data_15445 ####################### # Entry information # ####################### save_entry_information _Saveframe_category entry_information _Entry_title ; 15N relaxation and H/D exchange analysis of 15.5K free in solution ; _BMRB_accession_number 15445 _BMRB_flat_file_name bmr15445.str _Entry_type original _Submission_date 2007-08-27 _Accession_date 2007-08-27 _Entry_origination author _NMR_STAR_version 2.1.1 _Experimental_method NMR _Details . loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Soss Sarah E. . 2 Flynn Peter F. . stop_ loop_ _Saveframe_category_type _Saveframe_category_type_count heteronucl_NOE 2 T1_relaxation 2 T2_relaxation 2 H_exchange_protection_factors 1 H_exch_rates 1 S2_parameters 1 stop_ loop_ _Data_type _Data_type_count "T1 relaxation values" 191 "T2 relaxation values" 189 "order parameters" 95 "H exchange rates" 61 "H exchange protection factors" 61 stop_ loop_ _Revision_date _Revision_keyword _Revision_author _Revision_detail 2008-09-29 update BMRB 'add author sequence' 2008-06-26 original author 'original release' stop_ loop_ _Related_BMRB_accession_number _Relationship 7249 'Assigned chemical shifts' stop_ save_ ############################# # Citation for this entry # ############################# save_entry_citation _Saveframe_category entry_citation _Citation_full . _Citation_title 'Functional implications for a prototypical K-turn binding protein from structural and dynamical studies of 15.5K' _Citation_status published _Citation_type journal _CAS_abstract_code . _MEDLINE_UI_code . _PubMed_ID 18044964 loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Soss Sarah E. . 2 Flynn Peter F. . stop_ _Journal_abbreviation Biochemistry _Journal_volume 46 _Journal_issue 51 _Journal_CSD . _Book_chapter_title . _Book_volume . _Book_series . _Book_ISBN . _Conference_state_province . _Conference_abstract_number . _Page_first 14979 _Page_last 14986 _Year 2007 _Details . save_ ################################## # Molecular system description # ################################## save_assembly _Saveframe_category molecular_system _Mol_system_name 15.5K _Enzyme_commission_number . loop_ _Mol_system_component_name _Mol_label 15.5K $15.5K stop_ _System_molecular_weight . _System_physical_state native _System_oligomer_state ? _System_paramagnetic no _System_thiol_state . _Database_query_date . _Details . save_ ######################## # Monomeric polymers # ######################## save_15.5K _Saveframe_category monomeric_polymer _Mol_type polymer _Mol_polymer_class protein _Name_common 15.5K _Molecular_mass . _Mol_thiol_state unknown _Details . ############################## # Polymer residue sequence # ############################## _Residue_count 144 _Mol_residue_sequence ; MGHHHHHHSSGIEEGRMTEA DVNPKAYPLADAHLTKKLLD LVQQSCNYKQLRKGANEATK TLNRGISEFIVMAADAEPLE IILHLPLLCEDKNVPYVFVR SKQALGRACGVSRPVIACSV TIKEGSQLKQQIQSIQQSIE RLLV ; loop_ _Residue_seq_code _Residue_author_seq_code _Residue_label 1 -15 MET 2 -14 GLY 3 -13 HIS 4 -12 HIS 5 -11 HIS 6 -10 HIS 7 -9 HIS 8 -8 HIS 9 -7 SER 10 -6 SER 11 -5 GLY 12 -4 ILE 13 -3 GLU 14 -2 GLU 15 -1 GLY 16 0 ARG 17 1 MET 18 2 THR 19 3 GLU 20 4 ALA 21 5 ASP 22 6 VAL 23 7 ASN 24 8 PRO 25 9 LYS 26 10 ALA 27 11 TYR 28 12 PRO 29 13 LEU 30 14 ALA 31 15 ASP 32 16 ALA 33 17 HIS 34 18 LEU 35 19 THR 36 20 LYS 37 21 LYS 38 22 LEU 39 23 LEU 40 24 ASP 41 25 LEU 42 26 VAL 43 27 GLN 44 28 GLN 45 29 SER 46 30 CYS 47 31 ASN 48 32 TYR 49 33 LYS 50 34 GLN 51 35 LEU 52 36 ARG 53 37 LYS 54 38 GLY 55 39 ALA 56 40 ASN 57 41 GLU 58 42 ALA 59 43 THR 60 44 LYS 61 45 THR 62 46 LEU 63 47 ASN 64 48 ARG 65 49 GLY 66 50 ILE 67 51 SER 68 52 GLU 69 53 PHE 70 54 ILE 71 55 VAL 72 56 MET 73 57 ALA 74 58 ALA 75 59 ASP 76 60 ALA 77 61 GLU 78 62 PRO 79 63 LEU 80 64 GLU 81 65 ILE 82 66 ILE 83 67 LEU 84 68 HIS 85 69 LEU 86 70 PRO 87 71 LEU 88 72 LEU 89 73 CYS 90 74 GLU 91 75 ASP 92 76 LYS 93 77 ASN 94 78 VAL 95 79 PRO 96 80 TYR 97 81 VAL 98 82 PHE 99 83 VAL 100 84 ARG 101 85 SER 102 86 LYS 103 87 GLN 104 88 ALA 105 89 LEU 106 90 GLY 107 91 ARG 108 92 ALA 109 93 CYS 110 94 GLY 111 95 VAL 112 96 SER 113 97 ARG 114 98 PRO 115 99 VAL 116 100 ILE 117 101 ALA 118 102 CYS 119 103 SER 120 104 VAL 121 105 THR 122 106 ILE 123 107 LYS 124 108 GLU 125 109 GLY 126 110 SER 127 111 GLN 128 112 LEU 129 113 LYS 130 114 GLN 131 115 GLN 132 116 ILE 133 117 GLN 134 118 SER 135 119 ILE 136 120 GLN 137 121 GLN 138 122 SER 139 123 ILE 140 124 GLU 141 125 ARG 142 126 LEU 143 127 LEU 144 128 VAL stop_ _Sequence_homology_query_date . _Sequence_homology_query_revised_last_date 2015-09-23 loop_ _Database_name _Database_accession_code _Database_entry_mol_name _Sequence_query_to_submitted_percentage _Sequence_subject_length _Sequence_identity _Sequence_positive _Sequence_homology_expectation_value PDB 1E7K "Crystal Structure Of The Spliceosomal 15.5kd Protein Bound To A U4 Snrna Fragment" 88.89 128 100.00 100.00 5.81e-87 PDB 2JNB "Solution Structure Of Rna-Binding Protein 15.5k" 100.00 144 100.00 100.00 1.30e-100 PDB 2OZB "Structure Of A Human Prp31-15.5k-U4 Snrna Complex" 90.28 130 99.23 99.23 8.06e-88 PDB 3SIU "Structure Of A Hprp31-15.5k-U4atac 5' Stem Loop Complex, Monomeric Form" 90.28 130 99.23 99.23 8.06e-88 PDB 3SIV "Structure Of A Hprp31-15.5k-U4atac 5' Stem Loop Complex, Dimeric Form" 90.28 130 99.23 99.23 8.06e-88 DBJ BAA23363 "OTK27 [Homo sapiens]" 88.89 128 100.00 100.00 5.81e-87 DBJ BAB23329 "unnamed protein product [Mus musculus]" 88.89 128 99.22 100.00 1.36e-86 DBJ BAE01699 "unnamed protein product [Macaca fascicularis]" 88.89 128 100.00 100.00 5.81e-87 DBJ BAE22349 "unnamed protein product [Mus musculus]" 88.89 128 100.00 100.00 5.81e-87 DBJ BAE26537 "unnamed protein product [Mus musculus]" 88.89 128 100.00 100.00 5.81e-87 EMBL CAG30417 "NHP2L1 [Homo sapiens]" 88.89 128 100.00 100.00 5.81e-87 EMBL CAG46526 "NHP2L1 [Homo sapiens]" 88.89 128 100.00 100.00 5.81e-87 EMBL CAK54562 "NHP2L1 [synthetic construct]" 88.89 128 100.00 100.00 5.81e-87 EMBL CAK54861 "NHP2L1 [synthetic construct]" 88.89 128 100.00 100.00 5.81e-87 GB AAC72945 "OTK27 [Homo sapiens]" 88.89 128 100.00 100.00 5.81e-87 GB AAF06959 "15.5 kD RNA binding protein [Homo sapiens]" 88.89 128 100.00 100.00 5.81e-87 GB AAH05358 "NHP2 non-histone chromosome protein 2-like 1 (S. cerevisiae) [Homo sapiens]" 88.89 128 100.00 100.00 5.81e-87 GB AAH19282 "NHP2L1 protein, partial [Homo sapiens]" 88.89 128 100.00 100.00 5.81e-87 GB AAH26755 "NHP2 non-histone chromosome protein 2-like 1 (S. cerevisiae) [Mus musculus]" 88.89 128 100.00 100.00 5.81e-87 PRF 2210268A "nuclear protein-NHP2-like protein" 88.89 128 100.00 100.00 5.81e-87 REF NP_001003796 "NHP2-like protein 1 [Homo sapiens]" 88.89 128 100.00 100.00 5.81e-87 REF NP_001070472 "NHP2-like protein 1 [Bos taurus]" 88.89 128 100.00 100.00 5.81e-87 REF NP_001177155 "NHP2-like protein 1 [Sus scrofa]" 88.89 128 100.00 100.00 5.81e-87 REF NP_001177156 "NHP2-like protein 1 [Sus scrofa]" 88.89 128 100.00 100.00 5.81e-87 REF NP_001271884 "NHP2-like protein 1 [Macaca fascicularis]" 88.89 128 100.00 100.00 5.81e-87 SP P55769 "RecName: Full=NHP2-like protein 1; AltName: Full=High mobility group-like nuclear protein 2 homolog 1; AltName: Full=OTK27; Alt" 88.89 128 100.00 100.00 5.81e-87 SP P55770 "RecName: Full=NHP2-like protein 1; AltName: Full=High mobility group-like nuclear protein 2 homolog 1; AltName: Full=OTK27; Alt" 88.89 128 100.00 100.00 5.81e-87 SP Q3B8S0 "RecName: Full=NHP2-like protein 1; AltName: Full=High mobility group-like nuclear protein 2 homolog 1; AltName: Full=U4/U6.U5 t" 88.89 128 100.00 100.00 5.81e-87 SP Q4R5C6 "RecName: Full=NHP2-like protein 1; AltName: Full=High mobility group-like nuclear protein 2 homolog 1; AltName: Full=U4/U6.U5 t" 88.89 128 100.00 100.00 5.81e-87 SP Q9D0T1 "RecName: Full=NHP2-like protein 1; AltName: Full=Fertilization antigen 1; Short=FA-1; AltName: Full=High mobility group-like nu" 88.89 128 100.00 100.00 5.81e-87 TPG DAA29093 "TPA: NHP2-like protein 1 [Bos taurus]" 88.89 128 100.00 100.00 5.81e-87 stop_ save_ #################### # Natural source # #################### save_natural_source _Saveframe_category natural_source loop_ _Mol_label _Organism_name_common _NCBI_taxonomy_ID _Superkingdom _Kingdom _Genus _Species $15.5K Human 9606 Eukaryota Metazoa Homo sapiens stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Saveframe_category experimental_source loop_ _Mol_label _Production_method _Host_organism_name_common _Genus _Species _Strain _Vector_name $15.5K 'recombinant technology' . Escherichia coli . pET11a stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $15.5K 0.8 mM '[U-99% 15N]' D2O 8 % . 