Content for NMR-STAR saveframe, "heteronucl_T2_relaxation_2"
save_heteronucl_T2_relaxation_2
_Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation
_Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_2
_Heteronucl_T2_list.Entry_ID 52174
_Heteronucl_T2_list.ID 2
_Heteronucl_T2_list.Name 'Apo 800'
_Heteronucl_T2_list.Sample_condition_list_ID 1
_Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1
_Heteronucl_T2_list.Temp_calibration_method methanol
_Heteronucl_T2_list.Temp_control_method 'no temperature control applied'
_Heteronucl_T2_list.Spectrometer_frequency_1H 800
_Heteronucl_T2_list.T2_coherence_type S(+,-)
_Heteronucl_T2_list.T2_val_units s-1
_Heteronucl_T2_list.Rex_units .
_Heteronucl_T2_list.Details .
_Heteronucl_T2_list.Text_data_format text
_Heteronucl_T2_list.Text_data
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DATA CARRIER_FREQ (MHz)
81.086222
DATA NUCPMG (Hz)
@CARRIER_FREQ 1
50.00 50.00 100.00 100.00 150.00 150.00 200.00 200.00 250.00 250.00 250.00 300.00 400.00 500.00 750.00 1000.00
DATA ASSIGNMENTS
1 144
2 146
3 147
4 155
5 156
6 174
7 176
8 183
9 185
10 187
11 189
12 213
13 215
14 216
15 219
16 221
17 236
DATA R2 (s-1)
@CARRIER_FREQ 1
1 17.14 16.04 16.41 16.94 14.35 15.94 16.91 15.15 15.13 15.08 16.24 14.68 14.71 14.78 14.62 15.38
2 14.47 16.09 16.20 14.06 13.85 14.16 14.35 14.58 15.32 14.55 14.40 14.95 15.08 13.02 14.23 14.81
3 14.40 14.58 15.11 14.26 15.07 14.45 13.62 14.75 12.97 13.77 14.85 12.79 12.29 13.20 14.60 12.16
4 16.47 16.08 16.49 17.66 16.74 17.42 16.60 15.29 15.12 17.17 15.11 16.17 15.33 15.36 14.34 16.30
5 14.65 17.44 15.30 15.14 13.55 16.74 14.39 14.79 15.81 16.43 16.30 14.97 15.31 15.20 16.44 15.03
6 17.20 18.54 18.32 14.31 15.65 15.06 14.95 16.27 15.44 14.20 14.46 14.71 15.86 15.28 14.99 13.99
7 17.40 21.58 19.06 20.51 16.87 16.35 15.72 16.27 15.95 16.72 16.41 14.87 16.99 15.98 16.92 13.80
8 28.17 30.06 28.47 27.14 28.43 24.15 25.12 23.14 25.08 23.32 23.03 22.73 25.16 22.25 24.77 25.37
9 18.71 17.43 16.87 16.80 16.23 17.07 15.46 15.46 16.53 15.50 15.99 15.31 16.06 13.81 15.23 13.94
10 15.87 16.16 16.34 16.52 15.67 15.64 15.48 15.88 16.80 15.70 15.83 14.68 13.63 14.13 13.66 14.71
11 23.23 24.71 21.81 23.05 20.66 21.77 21.37 20.57 21.37 21.60 21.81 22.00 20.80 20.19 16.44 16.37
12 17.07 17.51 17.02 16.93 16.18 15.51 15.15 15.87 15.85 17.14 15.23 16.08 15.82 14.92 14.24 13.44
13 20.33 18.12 19.24 18.18 19.33 19.22 19.69 19.53 18.33 17.54 18.44 17.37 16.65 17.42 15.55 15.60
