BMRB Entry 51754

Title:
RC9
Deposition date:
2022-12-29
Original release date:
2023-02-20
Authors:
Smirnov, Serge; Vugmeyster, Liliya
Citation:

Citation: Vugmeyster, Liliya; Ostrovsky, Dmitry; Rodgers, Aryana; Gwin, Kirsten; Smirnov, Serge; McKnight, C James; Fu, Riqiang. "Persistence of Methionine Side Chain Mobility at Low Temperatures in a Nine-Residue Low Complexity Peptide, as Probed by 2 H Solid-State NMR"  Chemphyschem 25, e202300565-e202300565 (2024).
PubMed: 38175858

Assembly members:

Assembly members:
entity_1, polymer, 9 residues, 822.98 Da.

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
entity_1: GGKGMGFGL

Data sets:
Data typeCount
13C chemical shifts7
1H chemical shifts53

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1RC91

Entities:

Entity 1, RC9 9 residues - 822.98 Da.

1   GLYGLYLYSGLYMETGLYPHEGLYLEU

Samples:

sample_1: RC9 1.0625 mM

sample_conditions_1: ionic strength: 0 M; pH: 2; pressure: 1 atm; temperature: 285 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-13C HSQCsample_1isotropicsample_conditions_1
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-1H ROESYsample_1isotropicsample_conditions_1
2D 1H-1H NOESYsample_1isotropicsample_conditions_1

Software:

NMRPipe v11.1 Rev 2022.214.10.43 - processing

NMRView v9.2-b27 - chemical shift assignment

NMR spectrometers:

  • Bruker AVANCE III 500 MHz (1H Larmor frequency) MHz