8.201 0.002 1 189 13 13 A C1' C 88.800 0.048 1 190 13 13 A C2 C 151.907 0.003 1 191 13 13 A C2' C 73.152 0.014 1 192 13 13 A C3' C 73.092 0.014 1 193 13 13 A C4' C 81.407 0.011 1 194 13 13 A C5' C 65.356 0.004 1 195 13 13 A C8 C 138.372 0.006 1 196 14 14 A H1' H 5.697 0.002 1 197 14 14 A H2 H 7.717 0.002 1 198 14 14 A H2' H 4.592 0.003 1 199 14 14 A H3' H 4.560 0.002 1 200 14 14 A H4' H 4.545 0.001 1 201 14 14 A H5' H 4.482 0.001 2 202 14 14 A H5'' H 4.226 0.001 2 203 14 14 A H8 H 8.021 0.002 1 204 14 14 A C1' C 90.005 0.018 1 205 14 14 A C2 C 150.763 0.010 1 206 14 14 A C2' C 72.590 0.014 1 207 14 14 A C3' C 70.710 0.018 1 208 14 14 A C4' C 79.867 0.020 1 209 14 14 A C5' C 63.324 0.030 1 210 14 14 A C8 C 137.272 0.015 1 211 15 15 C H1' H 5.457 0.003 1 212 15 15 C H2' H 4.469 0.006 1 213 15 15 C H3' H 4.427 0.002 1 214 15 15 C H4' H 4.469 0.017 1 215 15 15 C H5 H 5.151 0.028 1 216 15 15 C H5' H 4.503 0.001 2 217 15 15 C H5'' H 4.101 0.005 2 218 15 15 C H6 H 7.400 0.017 1 219 15 15 C H41 H 8.108 0.001 1 220 15 15 C H42 H 6.641 0.004 1 221 15 15 C C1' C 90.851 0.021 1 222 15 15 C C2' C 72.793 0.005 1 223 15 15 C C3' C 69.909 0.025 1 224 15 15 C C4' C 79.149 0.022 1 225 15 15 C C5 C 94.754 0.019 1 226 15 15 C C5' C 62.464 0.021 1 227 15 15 C C6 C 137.768 0.031 1 228 16 16 G H1 H 12.325 0.006 1 229 16 16 G H1' H 5.743 0.003 1 230 16 16 G H2' H 4.698 0.001 1 231 16 16 G H3' H 4.567 0.002 1 232 16 16 G H4' H 4.494 0.003 1 233 16 16 G H5' H 4.488 0.003 2 234 16 16 G H5'' H 4.126 0.001 2 235 16 16 G H8 H 7.544 0.002 1 236 16 16 G C1' C 90.001 0.038 1 237 16 16 G C2' C 72.682 0.010 1 238 16 16 G C3' C 70.401 0.007 1 239 16 16 G C4' C 79.383 0.024 1 240 16 16 G C5' C 63.193 0.011 1 241 16 16 G C8 C 133.410 0.013 1 242 17 17 G H1 H 13.402 0.003 1 243 17 17 G H1' H 5.756 0.004 1 244 17 17 G H2' H 4.648 0.003 1 245 17 17 G H3' H 4.397 0.003 1 246 17 17 G H4' H 4.486 0.004 1 247 17 17 G H5' H 4.521 0.004 2 248 17 17 G H5'' H 4.088 0.002 2 249 17 17 G H8 H 7.241 0.003 1 250 17 17 G C1' C 90.327 0.016 1 251 17 17 G C2' C 72.498 0.012 1 252 17 17 G C3' C 69.905 0.010 1 253 17 17 G C4' C 79.337 0.008 1 254 17 17 G C5' C 62.457 0.003 1 255 17 17 G C8 C 133.272 0.006 1 256 18 18 U H1' H 5.557 0.003 1 257 18 18 U H2' H 4.149 0.002 1 258 18 18 U H3 H 12.234 0.006 1 259 18 18 U H3' H 4.540 0.003 1 260 18 18 U H4' H 4.414 0.003 1 261 18 18 U H5 H 5.430 0.022 1 262 18 18 U H5' H 4.535 0.004 2 263 18 18 U H5'' H 4.075 0.003 2 264 18 18 U H6 H 7.769 0.015 1 265 18 18 U C1' C 91.407 0.038 1 266 18 18 U C2' C 73.002 0.009 1 267 18 18 U C3' C 69.312 0.005 1 268 18 18 U C4' C 79.169 0.015 1 269 18 18 U C5 C 101.062 0.073 1 270 18 18 U C5' C 61.292 0.007 1 271 18 18 U C6 C 137.983 0.014 1 272 19 19 C H1' H 5.929 0.003 1 273 19 19 C H2' H 4.040 0.004 1 274 19 19 C H3' H 4.275 0.002 1 275 19 19 C H4' H 4.158 0.002 1 276 19 19 C H5 H 5.690 0.039 1 277 19 19 C H5' H 4.547 0.003 2 278 19 19 C H5'' H 4.050 0.004 2 279 19 19 C H6 H 7.826 0.017 1 280 19 19 C H41 H 8.425 0.002 1 281 19 19 C H42 H 6.870 0.006 1 282 19 19 C C1' C 89.825 0.025 1 283 19 19 C C2' C 74.805 0.003 1 284 19 19 C C3' C 67.169 0.007 1 285 19 19 C C4' C 80.645 0.011 1 286 19 19 C C5 C 95.249 0.027 1 287 19 19 C C5' C 62.504 0.009 1 288 19 19 C C6 C 140.352 0.025 1 stop_ save_