Content for NMR-STAR saveframe, "heteronucl_T2_relaxation_5"
save_heteronucl_T2_relaxation_5
_Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation
_Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_5
_Heteronucl_T2_list.Entry_ID 52175
_Heteronucl_T2_list.ID 5
_Heteronucl_T2_list.Name 'Lac 0.217 mM'
_Heteronucl_T2_list.Sample_condition_list_ID 1
_Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1
_Heteronucl_T2_list.Temp_calibration_method methanol
_Heteronucl_T2_list.Temp_control_method 'no temperature control applied'
_Heteronucl_T2_list.Spectrometer_frequency_1H 600
_Heteronucl_T2_list.T2_coherence_type S(+,-)
_Heteronucl_T2_list.T2_val_units s-1
_Heteronucl_T2_list.Rex_units .
_Heteronucl_T2_list.Details .
_Heteronucl_T2_list.Text_data_format text
_Heteronucl_T2_list.Text_data
;
DATA CARRIER_FREQ (MHz)
60.790000
DATA NUCPMG (Hz)
@CARRIER_FREQ 1
33.33 33.33 66.67 66.67 100.00 133.33 166.67 200.00 300.00 400.00 400.00 600.00 700.00 800.00 800.00 966.67
DATA ASSIGNMENTS
1 144
2 147
3 155
4 174
5 176
6 183
7 184
8 187
DATA R2 (s-1)
@CARRIER_FREQ 1
1 13.2846 13.1193 12.7761 13.0436 12.3934 12.7438 12.6485 12.2912 12.6567 12.4317 12.2872 11.8510 12.4502 12.2929 11.9368 11.7933
2 14.2120 14.5592 13.8591 14.3299 13.7288 14.1806 13.8037 13.8279 13.8910 13.7056 13.3649 12.7436 12.9477 12.6756 13.3708 12.7126
3 13.7300 14.0759 13.9475 13.6228 13.8858 13.5269 14.0177 13.6151 13.4198 13.0068 13.1055 13.3730 12.6532 12.7857 12.9477 13.0654
4 16.5306 16.2891 15.6767 15.5781 15.8237 15.3901 15.5326 14.3774 14.9543 14.1415 13.9536 13.5493 13.4883 13.0877 12.4220 12.9292
5 13.5975 14.2718 14.2322 13.7441 14.1439 13.6118 13.3087 13.0896 13.2435 13.1390 13.1858 13.0277 12.8445 12.3786 12.9864 12.5605
6 20.9113 21.1915 20.6541 20.1486 19.7565 19.9286 19.2523 19.1795 18.5295 18.6257 17.8178 17.2137 17.4359 17.0688 17.1052 17.2653
7 18.0813 18.7231 17.8281 17.9564 17.3594 17.1538 17.0291 16.3195 15.4442 14.8248 14.6859 13.7809 13.4443 13.0997 12.7750 12.7557
8 13.7541 13.7880 13.2369 13.7841 13.4697 13.3380 13.3088 13.0244 12.9112 12.7136 12.4461 12.6031 12.5601 12.3012 12.3107 11.7870
DATA R2ERRORS (s-1)
@CARRIER_FREQ 1
1 0.2416 0.2396 0.2356 0.2387 0.2312 0.2352 0.2341 0.2300 0.2342 0.2316 0.2300 0.2252 0.2318 0.2301 0.2261 0.2246
2 0.3146 0.3202 0.3090 0.3165 0.3070 0.3141 0.3082 0.3085 0.3095 0.3067 0.3015 0.2923 0.2953 0.2913 0.3016 0.2919
3 0.2486 0.2530 0.2513 0.2473 0.2506 0.2461 0.2522 0.2472 0.2448 0.2398 0.2410 0.2442 0.2356 0.2372 0.2391 0.2405
4 0.2201 0.2173 0.2105 0.2094 0.2121 0.2074 0.2089 0.1968 0.2027 0.1945 0.1927 0.1888 0.1882 0.1845 0.1785 0.1830
5 0.4078 0.4219 0.4211 0.4108 0.4192 0.4081 0.4020 0.3976 0.4007 0.3986 0.3995 0.3964 0.3928 0.3839 0.3956 0.3874
6 0.3593 0.3650 0.3542 0.3445 0.3371 0.3403 0.3280 0.3267 0.3153 0.3170 0.3035 0.2938 0.2973 0.2916 0.2921 0.2946
7 0.3599 0.3726 0.3551 0.3575 0.3463 0.3425 0.3402 0.3277 0.3131 0.3032 0.3011 0.2875 0.2827 0.2779 0.2735 0.2732
8 0.2506 0.2510 0.2442 0.2510 0.2471 0.2454 0.2451 0.2416 0.2403 0.2379 0.2348 0.2367 0.2362 0.2332 0.2333 0.2274
;
loop_
_Heteronucl_T2_experiment.Experiment_ID
_Heteronucl_T2_experiment.Experiment_name
_Heteronucl_T2_experiment.Sample_ID
_Heteronucl_T2_experiment.Sample_label
_Heteronucl_T2_experiment.Sample_state
_Heteronucl_T2_experiment.Entry_ID
_Heteronucl_T2_experiment.Heteronucl_T2_list_ID
1 '1H-15N CPMG' . . . 52175 5
stop_
loop_
_Heteronucl_T2_software.Software_ID
_Heteronucl_T2_software.Software_label
_Heteronucl_T2_software.Method_ID
_Heteronucl_T2_software.Method_label
_Heteronucl_T2_software.Entry_ID
_Heteronucl_T2_software.Heteronucl_T2_list_ID
1 $software_1 . . 52175 5
2 $software_2 . . 52175 5
stop_
save_