Content for NMR-STAR saveframe, "T1_list_1"
save_T1_list_1
_Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation
_Heteronucl_T1_list.Sf_framecode T1_list_1
_Heteronucl_T1_list.Entry_ID 6758
_Heteronucl_T1_list.ID 1
_Heteronucl_T1_list.Sample_condition_list_ID 1
_Heteronucl_T1_list.Sample_condition_list_label $conditions_1
_Heteronucl_T1_list.Spectrometer_frequency_1H 599.7
_Heteronucl_T1_list.T1_coherence_type 'single quantum'
_Heteronucl_T1_list.T1_val_units s
_Heteronucl_T1_list.Details
;
15N longitudinal T1 relaxation times were measured by the inversion-recovery
method (????????) using standard water flip-back methods [Grzesiek, S., and
Bax, A. (1993) J. Am. Chem. Soc. 115, 12594.]. Spectra was recorded as 128 x
512 complex matrices, with spectral widths of 8385 (1H) and 2200 (15N) Hz, with
16 scans per FID. Relaxation delays collected were: 0.03, 0.05, 0.07, 0.09,
0.20, 0.50, 0.70, 1.0, 1.3, 1.6 s. Duplicate spectra were recorded for 0.03 and
0.05 s to estimate the precision of peak intensities.
;
_Heteronucl_T1_list.Text_data_format .
_Heteronucl_T1_list.Text_data .
loop_
_Heteronucl_T1_experiment.Experiment_ID
_Heteronucl_T1_experiment.Experiment_name
_Heteronucl_T1_experiment.Sample_ID
_Heteronucl_T1_experiment.Sample_label
_Heteronucl_T1_experiment.Sample_state
_Heteronucl_T1_experiment.Entry_ID
_Heteronucl_T1_experiment.Heteronucl_T1_list_ID
8 2D_1H-15N_HSQC_(T1_flag) 1 $sample_1 isotropic 6758 1
stop_
loop_
_Heteronucl_T1_software.Software_ID
_Heteronucl_T1_software.Software_label
_Heteronucl_T1_software.Method_ID
_Heteronucl_T1_software.Method_label
_Heteronucl_T1_software.Entry_ID
_Heteronucl_T1_software.Heteronucl_T1_list_ID
1 $software_1 . . 6758 1
2 $software_2 . . 6758 1
stop_
loop_
_T1.ID
_T1.Assembly_atom_ID
_T1.Entity_assembly_ID
_T1.Entity_ID
_T1.Comp_index_ID
_T1.Seq_ID
_T1.Comp_ID
_T1.Atom_ID
_T1.Atom_type
_T1.Atom_isotope_number
_T1.Val
_T1.Val_err
_T1.Resonance_ID
_T1.Auth_entity_assembly_ID
_T1.Auth_seq_ID
_T1.Auth_comp_ID
_T1.Auth_atom_ID
_T1.Entry_ID
_T1.Heteronucl_T1_list_ID
1 . 1 1 12 12 ASP N N 15 0.833402784 0.00686274 . . . . . 6758 1
2 . 1 1 13 13 LEU N N 15 0.579743753 0.007351885 . . . . . 6758 1
3 . 1 1 16 16 PHE N N 15 1.063829787 0.011554663 . . . . . 6758 1
4 . 1 1 17 17 ARG N N 15 1.065076153 0.021644125 . . . . . 6758 1
5 . 1 1 18 18 VAL N N 15 0.987459267 0.010544725 . . . . . 6758 1
6 . 1 1 19 19 ALA N N 15 0.965903603 0.007901052 . . . . . 6758 1
7 . 1 1 20 20 THR N N 15 0.962278676 0.01380722 . . . . . 6758 1
8 . 1 1 21 21 TRP N N 15 0.954289531 0.053774985 . . . . . 6758 1
9 . 1 1 23 23 LEU N N 15 0.924812725 0.012482241 . . . . . 6758 1
10 . 1 1 25 25 GLY N N 15 1.072156106 0.06537091 . . . . . 6758 1
11 . 1 1 29 29 THR N N 15 0.956388676 0.01326128 . . . . . 6758 1
12 . 1 1 35 35 ASN N N 15 1.065984437 0.039598759 . . . . . 6758 1
