BMRB Entry 30343

Title:
PawL-Derived Peptide PLP-10 (trans conformer)
Deposition date:
2017-09-11
Original release date:
2018-03-01
Authors:
Fisher, M.; Mylne, J.; Howard, M.
Citation:

Citation: Fisher, Mark; Zhang, Jingjing; Taylor, Nicolas; Howard, Mark; Berkowitz, Oliver; Debowski, Aleksandra; Behsaz, Bahar; Whelan, James; Pevzner, Pavel; Mylne, Joshua. "A family of small, cyclic peptides buried in preproalbumin since the Eocene epoch"  Plant Direct 2, e00042-e00042 (2018).
PubMed: 30417166

Assembly members:

Assembly members:
entity_1, polymer, 6 residues, 634.679 Da.

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
entity_1: GSPLFD

Data typeCount
1H chemical shifts37

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1entity_11

Entities:

Entity 1, entity_1 6 residues - 634.679 Da.

1   GLYSERPROLEUPHEASP

Samples:

sample_1: PLP-10 1.0 mg/mL

sample_conditions_1: ionic strength: 1.5 mM; pH: 4.5; pressure: 1 atm; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-13C HSQCsample_1not availablesample_conditions_1
2D 1H-1H TOCSY 80sample_1not availablesample_conditions_1
2D 1H-1H ROESYsample_1not availablesample_conditions_1
2D DQF-COSYsample_1not availablesample_conditions_1
2D 1H-1H TOCSY 20sample_1not availablesample_conditions_1

Software:

CcpNMR v2.4.2, CCPN - data analysis

TOPSPIN v3.5, Bruker Biospin - collection

YASARA v16.7.22, Elmar Krieger - refinement, structure calculation

NMR spectrometers:

  • Bruker AvanceIII 600 MHz