'sodium azide' 0.1 % 'natural abundance' 'sodium chloride' 100 mM 'natural abundance' 'sodium phosphate' 100 mM 'natural abundance' stop_ save_ save_sample_2 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $15.5K 0.6 mM '[U-99% 15N]' D2O 95 % . H2O 5 % 'natural abundance' 'sodium chloride' 100 mM 'natural abundance' 'sodium phosphate' 100 mM 'natural abundance' stop_ save_ ############################ # Computer software used # ############################ save_Felix _Saveframe_category software _Name FELIX _Version 95.0 loop_ _Vendor _Address _Electronic_address 'Accelrys Software Inc.' . . stop_ loop_ _Task 'peak picking' processing stop_ _Details . save_ save_relxn2.2 _Saveframe_category software _Name relxn2.2 _Version . loop_ _Vendor _Address _Electronic_address 'Dr. Andrew Lee' . . stop_ loop_ _Task processing stop_ _Details 'model-free fitting' save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_spectrometer_1 _Saveframe_category NMR_spectrometer _Manufacturer Varian _Model INOVA _Field_strength 500 _Details . save_ save_spectrometer_2 _Saveframe_category NMR_spectrometer _Manufacturer Varian _Model INOVA _Field_strength 600 _Details . save_ ############################# # NMR applied experiments # ############################# save_2D_1H-15N_HSQC_1 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-15N HSQC' _Sample_label $sample_1 save_ save_2D_1H-15N_HSQC_2 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-15N HSQC' _Sample_label $sample_2 save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Saveframe_category sample_conditions _Details . loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units 'ionic strength' 200 . mM pH 6.0 . pH pressure 1 . atm temperature 293 . K stop_ save_ save_sample_conditions_2 _Saveframe_category sample_conditions _Details . loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units pD 6.52 . pH temperature 293 . K stop_ save_ save_heteronuclear_T1_list_1 _Saveframe_category T1_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 500 _T1_coherence_type Nz _T1_value_units s _Mol_system_component_name 15.5K _Text_data_format . _Text_data . loop_ _T1_ID _Residue_seq_code _Residue_label _Atom_name _T1_value _T1_value_error 1 17 MET N 0.5836 0.0109 2 18 THR N 0.6191 0.0124 3 19 GLU N 0.6036 0.0118 4 20 ALA N 0.649 0.0129 5 21 ASP N 0.6564 0.0161 6 22 VAL N 0.7212 0.0214 7 23 ASN N 0.7209 0.045 8 25 LYS N 0.7878 0.0483 9 26 ALA N 0.8132 0.0466 10 27 TYR N 0.8221 0.0635 11 30 ALA N 0.781 0.085 12 31 ASP N 0.8003 0.0534 13 32 ALA N 0.84 0.1502 14 33 HIS N 0.8639 0.0546 15 34 LEU N 0.8068 0.0729 16 35 THR N 0.8475 0.0972 17 36 LYS N 0.7752 0.0506 18 37 LYS N 0.8084 0.0589 19 38 LEU N 0.7671 0.0583 20 39 LEU N 0.7714 0.0787 21 41 LEU N 0.788 0.0541 22 45 SER N 0.8044 0.0775 23 47 ASN N 0.8548 0.049 24 48 TYR N 0.8634 0.0669 25 50 GLN N 0.7756 0.0511 26 51 LEU N 0.8465 0.0522 27 52 ARG N 0.7985 0.1054 28 53 LYS N 0.8322 0.081 29 54 GLY N 0.7787 0.0773 30 56 ASN N 1.0146 0.3616 31 59 THR N 0.7837 0.0906 32 61 THR N 0.8207 0.0631 33 62 LEU N 0.7609 0.0906 34 64 ARG N 0.8264 0.0684 35 65 GLY N 0.8192 0.068 36 66 ILE N 0.7873 0.0924 37 67 SER N 0.8077 0.0633 38 68 GLU N 0.7752 0.1993 39 69 PHE N 0.8356 0.0748 40 70 ILE N 0.7473 0.1037 41 72 MET N 0.774 0.0842 42 73 ALA N 0.7621 0.0703 43 74 ALA N 0.7751 0.0942 44 75 ASP N 0.7857 0.0538 45 76 ALA N 0.7472 0.0447 46 79 LEU N 0.8364 0.075 47 80 GLU N 0.7996 0.0528 48 81 ILE N 0.7465 0.0498 49 82 ILE N 0.8111 0.0926 50 83 LEU N 0.7835 0.0737 51 85 LEU N 0.7875 0.092 52 87 LEU N 0.7621 0.0632 53 88 LEU N 0.7506 0.0602 54 90 GLU N 0.7957 0.0552 55 91 ASP N 0.797 0.0464 56 93 ASN N 0.852 0.0623 57 96 TYR N 0.7768 0.0818 58 98 PHE N 0.7536 0.0987 59 99 VAL N 0.839 0.1136 60 100 ARG N 0.7665 0.0864 61 101 SER N 0.797 0.0562 62 102 LYS N 0.7991 0.2633 63 103 GLN N 0.7794 0.091 64 104 ALA N 0.8126 0.0584 65 105 LEU N 0.7896 0.0581 66 106 GLY N 0.8588 0.0914 67 107 ARG N 0.8384 0.05 68 108 ALA N 0.829 0.047 69 110 GLY N 0.7985 0.0531 70 111 VAL N 0.8142 0.0517 71 112 SER N 0.84 0.0827 72 113 ARG N 0.9288 0.036 73 115 VAL N 0.7786 0.0732 74 116 ILE N 0.8389 0.1367 75 118 CYS N 0.8085 0.0725 76 119 SER N 0.7611 0.0931 77 120 VAL N 0.8387 0.1071 78 121 THR N 0.7494 0.0739 79 123 LYS N 0.7468 0.0835 80 124 GLU N 0.7724 0.075 81 125 GLY N 0.8419 0.117 82 127 GLN N 0.7663 0.1147 83 128 LEU N 0.7702 0.0786 84 130 GLN N 0.8036 0.0424 85 133 GLN N 0.7782 0.0677 86 134 SER N 0.821 0.0473 87 135 ILE N 0.8431 0.0727 88 137 GLN N 0.8129 0.0573 89 138 SER N 0.8519 0.0613 90 141 ARG N 0.7896 0.0469 91 142 LEU N 0.8023 0.0639 92 143 LEU N 0.7748 0.05 93 144 VAL N 0.6701 0.0155 stop_ save_ save_heteronuclear_t1_list_2 _Saveframe_category T1_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1_coherence_type Nz _T1_value_units s _Mol_system_component_name 15.5K _Text_data_format . _Text_data . loop_ _T1_ID _Residue_seq_code _Residue_label _Atom_name _T1_value _T1_value_error 1 17 MET N 0.6463 0.004 2 18 THR N 0.6571 0.0043 3 19 GLU N 0.6568 0.0042 4 20 ALA N 0.7174 0.0047 5 21 ASP N 0.7105 0.0052 6 22 VAL N 0.7937 0.0067 7 23 ASN N 0.8162 0.0118 8 25 LYS N 0.8278 0.0114 9 26 ALA N 0.9038 0.0125 10 27 TYR N 0.929 0.0154 11 30 ALA N 0.8422 0.0175 12 31 ASP N 0.9172 0.0157 