Content for NMR-STAR saveframe, "methyl_R2_600"

    save_methyl_R2_600
   _Heteronucl_T2_list.Sf_category                   heteronucl_T2_relaxation
   _Heteronucl_T2_list.Sf_framecode                  methyl_R2_600
   _Heteronucl_T2_list.Entry_ID                      27447
   _Heteronucl_T2_list.ID                            2
   _Heteronucl_T2_list.Sample_condition_list_ID      1
   _Heteronucl_T2_list.Sample_condition_list_label   $sample_conditions_1
   _Heteronucl_T2_list.Temp_calibration_method       methanol
   _Heteronucl_T2_list.Temp_control_method           'single scan interleaving'
   _Heteronucl_T2_list.Spectrometer_frequency_1H     600
   _Heteronucl_T2_list.T2_coherence_type             S(+,-)
   _Heteronucl_T2_list.T2_val_units                  s-1
   _Heteronucl_T2_list.Rex_units                     s-1
   _Heteronucl_T2_list.Details
;
Slow-timescale methyl dynamics recorded using the latest version of the experiments by Korzhnev, Kay, et al.     
(J.Am.Chem.Soc. 126, 3964).
The following methyls should be excluded or used with caution due to resonance overlap:
CD2 of residues 12, 75, 81, 117, and 141
CD1 of residues 17, 57, 75, 97, and 117.
;
   _Heteronucl_T2_list.Text_data_format              .
   _Heteronucl_T2_list.Text_data                     .

   loop_
      _Heteronucl_T2_experiment.Experiment_ID
      _Heteronucl_T2_experiment.Experiment_name
      _Heteronucl_T2_experiment.Sample_ID
      _Heteronucl_T2_experiment.Sample_label
      _Heteronucl_T2_experiment.Sample_state
      _Heteronucl_T2_experiment.Entry_ID
      _Heteronucl_T2_experiment.Heteronucl_T2_list_ID

      11   '2D 1H-13C CPMG HMQC relaxation dispersion'   .   .   .   27447   2
   stop_

   loop_
      _Heteronucl_T2_software.Software_ID
      _Heteronucl_T2_software.Software_label
      _Heteronucl_T2_software.Method_ID
      _Heteronucl_T2_software.Method_label
      _Heteronucl_T2_software.Entry_ID
      _Heteronucl_T2_software.Heteronucl_T2_list_ID

      1   $SPARKY   .   .   27447   2
      5   $Origin   .   .   27447   2
   stop_

   loop_
      _T2.ID
      _T2.Assembly_atom_ID
      _T2.Entity_assembly_ID
      _T2.Entity_ID
      _T2.Comp_index_ID
      _T2.Seq_ID
      _T2.Comp_ID
      _T2.Atom_ID
      _T2.Atom_type
      _T2.Atom_isotope_number
      _T2.T2_val
      _T2.T2_val_err
      _T2.Rex_val
      _T2.Rex_err
      _T2.Resonance_ID
      _T2.Auth_entity_assembly_ID
      _T2.Auth_seq_ID
      _T2.Auth_comp_ID
      _T2.Auth_atom_ID
      _T2.Entry_ID
      _T2.Heteronucl_T2_list_ID

