Content for NMR-STAR saveframe, "spectral_peak_list_4"
save_spectral_peak_list_4
_Spectral_peak_list.Sf_category spectral_peak_list
_Spectral_peak_list.Sf_framecode spectral_peak_list_4
_Spectral_peak_list.Entry_ID 30550
_Spectral_peak_list.ID 4
_Spectral_peak_list.Name .
_Spectral_peak_list.Sample_ID 2
_Spectral_peak_list.Sample_label $sample_2
_Spectral_peak_list.Sample_condition_list_ID 1
_Spectral_peak_list.Sample_condition_list_label $sample_conditions_1
_Spectral_peak_list.Chem_shift_reference_ID .
_Spectral_peak_list.Chem_shift_reference_label .
_Spectral_peak_list.Experiment_ID 12
_Spectral_peak_list.Experiment_name '3D 12C-filtered-13C/15N-editedNOESY-HSQC'
_Spectral_peak_list.Experiment_class .
_Spectral_peak_list.Experiment_type .
_Spectral_peak_list.Number_of_spectral_dimensions 3
_Spectral_peak_list.Chemical_shift_list .
_Spectral_peak_list.Assigned_chem_shift_list_ID 1
_Spectral_peak_list.Assigned_chem_shift_list_label $assigned_chemical_shifts_1
_Spectral_peak_list.Details
;
Intermolecular NOEs between ligand and the amide protons of protein
Detection of 13C/15N occurs simultaneously
Automated peak picking with manual editing.
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_Spectral_peak_list.Text_data_format text
_Spectral_peak_list.Text_data
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Assignment w1 w2 w3 Height Volume
I46HG2*-I46CG2-F104HE* -0.618 15.411 6.699 -6.38E+05 -8.51E+06 bx
I46HG2*-I46CG2-F50HE* -0.620 15.415 6.824 -7.64E+05 -1.02E+07 bx
I46HG2*-I46CG2-F101HD* -0.620 15.440 7.076 -5.58E+05 -7.31E+06 bx
A100HB*-A100CB-F50HD* 0.147 15.869 6.719 -6.15E+05 -1.10E+07 bx
F2HB2-F2CB-F2HD* 3.034 40.237 6.929 5.88E+05 1.15E+07 bx
F2HB2-F2CB-? 3.038 40.237 7.072 2.45E+05 5.24E+06 bx
F2HB3-F2CB-F2HD* 2.609 40.200 6.932 6.44E+05 1.23E+07 bx
F31HB3-F31CB-F31HD* 3.341 36.641 6.819 3.06E+05 6.15E+06 bx
F31HB2-F31CB-F31HD* 3.109 36.641 6.820 3.45E+05 7.34E+06 bx
F2HA-F2CA-T3H 4.280 59.444 7.071 1.44E+06 2.66E+07 bx
F2HA-F2CA-F2HD* 4.281 59.444 6.917 5.55E+05 1.06E+07 bx
V4HA-V4CA-F2HE* 3.754 62.929 7.225 -2.71E+05 -4.99E+06 bx
V4HA-V4CA-F2HZ 3.754 62.929 7.393 -2.09E+05 -4.04E+06 bx
V4HG2*-V4CG2-? 0.977 21.660 7.362 -4.90E+05 -1.02E+07 bx
L55HD2*-L55CD2-F2HE* 0.614 21.683 7.232 -6.92E+05 -1.26E+07 bx