13 . 1 1 36 36 ILE N N 15 0.991866693 0.007433797 . . . . . 6758 1
14 . 1 1 41 41 LEU N N 15 0.952925481 0.005571595 . . . . . 6758 1
15 . 1 1 42 42 ILE N N 15 0.981257973 0.092164097 . . . . . 6758 1
16 . 1 1 43 43 SER N N 15 1.01461039 0.010715151 . . . . . 6758 1
17 . 1 1 44 44 GLY N N 15 0.859328005 0.018403935 . . . . . 6758 1
18 . 1 1 45 45 GLU N N 15 0.988630746 0.006097195 . . . . . 6758 1
19 . 1 1 46 46 ASN N N 15 1.067235859 0.00791735 . . . . . 6758 1
20 . 1 1 47 47 ALA N N 15 1.02124183 0.007247319 . . . . . 6758 1
21 . 1 1 49 49 ASP N N 15 1.018848701 0.01112349 . . . . . 6758 1
22 . 1 1 50 50 ILE N N 15 1.053962901 0.00603286 . . . . . 6758 1
23 . 1 1 51 51 LEU N N 15 0.998103603 0.018466489 . . . . . 6758 1
24 . 1 1 52 52 ALA N N 15 0.835770999 0.023114168 . . . . . 6758 1
25 . 1 1 53 53 VAL N N 15 1.019160212 0.013044577 . . . . . 6758 1
26 . 1 1 55 55 GLU N N 15 1.007049345 0.008901076 . . . . . 6758 1
27 . 1 1 56 56 ALA N N 15 1.00532824 0.009179217 . . . . . 6758 1
28 . 1 1 62 62 THR N N 15 0.964971533 0.0168645 . . . . . 6758 1
29 . 1 1 63 63 ALA N N 15 0.958956655 0.000920481 . . . . . 6758 1
30 . 1 1 64 64 VAL N N 15 1.090631476 0.012755924 . . . . . 6758 1
31 . 1 1 65 65 ASP N N 15 1.076194576 0.006408001 . . . . . 6758 1
32 . 1 1 66 66 THR N N 15 0.690894017 0.010712662 . . . . . 6758 1
33 . 1 1 67 67 GLY N N 15 0.969367972 0.00292177 . . . . . 6758 1
34 . 1 1 68 68 ARG N N 15 0.914829384 0.007254525 . . . . . 6758 1
35 . 1 1 69 69 VAL N N 15 1.013993105 0.011647921 . . . . . 6758 1
36 . 1 1 70 70 ILE N N 15 1.096852035 0.023721699 . . . . . 6758 1
37 . 1 1 72 72 SER N N 15 0.968616815 0.006802615 . . . . . 6758 1
38 . 1 1 74 74 GLY N N 15 0.855871277 0.005084384 . . . . . 6758 1
39 . 1 1 75 75 ILE N N 15 0.986874568 0.016839173 . . . . . 6758 1
40 . 1 1 78 78 ARG N N 15 0.971817298 0.002841571 . . . . . 6758 1
41 . 1 1 79 79 GLU N N 15 1.023646228 0.014236491 . . . . . 6758 1
42 . 1 1 80 80 LEU N N 15 0.964227172 0.024990357 . . . . . 6758 1
43 . 1 1 81 81 ILE N N 15 1.579030475 0.039092502 . . . . . 6758 1
44 . 1 1 84 84 LEU N N 15 0.988728495 0.012773758 . . . . . 6758 1
45 . 1 1 85 85 SER N N 15 0.883002208 0.017817538 . . . . . 6758 1
46 . 1 1 86 86 THR N N 15 0.950931913 0.03380467 . . . . . 6758 1
47 . 1 1 89 89 ARG N N 15 0.928160386 0.012661893 . . . . . 6758 1
48 . 1 1 91 91 GLN N N 15 0.961168781 0.015966259 . . . . . 6758 1
49 . 1 1 92 92 GLN N N 15 0.993245928 0.013397922 . . . . . 6758 1
50 . 1 1 96 96 TYR N N 15 0.968616815 0.007945685 . . . . . 6758 1
51 . 1 1 100 100 VAL N N 15 0.952653139 0.024100133 . . . . . 6758 1
52 . 1 1 101 101 ASP N N 15 1.038745196 0.049630947 . . . . . 6758 1
53 . 1 1 103 103 LEU N N 15 0.933706816 0.004291496 . . . . . 6758 1
54 . 1 1 104 104 GLY N N 15 0.965903603 0.02596309 . . . . . 6758 1
55 . 1 1 105 105 GLY N N 15 1.070778456 0.016887413 . . . . . 6758 1