      1    .   1   1   1     1     MET   CE    C   13   6.9619    0.1306   0.0000   0.2864   .   .   .   .   .   27447   2
      2    .   1   1   4     4     LEU   CD1   C   13   12.4349   0.1267   0.0000   0.2779   .   .   .   .   .   27447   2
      3    .   1   1   4     4     LEU   CD2   C   13   15.8342   0.2167   0.0000   0.4752   .   .   .   .   .   27447   2
      4    .   1   1   5     5     ALA   CB    C   13   14.9826   0.1352   0.0000   0.2965   .   .   .   .   .   27447   2
      5    .   1   1   8     8     ILE   CD1   C   13   13.8782   0.2961   0.0000   0.6493   .   .   .   .   .   27447   2
      6    .   1   1   10    10    ALA   CB    C   13   23.5472   0.2185   0.0000   0.4792   .   .   .   .   .   27447   2
      7    .   1   1   12    12    LEU   CD1   C   13   16.4177   0.2883   0.0000   0.6323   .   .   .   .   .   27447   2
      8    .   1   1   12    12    LEU   CD2   C   13   15.5885   0.1994   0.0000   0.4373   .   .   .   .   .   27447   2
      9    .   1   1   15    15    VAL   CG1   C   13   18.2136   0.3484   0.0000   0.7640   .   .   .   .   .   27447   2
      10   .   1   1   15    15    VAL   CG2   C   13   13.8357   0.2546   0.0000   0.5583   .   .   .   .   .   27447   2
      11   .   1   1   16    16    ILE   CD1   C   13   13.8033   0.2518   0.1512   0.5523   .   .   .   .   .   27447   2
      12   .   1   1   17    17    LEU   CD1   C   13   6.5181    0.3202   0.0000   0.7022   .   .   .   .   .   27447   2
      13   .   1   1   17    17    LEU   CD2   C   13   7.2196    0.1476   0.0000   0.3237   .   .   .   .   .   27447   2
      14   .   1   1   19    19    ALA   CB    C   13   15.6010   0.0840   0.8043   0.1842   .   .   .   .   .   27447   2
      15   .   1   1   25    25    ILE   CD1   C   13   16.5050   0.1243   1.0419   0.2726   .   .   .   .   .   27447   2
      16   .   1   1   26    26    LEU   CD1   C   13   12.7471   0.3512   0.0000   0.7703   .   .   .   .   .   27447   2
      17   .   1   1   26    26    LEU   CD2   C   13   12.1489   0.1625   0.0000   0.3563   .   .   .   .   .   27447   2
      18   .   1   1   27    27    ILE   CD1   C   13   10.6937   0.3250   1.2073   0.7127   .   .   .   .   .   27447   2
      19   .   1   1   34    34    VAL   CG1   C   13   11.9516   0.1305   0.8101   0.2862   .   .   .   .   .   27447   2
      20   .   1   1   34    34    VAL   CG2   C   13   11.5196   0.0811   0.5364   0.1778   .   .   .   .   .   27447   2
      21   .   1   1   35    35    ALA   CB    C   13   8.5412    0.0618   0.0000   0.1355   .   .   .   .   .   27447   2
      22   .   1   1   36    36    LEU   CD1   C   13   22.4372   0.3257   0.0000   0.7142   .   .   .   .   .   27447   2
      23   .   1   1   36    36    LEU   CD2   C   13   13.9195   0.1440   0.0000   0.3159   .   .   .   .   .   27447   2
      24   .   1   1   43    43    ILE   CD1   C   13   17.6117   0.1122   0.0000   0.2461   .   .   .   .   .   27447   2
      25   .   1   1   44    44    LEU   CD1   C   13   21.8220   0.3173   1.0292   0.6958   .   .   .   .   .   27447   2
      26   .   1   1   44    44    LEU   CD2   C   13   24.7068   0.3107   1.6308   0.6814   .   .   .   .   .   27447   2
      27   .   1   1   45    45    MET   CE    C   13   19.8564   0.1975   0.0000   0.4331   .   .   .   .   .   27447   2