L55HD2*-L55CD2-F2HZ 0.615 21.683 7.387 -6.66E+05 -1.20E+07 bx
Q70HB2-Q70CB-F2HZ 2.679 28.527 7.385 -1.27E+05 -2.37E+06 bx
Q70HB2-Q70CB-F2HE* 2.683 28.527 7.224 -6.22E+04 -1.31E+06 bx
L10HA-L10CA-Y13HD* 3.915 58.368 6.829 3.99E+05 7.19E+06 bx
M53HE*-M53CE-? 1.998 18.440 6.824 -1.43E+06 -2.09E+07 bx
M53HE*-M53CE-F50HD* 1.997 18.440 6.740 -3.70E+05 -4.99E+06 bx
Y13HA-Y13CA-Y13HD* 4.599 57.846 6.842 1.07E+06 1.59E+07 bx
Y13HB2-Y13CB-Y13HD* 3.024 36.766 6.836 3.64E+05 6.51E+06 bx
Y13HB3-Y13CB-Y13HD* 3.141 36.766 6.836 5.08E+05 9.35E+06 bx
M53HG2-M53CG-Y13HD* 2.604 34.604 6.811 3.69E+05 6.47E+06 bx
M53HG3-M53CG-Y13HD* 3.009 34.525 6.819 4.08E+05 6.36E+06 bx
M53HA-M53CA-Y13HE* 3.954 57.047 6.810 6.50E+05 1.01E+07 bx
T41HG2*-T41CG2-F31HZ 0.614 20.998 6.781 -3.29E+05 -3.79E+06 bx
T41HG2*-T41CG2-Y27HD* 0.615 20.990 6.988 -3.79E+05 -4.71E+06 bx
T41HG2*-T41CG2-Y27HE* 0.616 21.006 7.127 -4.68E+05 -4.88E+06 bx
Y27HB2-Y27CB-V28H 2.734 37.983 6.819 2.88E+05 4.41E+06 bx
Y27HB2-Y27CB-Y27HD* 2.735 37.929 6.979 3.26E+05 5.79E+06 bx
Y27HB3-Y27CB-Y27HD* 1.966 37.974 6.982 3.72E+05 6.07E+06 bx
Y27HB3-Y27CB-F31HE* 1.966 37.974 6.815 3.49E+05 5.64E+06 bx
Y27HB3-Y27CB-Y27HE* 1.966 37.974 7.122 1.47E+05 1.51E+06 bx
P24HB2-P24CB-Y27HD* 2.214 33.242 6.981 2.12E+05 4.42E+06 bx
P24HD3-P24CD-Y27HD* 3.187 51.377 6.988 1.97E+05 2.99E+06 bx
F31HA-F31CA-? 3.907 56.946 6.822 1.29E+06 2.05E+07 bx
F31HA-F31CA-F36HE* 3.905 56.946 6.583 2.87E+05 4.56E+06 bx
F31HA-F31CA-F36HD* 3.906 56.946 7.114 1.10E+05 1.35E+06 bx
T42HG2*-T42CG2-F31HE* 1.459 23.569 6.800 -1.07E+06 -1.62E+07 bx
T42HG2*-T42CG2-F36HD* 1.460 23.569 7.115 -1.28E+06 -2.02E+07 bx
T42HG2*-T42CG2-F101HE* 1.459 23.569 7.211 -5.95E+05 -9.35E+06 bx
T42HG2*-T42CG2-F101HZ 1.459 23.569 7.475 -1.96E+05 -1.87E+06 bx
P37HD3-P37CD-F31HE* 4.152 50.486 6.802 2.48E+05 4.45E+06 bx
P37HD2-P37CD-F31HE* 3.828 50.426 6.825 2.82E+05 3.60E+06 bx
I23HD1*-I23CD1-Y45HD* 0.901 12.851 6.348 -6.49E+05 -8.63E+06 bx
I23HD1*-I23CD1-F31HE* 0.901 12.812 6.794 -8.64E+05 -1.16E+07 bx
W34HB2-W34CB-W34HE3 3.312 25.446 7.950 -2.05E+05 -3.18E+06 bx
W34HB2-W34CB-W34HD1 3.311 25.446 7.425 -1.49E+05 -2.02E+06 bx
W34HB2-W34CB-W34H 3.316 25.446 8.307 -1.10E+05 -1.42E+06 bx
W34HB3-W34CB-W34HD1 3.866 25.392 7.409 -1.54E+05 -1.93E+06 bx
W34HB3-W34CB-W34HE3 3.862 25.392 7.956 -1.58E+05 -2.31E+06 bx
