Content for NMR-STAR saveframe, "heteronucl_T2_relaxation_4"
save_heteronucl_T2_relaxation_4
_Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation
_Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_4
_Heteronucl_T2_list.Entry_ID 52175
_Heteronucl_T2_list.ID 4
_Heteronucl_T2_list.Name 'Lac 0.166 mM'
_Heteronucl_T2_list.Sample_condition_list_ID 1
_Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1
_Heteronucl_T2_list.Temp_calibration_method methanol
_Heteronucl_T2_list.Temp_control_method 'no temperature control applied'
_Heteronucl_T2_list.Spectrometer_frequency_1H 600
_Heteronucl_T2_list.T2_coherence_type S(+,-)
_Heteronucl_T2_list.T2_val_units s-1
_Heteronucl_T2_list.Rex_units .
_Heteronucl_T2_list.Details .
_Heteronucl_T2_list.Text_data_format text
_Heteronucl_T2_list.Text_data
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DATA CARRIER_FREQ (MHz)
60.790000
DATA NUCPMG (Hz)
@CARRIER_FREQ 1
33.33 33.33 66.67 66.67 100.00 133.33 166.67 200.00 300.00 400.00 400.00 600.00 700.00 800.00 800.00 966.67
DATA ASSIGNMENTS
1 144
2 147
3 155
4 174
5 176
6 183
7 184
8 187
DATA R2 (s-1)
@CARRIER_FREQ 1
1 13.3744 13.8770 12.8075 13.3499 13.0238 13.0738 12.9183 13.0590 12.7158 13.0035 12.3902 12.3780 12.2969 12.3097 12.0098 11.9450
2 14.4093 14.7090 14.7595 14.1158 13.9466 13.8657 13.8796 13.5745 13.0541 13.4521 13.0305 13.0274 13.1463 11.8923 12.5889 12.8518
3 14.2459 14.8809 15.1248 14.0038 14.5497 14.4046 14.4440 14.1015 13.4645 13.5938 13.8969 13.5250 13.8475 13.4618 13.2634 13.4705
4 17.1364 16.4707 16.1879 16.3238 15.9148 16.1480 15.5466 15.2352 14.7064 14.4643 14.2171 13.6275 13.6425 12.9936 13.4480 13.0228
5 14.3101 14.6241 13.7313 14.2104 14.6345 13.8896 14.2174 13.4098 13.3914 13.3564 12.9430 13.0866 13.1923 12.7340 13.0248 12.8025
6 20.8491 21.9478 20.5635 20.9408 20.9510 20.5399 20.3416 19.8750 19.7521 18.5621 18.9281 18.2988 17.7354 17.5667 17.4512 17.5997
7 19.0856 18.4389 18.3981 18.6995 18.1321 17.2275 17.6258 16.7999 15.6784 14.9771 14.5620 14.0376 13.4124 12.7162 12.8439 12.7551
8 13.5595 14.4162 13.7054 13.3520 13.6202 13.3729 13.7952 13.3031 13.1568 12.7607 13.1954 12.2886 12.8019 12.6014 12.5026 12.8390
DATA R2ERRORS (s-1)
@CARRIER_FREQ 1
1 0.4115 0.4220 0.4001 0.4110 0.4044 0.4054 0.4023 0.4051 0.3983 0.4040 0.3919 0.3917 0.3902 0.3904 0.3848 0.3835
2 0.4525 0.4595 0.4606 0.4458 0.4420 0.4402 0.4405 0.4338 0.4227 0.4311 0.4222 0.4221 0.4246 0.3993 0.4131 0.4184
3 0.6948 0.7177 0.7267 0.6863 0.7056 0.7004 0.7018 0.6897 0.6679 0.6723 0.6826 0.6699 0.6809 0.6678 0.6612 0.6681
4 0.3993 0.3854 0.3797 0.3825 0.3743 0.3789 0.3672 0.3614 0.3517 0.3473 0.3430 0.3329 0.3332 0.3226 0.3299 0.3230
5 0.2822 0.2867 0.2740 0.2807 0.2869 0.2762 0.2808 0.2696 0.2694 0.2689 0.2634 0.2653 0.2667 0.2607 0.2645 0.2616
6 0.3151 0.3349 0.3101 0.3167 0.3168 0.3097 0.3063 0.2986 0.2965 0.2779 0.2835 0.2740 0.2658 0.2634 0.2618 0.2639
7 0.3335 0.3220 0.3213 0.3266 0.3167 0.3017 0.3082 0.2950 0.2781 0.2682 0.2625 0.2556 0.2477 0.2393 0.2408 0.2397
8 0.3761 0.3928 0.3789 0.3722 0.3773 0.3726 0.3806 0.3713 0.3686 0.3615 0.3693 0.3532 0.3622 0.3586 0.3569 0.3629
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loop_
_Heteronucl_T2_experiment.Experiment_ID
_Heteronucl_T2_experiment.Experiment_name
_Heteronucl_T2_experiment.Sample_ID
_Heteronucl_T2_experiment.Sample_label
_Heteronucl_T2_experiment.Sample_state
_Heteronucl_T2_experiment.Entry_ID
_Heteronucl_T2_experiment.Heteronucl_T2_list_ID
1 '1H-15N CPMG' . . . 52175 4
stop_
loop_
_Heteronucl_T2_software.Software_ID
_Heteronucl_T2_software.Software_label
_Heteronucl_T2_software.Method_ID
_Heteronucl_T2_software.Method_label
_Heteronucl_T2_software.Entry_ID
_Heteronucl_T2_software.Heteronucl_T2_list_ID
1 $software_1 . . 52175 4
2 $software_2 . . 52175 4
stop_
save_