      28   .   1   1   46    46    LEU   CD1   C   13   18.1064   0.1276   0.0000   0.2797   .   .   .   .   .   27447   2
      29   .   1   1   46    46    LEU   CD2   C   13   12.2937   0.1027   0.4965   0.2253   .   .   .   .   .   27447   2
      30   .   1   1   47    47    LEU   CD1   C   13   21.0071   0.2154   0.1215   0.4724   .   .   .   .   .   27447   2
      31   .   1   1   47    47    LEU   CD2   C   13   14.8438   0.1489   0.0000   0.3265   .   .   .   .   .   27447   2
      32   .   1   1   52    52    LEU   CD1   C   13   15.1423   0.1835   0.0000   0.4025   .   .   .   .   .   27447   2
      33   .   1   1   52    52    LEU   CD2   C   13   8.3180    0.1071   0.3808   0.2348   .   .   .   .   .   27447   2
      34   .   1   1   57    57    LEU   CD1   C   13   13.9535   0.1622   2.6176   0.3557   .   .   .   .   .   27447   2
      35   .   1   1   57    57    LEU   CD2   C   13   15.5822   0.1485   1.1224   0.3257   .   .   .   .   .   27447   2
      36   .   1   1   58    58    ALA   CB    C   13   10.4750   0.1741   0.0000   0.3817   .   .   .   .   .   27447   2
      37   .   1   1   61    61    LEU   CD1   C   13   13.2101   0.0995   1.1655   0.2182   .   .   .   .   .   27447   2
      38   .   1   1   61    61    LEU   CD2   C   13   11.8344   0.1110   0.0468   0.2434   .   .   .   .   .   27447   2
      39   .   1   1   63    63    VAL   CG1   C   13   13.0841   0.1618   0.0000   0.3548   .   .   .   .   .   27447   2
      40   .   1   1   63    63    VAL   CG2   C   13   16.6274   0.1186   0.3607   0.2602   .   .   .   .   .   27447   2
      41   .   1   1   66    66    ALA   CB    C   13   8.7181    0.2119   0.0000   0.4647   .   .   .   .   .   27447   2
      42   .   1   1   67    67    ALA   CB    C   13   12.3977   0.2115   0.0000   0.4638   .   .   .   .   .   27447   2
      43   .   1   1   68    68    VAL   CG1   C   13   16.1958   0.1491   0.0000   0.3270   .   .   .   .   .   27447   2
      44   .   1   1   68    68    VAL   CG2   C   13   16.1852   0.1649   0.2869   0.3617   .   .   .   .   .   27447   2
      45   .   1   1   71    71    ALA   CB    C   13   16.4111   0.1232   0.0000   0.2702   .   .   .   .   .   27447   2
      46   .   1   1   72    72    ILE   CD1   C   13   14.4297   0.0703   0.0000   0.1542   .   .   .   .   .   27447   2
      47   .   1   1   75    75    LEU   CD1   C   13   18.9691   0.1766   0.4137   0.3873   .   .   .   .   .   27447   2
      48   .   1   1   75    75    LEU   CD2   C   13   7.7167    0.2503   0.0000   0.5490   .   .   .   .   .   27447   2
      49   .   1   1   76    76    VAL   CG1   C   13   8.8568    0.1037   0.0000   0.2274   .   .   .   .   .   27447   2
      50   .   1   1   76    76    VAL   CG2   C   13   11.4735   0.2496   0.0000   0.5474   .   .   .   .   .   27447   2
      51   .   1   1   80    80    MET   CE    C   13   17.8305   0.1016   0.0000   0.2229   .   .   .   .   .   27447   2
      52   .   1   1   81    81    LEU   CD1   C   13   18.5909   0.1535   1.0279   0.3366   .   .   .   .   .   27447   2
      53   .   1   1   81    81    LEU   CD2   C   13   16.6103   0.1514   0.0000   0.3319   .   .   .   .   .   27447   2
      54   .   1   1   90    90    ALA   CB    C   13   6.4980    0.0600   0.0000   0.1316   .   .   .   .   .   27447   2
      55   .   1   1   92    92    VAL   CG1   C   13   7.2714    0.0633   0.2599   0.1389   .   .   .   .   .   27447   2