56 . 1 1 107 107 VAL N N 15 1.136363636 0.009374219 . . . . . 6758 1
57 . 1 1 111 111 LEU N N 15 1.098659635 0.010971967 . . . . . 6758 1
58 . 1 1 112 112 VAL N N 15 1.128286133 0.06774305 . . . . . 6758 1
59 . 1 1 113 113 SER N N 15 1.102414287 0.081157733 . . . . . 6758 1
60 . 1 1 114 114 ASN N N 15 0.795038957 0.01154275 . . . . . 6758 1
61 . 1 1 116 116 ARG N N 15 1.019160212 0.026755487 . . . . . 6758 1
62 . 1 1 117 117 ALA N N 15 0.863930886 0.015267286 . . . . . 6758 1
63 . 1 1 118 118 ASP N N 15 0.943930527 0.007182275 . . . . . 6758 1
64 . 1 1 119 119 GLU N N 15 0.960522524 0.004262811 . . . . . 6758 1
65 . 1 1 120 120 VAL N N 15 1.020408163 0.002191285 . . . . . 6758 1
66 . 1 1 121 121 PHE N N 15 0.975514584 0.011359984 . . . . . 6758 1
67 . 1 1 122 122 VAL N N 15 1.06621175 0.007786747 . . . . . 6758 1
68 . 1 1 123 123 LEU N N 15 0.97713504 0.012278238 . . . . . 6758 1
69 . 1 1 124 124 SER N N 15 0.324949633 0.001272067 . . . . . 6758 1
70 . 1 1 126 126 VAL N N 15 0.923275782 0.025670887 . . . . . 6758 1
71 . 1 1 127 127 ARG N N 15 0.958956655 0.004063376 . . . . . 6758 1
72 . 1 1 128 128 GLN N N 15 1.038421599 0.012329688 . . . . . 6758 1
73 . 1 1 129 129 GLY N N 15 1.03820598 0.002593354 . . . . . 6758 1
74 . 1 1 130 130 GLY N N 15 0.951565325 0.011733009 . . . . . 6758 1
75 . 1 1 131 131 ARG N N 15 1.090988436 0.033870957 . . . . . 6758 1
76 . 1 1 133 133 LEU N N 15 0.971439674 0.009625763 . . . . . 6758 1
77 . 1 1 134 134 LEU N N 15 1.025115325 0.002845201 . . . . . 6758 1
78 . 1 1 135 135 GLY N N 15 0.975800156 0.003056539 . . . . . 6758 1
79 . 1 1 136 136 ILE N N 15 1.170411985 0.027192805 . . . . . 6758 1
80 . 1 1 138 138 ILE N N 15 0.667200427 0.005294529 . . . . . 6758 1
81 . 1 1 139 139 GLY N N 15 1.02207686 0.015159941 . . . . . 6758 1
82 . 1 1 140 140 ASN N N 15 0.992260369 0.003061618 . . . . . 6758 1
83 . 1 1 142 142 ALA N N 15 0.995123893 0.004876107 . . . . . 6758 1
84 . 1 1 143 143 PHE N N 15 0.659413122 0.002531671 . . . . . 6758 1
85 . 1 1 145 145 THR N N 15 1.031459515 0.014784469 . . . . . 6758 1
86 . 1 1 146 146 ALA N N 15 0.990982063 0.012026964 . . . . . 6758 1
87 . 1 1 147 147 HIS N N 15 0.970120295 0.012197976 . . . . . 6758 1
88 . 1 1 148 148 ALA N N 15 0.984348853 0.009785753 . . . . . 6758 1
89 . 1 1 149 149 ILE N N 15 1.051193104 0.016726588 . . . . . 6758 1
90 . 1 1 150 150 ALA N N 15 0.934230194 0.003768117 . . . . . 6758 1
91 . 1 1 151 151 MET N N 15 1.052299274 0.005454058 . . . . . 6758 1
92 . 1 1 152 152 ARG N N 15 1.100231049 0.016463536 . . . . . 6758 1
93 . 1 1 153 153 ASN N N 15 1.011838511 0.016544871 . . . . . 6758 1
94 . 1 1 154 154 ASN N N 15 0.994332306 0.01140037 . . . . . 6758 1
95 . 1 1 155 155 ASP N N 15 1.020304051 0.010623784 . . . . . 6758 1
96 . 1 1 156 156 ALA N N 15 0.957212597 0.011685766 . . . . . 6758 1