13 32 ALA N 0.951 0.05 14 33 HIS N 0.8994 0.0132 15 34 LEU N 0.893 0.0156 16 35 THR N 0.8734 0.0188 17 36 LYS N 0.8716 0.0122 18 37 LYS N 0.8927 0.0137 19 38 LEU N 0.8901 0.0146 20 39 LEU N 0.881 0.0173 21 41 LEU N 0.8986 0.0139 22 45 SER N 0.8722 0.0157 23 47 ASN N 0.8911 0.0115 24 48 TYR N 0.9294 0.0155 25 50 GLN N 0.8527 0.0123 26 51 LEU N 0.8363 0.0116 27 52 ARG N 0.8999 0.022 28 53 LYS N 0.9116 0.0183 29 54 GLY N 0.8618 0.0184 30 56 ASN N 0.8315 0.081 31 57 GLU N 0.8511 0.0145 32 59 THR N 0.8794 0.0201 33 60 LYS N 0.8365 0.0139 34 61 THR N 0.8525 0.0155 35 62 LEU N 0.8316 0.017 36 64 ARG N 0.8775 0.0154 37 65 GLY N 0.8898 0.0142 38 66 ILE N 0.8676 0.0192 39 67 SER N 0.8448 0.0134 40 68 GLU N 0.8171 0.0344 41 69 PHE N 0.9023 0.0148 42 70 ILE N 0.8823 0.0268 43 72 MET N 0.8811 0.0208 44 73 ALA N 0.852 0.0159 45 74 ALA N 0.851 0.0204 46 75 ASP N 0.8602 0.0122 47 76 ALA N 0.8161 0.0101 48 79 LEU N 0.9447 0.0172 49 80 GLU N 0.876 0.0119 50 81 ILE N 0.8213 0.012 51 82 ILE N 0.8639 0.0197 52 83 LEU N 0.8037 0.0172 53 85 LEU N 0.838 0.018 54 87 LEU N 0.8777 0.015 55 88 LEU N 0.8526 0.0139 56 90 GLU N 0.8651 0.0129 57 91 ASP N 0.8573 0.0115 58 93 ASN N 0.8849 0.0133 59 96 TYR N 0.8643 0.0193 60 98 PHE N 0.8716 0.0223 61 99 VAL N 0.8581 0.0198 62 100 ARG N 0.8653 0.0183 63 101 SER N 0.8801 0.0142 64 103 GLN N 0.8811 0.0202 65 104 ALA N 0.8694 0.0138 66 105 LEU N 0.892 0.0158 67 106 GLY N 0.8956 0.0185 68 107 ARG N 0.8844 0.0118 69 108 ALA N 0.8661 0.0118 70 110 GLY N 0.8714 0.0133 71 111 VAL N 0.8707 0.012 72 112 SER N 0.9398 0.0234 73 113 ARG N 1.0194 0.0093 74 115 VAL N 0.8747 0.0168 75 116 ILE N 0.899 0.0273 76 117 ALA N 0.8638 0.0128 77 118 CYS N 0.8988 0.0157 78 119 SER N 0.8834 0.0205 79 120 VAL N 0.8589 0.0205 80 121 THR N 0.8364 0.0164 81 122 ILE N 0.8504 0.0187 82 123 LYS N 0.8692 0.02 83 124 GLU N 0.8844 0.0215 84 125 GLY N 0.9288 0.0306 85 127 GLN N 0.8444 0.0266 86 128 LEU N 0.8501 0.0175 87 129 LYS N 0.8622 0.0141 88 130 GLN N 0.8834 0.0104 89 133 GLN N 0.8879 0.0152 90 134 SER N 0.88 0.0117 91 135 ILE N 0.88 0.0156 92 136 GLN N 0.8443 0.0122 93 137 GLN N 0.8971 0.0141 94 138 SER N 0.9088 0.0144 95 141 ARG N 0.8577 0.0112 96 142 LEU N 0.8614 0.0152 97 143 LEU N 0.867 0.0114 98 144 VAL N 0.7271 0.0043 stop_ save_ save_heteronuclear_T2_list_1 _Saveframe_category T2_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 500 _T2_coherence_type Nz _T2_value_units s _Mol_system_component_name 15.5K _Text_data_format . _Text_data . loop_ _T2_ID _Residue_seq_code _Residue_label _Atom_name _T2_value _T2_value_error _Rex_value _Rex_error 1 17 MET N 0.1859 0.0038 . . 2 18 THR N 0.1734 0.0036 . . 3 19 GLU N 0.1577 0.0032 . . 4 20 ALA N 0.1352 0.0028 . . 5 21 ASP N 0.1165 0.0028 . . 6 22 VAL N 0.0971 0.003 . . 7 23 ASN N 0.0686 0.0043 . . 8 25 LYS N 0.0618 0.0037 . . 9 26 ALA N 0.0555 0.0034 . . 10 27 TYR N 0.0612 0.0045 . . 11 30 ALA N 0.0526 0.006 . . 12 31 ASP N 0.0626 0.0042 . . 13 32 ALA N 0.0493 0.0082 . . 14 33 HIS N 0.0578 0.0036 . . 15 34 LEU N 0.0505 0.0047 . . 16 35 THR N 0.0489 0.0058 . . 17 36 LYS N 0.0493 0.0039 . . 18 37 LYS N 0.0485 0.004 . . 19 38 LEU N 0.0502 0.0042 . . 20 39 LEU N 0.0513 0.0057 . . 21 41 LEU N 0.0479 0.0037 . . 22 45 SER N 0.0482 0.0047 . . 23 47 ASN N 0.0521 0.0031 . . 24 48 TYR N 0.0533 0.004 . . 25 50 GLN N 0.0561 0.0035 . . 26 51 LEU N 0.0527 0.0034 . . 27 52 ARG N 0.053 0.007 . . 28 53 LYS N 0.0566 0.0054 . . 29 54 GLY N 0.0613 0.0064 . . 30 56 ASN N 0.0524 0.0137 . . 31 59 THR N 0.0494 0.0058 . . 32 62 LEU N 0.037 0.0052 . . 33 64 ARG N 0.0529 0.0044 . . 34 65 GLY N 0.0575 0.0045 . . 35 66 ILE N 0.0571 0.0066 . . 36 67 SER N 0.0525 0.0039 . . 37 68 GLU N 0.0557 0.0137 . . 38 69 PHE N 0.0527 0.0046 . . 39 70 ILE N 0.0508 0.0074 . . 40 72 MET N 0.0643 0.0067 . . 41 73 ALA N 0.051 0.0051 . . 42 74 ALA N 0.0513 0.0067 . . 43 75 ASP N 0.0509 0.0036 . . 44 76 ALA N 0.051 0.0033 . . 45 79 LEU N 0.0566 0.0051 . . 46 80 GLU N 0.0532 0.0036 . . 47 81 ILE N 0.0494 0.0037 . . 48 82 ILE N 0.0503 0.0059 . . 49 83 LEU N 0.0547 0.0053 . . 50 85 LEU N 0.0454 0.0056 . . 51 87 LEU N 0.0574 0.005 . . 52 88 LEU N 0.0507 0.0044 . . 53 90 GLU N 0.0547 0.0039 . . 54 91 ASP N 0.054 0.0033 . . 55 93 ASN N 0.0536 0.0039 . . 56 96 TYR N 0.0489 0.0055 . . 57 98 PHE N 0.0517 0.0073 . . 58 99 VAL N 0.058 0.0078 . . 59 100 ARG N 0.0579 0.0066 . . 60 101 SER N 0.0595 0.0044 . . 61 102 LYS N 0.0569 0.0193 . . 62 103 GLN N 0.0513 0.0059 . . 63 104 ALA N 0.0527 0.0042 . . 64 105 LEU N 0.0509 0.0041 . . 65 106 GLY N 0.0526 0.0058 . . 66 107 ARG N 0.0489 0.0033 . . 67 108 ALA N 0.049 0.0032 . . 68 110 GLY N 0.0555 0.0038 . . 