      56   .   1   1   92    92    VAL   CG2   C   13   6.7170    0.0550   0.1837   0.1207   .   .   .   .   .   27447   2
      57   .   1   1   93    93    ILE   CD1   C   13   5.7949    0.0848   0.0000   0.1860   .   .   .   .   .   27447   2
      58   .   1   1   97    97    LEU   CD1   C   13   15.3046   0.2457   0.0000   0.5390   .   .   .   .   .   27447   2
      59   .   1   1   97    97    LEU   CD2   C   13   15.7715   0.1701   1.0776   0.3730   .   .   .   .   .   27447   2
      60   .   1   1   100   100   LEU   CD1   C   13   7.0754    0.1221   0.0000   0.2679   .   .   .   .   .   27447   2
      61   .   1   1   100   100   LEU   CD2   C   13   10.5269   0.1184   0.0000   0.2597   .   .   .   .   .   27447   2
      62   .   1   1   101   101   ALA   CB    C   13   30.5556   0.5810   0.8842   1.2741   .   .   .   .   .   27447   2
      63   .   1   1   104   104   ILE   CD1   C   13   13.8183   0.2215   0.7201   0.4857   .   .   .   .   .   27447   2
      64   .   1   1   105   105   ALA   CB    C   13   7.6864    0.1365   0.0000   0.2993   .   .   .   .   .   27447   2
      65   .   1   1   116   116   LEU   CD1   C   13   9.5874    0.2122   0.0000   0.4654   .   .   .   .   .   27447   2
      66   .   1   1   116   116   LEU   CD2   C   13   9.6924    0.1326   0.0000   0.2908   .   .   .   .   .   27447   2
      67   .   1   1   117   117   LEU   CD1   C   13   7.5635    0.0688   1.0559   0.1509   .   .   .   .   .   27447   2
      68   .   1   1   117   117   LEU   CD2   C   13   10.6176   0.2886   0.0000   0.6329   .   .   .   .   .   27447   2
      69   .   1   1   122   122   VAL   CG1   C   13   14.4771   0.1792   0.0000   0.3931   .   .   .   .   .   27447   2
      70   .   1   1   122   122   VAL   CG2   C   13   11.6218   0.2128   0.0000   0.4666   .   .   .   .   .   27447   2
      71   .   1   1   123   123   ALA   CB    C   13   9.8077    0.1320   0.0000   0.2894   .   .   .   .   .   27447   2
      72   .   1   1   133   133   VAL   CG1   C   13   15.3429   0.2166   0.0000   0.4751   .   .   .   .   .   27447   2
      73   .   1   1   133   133   VAL   CG2   C   13   7.3957    0.1609   0.0000   0.3529   .   .   .   .   .   27447   2
      74   .   1   1   134   134   ILE   CD1   C   13   13.7280   0.3167   0.0000   0.6946   .   .   .   .   .   27447   2
      75   .   1   1   138   138   LEU   CD1   C   13   15.2912   0.1334   0.0000   0.2926   .   .   .   .   .   27447   2
      76   .   1   1   138   138   LEU   CD2   C   13   13.1791   0.1526   0.0000   0.3347   .   .   .   .   .   27447   2
      77   .   1   1   140   140   ALA   CB    C   13   5.0425    0.1156   0.0000   0.2534   .   .   .   .   .   27447   2
      78   .   1   1   141   141   LEU   CD1   C   13   11.5511   0.2254   0.0000   0.4944   .   .   .   .   .   27447   2
      79   .   1   1   141   141   LEU   CD2   C   13   16.3299   0.2697   0.0000   0.5915   .   .   .   .   .   27447   2
      80   .   1   1   142   142   VAL   CG1   C   13   9.7077    0.0723   0.4112   0.1586   .   .   .   .   .   27447   2
      81   .   1   1   142   142   VAL   CG2   C   13   10.5288   0.1205   0.0000   0.2642   .   .   .   .   .   27447   2
      82   .   1   1   145   145   ILE   CD1   C   13   12.6319   0.1584   0.0000   0.3473   .   .   .   .   .   27447   2
   stop_
save_