14 12.51 12.30 11.67 11.79 12.29 12.12 12.14 11.93 11.70 11.79 11.92 11.86 11.71 11.72 11.24 11.42
15 21.46 22.11 23.00 23.27 23.08 22.07 25.82 22.91 23.67 21.24 22.52 24.78 23.91 21.90 23.21 19.98
16 16.73 16.47 16.57 14.73 14.27 16.13 14.59 15.34 15.82 14.66 15.32 16.23 13.92 14.37 14.15 14.74
17 19.11 18.39 17.70 18.62 16.04 17.38 15.79 16.43 17.91 15.20 16.30 16.56 18.04 14.26 15.57 15.75
DATA R2ERRORS (s-1)
@CARRIER_FREQ 1
1 0.99 0.96 0.97 0.99 0.91 0.95 0.98 0.93 0.93 0.93 0.96 0.92 0.92 0.92 0.92 0.94
2 0.91 0.95 0.96 0.90 0.89 0.90 0.90 0.91 0.93 0.91 0.91 0.92 0.92 0.87 0.90 0.92
3 0.95 0.95 0.97 0.95 0.97 0.95 0.93 0.96 0.91 0.93 0.96 0.91 0.89 0.92 0.96 0.89
4 1.18 1.17 1.18 1.23 1.19 1.22 1.19 1.14 1.13 1.21 1.13 1.17 1.14 1.14 1.11 1.17
5 1.07 1.16 1.09 1.08 1.03 1.14 1.06 1.07 1.11 1.13 1.12 1.08 1.09 1.08 1.13 1.08
6 1.55 1.62 1.61 1.42 1.48 1.45 1.45 1.51 1.47 1.41 1.43 1.44 1.49 1.46 1.45 1.41
7 1.16 1.34 1.23 1.29 1.15 1.13 1.10 1.12 1.11 1.14 1.13 1.08 1.15 1.11 1.15 1.04
8 1.68 1.80 1.70 1.62 1.69 1.45 1.50 1.40 1.50 1.41 1.40 1.38 1.51 1.36 1.49 1.52
9 0.70 0.67 0.66 0.66 0.65 0.66 0.63 0.63 0.65 0.63 0.64 0.63 0.64 0.60 0.63 0.60
10 0.41 0.41 0.41 0.42 0.41 0.40 0.40 0.41 0.42 0.41 0.41 0.39 0.38 0.39 0.38 0.39
11 0.79 0.84 0.76 0.79 0.73 0.75 0.74 0.72 0.74 0.75 0.76 0.76 0.73 0.72 0.63 0.63
12 0.91 0.92 0.91 0.90 0.88 0.86 0.85 0.87 0.87 0.91 0.86 0.88 0.87 0.85 0.83 0.81
13 1.01 0.94 0.98 0.95 0.98 0.98 0.99 0.99 0.95 0.93 0.95 0.92 0.90 0.92 0.87 0.87
14 0.14 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13
15 1.18 1.21 1.25 1.26 1.25 1.21 1.38 1.24 1.28 1.17 1.23 1.33 1.29 1.20 1.26 1.13
16 1.07 1.06 1.07 1.01 0.99 1.05 1.00 1.03 1.04 1.01 1.03 1.06 0.98 1.00 0.99 1.01
17 1.49 1.46 1.43 1.47 1.35 1.41 1.34 1.37 1.44 1.32 1.36 1.37 1.44 1.28 1.33 1.34
;
loop_
_Heteronucl_T2_experiment.Experiment_ID
_Heteronucl_T2_experiment.Experiment_name
_Heteronucl_T2_experiment.Sample_ID
_Heteronucl_T2_experiment.Sample_label
_Heteronucl_T2_experiment.Sample_state
_Heteronucl_T2_experiment.Entry_ID
_Heteronucl_T2_experiment.Heteronucl_T2_list_ID
2 '1H-15N CPMG' . . . 52174 2
stop_
loop_
_Heteronucl_T2_software.Software_ID
_Heteronucl_T2_software.Software_label
_Heteronucl_T2_software.Method_ID
_Heteronucl_T2_software.Method_label
_Heteronucl_T2_software.Entry_ID
_Heteronucl_T2_software.Heteronucl_T2_list_ID
1 $software_1 . . 52174 2
2 $software_2 . . 52174 2
stop_
save_