BMRB

Biological Magnetic Resonance Data Bank


A Repository for Data from NMR Spectroscopy on Proteins, Peptides, Nucleic Acids, and other Biomolecules
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BMRB Entry 5413

Title: pKa determinations for P2'-His OMTKY3   PubMed: 12627950

Authors: Song, Jikui; Laskowski, Michael; Qasim, Mohammad; Markley, John

Citation: Song, Jikui; Laskowski, Michael; Qasim, Mohammad; Markley, John. "NMR Determination of pKa Values for Asp, Glu, His, and Lys Mutants at Each Variable Contiguous Enzyme-inhibitor Contact Position of the Turkey Ovomucoid Third Domain"  Biochemistry 42, 2847-2856 (2003).

Assembly members:
P2'-His Turkey Ovomucoid Third Domain, polymer, 51 residues, Formula weight is not available

Natural source:   Common Name: Turkey   Taxonomy ID: 9103   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Meleagris gallopavo

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):
P2'-His Turkey Ovomucoid Third Domain: VDCSEYPKPACTLEHRPLCG SDNKTYGNKCNFCNAVVESN GTLTLSHFGKC

Data sets:
  • assigned_chemical_shifts
Data typeCount
pH NMR parameter values59
pKa values5

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1P2'-His OMTKY31

Entities:

Entity 1, P2'-His OMTKY3 51 residues - Formula weight is not available

1   VALASPCYSSERGLUTYRPROLYSPROALA
2   CYSTHRLEUGLUHISARGPROLEUCYSGLY
3   SERASPASNLYSTHRTYRGLYASNLYSCYS
4   ASNPHECYSASNALAVALVALGLUSERASN
5   GLYTHRLEUTHRLEUSERHISPHEGLYLYS
6   CYS

Samples:

sample_1: P2'-His Turkey Ovomucoid Third Domain 2 mM; KCl 100 mM; DSS 0.4 mM

conditions_set_1: ionic strength: 100 mM; pH: .; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
TOCSYsample_1not availableconditions_set_1

Software:

No software information available

NMR spectrometers:

  • Bruker DMX 500 MHz

Related Database Links:

BMRB 4068 42 4864 4865 507 5411 5414 5415 5448 5518 5519 5521
PDB
SWISS-PROT P05609 P52245 P52263 P68436