97 . 1 1 158 158 ALA N N 15 0.945984297 0.004766797 . . . . . 6758 1
98 . 1 1 159 159 LEU N N 15 0.967305088 0.005646848 . . . . . 6758 1
99 . 1 1 160 160 VAL N N 15 0.986582478 0.006466181 . . . . . 6758 1
100 . 1 1 161 161 GLU N N 15 0.964506173 0.008824565 . . . . . 6758 1
101 . 1 1 162 162 GLU N N 15 0.920471281 0.006055171 . . . . . 6758 1
102 . 1 1 163 163 VAL N N 15 0.947687642 0.006875168 . . . . . 6758 1
103 . 1 1 164 164 TYR N N 15 0.944376239 0.005652261 . . . . . 6758 1
104 . 1 1 165 165 ASN N N 15 0.926526452 0.00910229 . . . . . 6758 1
105 . 1 1 167 167 PHE N N 15 0.949577438 0.013535342 . . . . . 6758 1
106 . 1 1 168 168 ARG N N 15 0.997904401 0.00289624 . . . . . 6758 1
107 . 1 1 169 169 ASP N N 15 0.996611521 0.005492898 . . . . . 6758 1
108 . 1 1 170 170 SER N N 15 0.92945441 0.003120429 . . . . . 6758 1
109 . 1 1 171 171 ARG N N 15 1.01853738 0.016123768 . . . . . 6758 1
110 . 1 1 172 172 ASP N N 15 0.988826263 0.005209522 . . . . . 6758 1
111 . 1 1 174 174 VAL N N 15 0.93676815 0.006806109 . . . . . 6758 1
112 . 1 1 176 176 GLN N N 15 0.922594335 0.003417332 . . . . . 6758 1
113 . 1 1 177 177 ALA N N 15 0.971250971 0.010874348 . . . . . 6758 1
114 . 1 1 178 178 LEU N N 15 0.947059381 0.006866022 . . . . . 6758 1
115 . 1 1 179 179 ASN N N 15 0.997207818 0.008423718 . . . . . 6758 1
116 . 1 1 180 180 TRP N N 15 0.966744006 0.016927054 . . . . . 6758 1
117 . 1 1 181 181 MET N N 15 0.977517107 0.005573731 . . . . . 6758 1
118 . 1 1 182 182 ILE N N 15 0.995123893 0.006679353 . . . . . 6758 1
119 . 1 1 183 183 LEU N N 15 0.985221675 0.005662194 . . . . . 6758 1
120 . 1 1 184 184 GLY N N 15 0.9765625 0.006238483 . . . . . 6758 1
121 . 1 1 185 185 ASP N N 15 1 0.003613007 . . . . . 6758 1
122 . 1 1 186 186 PHE N N 15 0.990393186 0.012414676 . . . . . 6758 1
123 . 1 1 188 188 ARG N N 15 0.961168781 0.006042748 . . . . . 6758 1
124 . 1 1 189 189 GLU N N 15 0.944554642 0.0060157 . . . . . 6758 1
125 . 1 1 191 191 ALA N N 15 0.98000784 0.008720655 . . . . . 6758 1
126 . 1 1 192 192 ASP N N 15 0.979911808 0.006768014 . . . . . 6758 1
127 . 1 1 193 193 LEU N N 15 0.968710646 0.009858686 . . . . . 6758 1
128 . 1 1 194 194 GLU N N 15 0.985804416 0.01992826 . . . . . 6758 1
129 . 1 1 195 195 MET N N 15 0.982607841 0.01073675 . . . . . 6758 1
130 . 1 1 196 196 ASN N N 15 1.03626943 0.012498268 . . . . . 6758 1
131 . 1 1 198 198 THR N N 15 0.859401856 0.006698958 . . . . . 6758 1
132 . 1 1 199 199 VAL N N 15 0.885818053 0.008076646 . . . . . 6758 1
133 . 1 1 202 202 ARG N N 15 1.099989 0.037149958 . . . . . 6758 1
134 . 1 1 203 203 ARG N N 15 0.990982063 0.008418297 . . . . . 6758 1
135 . 1 1 204 204 ALA N N 15 0.945537065 0.012868149 . . . . . 6758 1
136 . 1 1 205 205 SER N N 15 0.989119683 0.01328609 . . . . . 6758 1
137 . 1 1 206 206 GLU N N 15 0.974089227 0.00161572 . . . . . 6758 1