69 111 VAL N 0.0546 0.0038 . . 70 112 SER N 0.0566 0.0052 . . 71 113 ARG N 0.078 0.0029 . . 72 115 VAL N 0.0517 0.0053 . . 73 116 ILE N 0.053 0.0084 . . 74 118 CYS N 0.0523 0.0047 . . 75 119 SER N 0.0526 0.0066 . . 76 120 VAL N 0.0528 0.0068 . . 77 121 THR N 0.0598 0.0058 . . 78 123 LYS N 0.0587 0.0067 . . 79 124 GLU N 0.0606 0.0058 . . 80 125 GLY N 0.0582 0.0069 . . 81 127 GLN N 0.0614 0.0081 . . 82 128 LEU N 0.0546 0.0054 . . 83 130 GLN N 0.0518 0.0028 . . 84 133 GLN N 0.0442 0.0042 . . 85 135 ILE N 0.0477 0.0043 . . 86 137 GLN N 0.0509 0.0038 . . 87 138 SER N 0.0509 0.0039 . . 88 141 ARG N 0.0513 0.0033 . . 89 142 LEU N 0.0512 0.0044 . . 90 143 LEU N 0.0592 0.004 . . 91 144 VAL N 0.114 0.0027 . . stop_ save_ save_heteronuclear_t2_list_2 _Saveframe_category T2_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T2_coherence_type Nz _T2_value_units s _Mol_system_component_name 15.5K _Text_data_format . _Text_data . loop_ _T2_ID _Residue_seq_code _Residue_label _Atom_name _T2_value _T2_value_error _Rex_value _Rex_error 1 17 MET N 0.1998 0.0031 . . 2 18 THR N 0.1865 0.003 . . 3 19 GLU N 0.1733 0.0026 . . 4 20 ALA N 0.1532 0.0022 . . 5 21 ASP N 0.1304 0.002 . . 6 22 VAL N 0.1083 0.0017 . . 7 23 ASN N 0.0834 0.0021 . . 8 25 LYS N 0.0735 0.0017 . . 9 26 ALA N 0.0676 0.0016 . . 10 27 TYR N 0.0717 0.0022 . . 11 30 ALA N 0.0649 0.0024 . . 12 31 ASP N 0.0706 0.002 . . 13 32 ALA N 0.0581 0.0055 . . 14 33 HIS N 0.0685 0.0016 . . 15 34 LEU N 0.0598 0.0019 . . 16 35 THR N 0.0613 0.0023 . . 17 36 LYS N 0.0622 0.0015 . . 18 37 LYS N 0.0627 0.0017 . . 19 38 LEU N 0.0593 0.0017 . . 20 39 LEU N 0.0619 0.0021 . . 21 41 LEU N 0.0552 0.0015 . . 22 45 SER N 0.0607 0.002 . . 23 47 ASN N 0.063 0.0014 . . 24 48 TYR N 0.0669 0.0018 . . 25 50 GLN N 0.0719 0.0018 . . 26 51 LEU N 0.0569 0.0014 . . 27 52 ARG N 0.0694 0.0029 . . 28 53 LYS N 0.0675 0.0024 . . 29 54 GLY N 0.0663 0.0025 . . 30 56 ASN N 0.0584 0.0102 . . 31 57 GLU N 0.0743 0.0022 . . 32 59 THR N 0.0626 0.0023 . . 33 60 LYS N 0.063 0.0017 . . 34 61 THR N 0.0631 0.0019 . . 35 62 LEU N 0.0631 0.0022 . . 36 64 ARG N 0.0714 0.002 . . 37 65 GLY N 0.0731 0.002 . . 38 66 ILE N 0.073 0.0027 . . 39 67 SER N 0.0673 0.0018 . . 40 68 GLU N 0.0688 0.0047 . . 41 69 PHE N 0.0692 0.002 . . 42 70 ILE N 0.0628 0.0032 . . 43 72 MET N 0.0699 0.0027 . . 44 73 ALA N 0.0649 0.0021 . . 45 74 ALA N 0.0673 0.0028 . . 46 75 ASP N 0.0652 0.0016 . . 47 76 ALA N 0.0616 0.0014 . . 48 79 LEU N 0.0718 0.0022 . . 49 80 GLU N 0.0683 0.0017 . . 50 81 ILE N 0.0604 0.0016 . . 51 82 ILE N 0.0657 0.0026 . . 52 83 LEU N 0.0533 0.0022 . . 53 85 LEU N 0.0626 0.0023 . . 54 87 LEU N 0.0725 0.0021 . . 55 88 LEU N 0.0634 0.0017 . . 56 90 GLU N 0.0653 0.0017 . . 57 91 ASP N 0.0706 0.0016 . . 58 93 ASN N 0.0648 0.0016 . . 59 96 TYR N 0.0623 0.0025 . . 60 98 PHE N 0.0624 0.0027 . . 61 99 VAL N 0.0739 0.0031 . . 62 100 ARG N 0.0646 0.0024 . . 63 101 SER N 0.069 0.0018 . . 64 103 GLN N 0.0617 0.0024 . . 65 104 ALA N 0.0672 0.0018 . . 66 105 LEU N 0.0587 0.0018 . . 67 106 GLY N 0.0603 0.0021 . . 68 107 ARG N 0.0564 0.0013 . . 69 108 ALA N 0.0611 0.0014 . . 70 110 GLY N 0.063 0.0016 . . 71 111 VAL N 0.0683 0.0016 . . 72 112 SER N 0.0714 0.0029 . . 73 113 ARG N 0.0898 0.0014 . . 74 115 VAL N 0.0647 0.0022 . . 75 116 ILE N 0.0724 0.0035 . . 76 117 ALA N 0.0607 0.0016 . . 77 118 CYS N 0.0644 0.002 . . 78 119 SER N 0.0675 0.0026 . . 79 120 VAL N 0.0604 0.0025 . . 80 121 THR N 0.0658 0.0022 . . 81 122 ILE N 0.0744 0.0025 . . 82 123 LYS N 0.0654 0.0026 . . 83 124 GLU N 0.0702 0.0031 . . 84 125 GLY N 0.0737 0.0041 . . 85 127 GLN N 0.0722 0.0041 . . 86 128 LEU N 0.0688 0.0024 . . 87 129 LYS N 0.0484 0.0015 . . 88 130 GLN N 0.0653 0.0014 . . 89 133 GLN N 0.0594 0.0018 . . 90 134 SER N 0.0641 0.0014 . . 91 135 ILE N 0.0587 0.0018 . . 92 136 GLN N 0.0943 0.0024 . . 93 137 GLN N 0.0654 0.0018 . . 94 138 SER N 0.0651 0.0017 . . 95 141 ARG N 0.0655 0.0015 . . 96 142 LEU N 0.0642 0.0019 . . 97 143 LEU N 0.0735 0.0017 . . 