W34HB3-W34CB-W34H 3.862 25.392 8.292 -6.70E+04 -1.23E+06 bx
I115HG2*-I115CG2-W34HH2 1.149 18.559 7.087 -8.75E+05 -1.31E+07 bx
I115HG2*-I115CG2-W34HZ3 1.149 18.559 7.199 -3.74E+05 -6.00E+06 bx
I115HG2*-I115CG2-F104HE* 1.152 18.505 6.697 -3.89E+05 -4.54E+06 bx
I46HD1*-I46CD1-F36HD* -0.466 7.828 7.099 -5.51E+05 -7.17E+06 bx
I46HD1*-I46CD1-Y45HD* -0.467 7.849 6.341 -4.83E+05 -6.56E+06 bx
I46HD1*-I46CD1-Y45HE* -0.465 7.828 6.441 -3.40E+05 -4.82E+06 bx
I46HD1*-I46CD1-F36HE* -0.465 7.828 6.592 -3.70E+05 -5.09E+06 bx
I46HD1*-I46CD1-F104HE* -0.467 7.828 6.691 -5.44E+05 -8.21E+06 bx
I46HD1*-I46CD1-F104HD* -0.467 7.856 6.823 -4.33E+05 -5.88E+06 bx
I46HD1*-I46CD1-? -0.465 7.828 7.215 -1.93E+05 -2.33E+06 bx
I46HG13-I46CG1-F101HD* 1.336 27.152 7.078 -1.90E+05 -2.68E+06 bx
I46HG12-I46CG1-F101HD* 0.794 27.160 7.081 -2.66E+05 -4.15E+06 bx
Y45HB3-Y45CB-Y45HD* 3.263 37.219 6.352 1.96E+05 3.46E+06 bx
Y45HB2-Y45CB-Y45HD* 3.049 37.219 6.349 2.84E+05 4.41E+06 bx
L21HD1*-L21CD1-Y45HD* 0.958 25.688 6.343 -3.60E+05 -4.26E+06 bx
V49HG2*-V49CG2-Y45HE* 0.392 22.663 6.460 -3.21E+05 -4.53E+06 bx
V49HG2*-V49CG2-Y45HD* 0.393 22.670 6.372 -1.85E+05 -2.97E+06 bx
V49HG2*-V49CG2-F50HD* 0.391 22.563 6.707 -1.05E+05 -2.05E+06 bx
V49HG2*-V49CG2-Y13HD* 0.391 22.563 6.833 -1.05E+05 -2.26E+06 bx
V18HG2*-V18CG2-Y45HE* 1.159 24.739 6.459 -6.09E+05 -8.39E+06 bx
V18HG2*-V18CG2-Y45HD* 1.161 24.739 6.338 -2.77E+05 -3.79E+06 bx
V18HG2*-V18CG2-F31HE* 1.160 24.739 6.810 -3.57E+05 -5.88E+06 bx
C17HB2-C17CB-Y45HE* 3.330 41.501 6.448 2.03E+05 3.15E+06 bx
C17HB2-C17CB-Y45HD* 3.330 41.448 6.338 1.43E+05 2.37E+06 bx
C17HB3-C17CB-Y45HD* 2.847 41.448 6.341 2.78E+05 4.05E+06 bx
C17HB3-C17CB-Y45HE* 2.845 41.448 6.464 2.02E+05 3.14E+06 bx
R14HA-R14CA-Y45HE* 4.364 59.889 6.483 3.96E+05 5.34E+06 bx
V49HG1*-V49CG1-F50HD* 0.890 22.660 6.723 -5.48E+05 -8.15E+06 bx
V49HG1*-V49CG1-Y13HD* 0.889 22.660 6.827 -5.76E+05 -8.12E+06 bx
F50HB2-F50CB-F50HD* 3.097 37.314 6.721 1.99E+05 3.24E+06 bx
F50HA-F50CA-F50HD* 4.223 58.386 6.721 7.37E+05 1.11E+07 bx
F56HB2-F56CB-F56HD* 2.940 45.033 6.722 5.08E+05 8.09E+06 bx
F56HB3-F56CB-F56HD* 2.544 45.029 6.716 5.15E+05 8.05E+06 bx
A100HA-A100CA-F56HD* 3.299 54.646 6.716 3.62E+05 5.67E+06 bx
A96HB*-A96CB-F56HD* 1.856 18.608 6.727 -3.32E+05 -4.91E+06 bx
