sample:  15N PfR48
conc:    ca. 0.5 mM
buffer:  20mM MES, 100mM NaCl, 5mM CaCl2, 10mM DTT
         0.02% azide, 100% D20
         pH 6.5   20C
prepared by: Rong
experiment:  gNhsqc 10 min.
instrument:  INOVA 600  probe 4477
acquired by:   jma

02/10/04
first time point of H/D exchange

ni=64; nt=4; 10min expts