98 144 VAL N 0.1354 0.0017 . . stop_ save_ save_heteronuclear_noe_list_1 _Saveframe_category heteronuclear_NOE _Details . loop_ _Experiment_label '2D 1H-15N HSQC' stop_ loop_ _Sample_label . stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 500 _Mol_system_component_name 15.5K _Atom_one_atom_name N _Atom_two_atom_name H _Heteronuclear_NOE_value_type 'relative intensities' _NOE_reference_value 2000 _NOE_reference_description 'Baseplane noise measurement' _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Heteronuclear_NOE_value _Heteronuclear_NOE_value_error 17 MET 0.1167734 0.0124022 18 THR 0.0328136 0.0121787 19 GLU 0.1610441 0.0127788 20 ALA 0.1235451 0.0125868 21 ASP 0.270137 0.0150203 22 VAL 0.3250851 0.0187462 23 ASN 0.4736995 0.0351426 25 LYS 0.6511292 0.0325745 26 ALA 0.7137361 0.031881 27 TYR 0.7012066 0.0379078 30 ALA 0.7393995 0.0547704 31 ASP 0.6891091 0.0332791 32 ALA 0.7477812 0.0556866 33 HIS 0.7300988 0.0285172 34 LEU 0.7918822 0.0463433 35 THR 0.884824 0.0591887 36 LYS 0.7713461 0.0398873 37 LYS 0.7537113 0.0387182 38 LEU 0.662607 0.0370904 39 LEU 0.7645566 0.0515888 41 LEU 0.6973547 0.0351838 45 SER 0.851222 0.0494237 47 ASN 0.6569102 0.0270043 48 TYR 0.7173518 0.0332881 50 GLN 0.736168 0.0310544 51 LEU 0.7121181 0.0298266 52 ARG 0.7163311 0.0524547 53 LYS 0.863872 0.0529792 54 GLY 0.6618114 0.0433935 56 ASN 0.5489223 0.0705117 59 THR 0.8353813 0.0455763 60 LYS 0.7526857 0.0371914 62 LEU 0.8181033 0.0540657 64 ARG 0.8247297 0.0411157 65 GLY 0.7548732 0.0350171 66 ILE 0.7811744 0.0496196 67 SER 0.8468966 0.0366606 68 GLU 0.7609984 0.0825488 69 PHE 0.805213 0.0400575 70 ILE 0.7364981 0.0579267 72 MET 0.5947284 0.0433232 73 ALA 0.7991094 0.0495641 74 ALA 0.6886392 0.0548635 75 ASP 0.7875299 0.0368578 76 ALA 0.7894626 0.0352463 79 LEU 0.6704895 0.041833 80 GLU 0.742331 0.0376962 81 ILE 0.6480404 0.0336987 82 ILE 0.7273574 0.0494793 83 LEU 0.7798306 0.047316 85 LEU 0.7540214 0.0460261 87 LEU 0.7079179 0.0422729 88 LEU 0.6976225 0.0399562 91 ASP 0.6732117 0.0279075 93 ASN 0.665246 0.0299591 96 TYR 0.8086199 0.0595601 98 PHE 0.6930575 0.0575752 99 VAL 0.7408852 0.0589847 100 ARG 0.8232126 0.057603 101 SER 0.7239723 0.0330106 102 LYS 0.8272467 0.1429245 103 GLN 0.8101242 0.0521958 104 ALA 0.7783837 0.0332325 106 GLY 0.7321889 0.0462342 107 ARG 0.7549911 0.0329469 108 ALA 0.8271925 0.0308398 110 GLY 0.7538946 0.0313306 111 VAL 0.7647952 0.0351198 112 SER 0.6743358 0.0397932 113 ARG 0.4869887 0.0210253 115 VAL 0.6154131 0.0401759 116 ILE 0.7671061 0.0670768 118 CYS 0.7792954 0.0435339 119 SER 0.7851172 0.054 120 VAL 0.7612705 0.0517552 121 THR 0.7042131 0.0411218 123 LYS 0.7556027 0.0479103 124 GLU 0.7717857 0.0424511 125 GLY 0.604816 0.0426849 127 GLN 0.66697 0.0530264 128 LEU 0.7990865 0.0447079 130 GLN 0.7979011 0.0281863 133 GLN 0.872839 0.0485366 134 SER 0.7718035 0.0294866 135 ILE 0.7529706 0.040372 137 GLN 0.7554936 0.0320546 138 SER 0.6577691 0.0302688 141 ARG 0.7985535 0.0338792 142 LEU 0.7334569 0.0392823 143 LEU 0.6558922 0.033127 144 VAL 0.147421 0.0141565 stop_ save_ save_heteronuclear_noe_list_2 _Saveframe_category heteronuclear_NOE _Details . loop_ _Experiment_label '2D 1H-15N HSQC' stop_ loop_ _Sample_label . stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _Mol_system_component_name 15.5K _Atom_one_atom_name N _Atom_two_atom_name H _Heteronuclear_NOE_value_type 'relative intensities' _NOE_reference_value 1500 _NOE_reference_description 'baseplane mean noise level' _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Heteronuclear_NOE_value _Heteronuclear_NOE_value_error 17 MET 0.1762539 0.0117503 18 THR 0.1794125 0.0129656 19 GLU 0.2280505 0.012736 20 ALA 0.1738227 0.0140687 21 ASP 0.3407168 0.0143862 22 VAL 0.377273 0.0166233 23 ASN 0.5214731 0.0244913 25 LYS 0.6322744 0.0233491 26 ALA 0.6242089 0.0236888 27 TYR 0.7376401 0.0284315 30 ALA 0.8015922 0.0341467 31 ASP 0.7228355 0.0246943 32 ALA 0.808473 0.0490357 33 HIS 0.8157986 0.0242697 34 LEU 0.8005082 0.0290623 35 THR 0.768654 0.0324099 36 LYS 0.7560502 0.0241987 37 LYS 0.8169903 0.0278892 38 LEU 0.7530488 0.0262113 39 LEU 0.7833434 0.0315395 41 LEU 0.8090914 0.0262221 45 SER 0.8220652 0.0301737 47 ASN 0.8161519 0.0221211 48 TYR 0.7716898 0.0265306 50 GLN 0.7531904 0.0238127 51 LEU 1.103264 0.0298754 52 ARG 0.7804552 0.0329636 53 LYS 0.7935073 0.0304748 54 GLY 0.8029344 0.0337713 56 ASN 0.8381737 0.0737069 57 GLU 0.4418795 0.0159772 59 THR 0.7927999 0.0311334 60 LYS 0.8406113 0.0270275 61 THR 0.7919878 0.0262868 62 LEU 0.7574532 0.0302565 64 ARG 0.7675026 0.0273621 65 GLY 0.793078 0.0258233 66 ILE 0.7977569 0.0324546 67 SER 0.7956108 0.0258153 68 GLU 0.7937472 0.0490255 69 PHE 0.7878584 0.0251989 70 ILE 0.8519548 0.0434523 72 MET 0.7377868 0.0360083 73 ALA 0.7541131 0.0294179 74 ALA 0.8003132 0.0378933 75 ASP 0.8229191 0.02542 76 ALA 0.8650809 0.0245488 79 LEU 0.7402585 0.0298235 80 GLU 0.758374 0.0247107 81 ILE 0.7330647 0.0264937 82 ILE 0.7626682 0.034917 83 LEU 1.160119 0.0417672 85 LEU 0.836879 0.0329469 87 LEU 0.7192651 0.0276522 88 LEU 0.7841647 0.027133 90 GLU 0.7498407 0.0219901 91 ASP 0.7889494 0.024028 93 ASN 0.7448253 0.0254224 94 VAL 0.7739514 0.0169125 96 TYR 0.7831696 0.03502 98 PHE 0.79129 0.038424 99 VAL 0.7980547 0.0344572 100 ARG 0.8078123 0.0319687 101 SER 0.8408121 