A96HB*-A96CB-W99HZ3 1.858 18.608 6.958 -2.54E+05 -2.74E+06 bx
A96HB*-A96CB-F56HZ 1.858 18.608 7.251 -4.41E+05 -6.45E+06 bx
A96HB*-A96CB-W99HE3 1.857 18.608 7.458 -5.88E+05 -8.02E+06 bx
V4HG1*-V4CG1-F2HD* 0.967 22.064 6.922 -3.56E+05 -4.06E+06 bx
V4HG1*-V4CG1-T3H 0.968 22.059 7.061 -5.79E+05 -6.84E+06 bx
V4HG1*-V4CG1-F2HE* 0.967 22.053 7.222 -1.00E+06 -1.36E+07 bx
V4HG1*-V4CG1-F2HZ 0.966 22.064 7.375 -3.46E+05 -5.68E+06 bx
H73HB2-H73CB-H73HD2 3.218 28.083 7.337 -1.13E+05 -1.85E+06 bx
H73HB3-H73CB-H73HD2 3.418 28.083 7.340 -1.48E+05 -2.41E+06 bx
P62HD2-P62CD-F56HD* 2.790 49.402 6.718 1.70E+05 2.48E+06 bx
P62HD2-P62CD-W99HH2 2.793 49.391 6.980 9.35E+04 1.19E+06 bx
M43HA-M43CA-F101HD* 3.630 61.247 7.079 -3.56E+05 -5.79E+06 bx
F101HA-F101CA-F104HD* 3.905 62.084 6.821 -2.49E+05 -3.07E+06 bx
F101HA-F101CA-F101HD* 3.904 62.084 7.081 -3.94E+05 -6.68E+06 bx
F101HB2-F101CB-F101HD* 2.927 40.156 7.087 2.84E+05 5.39E+06 bx
F101HB3-F101CB-F101HD* 3.141 40.135 7.086 5.47E+05 9.01E+06 bx
F36HB3-F36CB-F36HD* 3.106 40.135 7.108 8.73E+05 1.47E+07 bx
?-?-? 3.113 40.135 7.459 1.67E+05 2.97E+06 bx
M43HE*-M43CE-H98HD2 1.541 18.093 6.912 -1.31E+06 -1.01E+07 bx
M43HE*-M43CE-F101HD* 1.541 18.093 7.083 -1.11E+06 -9.63E+06 bx
M43HE*-M43CE-F101HE* 1.541 18.093 7.215 -6.91E+05 -6.03E+06 bx
K105HD2-K105CD-F101HE* 1.636 28.895 7.201 -1.63E+05 -3.23E+06 bx
Q108HB3-Q108CB-F104HD* 1.634 28.591 6.828 -4.32E+05 -6.83E+06 bx
F104HA-F104CA-F104HD* 4.380 60.501 6.824 -1.09E+06 -1.41E+07 bx
F104HB3-F104CB-F104HD* 2.887 39.016 6.819 3.52E+05 4.72E+06 bx
F104HB2-F104CB-F104HD* 3.065 38.970 6.821 4.51E+05 6.65E+06 bx
I115HD1*-I115CD1-F104HE* 1.150 15.102 6.706 -3.85E+05 -6.61E+06 bx
I115HD1*-I115CD1-F107HD* 1.149 15.102 7.025 -1.45E+06 -2.26E+07 bx
L71HD2*-L71CD2-F107HD* 0.992 23.667 7.026 -8.07E+05 -1.20E+07 bx
L71HD1*-L71CD1-F107HZ 0.416 26.787 6.991 -7.06E+05 -1.20E+07 bx
L114HD2*-L114CD2-F107HZ 1.041 25.689 6.973 -9.15E+05 -1.54E+07 bx
L114HD2*-L114CD2-F107HE* 1.042 25.689 7.050 -4.59E+05 -9.42E+06 bx
L114HD2*-L114CD2-L114H 1.041 25.689 7.290 -1.10E+05 -1.65E+06 bx
F107HA-F107CA-F107HD* 4.237 62.254 7.011 -8.52E+05 -1.64E+07 bx
F107HB2-F107CB-F107HD* 3.263 41.794 7.007 4.08E+05 7.50E+06 bx
F107HB3-F107CB-F107HD* 2.948 41.794 7.011 3.71E+05 7.25E+06 bx
V84HA-V84CA-F107HD* 3.400 67.002 7.020 -7.63E+05 -1.40E+07 bx
