Content for NMR-STAR saveframe, "heteronucl_T2_relaxation_3"
save_heteronucl_T2_relaxation_3
_Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation
_Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_3
_Heteronucl_T2_list.Entry_ID 52175
_Heteronucl_T2_list.ID 3
_Heteronucl_T2_list.Name 'Lac 0.086 mM'
_Heteronucl_T2_list.Sample_condition_list_ID 1
_Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1
_Heteronucl_T2_list.Temp_calibration_method methanol
_Heteronucl_T2_list.Temp_control_method 'no temperature control applied'
_Heteronucl_T2_list.Spectrometer_frequency_1H 600
_Heteronucl_T2_list.T2_coherence_type S(+,-)
_Heteronucl_T2_list.T2_val_units s-1
_Heteronucl_T2_list.Rex_units .
_Heteronucl_T2_list.Details .
_Heteronucl_T2_list.Text_data_format text
_Heteronucl_T2_list.Text_data
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DATA CARRIER_FREQ (MHz)
60.790000
DATA NUCPMG (Hz)
@CARRIER_FREQ 1
33.33 33.33 66.67 100.00 133.33 133.33 166.67 200.00 233.33 266.67 300.00 333.33 400.00 533.33 700.00 966.67
DATA ASSIGNMENTS
1 144
2 147
3 155
3 174
5 176
6 183
7 184
8 187
DATA R2 (s-1)
@CARRIER_FREQ 1
1 13.4038 13.5768 12.9488 12.8104 12.7792 13.0232 12.8922 12.6581 12.7251 12.8680 12.5756 12.3690 12.4636 12.4677 12.3122 12.0358
2 14.5270 14.1685 14.1477 14.5895 14.3950 14.0164 13.7418 13.5395 13.6785 13.8068 13.7807 13.6271 13.4463 13.0570 13.2562 13.0156
3 13.9559 14.2620 13.9549 13.8004 13.8307 13.9895 13.4499 13.7841 13.7656 13.5142 13.2882 13.2700 13.1822 13.1438 13.2886 12.8375
4 16.2763 16.1888 15.6882 15.4156 15.3181 15.0721 15.3041 15.1142 14.5900 14.0976 13.8477 14.3599 14.1428 13.0825 13.2059 12.6701
5 14.3562 14.3472 14.0132 14.3310 13.1846 13.8586 13.8947 13.2469 13.3031 13.2549 13.3576 13.2830 13.4125 12.8766 12.8987 12.3736
6 21.2650 21.6255 21.5746 19.9467 20.7788 20.4498 19.6092 19.5883 18.9497 18.9885 19.2185 19.1419 18.2425 17.6728 17.8008 17.1359
7 18.1929 18.6019 17.6558 17.2892 16.5382 16.6753 16.7238 15.5606 15.3650 15.1891 15.1600 15.0164 14.1506 13.3844 13.2730 12.4853
8 13.8652 13.5997 13.7446 13.2455 13.3473 13.1218 13.4039 13.3973 12.8959 12.9410 12.9448 12.6248 12.4093 12.5221 12.2934 12.4167
DATA R2ERRORS (s-1)
@CARRIER_FREQ 1
1 0.0734 0.0741 0.0718 0.0713 0.0712 0.0721 0.0716 0.0708 0.0710 0.0715 0.0705 0.0698 0.0701 0.0701 0.0696 0.0686
2 0.3315 0.3255 0.3251 0.3325 0.3292 0.3230 0.3185 0.3153 0.3175 0.3196 0.3192 0.3167 0.3138 0.3078 0.3109 0.3072
3 0.2522 0.2562 0.2522 0.2503 0.2506 0.2527 0.2459 0.2501 0.2498 0.2467 0.2439 0.2437 0.2426 0.2422 0.2439 0.2385
4 0.1972 0.1963 0.1912 0.1885 0.1876 0.1852 0.1875 0.1856 0.1807 0.1762 0.1740 0.1786 0.1766 0.1675 0.1685 0.1641
5 0.4603 0.4601 0.4523 0.4597 0.4339 0.4488 0.4496 0.4353 0.4365 0.4354 0.4377 0.4360 0.4389 0.4273 0.4278 0.4169
6 0.3052 0.3114 0.3106 0.2838 0.2971 0.2917 0.2786 0.2782 0.2687 0.2693 0.2727 0.2715 0.2586 0.2508 0.2525 0.2437
7 0.2672 0.2731 0.2596 0.2545 0.2446 0.2464 0.2470 0.2324 0.2300 0.2280 0.2276 0.2259 0.2162 0.2080 0.2068 0.1989
8 0.3148 0.3106 0.3129 0.3052 0.3067 0.3033 0.3076 0.3075 0.2999 0.3006 0.3007 0.2959 0.2928 0.2945 0.2912 0.2929
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loop_
_Heteronucl_T2_experiment.Experiment_ID
_Heteronucl_T2_experiment.Experiment_name
_Heteronucl_T2_experiment.Sample_ID
_Heteronucl_T2_experiment.Sample_label
_Heteronucl_T2_experiment.Sample_state
_Heteronucl_T2_experiment.Entry_ID
_Heteronucl_T2_experiment.Heteronucl_T2_list_ID
1 '1H-15N CPMG' . . . 52175 3
stop_
loop_
_Heteronucl_T2_software.Software_ID
_Heteronucl_T2_software.Software_label
_Heteronucl_T2_software.Method_ID
_Heteronucl_T2_software.Method_label
_Heteronucl_T2_software.Entry_ID
_Heteronucl_T2_software.Heteronucl_T2_list_ID
1 $software_1 . . 52175 3
2 $software_2 . . 52175 3
stop_
save_