0.0271174 103 GLN 0.786824 0.03176 105 LEU 0.7458159 0.0261813 106 GLY 0.7986084 0.0318434 107 ARG 0.7943165 0.0231324 110 GLY 0.7729318 0.0248608 111 VAL 0.7762496 0.023184 112 SER 0.66934 0.0283999 113 ARG 0.533134 0.01526 115 VAL 0.765058 0.0277826 116 ILE 0.7910511 0.0420821 117 ALA 0.8079818 0.0251439 118 CYS 0.7600079 0.0278485 119 SER 0.8174841 0.0346468 120 VAL 0.822257 0.0348798 121 THR 0.8051521 0.0285006 123 LYS 0.7708178 0.0315728 124 GLU 0.7544097 0.0300492 125 GLY 0.6700287 0.0337076 127 GLN 0.6167448 0.03355 128 LEU 0.73629 0.029968 129 LYS 0.8676507 0.0247493 130 GLN 0.7403266 0.0171345 133 GLN 0.8044739 0.026321 134 SER 0.8302156 0.0235522 135 ILE 0.7965128 0.0284652 137 GLN 0.8161854 0.0263514 138 SER 0.741752 0.0260457 141 ARG 0.7698381 0.0237703 142 LEU 0.7649573 0.0328283 143 LEU 0.6508988 0.0220377 144 VAL 0.2094722 0.01172 stop_ save_ save_order_parameter_list_1 _Saveframe_category S2_parameters _Details 'for tm= 11.75ns' loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Mol_system_component_name 15.5K _Tau_e_value_units . _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Atom_name _Model_fit _S2_value _S2_value_fit_error _Tau_e_value _Tau_e_value_fit_error _S2f_value _S2f_value_fit_error _S2s_value _S2s_value_fit_error _Tau_s_value _Tau_s_value_fit_error _S2H_value _S2H_value_fit_error _S2N_value _S2N_value_fit_error 17 MET N . 0.402 . . . . . . . . . . . . . 18 THR N . 0.407 . . . . . . . . . . . . . 19 GLU N . 0.453 . . . . . . . . . . . . . 20 ALA N . 0.548 . . . . . . . . . . . . . 21 ASP N . 0.613 . . . . . . . . . . . . . 22 VAL N . 0.739 . . . . . . . . . . . . . 23 ASN N . 0.846 . . . . . . . . . . . . . 25 LYS N . 0.908 . . . . . . . . . . . . . 26 ALA N . 0.881 . . . . . . . . . . . . . 27 TYR N . 0.862 . . . . . . . . . . . . . 30 ALA N . 0.959 . . . . . . . . . . . . . 31 ASP N . 0.868 . . . . . . . . . . . . . 32 ALA N . 0.864 . . . . . . . . . . . . . 33 HIS N . 0.899 . . . . . . . . . . . . . 34 LEU N . 0.922 . . . . . . . . . . . . . 35 THR N . 0.951 . . . . . . . . . . . . . 36 LYS N . 0.943 . . . . . . . . . . . . . 37 LYS N . 0.934 . . . . . . . . . . . . . 38 LEU N . 0.910 . . . . . . . . . . . . . 39 LEU N . 0.940 . . . . . . . . . . . . . 41 LEU N . 0.911 . . . . . . . . . . . . . 45 SER N . 0.961 . . . . . . . . . . . . . 47 ASN N . 0.914 . . . . . . . . . . . . . 48 TYR N . 0.885 . . . . . . . . . . . . . 50 GLN N . 0.926 . . . . . . . . . . . . . 51 LEU N . 1.020 . . . . . . . . . . . . . 52 ARG N . 0.899 . . . . . . . . . . . . . 53 LYS N . 0.900 . . . . . . . . . . . . . 54 GLY N . 0.930 . . . . . . . . . . . . . 56 ASN N . 0.973 . . . . . . . . . . . . . 57 GLU N . 0.844 . . . . . . . . . . . . . 59 THR N . 0.945 . . . . . . . . . . . . . 60 LYS N . 0.961 . . . . . . . . . . . . . 61 THR N . 0.941 . . . . . . . . . . . . . 62 LEU N . 0.959 . . . . . . . . . . . . . 64 ARG N . 0.911 . . . . . . . . . . . . . 65 GLY N . 0.896 . . . . . . . . . . . . . 66 ILE N . 0.915 . . . . . . . . . . . . . 67 SER N . 0.956 . . . . . . . . . . . . . 69 PHE N . 0.902 . . . . . . . . . . . . . 70 ILE N . 0.944 . . . . . . . . . . . . . 72 MET N . 0.890 . . . . . . . . . . . . . 73 ALA N . 0.949 . . . . . . . . . . . . . 74 ALA N . 0.943 . . . . . . . . . . . . . 75 ASP N . 0.952 . . . . . . . . . . . . . 76 ALA N . 0.990 . . . . . . . . . . . . . 79 LEU N . 0.851 . . . . . . . . . . . . . 80 GLU N . 0.919 . . . . . . . . . . . . . 81 ILE N . 0.952 . . . . . . . . . . . . . 82 ILE N . 0.937 . . . . . . . . . . . . . 83 LEU N . 0.909 . . . . . . . . . . . . . 85 LEU N . 0.968 . . . . . . . . . . . . . 87 LEU N . 0.895 . . . . . . . . . . . . . 88 LEU N . 0.953 . . . . . . . . . . . . . 90 GLU N . 0.933 . . . . . . . . . . . . . 91 ASP N . 0.924 . . . . . . . . . . . . . 93 ASN N . 0.914 . . . . . . . . . . . . . 96 TYR N . 0.956 . . . . . . . . . . . . . 98 PHE N . 0.943 . . . . . . . . . . . . . 99 VAL N . 0.922 . . . . . . . . . . . . . 100 ARG N . 0.943 . . . . . . . . . . . . . 101 SER N . 0.913 . . . . . . . . . . . . . 102 LYS N . 0.936 . . . . . . . . . . . . . 103 GLN N . 0.944 . . . . . . . . . . . . . 104 ALA N . 0.928 . . . . . . . . . . . . . 105 LEU N . 0.910 . . . . . . . . . . . . . 106 GLY N . 0.914 . . . . . . . . . . . . . 107 ARG N . 0.925 . . . . . . . . . . . . . 108 ALA N . 0.953 . . . . . . . . . . . . . 110 GLY N . 0.938 . . . . . . . . . . . . . 111 VAL N . 0.922 . . . . . . . . . . . . . 112 SER N . 0.853 . . . . . . . . . . . . . 113 ARG N . 0.726 . . . . . . . . . . . . . 115 VAL N . 0.922 . . . . . . . . . . . . . 116 ILE N . 0.892 . . . . . . . . . . . . . 117 ALA N . 