T42HA-T42CA-? 3.944 66.894 6.777 -6.69E+05 -9.45E+06 bx
V28HA-V28CA-V28H 2.912 66.894 6.829 -7.80E+05 -1.34E+07 bx
E83HB2-E83CB-F107HE* 2.253 29.508 7.020 -3.81E+05 -7.76E+06 bx
E83HB2-E83CB-? 2.249 29.508 7.202 -1.48E+05 -2.22E+06 bx
V84HG2*-V84CG2-F107HE* 0.566 23.867 7.007 -7.42E+05 -1.28E+07 bx
W34HA-W34CA-F36HE* 3.693 58.690 6.606 2.92E+05 5.82E+06 bx
I119HD1*-I119CD1-W34HH2 1.030 14.628 7.096 -2.31E+05 -3.57E+06 bx
I119HD1*-I119CD1-W34HZ2 1.030 14.628 7.436 -4.07E+05 -5.33E+06 bx
L114HD1*-L114CD1-F107HZ 1.022 23.968 6.967 -2.09E+05 -4.36E+06 bx
L114HD1*-L114CD1-F107HE* 1.022 23.968 7.039 -1.36E+05 -3.17E+06 bx
L10HD1*-L10CD1-Y13HD* 1.039 23.861 6.838 -2.92E+05 -4.79E+06 bx
V28HG2*-V28CG2-? 0.885 23.861 6.824 -3.01E+06 -3.38E+07 bx
W99HB3-W99CB-W99HE3 3.848 31.548 7.452 1.73E+05 2.92E+06 bx
K116HE2-K116CE-W34HE3 1.942 41.012 7.951 2.13E+05 3.85E+06 bx
Y45HA-Y45CA-Y45HD* 3.961 62.424 6.340 -2.57E+05 -4.60E+06 bx
C44HB2-C44CB-? 3.143 37.044 6.836 3.31E+05 6.71E+06 bx
L55HD2*-L55CD2-F56H 0.613 21.700 7.047 -1.79E+05 -2.83E+06 bx
L112HD1*-L112CD1-W34HE1 0.903 23.348 10.295 -2.40E+05 -2.47E+06 bx
L112HD1*-L112CD1-W34HZ2 0.907 23.348 7.432 -3.18E+05 -3.53E+06 bx
L112HD1*-L112CD1-W34HZ3 0.906 23.348 7.192 -2.00E+05 -2.46E+06 bx
L112HD1*-L112CD1-? 0.904 23.348 7.949 -5.62E+05 -6.86E+06 bx
L114HD2*-L114CD2-F107HZ 1.042 25.796 6.971 -1.10E+06 -1.58E+07 bx
L114HD1*-L114CD1-F107HZ 1.023 24.103 6.969 -4.09E+05 -5.56E+06 bx
L114HD2*-L114CD2-F107HE* 1.043 25.796 7.040 -6.26E+05 -1.01E+07 bx
V4HG2*-V4CG2-F2HE* 0.976 21.677 7.225 -4.23E+05 -7.03E+06 bx
;
loop_
_Spectral_dim.ID
_Spectral_dim.Axis_code
_Spectral_dim.Spectrometer_frequency
_Spectral_dim.Atom_type
_Spectral_dim.Atom_isotope_number
_Spectral_dim.Spectral_region
_Spectral_dim.Magnetization_linkage_ID
_Spectral_dim.Under_sampling_type
_Spectral_dim.Sweep_width
_Spectral_dim.Sweep_width_units
_Spectral_dim.Value_first_point
_Spectral_dim.Absolute_peak_positions
_Spectral_dim.Acquisition
_Spectral_dim.Center_frequency_offset
_Spectral_dim.Encoding_code
_Spectral_dim.Encoded_reduced_dimension_ID
_Spectral_dim.Entry_ID
_Spectral_dim.Spectral_peak_list_ID
1 . . H 1 HN 2 . 15 ppm . . . 4.97 . . 30550 4
2 . . N 15 N 1 . 75 ppm . . . 119.7 . . 30550 4
3 . . H 1 H . . 14 ppm . . . 4.97 . . 30550 4
stop_
save_