BMRB

Biological Magnetic Resonance Data Bank


A Repository for Data from NMR Spectroscopy on Proteins, Peptides, Nucleic Acids, and other Biomolecules
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BMRB Entry 6214

Title: Signal assignments and chemical-shift structural analysis of uniformly 13C, 15N-labeled peptide, mastoparan-X, by multidimensional solid-state NMR under magic-angle spinning   PubMed: 14872124

Authors: Fujiwara, Toshimichi; Todokoro, Yasuto; Hajime, Yanagishita; Midori, Tawarayama; Toshiyuki, Kohno; Kaori, Wakamatsu; Hideo, Akutsu

Citation: Fujiwara, Toshimichi; Todokoro, Yasuto; Hajime, Yanagishita; Midori, Tawarayama; Toshiyuki, Kohno; Kaori, Wakamatsu; Hideo, Akutsu. "Signal assignments and chemical-shift structural analysis of uniformly 13C, 15N-labeled peptide, mastoparan-X, by multidimensional solid-state NMR under magic-angle spinning"  J. Biomol. NMR 28, 311-325 (2004).

Assembly members:
mastoparan-X, polymer, 15 residues, Formula weight is not available

Natural source:   Common Name: Wasp   Taxonomy ID: 7443   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Vespa Vespa orientalis

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):
mastoparan-X: INWKGIAAMAKKLLG

Data sets:
Data typeCount
13C chemical shifts75
15N chemical shifts20

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1mastoparan-X1

Entities:

Entity 1, mastoparan-X 15 residues - Formula weight is not available

1   ILEASNTRPLYSGLYILEALAALAMETALA
2   LYSLYSLEULEUGLY

Samples:

sample_1: mastoparan-X, [U-95% 13C; U-95% 15N], 100%

EX-cod_1: pH: 7 na; temperature: 280 K

Experiments:

NameSampleSample stateSample conditions
13C-13C RFDRnot availablenot availablenot available
15N-13C ramp-CPnot availablenot availablenot available
CA-CBCGnot availablenot availablenot available
CA(NHCO)CAnot availablenot availablenot available
NH(CO)CACBnot availablenot availablenot available
COCACBnot availablenot availablenot available
NHCACBnot availablenot availablenot available

Software:

Felix v95,2000 -

NMR spectrometers:

  • Varian CMX-infinity 400 MHz
  • Varian CMX-infinity 500 MHz

Related Database Links:

GB AEM43051