138 . 1 1 207 207 ILE N N 15 0.73313783 0.005687438 . . . . . 6758 1
139 . 1 1 208 208 ILE N N 15 0.87009484 0.008639782 . . . . . 6758 1
140 . 1 1 211 211 ALA N N 15 0.975704947 0.023895213 . . . . . 6758 1
141 . 1 1 213 213 ALA N N 15 0.90983532 0.005831744 . . . . . 6758 1
142 . 1 1 214 214 THR N N 15 0.951927653 0.022161573 . . . . . 6758 1
143 . 1 1 216 216 THR N N 15 0.891186169 0.006157693 . . . . . 6758 1
144 . 1 1 219 219 ARG N N 15 0.950118765 0.104733556 . . . . . 6758 1
145 . 1 1 222 222 ASP N N 15 0.960522524 0.004169739 . . . . . 6758 1
146 . 1 1 223 223 TYR N N 15 0.929713648 0.010931634 . . . . . 6758 1
147 . 1 1 224 224 ALA N N 15 0.973899494 0.006204397 . . . . . 6758 1
148 . 1 1 225 225 VAL N N 15 0.964041261 0.007115387 . . . . . 6758 1
149 . 1 1 226 226 ALA N N 15 0.918526683 0.013700407 . . . . . 6758 1
150 . 1 1 227 227 GLY N N 15 0.957670944 0.019655092 . . . . . 6758 1
151 . 1 1 228 228 ASN N N 15 0.930838686 0.002606661 . . . . . 6758 1
152 . 1 1 230 230 VAL N N 15 0.885661146 0.00767457 . . . . . 6758 1
153 . 1 1 231 231 ALA N N 15 0.998502247 0.020346454 . . . . . 6758 1
154 . 1 1 232 232 PHE N N 15 1.035089535 0.007119949 . . . . . 6758 1
155 . 1 1 233 233 ARG N N 15 0.917431193 0.009438767 . . . . . 6758 1
156 . 1 1 235 235 SER N N 15 1.02574623 0.036840105 . . . . . 6758 1
157 . 1 1 237 237 LEU N N 15 0.983574309 0.007604202 . . . . . 6758 1
158 . 1 1 238 238 GLN N N 15 0.978665101 0.00636248 . . . . . 6758 1
159 . 1 1 239 239 ALA N N 15 1.019887812 0.007228046 . . . . . 6758 1
160 . 1 1 240 240 GLY N N 15 0.986485153 0.010225701 . . . . . 6758 1
161 . 1 1 241 241 ILE N N 15 0.991571641 0.01365554 . . . . . 6758 1
162 . 1 1 242 242 VAL N N 15 0.956205775 0.012786473 . . . . . 6758 1
163 . 1 1 243 243 TYR N N 15 0.864378944 0.006473621 . . . . . 6758 1
164 . 1 1 244 244 GLY N N 15 0.806776926 0.006694155 . . . . . 6758 1
165 . 1 1 246 246 ARG N N 15 0.924299843 0.00550025 . . . . . 6758 1
166 . 1 1 247 247 ARG N N 15 0.839560071 0.005605582 . . . . . 6758 1
167 . 1 1 248 248 THR N N 15 0.854189801 0.00854853 . . . . . 6758 1
168 . 1 1 249 249 GLN N N 15 0.879120879 0.004505524 . . . . . 6758 1
169 . 1 1 250 250 ILE N N 15 0.835701153 0.004282047 . . . . . 6758 1
170 . 1 1 251 251 SER N N 15 0.833611204 0.006866187 . . . . . 6758 1
171 . 1 1 252 252 SER N N 15 0.934666791 0.014730342 . . . . . 6758 1
172 . 1 1 255 255 PHE N N 15 1.060670344 0.005996323 . . . . . 6758 1
173 . 1 1 257 257 VAL N N 15 0.905633037 0.018154491 . . . . . 6758 1
174 . 1 1 258 258 GLY N N 15 0.987751877 0.013449565 . . . . . 6758 1
175 . 1 1 259 259 VAL N N 15 1.047449461 0.013333397 . . . . . 6758 1
176 . 1 1 260 260 SER N N 15 0.982800983 0.009459386 . . . . . 6758 1
177 . 1 1 261 261 ARG N N 15 0.900414191 0.007768536 . . . . . 6758 1
178 . 1 1 262 262 ARG N N 15 0.845308538 0.006843145 . . . . . 6758 1
stop_
save_