BMRB

Biological Magnetic Resonance Data Bank


A Repository for Data from NMR Spectroscopy on Proteins, Peptides, Nucleic Acids, and other Biomolecules
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BMRB Entry 10022

Title: 3D Structure of amyloid protofibrils of beta2-microglobulin fragment probed by solid-state NMR   PubMed: 17108084

Authors: Iwata, Kentaro; Fujiwara, Toshimichi; Matsuki, Yoh; Akutsu, Hideo; Takahashi, Satoshi; Naiki, Hironobu; Goto, Yuji

Citation: Iwata, Kentaro; Fujiwara, Toshimichi; Matsuki, Yoh; Akutsu, Hideo; Takahashi, Satoshi; Naiki, Hironobu; Goto, Yuji. "3D Structure of amyloid protofibrils of beta2-microglobulin fragment probed by solid-state NMR"  Proc. Natl. Acad. Sci. U.S.A. 103, 18119-18124 (2006).

Assembly members:
amyloid protofibrils of beta2-microglobulin fragment, polymer, 22 residues, Formula weight is not available

Natural source:   Common Name: human   Taxonomy ID: 9606   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Homo sapiens

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):
amyloid protofibrils of beta2-microglobulin fragment: SNFLNCYVSGFHPSDIEVDL LK

Data sets:
Data typeCount
13C chemical shifts113
15N chemical shifts26

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1K3 peptide of beta2-microglobulin1

Entities:

Entity 1, K3 peptide of beta2-microglobulin 22 residues - Formula weight is not available

1   SERASNPHELEUASNCYSTYRVALSERGLY
2   PHEHISPROSERASPILEGLUVALASPLEU
3   LEULYS

Samples:

sample_1: amyloid protofibrils of beta2-microglobulin fragment 10 ± 2 mg

condition_1: temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D-3D-13C-13C-RFDRsample_1not availablecondition_1
2D-3D-13C-13C-DARRsample_1not availablecondition_1
2D-13C-13C-SPCz5sample_1not availablecondition_1
2D-13C-13C-INADEQUATEsample_1not availablecondition_1
2D-3D-15N-13C-RFDRsample_1not availablecondition_1
3D-15N-13C-SPECIFIC_CPsample_1not availablecondition_1
2D-13C-HH-13C-SPIN_DIFFnot availablenot availablenot available

Software:

No software information available

NMR spectrometers:

  • Varian Infinity-500 500 MHz
  • Varian Infinity-600 600 MHz
  • Varian Infinity-700 700 MHz

Related Database Links:

BMRB 15480 16587 17165 17166 19099 19113 19116 19118 19119 19120 19121 19122 19123 3078 3079
PDB
DBJ BAA35182 BAE01010 BAE87778 BAG38125 BAG64583
EMBL CAA23830 CAG33347 CAH92078
GB AAA87972 AAA88008 AAA88837 AAB25312 AAB31321
REF NP_001009066 NP_001040602 NP_001127503 NP_001167006 NP_001271618
SP O77517 O77518 O77519 O77520 O77521