0.931 . . . . . . . . . . . . . 118 CYS N . 0.916 . . . . . . . . . . . . . 119 SER N . 0.923 . . . . . . . . . . . . . 120 VAL N . 0.964 . . . . . . . . . . . . . 121 THR N . 0.953 . . . . . . . . . . . . . 123 LYS N . 0.930 . . . . . . . . . . . . . 124 GLU N . 0.906 . . . . . . . . . . . . . 125 GLY N . 0.851 . . . . . . . . . . . . . 127 GLN N . 0.902 . . . . . . . . . . . . . 128 LEU N . 0.935 . . . . . . . . . . . . . 129 LYS N . 0.938 . . . . . . . . . . . . . 130 GLN N . 0.925 . . . . . . . . . . . . . 133 GLN N . 0.933 . . . . . . . . . . . . . 135 ILE N . 0.932 . . . . . . . . . . . . . 137 GLN N . 0.921 . . . . . . . . . . . . . 138 SER N . 0.886 . . . . . . . . . . . . . 141 ARG N . 0.946 . . . . . . . . . . . . . 142 LEU N . 0.943 . . . . . . . . . . . . . 143 LEU N . 0.889 . . . . . . . . . . . . . 144 VAL N . 0.587 . . . . . . . . . . . . . stop_ _Tau_s_value_units . save_ save_H_exch_rate_list_1 _Saveframe_category H_exchange_rates _Details . loop_ _Sample_label $sample_2 stop_ _Sample_conditions_label $sample_conditions_2 _H_exchange_rate_units min-1 _Mol_system_component_name 15.5K _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Atom_name _H_exchange_rate_value _H_exchange_rate_min_value _H_exchange_rate_max_value _H_exchange_rate_value_error 27 TYR H 1.75E-02 . . . 30 ALA H 3.34E-03 . . . 35 THR H 9.10E-03 . . . 36 LYS H 6.86E-02 . . . 37 LYS H 6.42E-03 . . . 38 LEU H 4.13E-04 . . . 39 LEU H 2.93E-04 . . . 41 LEU H 1.84E-04 . . . 43 GLN H 4.59E-04 . . . 45 SER H 1.37E-02 . . . 48 TYR H 8.87E-02 . . . 50 GLN H 2.45E-02 . . . 52 ARG H 5.10E-03 . . . 59 THR H 1.43E-03 . . . 60 LYS H 1.19E-02 . . . 61 THR H 8.55E-03 . . . 62 LEU H 5.85E-03 . . . 66 ILE H 5.34E-03 . . . 67 SER H 2.66E-02 . . . 68 GLU H 9.40E-04 . . . 69 PHE H 1.73E-04 . . . 70 ILE H 1.51E-04 . . . 72 MET H 3.35E-04 . . . 73 ALA H 5.05E-04 . . . 74 ALA H 9.22E-04 . . . 75 ASP H 6.30E-03 . . . 76 ALA H 6.23E-03 . . . 81 ILE H 7.67E-03 . . . 82 ILE H 9.22E-03 . . . 83 LEU H 8.16E-03 . . . 87 LEU H 5.13E-03 . . . 88 LEU H 6.74E-04 . . . 90 GLU H 4.92E-03 . . . 91 ASP H 1.73E-02 . . . 93 ASN H 4.72E-02 . . . 96 TYR H 3.15E-04 . . . 98 PHE H 3.22E-04 . . . 99 VAL H 2.49E-04 . . . 102 LYS H 1.90E-02 . . . 105 LEU H 9.29E-04 . . . 106 GLY H 1.25E-03 . . . 107 ARG H 1.45E-03 . . . 108 ALA H 1.34E-03 . . . 110 GLY H 1.84E-02 . . . 111 VAL H 9.53E-03 . . . 115 VAL H 7.89E-04 . . . 116 ILE H 1.22E-02 . . . 117 ALA H 9.84E-04 . . . 118 CYS H 1.10E-03 . . . 119 SER H 1.50E-03 . . . 120 VAL H 7.55E-04 . . . 121 THR H 9.49E-04 . . . 133 GLN H 1.34E-02 . . . 135 ILE H 1.02E-02 . . . 136 GLN H 3.07E-03 . . . 137 GLN H 5.25E-02 . . . 138 SER H 2.88E-02 . . . 141 ARG H 3.42E-02 . . . 142 LEU H 2.46E-02 . . . 143 LEU H 6.54E-03 . . . 144 VAL H 2.69E-02 . . . stop_ save_ save_H_exch_protection_factor_list_1 _Saveframe_category H_exchange_protection_factors _Details . _Sample_label $sample_conditions_2 _Sample_conditions_label $sample_conditions_2 _Standard_values_source_citation_label $entry_citation _Mol_system_component_name 15.5K _Text_data_format . _Text_data . loop_ _Residue_seq_code _Residue_label _Atom_name _H_exchange_protection_factor_value _H_exchange_protection_factor_value_error 27 TYR H 3.006385081 . 30 ALA H 3.787188706 . 35 THR H 3.285353904 . 36 LYS H 2.843837286 . 37 LYS H 3.792947194 . 38 LEU H 4.448106693 . 39 LEU H 4.266998058 . 41 LEU H 4.516740126 . 43 GLN H 4.778507291 . 45 SER H 3.952744022 . 48 TYR H 2.622295168 . 50 GLN H 3.310894103 . 52 ARG H 3.679812214 . 59 THR H 4.298516968 . 60 LYS H 3.604867599 . 61 THR H 3.642241265 . 62 LEU H 3.376857541 . 66 ILE H 3.233117469 . 67 SER H 3.236186491 . 68 GLU H 4.380079821 . 69 PHE H 4.920700638 . 70 ILE H 4.675432919 . 72 MET H 4.846804022 . 73 ALA H 4.927123239 . 74 ALA H 4.555636693 . 75 ASP H 3.451126073 . 76 ALA H 3.563628298 . 81 ILE H 2.78 . 82 ILE H 2.595683677 . 83 LEU H 2.802258899 . 87 LEU H 2.994044643 . 88 LEU H 3.905437696 . 90 GLU H 3.911919142 . 91 ASP H 2.89 . 93 ASN H 3.45619661 . 96 TYR H 4.512655964 . 98 PHE H 4.636564421 . 99 VAL H 4.485063664 . 102 LYS H 3.501211245 . 105 LEU H 3.975959322 . 106 GLY H 4.480408874 . 107 ARG H 4.605459432 . 108 ALA H 4.613958484 . 110 GLY H 4.072140789 . 111 VAL H 3.01 . 115 VAL H 3.681293158 . 116 ILE H 2.57 . 117 ALA H 4.297331261 . 118 CYS H 5.099021876 . 119 SER H 5.265192752 . 120 VAL H 4.240083432 . 121 THR H 4.336798862 . 133 GLN H 3.224608113 . 135 ILE H 3.08307115 . 136 GLN H 3.86299336 . 137 GLN H 3.059924498 . 138 SER H 3.630569916 . 141 ARG H 2.937170981 . 142 LEU H 2.773579992 . 143 LEU H 2.92 . 144 VAL H 0.379476739 . stop_ save_